JP5093029B2 - Cold rolled steel sheet and method for producing the same - Google Patents

Description

  The present invention relates to a cold-rolled steel sheet used by being formed into various shapes by press working or the like and a method for manufacturing the cold-rolled steel sheet. In particular, the present invention is suitable for a material of a part to be subjected to extremely strict molding such as a panel such as an outer side frame of an automobile, and has excellent deep drawability and small in-plane anisotropy of r value. The present invention relates to a cold rolled steel sheet and a manufacturing method thereof.

A member that frequently uses deep drawing, for example, a cold-rolled steel sheet used as a material for a member such as an automobile body panel, is required to have high deep drawing properties.

  In order to improve the deep drawability of the cold-rolled steel sheet, the carbon content in the steel is extremely low carbon steel, and further by adding carbonitride-generating elements such as Ti and Nb, It is effective to reduce solute nitrogen. This is because by reducing solute carbon and solute nitrogen, a {111} texture that is advantageous for deep drawability develops in the annealing process after cold rolling.

  It is also effective to refine the crystal grains of the hot-rolled steel sheet used for cold rolling. This is the part that was a grain boundary in the hot-rolled steel sheet used for cold rolling when a recrystallized structure was formed by releasing work strain from the cold rolled structure in the annealing process after cold rolling. This is because the {111} texture, which is advantageous for deep drawability, tends to develop as compared with the portion that was in the crystal grains. That is, the finer the crystal grains of the hot-rolled steel sheet used for cold rolling, the higher the ratio of the grain boundary part, so the deep drawability of the cold-rolled steel sheet after cold rolling and annealing becomes higher. It is.

  Thus, several methods have been proposed so far to improve the deep drawability of the cold-rolled steel sheet by utilizing the above-described refinement of crystal grains of the hot-rolled steel sheet.

For example, in Patent Document 1, hot rolling is performed with a finishing temperature of Ar ₃ point to (Ar ₃ point + 50 ° C.) and a final reduction ratio of 30% or more, and cooling is started immediately after hot rolling. In addition, an invention has been proposed in which cooling is performed such that the average cooling rate for 3 seconds from the start is 60 ° C./s or more, and in particular, the average cooling rate for 1 second from the start is 80 ° C./s or more.

Further, Patent Document 2 contains more than 0.050% Ti and 0.0003% or more of B, and is preferably rolled for 5 passes or more in the dynamic recrystallization temperature range, and the finish rolling temperature is set to (Ar ₃ point). An invention has been proposed in which hot rolling is performed at −20 ° C. or higher, and rapid cooling is started within 0.2 seconds after the completion of hot rolling.

Further, in Patent Document 3, the total rolling reduction ratio of two passes before the final pass is set to more than 45% and 70% or less, the rolling reduction rate of the final pass is set to 5% or more and 35% or less, and the finishing temperature is set at Ar ₃ points to (Ar An invention in which hot rolling is performed at ₃ points + 50 ° C., cooling is started at a cooling rate of 200 to 2000 ° C./sec within 1 second after completion of hot rolling, and cooling is performed from the finishing temperature to 650 to 850 ° C. Has been proposed.

Japanese Patent Laid-Open No. 5-112831 JP 2000-239786 A JP 2001-316727 A

  As described above, several methods for improving the deep drawability of cold-rolled steel sheets by refining the crystal grains of hot-rolled steel sheets have been proposed, all of which have problems in practical use, or originally intended Thus, the effect of improving the deep drawability of the cold-rolled steel sheet due to the refinement of crystal grains of the hot-rolled steel sheet cannot be fully enjoyed.

  That is, it is shown by the Example of patent document 1 that the extremely high final reduction rate of 40% or more is required in order to make a hot-rolled steel plate finer. For this reason, this method has a problem that the rolling load is excessive and it is difficult to apply to existing facilities, and the hot-rolled steel sheet obtained is likely to have a shape defect.

  Moreover, although the invention described in Patent Document 2 is described as if rolling in the dynamic recrystallization temperature range is optional, as is clear from the description of the examples, the hot-rolled steel sheet is stabilized. In order to obtain fine grains, rolling at a dynamic recrystallization low temperature range of dynamic recrystallization lower limit temperature to (dynamic recrystallization lower limit temperature + 80 ° C.) at 5 passes or more and a total rolling reduction of 80% or more is performed. is necessary. For this reason, this method requires precise rolling temperature management and pass schedule management, and there is a problem that industrial production is difficult.

  According to the method proposed in Patent Document 3, the above problem is solved. However, if the cooling start time is set to 0.5 seconds or less, the material greatly fluctuates due to a slight deviation in the cooling start time, and unevenness of the material occurs in the longitudinal direction of the steel sheet. The effect of refining the crystal grains of the hot-rolled steel sheet due to the rapid cooling of is insufficient. For this reason, this method cannot fully enjoy the effect of improving the deep drawability of the cold-rolled steel sheet due to the refinement of crystal grains of the originally intended hot-rolled steel sheet.

On the other hand, since the deep drawability of a steel sheet shows a good correlation with the Rankford value (r value), it is generally evaluated by the r value. The average r value (r _m ) or Δr is used as an index of the deep drawability of the steel sheet. However, it is difficult to evaluate the actual deep drawability only by the average r value (r _m ) due to the in-plane anisotropy of the r value. Even if Δr is evaluated together, the extremely low carbon steel targeted by the present invention has various in-plane anisotropy patterns of r value, so that the deep drawability may not be accurately evaluated. is there. In the prior art, examination from such a viewpoint is not sufficiently performed. In addition, sufficient studies have not been made on the in-plane anisotropy of TS that affects press formability.

  The present invention has been made in view of the above-described problems of the prior art, and can sufficiently enjoy the deep drawing property improvement effect of a cold-rolled steel sheet by refining the crystal grain of the originally intended hot-rolled steel sheet and is industrial. An object of the present invention is to provide a cold-rolled steel sheet that is easy to produce, highly practical, and excellent in deep drawability, and a manufacturing method thereof.

  In order to achieve the above object, the present inventors have fully enjoyed the effect of improving the deep drawability of a cold-rolled steel sheet by refining the crystal grains of the hot-rolled steel sheet, and in particular the in-plane anisotropy of the r value. In order to establish a small cold-rolled steel sheet and a manufacturing method thereof, intensive studies were conducted.

