CN106491779A - The processing method of ionized calcium water soluble preparation and product - Google Patents
The processing method of ionized calcium water soluble preparation and product Download PDFInfo
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- CN106491779A CN106491779A CN201610922523.0A CN201610922523A CN106491779A CN 106491779 A CN106491779 A CN 106491779A CN 201610922523 A CN201610922523 A CN 201610922523A CN 106491779 A CN106491779 A CN 106491779A
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- water soluble
- ionized calcium
- soluble preparation
- calcium
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- 239000011575 calcium Substances 0.000 title claims abstract description 63
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 title claims abstract description 60
- 229910052791 calcium Inorganic materials 0.000 title claims abstract description 60
- 238000002360 preparation method Methods 0.000 title claims abstract description 37
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 34
- 238000003672 processing method Methods 0.000 title claims abstract description 7
- 210000000582 semen Anatomy 0.000 claims abstract description 17
- 244000293323 Cosmos caudatus Species 0.000 claims abstract description 11
- 235000005956 Cosmos caudatus Nutrition 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 11
- 235000015170 shellfish Nutrition 0.000 claims abstract description 11
- 101000693916 Gallus gallus Albumin Proteins 0.000 claims abstract description 6
- 239000000463 material Substances 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 11
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 6
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 6
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- 239000007789 gas Substances 0.000 claims description 4
- 239000003570 air Substances 0.000 claims description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 3
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims description 3
- 239000000292 calcium oxide Substances 0.000 claims description 3
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 3
- 239000001569 carbon dioxide Substances 0.000 claims description 3
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims description 3
- 230000018044 dehydration Effects 0.000 claims description 3
- 238000006297 dehydration reaction Methods 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- 239000004744 fabric Substances 0.000 claims description 3
- 229960002163 hydrogen peroxide Drugs 0.000 claims description 3
- 230000003301 hydrolyzing effect Effects 0.000 claims description 3
- 238000006386 neutralization reaction Methods 0.000 claims description 3
- 229910052757 nitrogen Inorganic materials 0.000 claims description 3
- 239000001301 oxygen Substances 0.000 claims description 3
- 229910052760 oxygen Inorganic materials 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- 238000010298 pulverizing process Methods 0.000 claims description 3
- 238000000746 purification Methods 0.000 claims description 3
- 230000005855 radiation Effects 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 230000001954 sterilising effect Effects 0.000 claims description 3
- 238000004781 supercooling Methods 0.000 claims description 3
- 239000011882 ultra-fine particle Substances 0.000 claims description 3
- 238000012216 screening Methods 0.000 claims description 2
- 238000004659 sterilization and disinfection Methods 0.000 claims description 2
- 239000008187 granular material Substances 0.000 claims 1
- 239000011573 trace mineral Substances 0.000 abstract description 8
- 235000013619 trace mineral Nutrition 0.000 abstract description 8
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract description 5
- 239000011707 mineral Substances 0.000 abstract description 2
- 235000010755 mineral Nutrition 0.000 abstract description 2
- 229960005069 calcium Drugs 0.000 description 48
- 241001465754 Metazoa Species 0.000 description 10
- 210000000689 upper leg Anatomy 0.000 description 9
- 239000000047 product Substances 0.000 description 8
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 6
- 229910052698 phosphorus Inorganic materials 0.000 description 6
- 239000011574 phosphorus Substances 0.000 description 6
- 238000002474 experimental method Methods 0.000 description 5
- 241000700159 Rattus Species 0.000 description 4
- 230000002146 bilateral effect Effects 0.000 description 4
- 210000004369 blood Anatomy 0.000 description 4
- 239000008280 blood Substances 0.000 description 4
- 230000014759 maintenance of location Effects 0.000 description 4
- 210000002966 serum Anatomy 0.000 description 4
- 102000009027 Albumins Human genes 0.000 description 3
- 108010088751 Albumins Proteins 0.000 description 3
- 241000287828 Gallus gallus Species 0.000 description 3
- 241001299723 Limonia <Rutaceae> Species 0.000 description 3
- 241001523579 Ostrea Species 0.000 description 3
- 241001529739 Prunella <angiosperm> Species 0.000 description 3
- 230000003913 calcium metabolism Effects 0.000 description 3
