[go: up one dir, main page]
More Web Proxy on the site http://driver.im/

JPS5699450A - Preparation of n-acyl-n-substituted formamide derivative - Google Patents

Preparation of n-acyl-n-substituted formamide derivative

Info

Publication number
JPS5699450A
JPS5699450A JP16659180A JP16659180A JPS5699450A JP S5699450 A JPS5699450 A JP S5699450A JP 16659180 A JP16659180 A JP 16659180A JP 16659180 A JP16659180 A JP 16659180A JP S5699450 A JPS5699450 A JP S5699450A
Authority
JP
Japan
Prior art keywords
acyl
addition product
triethylsilane
isocyanate
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP16659180A
Other languages
Japanese (ja)
Other versions
JPS5748145B2 (en
Inventor
Yoichiro Nagai
Iwao Oshima
Shinichi Inaba
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sagami Chemical Research Institute
Original Assignee
Sagami Chemical Research Institute
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sagami Chemical Research Institute filed Critical Sagami Chemical Research Institute
Priority to JP16659180A priority Critical patent/JPS5699450A/en
Publication of JPS5699450A publication Critical patent/JPS5699450A/en
Publication of JPS5748145B2 publication Critical patent/JPS5748145B2/ja
Granted legal-status Critical Current

Links

Classifications

    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PURPOSE: To obtain the titled compound useful as a polar solvent in high yield and purity, by reacting an isocyanate with triethylsilane in the presence of a Pd catalyst, and treating the addition product with an acid halide.
CONSTITUTION: An isocyanate is reacted with an equimolar amount of triethylsilane in the presence of PdCl2 or Pd-active carbon catalyst to give an addition product. The reaction is carried out in a dry inert atmosphere at a temperature of 80W130°C. The resultant addition product is then isolated by distillation, and treated with an acid halide to afford an N-acyl-N-substituted formainde derivative, which is a useful substance as a synthetic intermediate for amino acids, peptides, etc.
COPYRIGHT: (C)1981,JPO&Japio
JP16659180A 1980-11-28 1980-11-28 Preparation of n-acyl-n-substituted formamide derivative Granted JPS5699450A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP16659180A JPS5699450A (en) 1980-11-28 1980-11-28 Preparation of n-acyl-n-substituted formamide derivative

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP16659180A JPS5699450A (en) 1980-11-28 1980-11-28 Preparation of n-acyl-n-substituted formamide derivative

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
JP12163373A Division JPS5621030B2 (en) 1973-10-31 1973-10-31

Publications (2)

Publication Number Publication Date
JPS5699450A true JPS5699450A (en) 1981-08-10
JPS5748145B2 JPS5748145B2 (en) 1982-10-14

Family

ID=15834113

Family Applications (1)

Application Number Title Priority Date Filing Date
JP16659180A Granted JPS5699450A (en) 1980-11-28 1980-11-28 Preparation of n-acyl-n-substituted formamide derivative

Country Status (1)

Country Link
JP (1) JPS5699450A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2973371A1 (en) * 2011-04-04 2012-10-05 Commissariat Energie Atomique Preparing a formamide compound, comprises reacting an amine compound with carbon dioxide in the presence of a catalyst and silane compound
FR2975395A1 (en) * 2011-05-16 2012-11-23 Commissariat Energie Atomique Preparing formamide compound, comprises reacting amine compound with carbon dioxide in the presence of a catalyst and a silane compound
WO2012137152A3 (en) * 2011-04-04 2012-12-27 Commissariat A L'energie Atomique Et Aux Energies Alternatives Method for preparing formamide compounds

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6414430U (en) * 1987-07-14 1989-01-25
JPH0733739U (en) * 1993-12-09 1995-06-23 池田物産株式会社 Terminal fixing structure for vehicle floor carpet
JPH0735171U (en) * 1993-12-13 1995-06-27 池田物産株式会社 Terminal fixing structure for vehicle floor carpet

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2973371A1 (en) * 2011-04-04 2012-10-05 Commissariat Energie Atomique Preparing a formamide compound, comprises reacting an amine compound with carbon dioxide in the presence of a catalyst and silane compound
WO2012137152A3 (en) * 2011-04-04 2012-12-27 Commissariat A L'energie Atomique Et Aux Energies Alternatives Method for preparing formamide compounds
US8877971B2 (en) 2011-04-04 2014-11-04 Commissariat A L'energie Atomique Et Aux Energies Alternatives Method for preparing formamide compounds
FR2975395A1 (en) * 2011-05-16 2012-11-23 Commissariat Energie Atomique Preparing formamide compound, comprises reacting amine compound with carbon dioxide in the presence of a catalyst and a silane compound

Also Published As

Publication number Publication date
JPS5748145B2 (en) 1982-10-14

Similar Documents

Publication Publication Date Title
JPS5699450A (en) Preparation of n-acyl-n-substituted formamide derivative
JPS57116038A (en) Preparation of 3-cyano-3,5,5-trimethylcyclohexanone
JPS5246026A (en) Process for preparation of isocyanate compounds
EP0169650A3 (en) Process for preparing aromatic urethanes from nitroaromatic compounds
JPS6483055A (en) Production of peptide and aspartic acid derivative
JPS56158792A (en) Preparation of amineborane
JPS5731682A (en) Preparation of alkylene carbonate
JPS5444675A (en) Production of 3-hydroxy-4-pyrone analog
JPS5673060A (en) Preparation of indoel or indole derivative
JPS54157566A (en) Preparation of nucleoside
JPS5257142A (en) Process for preparing dihalovinyl-cyclopropanecarboxylic acid derivati ves
JPS51138649A (en) P rocess for preparing cyclohexene
JPS5490184A (en) Preparation of 5-fluoro-orotic acid
SU472926A1 (en) The method of obtaining 5-chloropentadiene1,3
JPS5653652A (en) Preparation of indole or indole derivative
JPS57145825A (en) Preparation of ketonic compound from alicyclic carboxylic acid
JPS5626859A (en) Alpha-halogeno-beta-aminopropionitrile
JPS5735564A (en) Preparation of indole or indole derivative
JPS5538347A (en) Preparation of indazoleacetic acids
JPS57183731A (en) 9-hydroxy-7-nonen-1-al and its preparation
JPS6450843A (en) Production of methacrylic acid ester
JPS54157561A (en) Preparation of n-substituted imidazole
JPS56150092A (en) Preparation of aroylaminopenicillanic ester sulfoxide
JPS5659727A (en) Preparation of substituted phenol
JPS56123972A (en) Preparation of 1,3-dialkyl-4-benzoyl-5-hydroxypyrazole compound