As a result, the steel ingot or steel slab having a predetermined chemical composition is subjected to hot rolling to complete rolling at (Ar ₃ point −30 ° C.) or more, and 400 ° C. / By cooling to 750 ° C. at an average cooling rate of at least 2 seconds, a hot-rolled steel sheet having a gradient structure in which the grain size decreases from the center of the sheet thickness to the steel sheet surface is obtained. It has been found that by annealing, it is possible to stably produce a cold-rolled steel sheet having excellent deep drawing characteristics that has been difficult in the past. The details of the study are described below.

  (A) As a method of refining the crystal grains of the hot-rolled steel sheet, a method of rapidly cooling immediately after hot rolling for the purpose of increasing the strength by refining the crystal grains when the hot-rolled steel sheet is mainly used as the final product. Has been studied in the past. Since these conventional technologies are intended to increase the strength of hot-rolled steel sheets, the steel types to be studied are low carbon steels with relatively high C content, and extremely low carbon with extremely low C content. Not enough studies have been done on steel.

  (B) On the other hand, in order to obtain a cold-rolled steel sheet excellent in deep drawability as intended by the present invention, it is necessary to use an ultra-low carbon steel having a low C content. However, because ultra-low carbon steel has high grain growth, crystal grains cannot be refined under cooling conditions that have been studied for the purpose of increasing the strength of hot-rolled steel sheets. It has been clarified by the present inventors that the effect of improving the deep drawability of the cold-rolled steel sheet due to the refinement of crystal grains of the rolled steel sheet cannot be fully enjoyed.

  (C) That is, a large shear strain is introduced into the vicinity of the surface of the steel sheet due to the friction between the steel sheet and the rolling roll that occurs during hot rolling. For this reason, the distribution in the thickness direction of the strain applied by hot rolling increases from the center of the thickness toward the steel plate surface. Therefore, originally, a hot-rolled steel sheet having a gradient structure in which the grain size decreases from the center of the sheet thickness to the steel sheet surface is obtained. However, since a large amount of strain also means a large driving force for recovery and recrystallization, grain growth easily proceeds unless appropriate cooling is performed. In particular, since the ultra-low carbon steel targeted by the present invention has high grain growth properties, the progress of grain growth in the region near the steel sheet surface becomes remarkable in combination with the high grain growth properties. As a result, the conventional technique cannot achieve the refinement of the original crystal grains in the region near the steel plate surface of the hot-rolled steel plate. Moreover, since it was such a situation, it has not been considered at all heretofore that the effect of refining crystal grains can be remarkably obtained by the shear strain introduced into the vicinity of the steel sheet surface. For this reason, the steel sheet after cold rolling and annealing in the prior art has insufficiently developed texture that is favorable for deep drawability in the region near the steel sheet surface, and the deep drawability as a whole steel plate can be sufficiently improved. There was no.

  (D) In Patent Document 3, when the cooling start time after hot rolling is 0.5 seconds or less, the material greatly fluctuates due to a slight shift in the cooling start time, and the material is not uniform in the longitudinal direction of the steel sheet. It is speculated that this is exactly the reason why it occurs. That is, since the cooling conditions studied in Patent Document 3 are those that have been studied for the purpose of increasing the strength of conventional hot-rolled steel sheets, the extremely low carbon steel having remarkable grain growth properties. The grain growth proceeds in the region near the steel sheet surface, and the degree of progress of the grain growth in the region near the steel sheet surface varies greatly due to a slight deviation in the cooling start time. As a result, it is inferred that the material greatly fluctuated.

(E) Therefore, for ultra-low carbon steel having a remarkable grain growth property, as a result of examining in detail the conditions for fully enjoying the effect of improving the deep drawability of the cold-rolled steel sheet by refining the crystal grains of the hot-rolled steel sheet, The ultra-low carbon steel having a specific chemical composition containing Ti and Nb is hot-rolled to complete the rolling at (Ar ₃ point-30 ° C) or more, and within 400 seconds within 400 seconds after the hot rolling is completed. The new knowledge that it is most important to cool to 750 ° C. at an average cooling rate of at least ° C./second was obtained. This became apparent for the first time by examining in detail the cooling conditions in the region immediately after hot rolling, which has not been studied in the past.

  What should be noted here is that the cooling conditions after hot rolling are defined not by the time from completion of hot rolling to the start of rapid cooling, but by the time required for cooling to 750 ° C. after completion of hot rolling. By setting this time to 0.5 seconds or less, if the average cooling rate is 400 ° C./second or more, high characteristics can be obtained stably regardless of the cooling start time. is there. Furthermore, since it is not necessary to perform hot rolling under large pressure, it can be easily applied to industrial production.

  (F) By applying the cooling condition of the above item (e), the progress of grain growth in the region near the surface of the steel plate having a large amount of strain described in the above item (c) is suppressed, and the original crystal grains in that region are suppressed. This makes it possible to achieve an excellent deep drawability after cold rolling and annealing. That is, as described in the above section (c), the distribution of strain applied by hot rolling in the thickness direction increases from the center of the thickness to the surface of the steel plate. In steel, strain in the region near the surface of the steel sheet is released very easily. Therefore, it is difficult to refine the original crystal grains in this region, but the cooling condition described in the above item (e) is applied. As a result, the release of these strains is suppressed, and the original crystal grains can be refined even in the vicinity of the steel sheet surface. And thereby, a hot-rolled steel sheet having a gradient structure in which the grain size decreases from the sheet thickness center portion to the steel sheet surface is obtained, and the sheet thickness center is obtained by subjecting the steel sheet having such a structure to cold rolling and annealing. It is possible to sufficiently develop the texture that improves the r value and lowers the in-plane anisotropy of the r value not only in the region but also in the vicinity of the steel sheet surface, and significantly improves the deep drawability of the steel sheet as a whole. Can do it.

(G) This is to improve the deep drawability of the steel sheet as a whole by encouraging the development of a texture that is advantageous for deep drawability in the region near the surface of the steel sheet. The ferrite average crystal grain size at the 1/4 depth position of the plate thickness from the steel sheet surface is 16 μm or less, and the ferrite average crystal grain size ( _ds ) at the 1/16 depth position of the plate thickness from the steel sheet surface And the ratio (d _s / d _c ) of the ferrite average crystal grain size (d _c ) at the center position of the plate thickness to 0.90 or less.

  (H) Thus, since the shear strain introduced into the steel plate surface vicinity region by friction between the steel plate and the rolling roll during hot rolling is utilized to the maximum in the refinement of crystal grains, Producing cold-rolled steel sheets with good deep drawability without introducing a special cooling device with extremely high cooling capacity even when the thickness of hot-rolled steel sheets is difficult to increase the cooling rate. be able to. If the grain refinement of the hot-rolled steel sheet is realized as described above, the mechanical properties of the cold-rolled steel sheet after the subsequent cold rolling and annealing become isotropic, so the in-plane anisotropy of TS Reduction is also possible.

