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WO2018198563A1 - Composition d'agent de coiffage - Google Patents

Composition d'agent de coiffage Download PDF

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Publication number
WO2018198563A1
WO2018198563A1 PCT/JP2018/010101 JP2018010101W WO2018198563A1 WO 2018198563 A1 WO2018198563 A1 WO 2018198563A1 JP 2018010101 W JP2018010101 W JP 2018010101W WO 2018198563 A1 WO2018198563 A1 WO 2018198563A1
Authority
WO
WIPO (PCT)
Prior art keywords
component
mass
hair
content
hairdressing composition
Prior art date
Application number
PCT/JP2018/010101
Other languages
English (en)
Japanese (ja)
Inventor
藤田範子
橋本佳和
森野修
Original Assignee
株式会社マンダム
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 株式会社マンダム filed Critical 株式会社マンダム
Priority to CN201880005678.5A priority Critical patent/CN110177538B/zh
Priority to KR1020197018981A priority patent/KR102226577B1/ko
Priority to JP2019515140A priority patent/JP6784834B2/ja
Publication of WO2018198563A1 publication Critical patent/WO2018198563A1/fr

Links

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25—Silicon; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/29—Titanium; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/55—Phosphorus compounds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67—Vitamins
    • A61K8/678—Tocopherol, i.e. vitamin E
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8158—Homopolymers or copolymers of amides or imides, e.g. (meth) acrylamide; Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/06—Preparations for styling the hair, e.g. by temporary shaping or colouring
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/48—Thickener, Thickening system
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59—Mixtures
    • A61K2800/596—Mixtures of surface active compounds

