CN110590413A - Ionic calcium water-soluble mineral fertilizer - Google Patents
Ionic calcium water-soluble mineral fertilizer Download PDFInfo
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- CN110590413A CN110590413A CN201810598159.6A CN201810598159A CN110590413A CN 110590413 A CN110590413 A CN 110590413A CN 201810598159 A CN201810598159 A CN 201810598159A CN 110590413 A CN110590413 A CN 110590413A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B17/00—Other phosphatic fertilisers, e.g. soft rock phosphates, bone meal
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D3/00—Calcareous fertilisers
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Abstract
The processing method of the ionic calcium water-soluble mineral fertilizer comprises the steps of preparing 100 parts by weight of oyster shell, 70 parts by weight of shell of pearl oyster, 5 parts by weight of pearl powder, 20 parts by weight of calcium carbonate and 5 parts by weight of keel; respectively grinding the raw materials; calcining the raw materials except calcium carbonate at high temperature, and preparing ultrafine particles by using a high-frequency plasma ultrafine nanoparticle preparation technology; adding distilled water, heating and refluxing; fully drying after cooling; storing for 2 weeks at constant temperature and saturated humidity in a dark place; preparing ultrafine particles by using a high-frequency plasma generator to obtain ultrafine particles; mixing and stirring the raw materials, calcium carbonate and distilled water into paste and storing for 48 hours; then the ultrafine particles are prepared by high-temperature calcination, decomposition in a plasma reaction furnace and the like, namely the ionized calcium water-soluble mineral fertilizer. The ionic calcium water-soluble mineral fertilizer is low in dosage, convenient to use, low in cost, easy to dissolve in water and high in nutrient utilization rate.
Description
Technical Field
The invention relates to an ionic calcium water-soluble mineral fertilizer.
Background
In the existing land, because chemical fertilizers and pesticides are used for many years, the environment is damaged, the soil is hardened, the utilization rate of various fertilizers is very low, and a fertilizer which has high utilization rate of nutrient components, low cost and convenient use and can improve the soil environment is urgently needed.
Disclosure of Invention
The invention aims to provide the ionized calcium water-soluble mineral fertilizer which has the advantages of small dosage, convenient use, low use cost, high water solubility, high nutrient utilization rate and capability of improving the soil environment, and is easy to be absorbed by plants.
The ionic calcium water-soluble mineral fertilizer is prepared by the following processing method:
A. preparing 100 parts of oyster shell, 70 parts of shell of pearl oyster, 5 parts of pearl powder, 20 parts of calcium carbonate and 5 parts of keel;
B. screening the raw materials, respectively grinding and respectively placing;
C. b, putting the raw materials except the calcium carbonate processed in the step B into a high-temperature calcining furnace, sealing and pressurizing to 0.8 MPa-1.2MPa, and calcining for 30-50 minutes at a high temperature of more than 500 ℃;
D. c, preparing the raw material obtained in the step C into ultrafine particles by using a technology of preparing ultrafine nanoparticles by using high-frequency plasmas, wherein the technology of preparing ultrafine nanoparticles by using high-frequency plasmas comprises the steps of preparing plasmas by using a high-frequency plasma generator to make air or oxygen or nitrogen at the temperature of 1000-1500 ℃, then staying the raw material in a plasma reaction furnace for 0.1-0.5 seconds, controlling the temperature in the plasma reaction furnace to be 1000-1500 ℃, then performing cooling cyclone separation and cloth bag collection to prepare ultrafine particles;
E. d, adding 5-7 parts by weight of distilled water into the raw material obtained in the step D, and heating and refluxing for 80-100 minutes;
F. e, cooling the raw material obtained in the step E, and fully drying in a hot air circulation drying box;
G. storing the raw materials obtained in the step F for 2 weeks at a constant temperature and saturated humidity in a dark place, wherein the constant temperature range is 20-22 ℃;
H. preparing air or oxygen or nitrogen into plasma at the temperature of 1000-1500 ℃ by using a high-frequency plasma generator, then staying the raw material obtained in the step E in a plasma reaction furnace for 0.1-0.5 second, wherein the temperature of the plasma reaction furnace is 1000-1500 ℃, and then performing cooling cyclone separation and cloth bag collection to prepare ultrafine particles;
I. and D, mixing the raw material obtained in the step F, 20 parts by weight of the calcium carbonate crushed in the step B and distilled water, stirring the mixture into paste, and storing the paste for 48 hours.