  The present invention is based on the above new findings, and the gist thereof is as follows.

[1] By mass%, C: 0.0050% or less, Si: 0.1% or less, Mn: 0.50% or less, P: 0.025% or less, S: 0.010% or less, Al: 0 .0005 to 0.10%, N: 0.0040% or less, Ti: 0.001 to 0.10% and Nb: 0.001 to 0.10% and satisfying the following formula (1) has a chemical composition the balance being Fe and impurities, the following formula (2) from the obtained TS _m is 335MPa or less, the following equation (3) obtained from r _m is 1.70 or more, determined from the following formula (4) A cold-rolled steel sheet having an absolute value (| Δr |) of Δr of 0.46 or less and r _min obtained from the following formula (5) of 1.60 or more.
(C / 12 + N / 14 + S / 32) / (Ti / 48 + Nb / 93) ≦ 1.4 (1)
TS _m = (TS ₀ + 2TS ₄₅ + TS ₉₀ ) / 4 (2)
r _m = (r ₀ + 2r ₄₅ + r ₉₀ ) / 4 (3)
Δr = (r ₀ −2r ₄₅ + r ₉₀ ) / 2 (4)
r _min = min [r ₀ , r ₄₅ , r ₉₀ ] (5)
Here, the element symbol in the formula (1) is the content (unit: mass%) of each element in the steel, and TS ₀ , TS ₄₅ and TS ₉₀ in the formula (2) are respectively in the rolling direction. TS in the directions of 0 °, 45 ° and 90 °, and r ₀ , r ₄₅ and r ₉₀ in the formulas (3) to (5) are 0 °, 45 ° and 90 ° with respect to the rolling direction, respectively. For the r value in the direction, min [] in equation (5) means a function that returns the minimum value of the arguments in [].

[2] Furthermore, the cold rolled steel sheet according to [1] above, wherein an absolute value (| ΔTS |) of ΔTS obtained from the following formula (6) is 9 MPa or less.
ΔTS = (TS ₀ −2TS ₄₅ + TS ₉₀ ) / 2 (6)
Here, TS ₀ , TS ₄₅ and TS ₉₀ in the formula (6) mean TS in directions of 0 °, 45 ° and 90 ° with respect to the rolling direction, respectively.

[3] Having the chemical composition described in [1] above, the ferrite average crystal grain size at a ¼ depth position of the plate thickness from the steel plate surface is 16 μm or less, and 1 / of the plate thickness from the steel plate surface. The steel sheet having a ratio (d _s / d _c ) of the ferrite average crystal grain size (d _s ) at the 16th depth position to the ferrite average crystal grain size (d _c ) at the plate thickness center position is 0.90 or less. Rate: A cold-rolled steel sheet obtained by performing cold rolling at 60 to 95% and then annealing at a temperature range of 750 to 880 ° C.

[4] Method for producing cold-rolled steel sheet comprising the following steps (A) to (D):
(A) The steel ingot or steel slab having the chemical composition described in [1] above is subjected to hot rolling to complete rolling at (Ar ₃ point −30 ° C.) or more, and 0.5 seconds after completion of hot rolling A hot rolling step in which the steel sheet is cooled to 750 ° C. at an average cooling rate of 400 ° C./second or more and wound in a temperature range of 400 ° C. or more and less than 640 ° C. to form a hot-rolled steel sheet;
(B) Pickling step of pickling the hot-rolled steel sheet to obtain a pickled steel sheet;
(C) a cold rolling step of subjecting the pickled steel sheet to a cold rolling of 60 to 95% to obtain a cold rolled steel sheet; and (D) annealing the cold rolled steel sheet in a temperature range of 750 to 880 ° C. Annealing process.

[5] Having the chemical composition described in [1] above, the ferrite average crystal grain size at a 1/4 depth position of the plate thickness from the steel plate surface is 16 μm or less, and 1 / of the plate thickness from the steel plate surface. The steel sheet having a ratio (d _s / d _c ) of the ferrite average crystal grain size (d _s ) at the 16th depth position to the ferrite average crystal grain size (d _c ) at the plate thickness center position is 0.90 or less. Rate: A method for producing a cold-rolled steel sheet, which is subjected to annealing in a temperature range of 750 to 880 ° C. after performing cold rolling of 60 to 95%.

  [6] The method for producing a cold-rolled steel sheet according to the above [4] or [5], wherein the steel sheet subjected to the cold rolling has a thickness of 2.8 mm or more.

  According to the method of the present invention, a cold-rolled steel sheet excellent in deep drawability, which can be used for severe processing such as integral molding of automobile parts, can be easily manufactured with high productivity.

(1) Chemical composition C: 0.0050% or less C is an element contained as an impurity and has an effect of reducing ductility and deep drawability. For this reason, C content shall be 0.0050% or less. Preferably it is 0.0040% or less, More preferably, it is 0.0030% or less. Since the lower the C content, the better. Therefore, the lower limit of the C content need not be specified. However, excessive reduction of the C content results in a significant increase in refining costs. Therefore, from the viewpoint of refining costs, the C content is preferably 0.0005% or more.

Si: 0.1% or less Si is an element contained as an impurity, and has an effect of inhibiting the development of a texture effective for improving deep drawability and lowering deep drawability. For this reason, Si content shall be 0.1% or less. Preferably it is 0.05% or less, More preferably, it is 0.03% or less. The lower the Si content, the better. Therefore, the lower limit of the Si content need not be specified. However, excessive reduction of the Si content results in a significant increase in manufacturing costs. Therefore, from the viewpoint of manufacturing cost, the Si content is preferably 0.001% or more. More preferably, it is 0.005% or more.

Mn: 0.50% or less Although Mn is an element contained as an impurity, it has an effect of fixing S as MnS and suppressing red hot brittleness of steel due to FeS formation. Therefore, you may make it contain as needed. On the other hand, if the Mn content is excessive, the deep drawability and ductility deteriorate significantly, so the Mn content is 0.5% or less. Preferably it is 0.3% or less, More preferably, it is 0.2% or less. In addition, it is preferable to make Mn content 0.05% or more from a viewpoint of suppressing the red hot brittleness of steel.