Definitions

  • the present invention relates to a hair styling composition used for a hair styling agent for shaping hair.
  • This application claims the priority of Japanese Patent Application No. 2017-088806 and Japanese Patent Application No. 2017-088807 for which it applied to Japan on April 27, 2017, and uses the content here.
  • the hair styling properties can be combined to form a hair bundle.
  • Characteristics to make (arrangement), characteristics to solidify hair, characteristics to start up hair, characteristics to maintain hairstyle for a long time, characteristics to impart gloss (gloss) to hair, and smoothness by improving the sliding between hairs The characteristic etc. are mentioned.
  • the hair styling agent is designed to exhibit one or more of the above characteristics according to the target hair style, the target hair quality, and the like.
  • properties and dosage forms of the hairdressing composition such as liquid, wax, gel, and grease, each having different usability, usability, and hairstyling properties.
  • a waxy hairdressing composition using wax as a hair setting component is known.
  • a wax-like hair styling composition is excellent in the ease of starting up the hair and the ease of arranging the hair bundle (arranging power). On the other hand, it tends to be sticky at the time of application, and is poor in wash-off property.
  • a gel hairdressing composition using a film-forming polymer as a hair set component and blended with a gelling agent such as carboxyvinyl polymer is known (for example, Patent Document 1). Since such a gel-like hairdressing composition has a certain degree of viscosity, the gel-like hairdressing composition is resistant to dripping when used for hand from a tube container or the like, and is excellent in handleability. In addition, it has good spreadability when applied to hair and is excellent in applicability. In addition, the gel-like hairdressing composition forms a film on the surface of the hair by the action of the film-forming polymer that is blended, so that it has excellent properties for hardening the hair and for maintaining the hairstyle for a long time. On the other hand, it is inferior in that it is difficult to make a hair flow due to its low arranging power and a natural finish is not obtained when a film is formed.
  • grease-like hair conditioner compositions (so-called hair grease and water grease) have been known as hair conditioner compositions that impart gloss to hair and are easy to wear (for example, patents).
  • Literature 2 etc. The grease-like hair styling composition contains water and a relatively large amount of a hydrophilic nonionic surfactant, and is harder than a gel-like hair styling composition and has a property of having no fluidity or extremely low fluidity. Yes. For this reason, it can be used by filling a jar container etc. and taking an appropriate amount with a finger from the container, etc., and it is easy to handle. ing.
  • the hairstyle hair-styled by the conventional grease-like hairdressing composition is such that the hair is pressed along the shape of the head from the root, the hair does not form a hair bundle, It was flat. Moreover, glossiness, such as gloss, was strong. Thus, the conventional grease-like hairdressing composition does not require a natural finished hairstyle.
  • a hairdressing composition capable of performing hairdressing so as to have a natural finish while having the properties, arranging power and operability of the grease-like hairdressing composition.
  • the object of the present invention is to improve the operability during hair styling, to form fine hair bundles, to enhance the hair bundle binding characteristics (arrangement force), to raise the hair bundle from the root, and to improve the hairstyle.
  • An object of the present invention is to provide a hair styling composition that is excellent in the property of maintaining time and that suppresses glossiness after hair styling.
  • component (A) one or more powders selected from the group consisting of silica, talc, titanium oxide, and mica
  • the present invention is a hair styling composition
  • a hair styling composition comprising the following component (A), the following component (B), the following component (C), the following component (D), and the following component (E).
  • the content of the component (A) is 0.5 to 5.0% by mass relative to 100% by mass of the product, and the total content of the following component (B1) and the following component (B2) is 3.0 to 25.0 mass %
  • the content of the component (C) is 0.1 to 1.5% by mass
  • the content of the component (D) is 0.05 to 1.5% by mass
  • the component (B1) and the component Hair conditioner composition wherein the mass ratio [(B1) / ⁇ (B1) + (B2) ⁇ ] of the content of the component (B1) to the total content of (B2) is 0.1 to 0.9 I will provide a.
  • component (B) contains the following component (B3).
  • Component (B3) Polyoxyethylene hydrogenated castor oil having an average addition mole number of oxyethylene of 5 or more and less than 45
  • the component (C) is preferably an (acrylates / behenes methacrylate-25) copolymer.
  • the hairdressing composition of the present invention may contain the following component (F), and the content of the component (F) may be 0.1 to 7.0% by mass relative to 100% by mass of the hairdressing composition.
  • the hairdressing composition of the present invention does not contain diglycerin, polyglycerin, and dipropylene glycol, or the total content of diglycerin, polyglycerin, and propylene glycol with respect to 100% by mass of the hairdressing composition. It is preferable that it is less than 5 mass%.
  • the hair styling composition of the present invention is capable of forming fine hair bundles, and is excellent in characteristics (arrangement force) that allows the hair bundles to bend freely and arranges the hair bundles from the root. For this reason, according to the hairdressing composition of the present invention, it is possible to form a hairstyle that is sufficiently combed while raising the hair bundle from the root, which was impossible with the conventional grease-like hairdressing composition. . In addition, the gloss after hair styling is suppressed. For this reason, according to the hairdressing composition of the present invention, it is possible to form a hairstyle that has a more natural finish as compared with the conventional grease-like hairdressing composition while being sufficiently obscured. In addition, after hair styling, the hairstyle is retained for a long time. Furthermore, it is excellent in operability, can be used by filling a jar container etc., taking an appropriate amount with a finger from the container without dripping down, etc., and it is easy to handle and also has good spread when applied to hair. Excellent coating properties.
  • the hairdressing composition of the present invention comprises one or more powders selected from the group consisting of silica, talc, titanium oxide, and mica; polyoxyethylene hydrogenated castor oil; (meth) acrylic acid and / or (meth) acrylic A polymer obtained by using an acid alkyl ester and a polyoxyethylene alkyl ether of (meth) acrylic acid; a carboxyvinyl polymer and / or an alkyl-modified carboxyvinyl polymer; and at least water.
  • the polyoxyethylene hydrogenated castor oil contains at least polyoxyethylene hydrogenated castor oil having an average addition mole number of oxyethylene of 45 to 65 and polyoxyethylene hydrogenated castor oil having an average addition mole number of oxyethylene of 75 to 125.