- 230000035622 drinking Effects 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 239000013589 supplement Substances 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 235000013361 beverage Nutrition 0.000 description 2
- 230000037396 body weight Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000007952 growth promoter Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 230000000968 intestinal effect Effects 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 210000002700 urine Anatomy 0.000 description 2
- 206010006956 Calcium deficiency Diseases 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 206010028813 Nausea Diseases 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- 244000144987 brood Species 0.000 description 1
- MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical compound [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 description 1
- 239000001527 calcium lactate Substances 0.000 description 1
- 229960002401 calcium lactate Drugs 0.000 description 1
- 235000011086 calcium lactate Nutrition 0.000 description 1
- 230000002490 cerebral effect Effects 0.000 description 1
- 230000001684 chronic effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 230000008693 nausea Effects 0.000 description 1
- 210000000653 nervous system Anatomy 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- RECVMTHOQWMYFX-UHFFFAOYSA-N oxygen(1+) dihydride Chemical group [OH2+] RECVMTHOQWMYFX-UHFFFAOYSA-N 0.000 description 1
- 230000001575 pathological effect Effects 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 239000013535 sea water Substances 0.000 description 1
- 230000014860 sensory perception of taste Effects 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 210000000952 spleen Anatomy 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 235000019640 taste Nutrition 0.000 description 1
- 210000002435 tendon Anatomy 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/56—Materials from animals other than mammals
- A61K35/618—Molluscs, e.g. fresh-water molluscs, oysters, clams, squids, octopus, cuttlefish, snails or slugs
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/06—Aluminium, calcium or magnesium; Compounds thereof, e.g. clay
- A61K33/10—Carbonates; Bicarbonates
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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-
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/12—Materials from mammals; Compositions comprising non-specified tissues or cells; Compositions comprising non-embryonic stem cells; Genetically modified cells
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- A61K35/57—Birds; Materials from birds, e.g. eggs, feathers, egg white, egg yolk or endothelium corneum gigeriae galli
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/47—Euphorbiaceae (Spurge family), e.g. Ricinus (castorbean)
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- A61K36/18—Magnoliophyta (angiosperms)
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- A61K36/72—Rhamnaceae (Buckthorn family), e.g. buckthorn, chewstick or umbrella-tree
- A61K36/725—Ziziphus, e.g. jujube
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Abstract
The present invention relates to a kind of processing method of ionized calcium water soluble preparation and product.Ionized calcium water soluble preparation includes the raw material of following weight：100 120 parts of Concha Ostreae, 20 28 parts of Stalactitum, 60 72 parts of Margarita, 55 65 parts of heptangle shellfish, 70 85 parts of Os Draconis, 28 35 parts of Semen Ricini, 25 34 parts of Radix Salviae Miltiorrhizae, 17 22 parts of Spica Prunellae, 12 18 parts of Fructus Crataegi, 10 15 parts of Semen Ziziphi Spinosae, 25 32 parts of Fructus Citri Limoniae, 40 62 parts of Os Equi Asini, 20 26 parts of Chicken Albumin.The ionized calcium water soluble preparation, calcium content are high, and degree of ionization is good, it is ionized calcium activated water, is easily absorbed by the body, pH value is 14 after bath, the acid-base balance of human body can be adjusted, various trace elements and the mineral of needed by human body is supplemented, and human absorptivity is reached more than 95%.
Description
Technical field
The present invention relates to a kind of health-preserving food with health care, and in particular to a kind of ionized calcium water soluble preparation plus
Work method and product.
Background technology
Increasingly serious with environmental pollution, and food-safety problem emerges in an endless stream, human health level increasingly becomes
To in weakly acidic subhealth state body constitution, and existing health promoting product still has very in the effect of the aspects such as the acid-base balance for adjusting human body
Improve greatly space.
Ionized calcium can neutralize body metabolism and be absorbed into from the external world each in human body because existing in ionic formses in human body
Kind of acidic materials, make blood and body fluid in normal weak base state, at this moment the cell of human body be in optimal physiological statuss, its
Physiologically active and regeneration power are most strong.If keeping this physiological statuss for a long time, human body is with regard to natural health.