P: 0.025% or less P is an element contained as an impurity and has an effect of reducing ductility. Therefore, the P content is 0.025% or less. Preferably it is 0.020% or less, More preferably, it is 0.015% or less. The lower the P content, the better. Therefore, the lower limit of the P content is not particularly limited. However, excessive reduction of the P content causes a significant increase in production cost, so the P content is preferably 0.001% or more.

S: 0.010% or less S is an impurity element and has an effect of reducing ductility and deep drawability. For this reason, S content shall be 0.010% or less. Preferably it is 0.008 or less, More preferably, it is 0.005%. The smaller the S content, the better. Therefore, the lower limit of the S content need not be specified. However, excessive reduction of the S content results in a significant increase in manufacturing costs. Therefore, from the viewpoint of manufacturing cost, the S content is preferably 0.0003% or more.

Al: 0.0005 to 0.10%
Al has the effect | action which deoxidizes molten steel. In order to obtain this effect, the Al content is set to 0.0005% or more. Preferably it is 0.005% or more, More preferably, it is 0.010% or more, More preferably, it is 0.020% or more. On the other hand, when the Al content is excessive, the ductility is remarkably lowered, so the Al content is 0.10% or less. Preferably it is 0.08% or less, More preferably, it is 0.05% or less, More preferably, it is 0.04% or less.

N: 0.0040% or less N is an impurity element and has an effect of reducing ductility and deep drawability. For this reason, N content shall be 0.0040% or less. Preferably it is 0.0035% or less, More preferably, it is 0.0030% or less. More preferred is 0.0025% or less. The lower the N content, the better. Therefore, the lower limit of the N content need not be specified. However, excessive reduction of the N content results in a significant increase in manufacturing costs. Therefore, from the viewpoint of manufacturing cost, the N content is preferably 0.0003% or more.

Ti: 0.001 to 0.10%
Ti forms carbonitrides to reduce solute C and solute N, and has the effect of improving deep drawability and ductility. For this reason, Ti content shall be 0.001% or more. On the other hand, even if Ti is contained in excess of 0.10%, not only the effect due to the above action is saturated, but also the cost is increased, the steel is hardened and the workability is deteriorated. Therefore, the Ti content is 0.10% or less. More preferably, it is 0.08% or less, More preferably, it is 0.07% or less.

Nb: 0.001 to 0.10%
Nb has the effect | action which reduces solid solution C and solid solution N by forming carbonitride, and improves deep drawability and ductility. Moreover, it also has the effect | action which refines | miniaturizes the crystal grain of a hot-rolled sheet. For this reason, Nb content shall be 0.001% or more. On the other hand, if the Nb content exceeds 0.10%, the recrystallization temperature increases, and the annealing temperature necessary to obtain the required performance becomes high, resulting in damage to the annealing equipment and an increase in manufacturing cost. Therefore, the Nb content is 0.10% or less. Preferably it is 0.05% or less, More preferably, it is 0.03% or less.

The contents of Ti and Nb must further satisfy the following formula (1). The left side of the formula (1) is a parameter formula that represents the equivalent ratio of Ti and Nb to C, N, and S that combines with Ti and Nb to form a compound. The smaller this value, the more the Ti and Nb described above. The effect of improving the deep drawability and ductility due to can be expressed more reliably. The right side of formula (1) is preferably 1.2, more preferably 1.0, more preferably 0.8, and most preferably 0.6. Since the lower limit of the value of the parameter expression on the left side of the expression (1) is naturally determined by the upper limit values of the Ti and Nb contents, it does not need to be specified in particular. However, the value of the parameter expression is not excessively small. Since it means a decrease in the efficiency of addition of Ti and Nb, it is preferably 0.01 or more. More preferably, it is 0.05 or more, More preferably, it is 0.10 or more.
(C / 12 + N / 14 + S / 32) / (Ti / 48 + Nb / 93) ≦ 1.4 (1)

  A steel ingot or steel slab provided for the method for producing a cold-rolled steel sheet of the present invention contains each of the above elements, satisfies the above formula (1), and the remainder has a chemical composition composed of Fe and impurities. It is.

(2) Mechanical properties TS _m: the strength of 335MPa or less steel is too high press formability is degraded. Therefore, the TS _m obtained from the following formula (2) (Mean TS) or less 335MPa. Preferably it is 330 MPa or less, More preferably, it is 325 MPa or less, More preferably, it is 320 MPa or less.
TS _m = (TS ₀ + 2TS ₄₅ + TS ₉₀ ) / 4 (2)

r _m: 1.70 or more,
| Δr |: 0.46 or less,
r _min : 1.60 or more Since the deep drawability of the steel sheet shows a good correlation with the Rankford value (r value), the deep drawability is also evaluated based on the r value in the present invention.

Since r _m (average r value) obtained from the following formula (3) indicates an average value in three directions of 0 ° direction, 45 ° direction and 90 ° direction with respect to the rolling direction, This is important in evaluating the overall level of deep drawability. Therefore, to 1.70 above the r _m in the present invention. Preferably it is 1.75 or more, More preferably, it is 1.80 or more, More preferably, it is 1.85 or more.
r _m = (r ₀ + 2r ₄₅ + r ₉₀ ) / 4 (3)

However, even if the r _m is high, when the in-plane anisotropy of r value is large, will be dominated deep drawability of the entire steel sheet by mechanical properties of the most r value is low direction, r _m However, there are cases where good deep drawability cannot be obtained for a high value. In addition, earrings are likely to occur, and the yield may be reduced. Therefore, in the present invention, the absolute value (| Δr |) of Δr generally used as an index of the in-plane anisotropy of the r value is set to 0.46 or less. Δr is obtained from the following equation (4). | Δr | is preferably 0.40 or less, more preferably 0.38 or less, more preferably 0.35 or less, and most preferably 0.30 or less.
Δr = (r ₀ −2r ₄₅ + r ₉₀ ) / 2 (4)

However, the evaluation of the in-plane anisotropy of the r value by | Δr | is based on the typical in-plane anisotropy of the r value that r ₄₅ is lower than r ₀ and r ₉₀ as in the low carbon steel. It is appropriate for the steel plate to have, but since r ₀ and r ₉₀ are not evaluated separately, r ₄₅ may be higher than r ₀ or r ₉₀ as in extremely low carbon steel. For steel plates having in-plane anisotropy of values, this may not be appropriate. Therefore, in addition to | Δr | that is generally used as an index of in-plane anisotropy of the r value in the present invention, r _min (minimum r value) obtained from the following equation (5) is 1.60. That's it. Preferably it is 1.65 or more, More preferably, it is 1.70 or more, More preferably, it is 1.75 or more.
r _min = min [r ₀ , r ₄₅ , r ₉₀ ] (5)

| ΔTS |: 9 MPa or less In the same way as the above-described idea for the in-plane anisotropy of the r value, even when TS _m is 335 MPa or less, Since the press formability of the entire steel sheet may be governed by the mechanical properties of the high TS direction, the absolute value of ΔTS (|) obtained from the following formula (6) in order to ensure good press formability (| ΔTS |) is preferably 9 MPa or less. More preferably, it is 4.5 MPa or less, More preferably, it is 3 MPa or less.
ΔTS = (TS ₀ −2TS ₄₅ + TS ₉₀ ) / 2 (6)