J. Putting the raw material obtained in the step I into a high-temperature calcining furnace, sealing and pressurizing to 1.0-1.3 MPa, and calcining for 30-50 minutes at the high temperature of more than 500 ℃;
K. preparing air or oxygen or nitrogen into plasma at the temperature of 2000 ℃ plus materials at 1000 ℃ by using a high-frequency plasma generator, then staying the raw materials obtained in the step J in a plasma reaction furnace for 0.2-0.5 second, wherein the temperature in the plasma reaction furnace is 2000 ℃ plus materials, then cooling, drying, cyclone separation and cloth bag collection are carried out to prepare ultrafine particles, and the moisture of the ultrafine particles is controlled below 0.5%, thus obtaining the ionized calcium water-soluble mineral fertilizer.
Due to the adoption of the special formula and the unique process steps, the ionic calcium water-soluble mineral fertilizer has the following beneficial effects:
1. the ionic calcium water-soluble mineral fertilizer contains more than or equal to 23 percent of calcium, more than or equal to 9 percent of magnesium, more than or equal to 6 percent of potassium, and trace elements: copper, iron, zinc, boron, manganese, molybdenum and chlorine are more than or equal to 2 percent, total nutrients are more than or equal to 60 percent, the fertilizer is easily dissolved in water, and the fertilizer is dissolved under the action of weak acid secreted by plant roots and microorganisms for being absorbed by crops, so that trace element deficiency and nutritional disorder can be quickly corrected.
2. Can supplement calcium, phosphorus, potassium, iron, magnesium and other elements lacking in soil, regulate the pH value of the soil, passivate and lighten the pollution of heavy metal elements, and protect and improve the soil environment.
3. The penetrability is strong, the dormant state of the seeds is quickly broken, the emergence of the seeds is quick, the soil arching capability is strong, the activity of plant cells can be improved, and the plant aging is delayed;
4. the fertilizer is particularly suitable for facility agriculture such as spray irrigation, drip irrigation and the like, realizes water and fertilizer integration, achieves the effects of saving water, fertilizer and labor, and is convenient to use.
5. Because the content of the nutrient components is high, the dosage is small and the use cost is low. For example, rice seeds are soaked and sprayed, and only 2.5-3 g of the ionized calcium water-soluble mineral fertilizer is needed for soaking rice seeds in a greenhouse. The foliage is sprayed once 7 to 10 days after sowing, only 2 to 3 grams of the ionized calcium water-soluble mineral fertilizer is needed for one greenhouse, the foliage is sprayed once before transplanting, only 2 to 3 grams of the ionized calcium water-soluble mineral fertilizer is needed for one greenhouse, the foliage is sprayed once before the spike of the paddy field is pulled, only 15 grams of the paddy field is needed for 1 hectare, and 450 jin of water is added.
The ionic calcium water-soluble mineral fertilizer of the present invention will be further described below.