Active ionized calcium is a kind of water-soluble high-efficient ion calcium preparation, has important physiological action to human body.External extensively application
In adding in various food, beverage, make reinforcing, remedy diet beverage, can health invigorating, intelligence, and the chronic calcium deficiency for the treatment of
And some diseases for causing, plant growing is may additionally facilitate, fruit tree fruiting rate is improved, promotes Fish, domestic animal growth promoter.It and phosphorus
The calcium preparation such as sour hydrogen calcium, calcium lactate are compared, and calcium content is high, and is easily absorbed by cell, is used conveniently and safely.At present, the country not yet gives birth to
Produce and apply, and foreign countries are mainly prepared using sea water ion exchange process and calcic shell high-temperature heating, the method for ionization.
Content of the invention
It is an object of the invention to provide a kind of calcium content is high, easily absorb, effectively adjust the ionized calcium of human acid-base balance
Water soluble preparation and its processing method.
The present invention is achieved by the following technical solutions：
Ionized calcium water soluble preparation, is characterized in that the raw material including following weight：Concha Ostreae 100-120
Part, Stalactitum 20-28 parts, Margarita 60-72 parts, heptangle shellfish 55-65 parts, Os Draconis 70-85 parts, Semen Ricini 28-35 parts, Radix Salviae Miltiorrhizae 25-
34 parts, Spica Prunellae 17-22 parts, Fructus Crataegi 12-18 parts, Semen Ziziphi Spinosae 10-15 parts, Fructus Citri Limoniae 25-32 parts, Os Equi Asini 40-62 parts, Chicken Albumin
20-26 parts.
Preferably, the ionized calcium water soluble preparation includes the raw material of following weight：120 parts of Concha Ostreae, clock breast
20 parts of stone, 60 parts of Margarita, 65 parts of heptangle shellfish, 78 parts of Os Draconis, 32 parts of Semen Ricini, 30 parts of Radix Salviae Miltiorrhizae, 17 parts of Spica Prunellae, 18 parts of Fructus Crataegi,
15 parts of Semen Ziziphi Spinosae, 25 parts of Fructus Citri Limoniae, 55 parts of Os Equi Asini, 23 parts of Chicken Albumin.
The processing method of the ionized calcium water soluble preparation, including step in detail below：
(1). Concha Ostreae, Margarita, heptangle shellfish are extractd cedductor, outside scale removal is cleaned to drench and done；
(2). soaked 3-5 days with strong base solution, carry out deacetylated process, it is 6.5-7 that then neutralization makes pH value；
(3). soaked 4-6 days with hydrogenperoxide steam generator, hydrolytic purification；
(4). above-mentioned shell class material is crushed using existing process, and after carrying out cleaning to other raw materials, screening, then with shell class
Material carries out dries pulverizing together, and material particle size reaches more than 350 mesh；
(5). step (4) resulting materials are placed in high temperature furnace, heated at constant temperature at 600 DEG C, then constant temperature at 800 DEG C
Heating, finally heated at constant temperature 3-4 hour at 1200 DEG C, discharging to osculum without aqueous vapor, cools down；
(6). above dehydration product is placed in high-temperature vacuum furnace, in 1800 DEG C of constant temperature 5 hours under gas shield, by temperature
Degree is raised to 2100 DEG C of constant temperature 2 hours, to white clumpy solid is generated, is cooled to room temperature；
(7). air or oxygen or nitrogen are made at a temperature of 2000-3000 DEG C using Radio-frequency plasma torch
Gas ions, then in the plasma reactor by step (6) gained white clumpy solid at 2000-3000 DEG C, the time of staying is
Ultrafine particle calcium oxide and carbon dioxide is decomposed under conditions of the 0.2-0.4 seconds, then is collected through supercooling, cyclonic separation, cloth bag
Prepare the ultra-fine grain that granularity is less than 0.2 μm, you can obtain water-soluble calcium preparation.
Preferably, step (7) obtain final products through radiation sterilization after preparing ultra-fine grain.
Using method：
The ionized calcium water soluble preparation of the present invention brews 1000-1200 milliliters pure water as daily drunk water per 0.4 gram,
Can be with supplement calcium and various trace element and mineral.