(3) Structure of steel sheet to be subjected to cold rolling After cold rolling and annealing, in order to obtain a cold-rolled steel sheet having excellent deep drawability, particularly in-plane anisotropy, that is, having a small | Δr | The ferrite average crystal grain size at a 1/4 depth position of the plate thickness from the surface of the steel plate is set to 16 μm or less. Since the ferrite average crystal grain size at the 1/4 depth position of the plate thickness from the surface of the steel sheet is a representative value of the ferrite average crystal grain size as the entire steel sheet, the ferrite average crystal grain size at the position exceeds 16 μm. And, the deterioration of deep drawability after cold rolling and annealing, particularly the increase of Δr becomes remarkable. Therefore, the ferrite average crystal grain size at the 1/4 depth position of the plate thickness from the surface of the steel plate is set to 16 μm or less. Preferably it is 15 micrometers or less, More preferably, it is 14 micrometers or less. As the ferrite average crystal grain size is finer, deep drawability after cold rolling and annealing is improved, so the lower limit of the ferrite average crystal grain size does not need to be particularly limited. However, remarkably miniaturization of crystal grains requires a high cooling capacity, and the cooling equipment becomes large in order to increase the cooling capacity, increasing the manufacturing cost. For this reason, it is preferable that the ferrite average crystal grain size in the position of 1/4 depth of the plate thickness from the surface of the steel plate is 2 μm or more.

Further, after cold rolling and annealing, in order to obtain a cold-rolled steel sheet having excellent deep drawability, in particular, | Δr |, at a depth position of 1/16 of the sheet thickness from the surface of the steel sheet subjected to cold rolling. The ratio (d _s / d _c ) between the ferrite average crystal grain size (d _s ) and the ferrite average crystal grain size (d _c ) at the plate thickness center position is preferably 0.90 or less. In the present invention, a large amount of strain is imparted in the hot rolling compared to the central portion of the plate thickness, so that it is expected that the crystal grains will be refined and that the crystal grains are difficult to refine due to remarkable grain growth. In the region near the surface of the steel plate accompanied with, the crystal grains are refined by suppressing the significant grain growth by applying appropriate cooling. Therefore, d _s / d _c, the present invention is an index showing whether miniaturization of interest is achieved. In other words, the fact that d _s / d _c is low, indicates that the miniaturization of the present invention is intended by proper cooling is performed is realized, that d _s / d _c is high, It shows that the refinement intended by the present invention has not been realized because the grain growth cannot be suppressed due to inappropriate cooling.

If d _s / d _c is greater than 0.90, after cold rolling and annealing, deep drawability deterioration, especially | which may lead to increase of | [Delta] r. Preferably it is 0.85 or less, More preferably, it is 0.80 or less, More preferably, it is 0.75 or less, Most preferably, it is 0.70 or less. as d _s / d _c is small, the lower limit of d _s / d _c so improves deep drawability after cold rolling and annealing need not be particularly limited. However, it takes a high cooling capacity is a significant reduction in d _s / d _c, cooling equipment increase manufacturing cost becomes large-scale in order to increase the cooling capacity. Therefore, d _s / d _c is preferably set to 0.20 or more.

  In order to further develop the texture of the cold-rolled steel sheet and further improve the deep drawability after cold rolling and annealing, the depth position of 1/16 of the sheet thickness from the surface of the steel sheet used for cold rolling , The density of {110} <223> orientation is 2 times or more, preferably 3 times or more, and the density of {211} <111> orientation is 1.5 times or more, preferably 2 It is preferable to make it 0.0 times or more.

(4) applying between completing hot rolling rolling at a steel ingot or slab (Ar ₃ point -30 ° C.) or higher having the chemical compositions was hot roll above.

  The present invention accumulates strain in the austenite crystal grains by hot rolling, suppresses release of the strain by cooling after hot rolling, and when the strain becomes a predetermined low temperature region, The crystal grains are refined by rapidly promoting the transformation from austenite to ferrite. Therefore, hot rolling is basically performed in the austenite region. However, since heat is removed by contact with a metal rolling roll during hot rolling, local transformation often occurs in the outermost layer region from the surface of the steel plate to a depth of 10 to 100 μm. In particular, in the steel type having an extremely low C content as in the present invention, such local transformation is likely to occur in the outermost layer region. As a method for preventing such local transformation, it is conceivable to raise the finishing temperature. However, as will be described later, increasing the finishing temperature makes it difficult to refine the crystal grains, resulting in coarsening of the crystal grains throughout the plate thickness. Therefore, the essence of the invention is impaired.

Therefore, when the present inventor examined in detail, the effect of the outermost layer region of the steel sheet on the mechanical properties is small, and if the region where transformation occurs is 1/32 or less of the plate thickness, the properties of the final product are damaged so much. It became clear that And, in order to set the region where transformation occurs to 1/32 or less of the plate thickness, the hot rolling completion temperature (hereinafter also referred to as “finishing temperature”) may be set to (Ar ₃ point −30 ° C.) or more. Also turned out. Accordingly, the finishing temperature is (Ar ₃ point-30 ° C.) or higher. In order to further improve the deep drawability of the cold-rolled steel sheet after the cold rolling and annealing, the finishing temperature is preferably set to Ar ₃ point or higher. The finishing temperature is preferably closer to the Ar ₃ point. This is because when the finishing temperature is high, the strain accumulated in the austenite crystal grains is easily released by hot rolling, and it becomes impossible to efficiently refine the crystal grains by the mechanism described above. . Accordingly, the finishing temperature is preferably (Ar ₃ point + 100 ° C.) or lower, more preferably (Ar ₃ point + 80 ° C.) or lower, and more preferably (Ar ₃ point + 60 ° C.) or lower. In addition, the said temperature is the surface temperature of a steel plate, and can be measured with a radiation thermometer etc.