Detailed Description
The ionic calcium water-soluble mineral fertilizer is prepared by the following processing method:
A. preparing 100 parts of oyster shell, 70 parts of shell of pearl oyster, 5 parts of pearl powder, 20 parts of calcium carbonate and 5 parts of keel; the other names of the keels are NaGAGU, raw keel, calcined keel, Wuhua keel, blue keel, hua keel and white keel;
B. screening the raw materials, respectively grinding and respectively placing;
C. b, putting the raw materials except the calcium carbonate processed in the step B into a high-temperature calcining furnace, sealing and pressurizing to 0.8 MPa-1.2MPa, and calcining for 30-50 minutes at a high temperature of more than 500 ℃;
D. c, preparing the raw material obtained in the step C into ultrafine particles by using a technology of preparing ultrafine nanoparticles by using high-frequency plasmas, wherein the technology of preparing ultrafine nanoparticles by using high-frequency plasmas comprises the steps of preparing plasmas by using a high-frequency plasma generator to make air or oxygen or nitrogen at the temperature of 1000-1500 ℃, then staying the raw material in a plasma reaction furnace for 0.1-0.5 seconds, controlling the temperature in the plasma reaction furnace to be 1000-1500 ℃, then performing cooling cyclone separation and cloth bag collection to prepare ultrafine particles;
E. d, adding 5-7 parts by weight of distilled water into the raw material obtained in the step D, and heating and refluxing for 80-100 minutes;
F. e, cooling the raw material obtained in the step E, and fully drying in a hot air circulation drying box;
G. storing the raw material obtained in the step F in a dark place under constant temperature and saturated humidity for 2 weeks, wherein the constant temperature range is 20-22 ℃;
H. preparing air or oxygen or nitrogen into plasma at the temperature of 1000-1500 ℃ by using a high-frequency plasma generator, then staying the raw material obtained in the step E in a plasma reaction furnace for 0.1-0.5 second, wherein the temperature of the plasma reaction furnace is 1000-1500 ℃, and then performing cooling cyclone separation and cloth bag collection to prepare ultrafine particles;
I. and D, mixing the raw material obtained in the step F, 20 parts by weight of the calcium carbonate crushed in the step B and distilled water, stirring the mixture into paste, and storing the paste for 48 hours.
J. Putting the raw material obtained in the step I into a high-temperature calcinator, sealing and pressurizing the raw material at 1.0-1.3 MPa, and calcining the raw material at the high temperature of more than 500 ℃ for 30-50 minutes;
K. preparing air or oxygen or nitrogen into plasma at the temperature of 2000 ℃ plus materials at 1000 ℃ by using a high-frequency plasma generator, then staying the raw materials obtained in the step J in a plasma reaction furnace for 0.2-0.5 second, wherein the temperature in the plasma reaction furnace is 2000 ℃ plus materials, then cooling, drying, cyclone separation and cloth bag collection are carried out to prepare ultrafine particles, and the moisture of the ultrafine particles is controlled below 0.5%, thus obtaining the ionized calcium water-soluble mineral fertilizer.
In the specific implementation process, preferably, the step C is closed and pressurized to 0.9 MPa-1.1 MPa, and is subjected to high-temperature calcination at 550 ℃ to 700 ℃ for 35-45 minutes; step E, adding distilled water into the raw material obtained in the step D, and heating and refluxing for 85-95 minutes; and step J, putting the raw material obtained in the step I into a high-temperature calcinator, sealing and pressurizing to 1.1-1.2 MPa, and calcining at 550-700 ℃ for 35-45 minutes.
In the specific implementation process, preferably, in the step K, air or oxygen or nitrogen is made into plasma at the temperature of 1500-.
The ion calcium water-soluble mineral fertilizer is full-nutrient and instant in water, and can quickly correct trace element deficiency and malnutrition. Adjusting the acid-base balance of the crop, supplementing nutrition, removing toxins, and activating the activity of the enzymes of the new object. Degrading and eliminating crop heavy metal and pesticide residue, promoting plant balanced growth, increasing yield, improving quality, high resistance and prolonging preservation period. Experiments prove that the content of calcium ions in the mature paddy and the fruits can be improved by about 30 percent.
The ionic calcium water-soluble mineral fertilizer is convenient to use, and can be applied by various different application methods, such as water-flushing application, root irrigation, foliage spraying, soilless culture, hole application and the like.
The ionic calcium water-soluble mineral fertilizer can be widely applied to crops, and specific use methods include the following steps:
1. corn (corn)
When in seed dressing, 10 g of ionized calcium water-soluble mineral fertilizer is used per 100 jin of seeds, 5-10 jin of water is added, and the ionized calcium water-soluble mineral fertilizer is sprayed on the seeds, stirred uniformly and dried to be sown. The fertilizer is sprayed once after the corn is topdressed in the field, 30 g of the fertilizer is sprayed in each hectare, and 450 jin of water is added for field spraying.
