CN1526411A - Technological process of preparing water soluble marine pearl powder - Google Patents
Technological process of preparing water soluble marine pearl powder Download PDFInfo
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- CN1526411A CN1526411A CNA031192343A CN03119234A CN1526411A CN 1526411 A CN1526411 A CN 1526411A CN A031192343 A CNA031192343 A CN A031192343A CN 03119234 A CN03119234 A CN 03119234A CN 1526411 A CN1526411 A CN 1526411A
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Abstract
The present invention is technological process of preparing water soluble marine pearl powder. The technological process includes separate chemical degradation, biodegradation and modifying activation of chitosan, active polypeptide and other organic components, ionic calcium and trace elements in marine pearl, so that they have high ionizing degree, high water solubility, high absorption and utilization rate, high grade and quality and fast acting.
Description
Technical field
The present invention relates to a kind of manufacture method of Margarita powder, especially a kind of method of making water solublity ocean Margarita powder.
Background technology
Margarita not only is considered luxurious ornament since ancient times, also becomes precious medicine, and it has cosmetology, the effect of life lengthening, especially ocean Margarita, and medical value is higher.As everyone knows, the ocean Margarita comprises chitin, organic principle and ionized calcium and various trace elements such as active polypeptide.But these nutritional labelings have been destroyed its activity during fabrication, make its water solubility low, and absorption rate is low, and produce effects speed is low, and its nutritional labeling is difficult to be absorbed by the body.
Summary of the invention
To make the Margarita powder water solublity low in order to overcome in the prior art in the present invention, its product activity is low, the shortcoming that nutritional labeling is difficult to be absorbed by the body, a kind of degree of ionization height that has is provided, the water solubility height, the absorption rate height, grade quality height, the fast process of producing water solublity ocean Margarita powder of produce effects.
The present invention produces the process of water solublity ocean Margarita powder, comprises the steps:
(1) the acetyl method is taken off in employing, peels off the acetyl substrate of removing the ocean Concha Margaritifera;
(2) adopt the physics squeezing and pressing method, the female and shellfish pearl powder of broken marine pearl oyster reaches more than 300 orders its granularity;
(3) place pressurized tank to activate described marine pearl oyster mother and shellfish pearl powder, pressurized tank pressurization 0.1～0.3 MPa 3-6 hour, makes macromole Margarita organic matter wherein separate with the molecular state inanimate matter;
(4) isolating organic substance in the step (3) added account for this Organic substance weight 5～8%, concentration is 10～30% hydrochloric acid, carries out chemical degradation, obtains ocean pearl active crystallite chitin;
(5) with the residue in the step (4), add the protease that accounts for residue weight 5～10% down at 25～45 ℃ and carry out biological enzymolysis, obtain micromolecule active polypeptide;
(6) isolating inorganic substances in the step (3) are added electrolyte, modified active obtains ion activity calcium and multiple micronutrient element;
(7) to step (4), (5) and (6) gained material carries out purification respectively;
(8) the purification thing to step (4) carries out the far infrared centrifugal spray drying, makes active polysaccharide dry powder;
(9) the purification thing to step (5) carries out lyophilization, makes active polypeptide dry powder;
(10) the purification thing to step (6) carries out the far infrared centrifugal spray drying, makes active ionized calcium dry powder;
(11) with step (8), (9) and (10) gains mix, and with the co-60 radiation sterilization, obtain final water solublity ocean Margarita powder product.
The present invention produces the process of water solublity ocean Margarita powder, wherein in the step (5) is 1: 2 ratio with the ratio of described inorganic matter and electrolyte, adds concentration and be 10～30% acetic acid electrolyte, carries out electrolysis.
Advantage of the present invention and good effect are: the degree of ionization height of product, and water solubility reaches 99～100%, and the absorbance utilization can reach more than 95%, and produce effects speed is 3～7 days, and its nutrition is very easily absorbed by human consumption.Nontoxic, have no side effect.
The present invention produces other details of process of water solublity ocean Margarita powder and characteristics can be cheer and bright in conjunction with the embodiment that describes in detail.
The specific embodiment
The process of process of the present invention, step is as follows:
At first adopt and catch marine pearl oyster, extract cedductor; With its outside scale removal, clean up, drench and do; Soaked 3～7 days with strong base solution, take off acetyl and handle; Neutralization makes its PH=6.5～7 then; Adopt the physics squeezing and pressing method, behind broken marine pearl oyster mother and shellfish pearl powder 150 orders, the water mill refinement reaches more than 300 orders its granularity; Soaked 4～6 days hydrolytic purification with hydrogenperoxide steam generator;
Above-mentioned steps is a prior art, the invention is characterized in:
Gained marine pearl oyster mother and shellfish pearl powder in the above-mentioned steps are placed the electrothermic warm water pressurized tank, add the pressurized tank of 0.1～0.3 MPa, 3～6 hours, making wherein, the macromole organic matter of Margarita powder separated with the molecular state inanimate matter;
Isolating organic substance in the above-mentioned steps added account for this Organic substance weight 5～8%, concentration is 10～30% hydrochloric acid, carries out chemical degradation, obtains ocean pearl active crystallite chitin;
With the residue in the above-mentioned chemical degradation step of step, add the protease that accounts for residue weight 5～10% down at 25～45 ℃ and carry out biological enzymolysis, obtain micromolecule active polypeptide;
With isolating inorganic substances in the above-mentioned steps, be 1: 2 ratio with the ratio of described inorganic matter and electrolyte, add concentration and be 10～30% acetic acid electrolyte, carry out electrolysis, modified active obtains ion activity calcium and multiple micronutrient element;
To above-mentioned steps gained material ocean pearl active crystallite chitin, micromolecule active polypeptide and ion activity calcium and multiple micronutrient element carry out purification respectively;
Again the thing ocean pearl active crystallite chitin behind the purification is carried out the far infrared centrifugal spray drying, make active polysaccharide dry powder, its water content is 6 ± 2%;
Micromolecule active polypeptide behind the purification is carried out lyophilization, make active polypeptide dry powder, its water content is 6 ± 2%;
Ion activity calcium behind the purification and multiple micronutrient element are carried out the far infrared centrifugal spray drying, make active ionized calcium dry powder, its water content is 6 ± 2%;
With active polysaccharide dry powder, active polypeptide dry powder and active ionized calcium dry powder blend with the co-60 radiation sterilization, obtain final water solublity ocean Margarita powder product.