The temperature of the steel ingot or steel slab to be subjected to hot rolling may be determined from the viewpoint of the finishing temperature, so it is not necessary to limit it in particular, but if it is less than 1000 ° C, a finishing temperature of not less than (Ar ₃ point -30 ° C) is secured. It is generally difficult to do this, and when it exceeds 1280 ° C., the heating cost increases and the yield decreases due to scale loss. Therefore, the temperature is preferably 1000 to 1280 ° C. The lower the temperature, the better the ductility and deep drawability of the cold-rolled steel sheet as the final product. Therefore, the temperature is further preferably 1200 ° C. or lower, and more preferably 1150 ° C. or lower.

When the steel ingot or slab to be subjected to hot rolling is a so-called cold slab cooled to room temperature, for example, a temperature range below Ar ₃ points, it needs to be heated to a temperature range above Ac ₃ points. In the case of a steel ingot or steel slab in a high temperature state after casting or after piece rolling, it is not necessary to perform special heating if the finishing temperature can be secured.

The equipment for performing hot rolling may be either a reverse mill or a tandem mill. From the viewpoint of industrial productivity, it is preferable to use a tandem mill for at least the last several stages. The rolling reduction in the hot rolling is 45% in thickness reduction rate in the temperature range from (Ar ₃ point + 180 ° C.) to the completion of the hot rolling from the viewpoint of efficiently accumulating strain in the austenite crystal grains by hot rolling. % Or more is preferable. The temperature range is more preferably from (Ar ₃ point + 160 ° C) to completion of hot rolling, more preferably from (Ar ₃ point + 140 ° C) to completion of hot rolling, (Ar ₃ point +120). Most preferably, the temperature is from completion of hot rolling to completion of hot rolling. The plate thickness reduction rate is more preferably 50% or more, more preferably 55% or more, and most preferably 60% or more.

  Hot rolling does not have to be performed in one pass, and may be continuous multi-pass rolling. The amount of reduction per pass is preferably 10 to 60%, and more preferably 15 to 60%. Increasing the amount of reduction per pass can efficiently accumulate strain in the austenite crystal grains, which is preferable from the viewpoint of refining the crystal grains of the hot-rolled steel sheet. Since there is a concern that the productivity may be hindered due to difficulty in securing the shape of the steel sheet, the amount of reduction per pass is limited from this viewpoint. According to the present invention, even in rolling in a plurality of passes with a reduction amount of 40% or less per pass, finer ferrite grains can be obtained than in the prior art that requires a large reduction, so that industrial production is easy. It is.

(5) Cooling after hot rolling Cooling to 750 ° C. at an average cooling rate of 400 ° C./second or more within 0.5 seconds after completion of hot rolling, and winding in a temperature range of 400 ° C. or more and less than 640 ° C.

  The present invention accumulates strain in the austenite crystal grains by hot rolling, suppresses release of the strain by cooling after hot rolling, and when the strain becomes a predetermined low temperature region, The crystal grains are refined by rapidly promoting the transformation from austenite to ferrite. Therefore, by cooling to 750 ° C. at an average cooling rate of 400 ° C./second or more within 0.5 seconds after completion of hot rolling, the release of strain accumulated in the austenite crystal grains by hot rolling is 750 ° C. or less. The crystal grains are refined by rapidly promoting the transformation from austenite to ferrite using the strain as a driving force in a temperature range of 750 ° C. or lower.

  The cooling time from completion of hot rolling to 750 ° C. exceeds 0.5 seconds, the average cooling rate from the completion temperature of hot rolling to 750 ° C. is less than 400 ° C./second, or the cooling completion temperature is 750 ° C. If it exceeds, the strain accumulated in the austenite crystal grains by hot rolling is easily released in a temperature range exceeding 750 ° C., and it becomes difficult to refine the crystal grains of the hot-rolled steel sheet. is there. The average cooling rate here means an average cooling rate in a portion where forced cooling is performed by water cooling or the like, excluding the air cooling portion.

  The shorter the cooling time from completion of hot rolling to 750 ° C., the more the release of the strain can be suppressed, so the lower limit is not particularly required. It is preferably 0.40 seconds or less, and more preferably 0.36 seconds or less. In order to further improve the deep drawability of the cold-rolled steel sheet after cold rolling and annealing, the cooling time from completion of hot rolling to 650 ° C. is preferably 0.75 seconds or less, 0.65 seconds More preferably, it is more preferably 0.61 seconds or less.

  Since the higher the average cooling rate, the more the release of the strain can be suppressed, the upper limit need not be specified. It is preferably 500 ° C./second or more, more preferably 600 ° C./second or more, more preferably 700 ° C./second or more, and most preferably 800 ° C./second or more.

  It is not necessary to specify the upper limit of the average cooling rate from the viewpoint of deep drawability after cold rolling and annealing, but in order to increase the cooling capacity, not only the cooling equipment becomes large and the manufacturing cost increases, but also uneven cooling occurs. Or control of cooling stop temperature may become difficult. For this reason, it is good also as 2000 degrees C / second or less.

  The cooling completion temperature is preferably as low as possible within a range in which the coiling temperature described later can be secured, since the release of the strain can be suppressed. Accordingly, the temperature is preferably 700 ° C. or lower, and more preferably 650 ° C. or lower.

  In the process from the completion of cooling to winding, remarkable grain growth is unlikely to occur due to the high nucleation density of ferrite and the relatively low temperature range. Therefore, the average cooling rate in the above process does not need to be specified and may be allowed to cool. However, since a certain degree of grain growth can occur, water cooling may be performed in order to more reliably suppress crystal grain coarsening. In the case of water cooling, the average cooling rate is preferably 10 ° C./second or more. More preferably, it is 20 degreeC / second or more, More preferably, it is 30 degreeC / second or more.

  Winding is performed in a temperature range of 400 ° C. or higher and lower than 640 ° C. When the coiling temperature is 640 ° C. or higher, crystal grains may be coarsened during the slow cooling after coiling, or iron-phosphorus compounds may precipitate, and the deep drawability after cold rolling and annealing may be reduced. Furthermore, problems such as generation of surface defects and a decrease in yield due to scale loss may occur. Therefore, the coiling temperature is less than 640 ° C. The cold-rolled steel sheet according to the present invention is less affected by the coiling temperature on the deep drawability of the cold-rolled steel sheet after cold rolling and annealing than the prior art. There is no need to increase the temperature. Therefore, generation | occurrence | production of a surface flaw can be suppressed by restraining coiling temperature lower than a prior art. From such a viewpoint, the winding temperature is preferably 620 ° C. or lower, more preferably 600 ° C. or lower. On the other hand, when the coiling temperature is lower than 400 ° C., fine carbonitride precipitates or carbonitride is insufficiently precipitated, so that solid solution C or solid solution N remains, and cold rolling is performed. And deep drawability after annealing may be reduced. Therefore, the coiling temperature is 400 ° C. or higher. Preferably it is 450 degreeC or more, More preferably, it is 500 degreeC or more.