2. Soybean
When in seed dressing, 5 g of mineral fertilizer is conditioned by ionized calcium water-soluble soil every 100 jin of seeds, 5-10 jin of water is added, and the mineral fertilizer is sprayed on the seeds, stirred uniformly and dried to be sown. Spraying 30 g of water and 450 jin of water in the field at the end of July of the Honda in the beginning of the first eighths of the month.
3. Potato
When in seed dressing, 10 g of ionized calcium water-soluble mineral fertilizer is used for every 500 jin of potatoes, 10 jin of water is added to the ionized calcium water-soluble mineral fertilizer, the ionized calcium water-soluble mineral fertilizer is sprayed on the seed potatoes, the seed potatoes are uniformly stirred and dried in the shade, and then mechanical sowing or manual planting can be carried out. Spraying once in the beginning of July at the end of June of the Honda, and spraying with 30 g of ionized calcium water-soluble mineral fertilizer and 450 jin of water in the field.
4. Strawberry
Soaking seeds for accelerating germination, adding 5-10 jin of water into 1 g of ionized calcium water-soluble mineral fertilizer, soaking 2 jin of seeds, fishing out for 24 hours, and wrapping with sand cloth for accelerating germination and sowing. The strawberries are planted on land, 15-20 g of ionized calcium water-soluble mineral fertilizer is used per hectare, and 450 jin of water is added for field spraying. Spraying 30 g of water every land measure equal to fifteen mu in most parts of the Northeast hectare before flowering and fruiting, and adding 450 jin of water for field spraying. And (3) cultivating in a greenhouse, spraying the strawberries once after field planting, and uniformly spraying 5 g of ionized calcium water-soluble mineral fertilizer and 30 jin of water on the seedlings in a greenhouse of 300 square meters. Spraying the fertilizer once again before blooming and fruiting, and uniformly spraying 1 g of ionized calcium water-soluble mineral fertilizer and 30 jin of water on plants.
The ionized calcium water-soluble mineral fertilizer can also be used for soil improvement, diluted ionized calcium water-soluble mineral fertilizer water is sprayed on the whole land, the fertilizer water is sprayed before sowing, and if the effect of raining is optimal after spraying, the fertilizer water is sprayed again in the next day if the rain does not fall. The recommended dosage of the ionized calcium water-soluble mineral fertilizer for improving the soil is 2 g per mu of land, and 500 jin of water is added.
The above-mentioned embodiments are merely illustrative of the preferred embodiments of the present invention, and do not limit the scope of the present invention, and various modifications and improvements of the technical solution of the present invention by those skilled in the art should fall within the protection scope defined by the claims of the present invention without departing from the spirit of the present invention.
Claims (3)
1. The ionic calcium water-soluble mineral fertilizer is characterized by being prepared by adopting the following processing method:
A. preparing 100 parts of oyster shell, 70 parts of shell of pearl oyster, 5 parts of pearl powder, 20 parts of calcium carbonate and 5 parts of keel;
B. screening the raw materials, respectively grinding and respectively placing;
C. b, putting the raw materials except the calcium carbonate processed in the step B into a high-temperature calcining furnace, sealing and pressurizing to 0.8 MPa-1.2MPa, and calcining for 30-50 minutes at a high temperature of more than 500 ℃;
D. c, preparing the raw material obtained in the step C into ultrafine particles by using a technology of preparing ultrafine nanoparticles by using high-frequency plasmas, wherein the technology of preparing ultrafine nanoparticles by using high-frequency plasmas comprises the steps of preparing plasmas by using a high-frequency plasma generator to make air or oxygen or nitrogen at the temperature of 1000-1500 ℃, then staying the raw material in a plasma reaction furnace for 0.1-0.5 seconds, controlling the temperature in the plasma reaction furnace to be 1000-1500 ℃, then performing cooling cyclone separation and cloth bag collection to prepare ultrafine particles;
E. d, adding 5-7 parts by weight of distilled water into the raw material obtained in the step D, and heating and refluxing for 80-100 minutes;
F. e, cooling the raw material obtained in the step E, and drying in a hot air circulation drying box;