The ionized calcium water soluble preparation, calcium content are high, and degree of ionization is good, is ionized calcium activated water, is easily inhaled by human body
Receive, pH value is 14 after bath, the acid-base balance of human body can be adjusted, supplement various trace elements and the mineral of needed by human body,
And human absorptivity reaches more than 95%.
Specific embodiment
The specific embodiment of the present invention given below, for being further described to the present invention.
Embodiment 1
The ionized calcium water soluble preparation of the present embodiment, preparation process are as follows：
Get the raw material of corresponding proportioning ready：100kg Concha Ostreaes, 28kg Stalactitums, 68kg Margaritas, 55kg heptangle shellfishes, 35kg
Semen Ricini, 25kg Radix Salviae Miltiorrhizaes, 20kg Spica Prunellaes, 12kg Fructus Crataegis, 13kg Semen Ziziphi Spinosaes, 32kg Fructus Citri Limoniaes, 40kg Os Equi Asini, 26kg Chicken Albumins.
Concha Ostreae, Margarita, heptangle shellfish are extractd cedductor, outside scale removal is cleaned to drench and done.3-5 is soaked afterwards with strong base solution
My god, deacetylated process is carried out, it is 6.5-7 that then neutralization makes pH value.Soaked 4-6 days with hydrogenperoxide steam generator again, hydrolytic purification.
Above-mentioned shell class material is crushed using existing process；To Stalactitum, Os Draconis, Semen Ricini, Radix Salviae Miltiorrhizae, Spica Prunellae, Fructus Crataegi, Ziziphi Spinosae
The raw materials such as core, Fructus Citri Limoniae, Os Equi Asini, Chicken Albumin carry out cleaning, screen after, then carry out dries pulverizing together with above-mentioned shell class material,
Material particle size reaches more than 350 mesh.
Resulting materials after crushing are placed in high temperature furnace, heated at constant temperature at 600 DEG C, then heated at constant temperature at 800 DEG C,
Last heated at constant temperature 3-4 hour at 1200 DEG C, discharging to osculum without aqueous vapor, cooling.
Again above dehydration product is placed in high-temperature vacuum furnace, in 1800 DEG C of constant temperature 5 hours under gas shield, by temperature
It is raised to 2100 DEG C of constant temperature 2 hours, to white clumpy solid is generated, is cooled to room temperature.
Air or oxygen or nitrogen are made plasma at a temperature of 2000-3000 DEG C using Radio-frequency plasma torch
Body, then in the plasma reactor by gained white clumpy solid at 2000-3000 DEG C, the time of staying is the 0.2-0.4 seconds
Under the conditions of be decomposed into ultrafine particle calcium oxide and carbon dioxide, then collect through supercooling, cyclonic separation, cloth bag and prepare granularity and be
Less than 0.2 μm of ultra-fine grain, you can obtain water-soluble calcium preparation.
Preferably, the ultra-fine grain for preparing obtains final products after sterilizing via radiation again.
Embodiment 2
The ionized calcium water soluble preparation of the present embodiment of the present embodiment, its preparation are basically identical with embodiment 1, and difference is
Parts by weight of raw materials proportioning is as follows：120kg Concha Ostreaes, 20kg Stalactitums, 60kg Margaritas, 65kg heptangle shellfishes, 70kg Os Draconis, 32kg
Semen Ricini, 30kg Radix Salviae Miltiorrhizaes, 17kg Spica Prunellaes, 18kg Fructus Crataegis, 15kg Semen Ziziphi Spinosaes, 25kg Fructus Citri Limoniaes, 55kg Os Equi Asini, 23kg Chicken Albumins.
Embodiment 3
The ionized calcium water soluble preparation of the present embodiment of the present embodiment, its preparation are basically identical with embodiment 1, and difference is
Parts by weight of raw materials proportioning is as follows：110kg Concha Ostreaes, 25kg Stalactitums, 72kg Margaritas, 60kg heptangle shellfishes, 85kg Os Draconis, 28kg
Semen Ricini, 34kg Radix Salviae Miltiorrhizaes, 22kg Spica Prunellaes, 16kg Fructus Crataegis, 10kg Semen Ziziphi Spinosaes, 28kg Fructus Citri Limoniaes, 62kg Os Equi Asini, 20kg Chicken Albumins.