(6) Cooling facility In the present invention, the facility for performing the above cooling is not limited. Industrially, it is preferable to use a water spray device having a high water density. For example, a water spray header can be arrange | positioned between rolling plate conveyance rollers, and it can cool by injecting high-pressure water with sufficient water quantity density from the upper and lower sides of a plate.

(7) Pickling Pickling is performed on the hot-rolled steel sheet obtained by the hot rolling. The pickling in the present invention is intended only for removal of the scale formed on the surface of the hot-rolled steel sheet. Therefore, the mode of pickling need not be particularly limited and may be a conventional method.

(8) Cold rolling The pickled steel sheet obtained by the above pickling is subjected to cold rolling at a rolling reduction of 60 to 95%. In the case of extremely low carbon steel, the r value after annealing tends to increase as the cold rolling rate increases to some extent. If the rolling reduction of cold rolling is less than 60%, the improvement of the r value after annealing is insufficient, which is not preferable. On the other hand, when the rolling reduction of cold rolling exceeds 95%, a texture that deteriorates deep drawability develops, and on the contrary, the r value after annealing is lowered. Moreover, the productivity of cold rolling also decreases. Therefore, the rolling reduction of cold rolling is set to 60 to 95%.

  The sheet thickness of the steel sheet to be subjected to cold rolling is preferably 2.8 mm or more from the viewpoint of achieving both productivity and cold rolling rate. Furthermore, 3.0 mm or more is preferable, More preferably, it is 3.2 mm or more.

(9) Annealing The cold rolled steel sheet obtained by the cold rolling is annealed in a temperature range of 750 to 880 ° C.
When the annealing temperature is less than 750 ° C., recrystallization becomes insufficient, and the obtained steel sheet becomes hard, and elongation and deep drawability deteriorate. On the other hand, when the annealing temperature exceeds 880 ° C., not only the production cost is increased, but also transformation to austenite occurs and formation of a texture preferable for the r value is hindered. Therefore, the annealing temperature is 750 to 880 ° C. The lower limit of the annealing temperature is preferably 780 ° C. or higher, more preferably 800 ° C. or higher. The upper limit is preferably 850 ° C. or less, and more preferably 830 ° C. or less.

  The annealing method may be either continuous annealing or box annealing. Moreover, you may perform hot dip galvanization or alloying hot dip galvanization after annealing using a continuous hot dip galvanization line. Moreover, you may give electroplating, for example, Zn type plating, to the steel plate after annealing.

  When performing continuous annealing, it is preferable that the annealing time maintained in the temperature range of 750 to 880 ° C. is 10 to 130 seconds. If the soaking time is 10 seconds or less, recrystallization may be insufficient. On the other hand, if it exceeds 130 seconds, the manufacturing cost increases. The annealing time is more preferably 20 seconds or longer, and more preferably 30 seconds or longer. On the other hand, the upper limit is more preferably 100 seconds or less, and more preferably 60 seconds or less.

(6) Skin pass rolling When there is a concern about yield point elongation, it is preferable to perform skin pass rolling with an elongation of 0.5 to 2% after annealing in order to suppress stretcher strain during press molding.

A steel slab having the chemical composition shown in Table 1 is heated to 1200 ° C., and then subjected to hot rolling, cooling control and winding simulation under the conditions shown in Table 2 using an experimental rolling mill. A 5 mm hot-rolled steel sheet was obtained. Here, cooling was performed from the temperature after stopping cooling to the temperature of the winding simulation. Then, after removing the scale on the surface of the hot-rolled steel sheet by pickling, the steel sheet was cold-rolled at a reduction rate of 80% to obtain a sheet thickness of 0.7 mm. After performing annealing equivalent to continuous annealing at a heating rate of 10 ° C./second, a soaking temperature of 820 ° C., a soaking time of 30 seconds, and a cooling rate of 10 ° C./second, 1% temper rolling was performed.

  In the winding simulation, the steel sheet cooled to the winding temperature is placed in an electric furnace maintained at a temperature corresponding to the winding temperature, held at that temperature for 30 minutes, and then cooled at 20 ° C./hour. This is performed by simulating the temperature history after winding.

The above-mentioned hot-rolled steel sheet was subjected to crystal orientation analysis using an EBSP (Electron Back Scattering Pattern) method, thereby obtaining an average crystal grain size of ferrite at a ¼ depth position from the steel sheet surface. In addition, the average crystal grain size (d _s ) at the 1/16 depth position of the plate thickness from the steel sheet surface and the average crystal grain size (d _c ) at the plate thickness center position are measured, and the ratio (d _s / d _c) was determined. Further, a three-dimensional texture analysis is performed from {110}, {200}, {211} pole figures measured by X-ray diffraction at a position of 1/16 depth from the steel sheet surface, and {110} <223>. And the density for random in the {211} <111> orientation.

The cold-rolled steel sheet thus obtained was subjected to a tensile test by collecting JIS No. 5 test pieces in directions of 0 °, 45 ° and 90 ° with respect to the rolling direction. YS _m , TS _m and El _m are average values in the 0 °, 45 ° and 90 ° directions with respect to the rolling direction calculated by the following equations.
YS _m = (YS ₀ + 2YS ₄₅ + YS ₉₀ ) / 4
TS _m = (TS ₀ + 2TS ₄₅ + TS ₉₀ ) / 4
_{El m = (El 0 + 2El} 45 + El 90) / 4
Here, YS ₀ , YS ₄₅ , YS ₉₀ , TS ₀ , TS ₄₅ , TS ₉₀ , El ₀ , El ₄₅ and El ₉₀ are YS, TS in the directions of 0 °, 45 ° and 90 ° with respect to the rolling direction. And El are shown respectively.

These test results are shown in Table 3. Moreover, about the test numbers 1-3 regarding the steel type A and the steel type B among the test results of Table 3, the cooling time from completion of hot rolling to 750 ° C. and 1/4 of the plate thickness from the steel sheet surface. the relationship between the average crystal grain diameter at a depth position in FIG. 1, respectively the relationship between the cooling time and d _s / d _c from hot rolling finished to 750 ° C. in FIG. The relationship between the cooling time from the completion of hot rolling to 750 ° C. and the average r value and minimum r value of the cold rolled sheet is shown in FIG. 3, and the cooling time from the completion of hot rolling to 750 ° C. and the | The relationship with Δr | is shown in FIG. Further, FIG. 5 shows the relationship between the cooling time from completion of hot rolling to 750 ° C. and | ΔTS | of the cold rolled sheet.