G. storing the raw materials obtained in the step F for 2 weeks at a constant temperature and saturated humidity in a dark place, wherein the constant temperature range is 20-22 ℃;
H. preparing air or oxygen or nitrogen into plasma at the temperature of 1000-1500 ℃ by using a high-frequency plasma generator, then staying the raw material obtained in the step E in a plasma reaction furnace for 0.1-0.5 second, wherein the temperature of the plasma reaction furnace is 1000-1500 ℃, and then performing cooling cyclone separation and cloth bag collection to prepare ultrafine particles;
I. mixing the raw material obtained in the step F, 20 parts by weight of calcium carbonate crushed in the step B and distilled water, stirring into paste, and storing for 48 hours;
J. putting the raw material obtained in the step I into a high-temperature calcining furnace, sealing and pressurizing to 1.0-1.3 MPa, and calcining for 30-50 minutes at the high temperature of more than 500 ℃;
K. preparing air or oxygen or nitrogen into plasma at the temperature of 2000 ℃ plus materials at 1000 ℃ by using a high-frequency plasma generator, then staying the raw materials obtained in the step J in a plasma reaction furnace for 0.2-0.5 second, wherein the temperature in the plasma reaction furnace is 2000 ℃ plus materials, then cooling, drying, cyclone separation and cloth bag collection are carried out to prepare ultrafine particles, and the moisture of the ultrafine particles is controlled below 0.5%, thus obtaining the ionized calcium water-soluble mineral fertilizer.
2. The ionic calcium water-soluble mineral fertilizer according to claim 1, characterized in that: c, sealing and pressurizing to 0.9-1.1 MPa, and calcining at 550-700 ℃ for 35-45 minutes; adding 5-6 parts by weight of distilled water into the raw material obtained in the step D, and heating and refluxing for 85-95 minutes; and step J, putting the raw material obtained in the step I into a high-temperature calcinator, sealing and pressurizing to 1.1-1.2 MPa, and calcining at 550-700 ℃ for 35-45 minutes.
3. The ionic calcium water-soluble mineral fertilizer according to claim 2, characterized in that: and in the step K, preparing air or oxygen or nitrogen into plasma at the temperature of 1500-1900 ℃ by using a high-frequency plasma generator, then staying the raw material obtained in the step J in a plasma reaction furnace for 0.3-0.4 second, wherein the temperature in the plasma reaction furnace is 1500-1900 ℃, and then cooling, drying, cyclone separation and cloth bag collection are carried out to prepare the ultrafine particles, wherein the moisture content is controlled to be below 0.5%.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810598159.6A CN110590413A (en) | 2018-06-12 | 2018-06-12 | Ionic calcium water-soluble mineral fertilizer |
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| CN201810598159.6A CN110590413A (en) | 2018-06-12 | 2018-06-12 | Ionic calcium water-soluble mineral fertilizer |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113501733A (en) * | 2021-08-09 | 2021-10-15 | 安徽省司尔特肥业股份有限公司 | Special functional bio-organic fertilizer for hickory and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1085876A (en) * | 1993-11-05 | 1994-04-27 | 中国科学院化工冶金研究所 | Plasma body prepares the method for Namigai |
| CN104055186A (en) * | 2014-07-09 | 2014-09-24 | 舒文一 | Processing method and product of ionized calcium solid drink |
| CN106491779A (en) * | 2016-10-19 | 2017-03-15 | 时传彬 | The processing method of ionized calcium water soluble preparation and product |
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2018
- 2018-06-12 CN CN201810598159.6A patent/CN110590413A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1085876A (en) * | 1993-11-05 | 1994-04-27 | 中国科学院化工冶金研究所 | Plasma body prepares the method for Namigai |
| CN104055186A (en) * | 2014-07-09 | 2014-09-24 | 舒文一 | Processing method and product of ionized calcium solid drink |
| CN106491779A (en) * | 2016-10-19 | 2017-03-15 | 时传彬 | The processing method of ionized calcium water soluble preparation and product |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113501733A (en) * | 2021-08-09 | 2021-10-15 | 安徽省司尔特肥业股份有限公司 | Special functional bio-organic fertilizer for hickory and preparation method thereof |
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Application publication date: 20191220 |
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