Using method：
The ionized calcium water soluble preparation of the present invention brews 1000-1200 milliliters pure water as daily drunk water per 0.4 gram,
Can be with supplement calcium and various trace element and mineral.
The present invention ionized calcium water soluble preparation, the percentage by weight of its calcium more than 55%, also containing ferrum, potassium, sodium,
Zinc, magnesium, phosphorus, copper various trace elements and mineral, product is powder, fineness of powder more than 3500 mesh, the water-soluble calcium
The crowd of preparation liver and gall imbalance is bitterness when drinking by operation instruction, and spleen, stomach, intestinal, the crowd of lung imbalance are drunk by operation instruction
When be micro-puckery taste, kidney, the crowd of bladder imbalance are micro- fishy smell when drinking by operation instruction, and the heart, blood, the crowd of small intestinal imbalance are by making
It is acescency when being drunk with explanation, cerebral nervous system imbalance and Low crowd are slight nausea sense when drinking by operation instruction, are good for
It is sweet sense of taste when Kang Renqun is drunk by operation instruction.
The performance of the ionized calcium water soluble preparation of the present invention is detected by zoopery.
Method of testing
Select wister male white rats, raw after wean within 28 days, body weight in 60-70g, after laboratory observation three days, with
Machine is divided into 4 groups, 10 per group, puts to death one group of animal before experiment starts, and adopts bilateral femur and surveys calcium, phosphorus content in femur.Other 3
Group raises the ionized calcium water soluble preparation with above-described embodiment 1-3 respectively.
Experiment periods are fed 28 days, and animal single cage is raised, and drink ionized water, and ad lib records feedstuff intake, day by day per four
Its body weight of title, terminates to collect excrement and urine in first three day in experiment, at the end of experiment, by animal sacrificed by decapitation, makees corpse big
Body pathological observation, and animal blood inspection serum calcium is adopted, while adopting bilateral femur, net tendon forceps are picked, survey calcium content in femur, calculated
The Retention of calcium in femur.
Calcium in feedstuff, sample, excrement, urine, femur is determined with atomic absorption spectrophotometer, and in blood, calcium, phosphorus content are used
Automatic biochemical analyzer is determined.
(1) calcium metabolism experimental result
The calcium metabolism result of each group Mus
(2) rats with bilateral femur calcium content and Retention experimental result
Rats with bilateral femur calcium content and Retention
(3) calcium, phosphorus detection result in rat blood serum
| Group | Calcium (mg%) | Phosphorus (mg%) | Ca/P |
| Embodiment 1 | 11.25 | 10.82 | 1.04 |
| Embodiment 2 | 11.89 | 11.16 | 1.07 |
| Embodiment 3 | 11.56 | 10.98 | 1.05 |
Find out from the experiment of animal calcium metabolism and the Retention result of femur calcium, ionized calcium water soluble preparation is in animal body
Absorption rate is can be seen that from animal Determination of Calcium in Serum, Ca/P more than 95%：The ionized calcium water soluble preparation of the present invention is in reality
Animal serum calcium, Ca/P can be maintained under the conditions of testing within range of normal value.
The to sum up ionized calcium water soluble preparation of the analysis shows present invention absorbing preferably in animal body, can be more effective
Ground supply is calcareous, and under conditions of other allowance of nutrients abundances, it is to can ensure that and promote to give appropriate active ionized calcium
Brood growth promoter.And usage is easy, is a kind of food enrichment that widely can be utilized, is to increase calcium in meals
One good approach in source.
The preferred embodiment of the present invention described in detail above, but, the present invention is not limited in above-mentioned embodiment
Detail, the present invention range of the technology design in, multiple simple deformations can be carried out to technical scheme, this
A little simple deformations belong to protection scope of the present invention.
It is further to note that each particular technique feature described in above-mentioned specific embodiment, in not lance
In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to various can
The compound mode of energy is no longer separately illustrated.
Additionally, combination in any can also be carried out between a variety of embodiments of the present invention, as long as which is without prejudice to this
The thought of invention, its should equally be considered as content disclosed in this invention.