The present invention with chitin, micromolecule active polypeptide and the ion activity calcium of ocean Margarita and multiple micronutrient element simultaneously first, extract respectively, and keep their activity, made full use of the female and shellfish pearl of marine pearl oyster, reach very easily and be absorbed by the body the purpose that water solubility is high.
Claims (3)
1. the present invention produces the process of water solublity ocean Margarita powder, comprises the steps:
(1) the acetyl method is taken off in employing, peels off the acetyl substrate of removing the ocean Concha Margaritifera;
(2) adopt the physics squeezing and pressing method, the female and shellfish pearl powder of broken marine pearl oyster reaches more than 300 orders its granularity;
(3) place pressurized tank to activate described marine pearl oyster mother and shellfish pearl powder, pressurized tank pressurization 0.1～0.3 MPa 3-6 hour, makes macromole Margarita organic matter wherein separate with the molecular state inanimate matter;
(4) isolating organic substance in the step (3) added account for this Organic substance weight 5～8%, concentration is 10～30% hydrochloric acid, carries out chemical degradation, obtains ocean pearl active crystallite chitin;
(5) with the residue in the step (4), add the protease that accounts for residue weight 5～10% down at 25～45 ℃ and carry out biological enzymolysis, obtain micromolecule active polypeptide;
(6) isolating inorganic substances in the step (3) are added electrolyte, modified active obtains ion activity calcium and multiple micronutrient element;
(7) to step (4), (5) and (6) gained material carries out purification respectively;
(8) the purification thing to step (4) carries out the far infrared centrifugal spray drying, makes active polysaccharide dry powder;
(9) the purification thing to step (5) carries out lyophilization, makes active polypeptide dry powder;
(10) the purification thing to step (6) carries out the far infrared centrifugal spray drying, makes active ionized calcium dry powder;
(11) with step (8), (9) and (10) gains mix.
2. method according to claim 1 is characterized in that in the step (5) that ratio with described inorganic matter and electrolyte is 1: 2 a ratio, adds concentration and be 10～30% acetic acid electrolyte, carries out electrolysis.
3. method according to claim 1 and 2 is characterized in that adding the step of using co-60 radiation in step (11) back, is used for radiation sterilization, obtains final water solublity ocean Margarita powder product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB031192343A CN1226038C (en) | 2003-03-06 | 2003-03-06 | Technological process of preparing water soluble marine pearl powder |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB031192343A CN1226038C (en) | 2003-03-06 | 2003-03-06 | Technological process of preparing water soluble marine pearl powder |
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| CN1526411A true CN1526411A (en) | 2004-09-08 |
| CN1226038C CN1226038C (en) | 2005-11-09 |
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| CNB031192343A Expired - Fee Related CN1226038C (en) | 2003-03-06 | 2003-03-06 | Technological process of preparing water soluble marine pearl powder |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1325063C (en) * | 2005-06-15 | 2007-07-11 | 宋廷生 | L-amino acid water-soluble pearl powder and its preparing method |
| CN106491779A (en) * | 2016-10-19 | 2017-03-15 | 时传彬 | The processing method of ionized calcium water soluble preparation and product |
| CN107982188A (en) * | 2017-12-05 | 2018-05-04 | 杭州鑫伟低碳技术研发有限公司 | A kind of Astaxanthin In Haematococcus Pluvialis freckle removing and whitening frost |
| CN112294744A (en) * | 2020-10-28 | 2021-02-02 | 湖州欧利生物科技有限公司 | Preparation process of enzymolysis pearl freeze-dried powder |
-
2003
- 2003-03-06 CN CNB031192343A patent/CN1226038C/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1325063C (en) * | 2005-06-15 | 2007-07-11 | 宋廷生 | L-amino acid water-soluble pearl powder and its preparing method |
| CN106491779A (en) * | 2016-10-19 | 2017-03-15 | 时传彬 | The processing method of ionized calcium water soluble preparation and product |
| CN107982188A (en) * | 2017-12-05 | 2018-05-04 | 杭州鑫伟低碳技术研发有限公司 | A kind of Astaxanthin In Haematococcus Pluvialis freckle removing and whitening frost |
| CN112294744A (en) * | 2020-10-28 | 2021-02-02 | 湖州欧利生物科技有限公司 | Preparation process of enzymolysis pearl freeze-dried powder |
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| Publication number | Publication date |
|---|---|
| CN1226038C (en) | 2005-11-09 |
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