  As shown in FIGS. 1 to 5, the cooling time from completion of hot rolling to 750 ° C. is within 0.5 seconds, and the cooling rate is set to 400 ° C./second or more, so that it is stable and desired regardless of the cooling rate. The average grain size of ferrite and the grain size ratio between the surface layer and the center of the thickness of the hot-rolled steel sheet are obtained, the effect of improving the average r value and the minimum r value in the cold-rolled steel sheet, and | Δr | Reduction effect is obtained.

  As is apparent from Tables 2 and 3, in the trial numbers 1, 2, 4, 5, 7-9, 12, 14 and 16 that satisfy the conditions of the present invention, all have good deep drawability, particularly r value. A cold-rolled steel sheet having a small in-plane anisotropy was obtained. In each of the inventive examples, the average r value increases and the minimum r value increases remarkably as compared with the comparative example of the same steel type, and | Δr | and | ΔTS | Moreover, it is a cold-rolled steel sheet having small in-plane anisotropy and excellent deep drawability.

According to the method of the present invention, a cold-rolled steel sheet excellent in deep drawability, which can be used for severe processing such as integral molding of automobile parts, can be easily manufactured with high productivity.

The figure which shows the relationship between the cooling time from hot rolling completion to 750 degreeC, and the average crystal grain diameter in the 1/4 depth position of sheet thickness from the steel plate surface. Diagram showing the relationship between the cooling time and d _s / d _c from hot rolling finished to 750 ° C. The figure which shows the relationship between the cooling time from the completion of hot rolling to 750 ° C., the average r value and the minimum r value of the cold rolled sheet The figure which shows the relationship between the cooling time from completion of hot rolling to 750 ° C. and | Δr | of the cold rolled sheet The figure which shows the relationship between the cooling time from the completion of hot rolling to 750 ° C. and | ΔTS |

Claims (6)

In mass%, C: 0.0050% or less, Si: 0.1% or less, Mn: 0.50% or less, P: 0.025% or less, S: 0.010% or less, Al: 0.0005 0.10%, N: 0.0040% or less, Ti: 0.001 to 0.10%, and Nb: 0.001 to 0.10%, satisfying the following formula (1), the balance Fe and has a chemical composition consisting of impurities, the following formula (2) from TS _m sought to 335MPa or less, the following equation (3) obtained from r _m is 1.70 or more, the Δr obtained by the following equation (4) A cold-rolled steel sheet having an absolute value (| Δr |) of 0.46 or less and an r _min obtained from the following formula (5) of 1.60 or more.
(C / 12 + N / 14 + S / 32) / (Ti / 48 + Nb / 93) ≦ 1.4 (1)
TS _m = (TS ₀ + 2TS ₄₅ + TS ₉₀ ) / 4 (2)
r _m = (r ₀ + 2r ₄₅ + r ₉₀ ) / 4 (3)
Δr = (r ₀ −2r ₄₅ + r ₉₀ ) / 2 (4)
r _min = min [r ₀ , r ₄₅ , r ₉₀ ] (5)
Here, the element symbol in the formula (1) is the content (unit: mass%) of each element in the steel, and TS ₀ , TS ₄₅ and TS ₉₀ in the formula (2) are respectively in the rolling direction. TS in the directions of 0 °, 45 ° and 90 °, and r ₀ , r ₄₅ and r ₉₀ in the formulas (3) to (5) are 0 °, 45 ° and 90 ° with respect to the rolling direction, respectively. For the r value in the direction, min [] in equation (5) means a function that returns the minimum value of the arguments in []. Furthermore, the absolute value (| (DELTA) TS |) of (DELTA) TS calculated | required from following formula (6) is 9 Mpa or less, The cold-rolled steel plate of Claim 1 characterized by the above-mentioned.
ΔTS = (TS ₀ −2TS ₄₅ + TS ₉₀ ) / 2 (6)
Here, TS ₀ , TS ₄₅ and TS ₉₀ in the formula (6) mean TS in directions of 0 °, 45 ° and 90 ° with respect to the rolling direction, respectively. While having the chemical composition of claim 1, the ferrite average crystal grain size at the 1/4 depth position of the plate thickness from the steel plate surface is 16 μm or less, and the 1/16 depth position of the plate thickness from the steel plate surface The steel sheet having a ratio (d _s / d _c ) of the ferrite average crystal grain size (d _s ) and the ferrite average crystal grain size (d _c ) at the center of the plate thickness of 0.90 or less to a reduction ratio of 60 to A cold-rolled steel sheet obtained by performing annealing in a temperature range of 750 to 880 ° C after performing 95% cold rolling. A method for producing a cold-rolled steel sheet comprising the following steps (A) to (D):
(A) The steel ingot or steel slab having the chemical composition according to claim 1 is subjected to hot rolling to complete rolling at (Ar ₃ point-30 ° C) or more, and within 0.5 seconds after completion of hot rolling A hot rolling step in which the steel sheet is cooled to 750 ° C. at an average cooling rate of 400 ° C./second or more and wound into a hot rolled steel sheet in a temperature range of 400 ° C. or more and less than 640 ° C .;
(B) Pickling step of pickling the hot-rolled steel sheet to obtain a pickled steel sheet;
(C) a cold rolling step of subjecting the pickled steel sheet to a cold rolling of 60 to 95% to obtain a cold rolled steel sheet; and (D) annealing the cold rolled steel sheet in a temperature range of 750 to 880 ° C. Annealing process. While having the chemical composition of claim 1, the ferrite average crystal grain size at the 1/4 depth position of the plate thickness from the steel plate surface is 16 μm or less, and the 1/16 depth position of the plate thickness from the steel plate surface The steel sheet having a ratio (d _s / d _c ) of the ferrite average crystal grain size (d _s ) and the ferrite average crystal grain size (d _c ) at the center of the plate thickness of 0.90 or less to a reduction ratio of 60 to A method for producing a cold-rolled steel sheet, comprising performing annealing in a temperature range of 750 to 880 ° C after performing 95% cold rolling. The method for producing a cold-rolled steel sheet according to claim 4 or 5, wherein a thickness of the steel sheet subjected to the cold rolling is 2.8 mm or more.

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