Claims (4)
1. ionized calcium water soluble preparation, it is characterised in that including the raw material of following weight：Concha Ostreae 100-120 parts, clock
Mammary calculus 20-28 parts, Margarita 60-72 parts, heptangle shellfish 55-65 parts, Os Draconis 70-85 parts, Semen Ricini 28-35 parts, Radix Salviae Miltiorrhizae 25-34 parts,
Spica Prunellae 17-22 parts, Fructus Crataegi 12-18 parts, Semen Ziziphi Spinosae 10-15 parts, Fructus Citri Limoniae 25-32 parts, Os Equi Asini 40-62 parts, Chicken Albumin 20-26
Part.
2. ionized calcium water soluble preparation as claimed in claim 1, it is characterised in that the ionized calcium water soluble preparation include with
The raw material of lower weight：120 parts of Concha Ostreae, 20 parts of Stalactitum, 60 parts of Margarita, 65 parts of heptangle shellfish, 78 parts of Os Draconis, Semen Ricini
32 parts, 30 parts of Radix Salviae Miltiorrhizae, 17 parts of Spica Prunellae, 18 parts of Fructus Crataegi, 15 parts of Semen Ziziphi Spinosae, 25 parts of Fructus Citri Limoniae, 55 parts of Os Equi Asini, 23 parts of Chicken Albumin.
3. the processing method of ionized calcium water soluble preparation as claimed in claim 1 or 2, it is characterised in that including walking in detail below
Suddenly：
(1). Concha Ostreae, Margarita, heptangle shellfish are extractd cedductor, outside scale removal is cleaned to drench and done；
(2). soaked 3-5 days with strong base solution, carry out deacetylated process, it is 6.5-7 that then neutralization makes pH value；
(3). soaked 4-6 days with hydrogenperoxide steam generator, hydrolytic purification；
(4). above-mentioned shell class material is crushed using existing process, and after carrying out cleaning to other raw materials, screening, then with shell class material
Dries pulverizing is carried out together, and material particle size reaches more than 350 mesh；
(5). step (4) resulting materials are placed in high temperature furnace, heated at constant temperature at 600 DEG C, then at 800 DEG C, constant temperature adds
Heat, finally heated at constant temperature 3-4 hour at 1200 DEG C, discharging to osculum without aqueous vapor, cools down；
(6). above dehydration product is placed in high-temperature vacuum furnace, in 1800 DEG C of constant temperature 5 hours under gas shield, by temperature liter
Constant temperature 2 hours again to after 2100 DEG C, to white clumpy solid is generated, are cooled to room temperature；
(7). air or oxygen or nitrogen are made plasma at a temperature of 2000-3000 DEG C using Radio-frequency plasma torch
Body, then in plasma reactor by step (6) gained white clumpy solid at 2000-3000 DEG C, the time of staying is 0.2-
Ultrafine particle calcium oxide and carbon dioxide is decomposed under conditions of 0.4 second, then collects preparation through supercooling, cyclonic separation, cloth bag
Go out the ultra-fine grain that granularity is less than 0.2 μm, you can obtain water-soluble calcium preparation.
4. the processing method of ionized calcium water soluble preparation as claimed in claim 3, it is characterised in that step (7) prepare ultra-fine
Final products are obtained through radiation sterilization after granule.
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| CN110574888A (en) * | 2018-06-09 | 2019-12-17 | 时海棋 | Processing method of multiple trace element ionized product for adjusting acid-base balance |
| CN110590413A (en) * | 2018-06-12 | 2019-12-20 | 舒文一 | Ionic calcium water-soluble mineral fertilizer |
| CN111019783A (en) * | 2020-01-02 | 2020-04-17 | 舒文一 | Ionic calcium water-soluble agent applied to brewing process and application method thereof |
| CN111117834A (en) * | 2020-01-02 | 2020-05-08 | 舒文一 | Ionic calcium water-soluble agent for high-yield fermentation process and use method thereof |
| CN111358007A (en) * | 2020-03-31 | 2020-07-03 | 石林道商生物科技有限公司 | Preparation for balancing body containing stalactite biological calcium and production method thereof |
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