  • component (A) one or more powders selected from the group consisting of silica, talc, titanium oxide, and mica may be referred to as “component (A)”.
  • component (B1) The polyoxyethylene hydrogenated castor oil having an average addition mole number of 45 to 65 of oxyethylene is “component (B1)”, and the polyoxyethylene hydrogenated castor oil having an average addition mole number of oxyethylene of 75 to 125 is “component ( B2) ”may be referred to, and the polyoxyethylene hydrogenated castor oil containing the component (B1) and the component (B2) may be referred to as“ component (B) ”.
  • component (C) the polymer obtained by using the (meth) acrylic acid and / or the (meth) acrylic acid alkyl ester and the (meth) acrylic acid polyoxyethylene alkyl ether
  • component (D) the carboxyvinyl polymer and / or the alkyl-modified carboxyvinyl polymer
  • component (E) The water may be referred to as “component (E)”.
  • the hairdressing composition of the present invention contains at least a component (A), a component (B), a component (C), a component (D), and a component (E).
  • the hairdressing composition of the present invention may contain components other than the above components (A) to (E).
  • each component contained in the hairdressing composition of the present invention for example, component (A), component (B), component (C), component (D), and components other than components (A) to (E)
  • each component, etc. only 1 type may be used, respectively, and 2 or more types may be used.
  • the component (A) is one or more powders selected from the group consisting of silica, talc, titanium oxide, and mica.
  • the component (A) may use only 1 type and may use 2 or more types.
  • silica known or commonly used silica (anhydrous silicic acid) can be used.
  • the silica may be silicic anhydride (hydrophilic silica) that has not been hydrophobized or may be hydrophobized silicic anhydride. Further, the silica may be silica surface-treated with amino acid, ester, lecithin or the like. The silica may be so-called easily disintegrating silica particles. The said silica may use only 1 type and may use 2 or more types.
  • the hydrophobized silicic anhydride is a substance obtained by hydrophobizing silicic anhydride (for example, untreated silicic anhydride).
  • the treating agent used for the hydrophobizing treatment include organic silyl compounds and silicone compounds.
  • the organic silyl compound include methyltrichlorosilane, dimethyldichlorosilane, trimethylchlorosilane, hexamethyldisilazane, methyltrialkoxysilane, dimethyldialkoxysilane, trimethylalkoxysilane, ethyltrichlorosilane, propyltrichlorosilane, hexyltrichlorosilane, long Examples include chain alkyl trichlorosilane, ethyl trialkoxy silane, propyl trialkoxy silane, hexyl trialkoxy silane, long chain alkyl trialkoxy silane, methacryl silane, fluoroalkyl silane, and perflu
  • silicone compound examples include dimethylpolysiloxane (silicone oil), methylphenylpolysiloxane, methylhydrogenpolysiloxane, and amino-modified silicone.
  • a publicly known method can be adopted as a method of the above-mentioned hydrophobic treatment.
  • the hydrophobic treatment method include a liquid phase method, a gas phase method, and an autoclave method.
  • hydrophobized silicic anhydride examples include dimethylsiloxylated silicic anhydride, trimethylsiloxylated silicic anhydride, octylsiloxylated silicic anhydride, silicone oil-treated silicic anhydride, methacrylsiloxylated silicic anhydride, and the like.
  • the above easily disintegratable silica particles are particles formed by aggregating a plurality of silica primary particles. Although it does not specifically limit as said silica primary particle, For example, a spherical silica particle, a scale-like silica particle, an amorphous silica particle, etc. are mentioned.
  • the average particle diameter of the silica primary particles is not particularly limited.
  • the easily disintegratable silica particles may contain components other than silica.
  • the component other than the silica (hereinafter may be referred to as “encapsulated component”) is not particularly limited, and examples thereof include surfactants, polyhydric alcohols, higher alcohols, sugar alcohols, silicone oils, sequestering agents, Examples include antioxidants, plant extracts, dyes, pigments, fragrances, moisturizers, vitamins, amino acids, and refreshing agents. Of these components, amino acids, silicone oils and vitamins are preferred. Although it does not specifically limit as said amino acids, Dilauroyl glutamate ricin Na (For example, Asahi Kasei Co., Ltd. make, brand name "Perisea”), a trimethylglycine, glutamic acid, etc.
  • the easily disintegratable silica particles encapsulate the inclusion component
  • the inclusion component is released when the easily disintegratable silica particles are disintegrated during hair styling, and an effect corresponding to the type of the inclusion component is exhibited.
  • the easily disintegratable silica particles encapsulate amino acids, thereby exhibiting a hair damage care function. It does not specifically limit as a manufacturing method of the said easily disintegrating silica particle, A well-known method can be used.
  • the oil absorption amount of the silica is preferably 100 mL / 100 g or more, more preferably 150 mL / 100 g or more, and further preferably 200 mL / 100 g or more.
  • the oil absorption amount of the silica is preferably 1000 mL / 100 g or less, more preferably 800 mL / 100 g or less, and still more preferably 700 mL / 100 g or less. In the present specification, the oil absorption is measured according to the method described in JIS K5101.
  • the average particle size (average primary particle size) of the silica is preferably 0.1 nm or more, more preferably 5 nm or more.
  • the average particle size of the silica is preferably 10 ⁇ m or less, more preferably 5 ⁇ m or less.
  • the average particle diameter of a component (A) is a volume average particle diameter, and can be measured using the particle size distribution measuring apparatus by a laser diffraction method. Examples of the particle size distribution measuring apparatus include “LA-920” manufactured by Horiba, Ltd.
  • the silica can be a commercial product.
  • Examples of commercially available silicic anhydride include, for example, the product name “SILICA PEARL P-4M”, the product name “SILICA PEARL 20CG” (manufactured by JGC Catalysts & Chemicals Co., Ltd.), and the product name “SILICA MICRO BEAD P-1500” ( Manufactured by Catalytic Chemical Industry Co., Ltd.), product name “Siricia 320”, product name “Siricia 310P”, product name “Siricia 250”, product name “Siricia 250N”, product name “Siricia 350”, product name “Siricia 370”, Product name “Silicia 380”, Product name “Silicia 420”, Product name “Silicia 430”, Product name “Silicia 440”, Product name “Silicia 450”, Product name “Silicia 470” (Fuji Silysia Chemical Co., Ltd.
  • Examples of commercially available dimethylsiloxylated silicic acid include a trade name “AEROSIL R972”, a trade name “AEROSIL R974”, a trade name “AEROSIL R9200” (manufactured by Nippon Aerosil Co., Ltd.), and the like.
  • Commercially available products of trimethylsiloxylated silicic acid include, for example, trade name “AEROSIL RX200”, trade name “AEROSIL R8200”, trade name “AEROSIL RX300”, trade name “AEROSIL R812S” (above, manufactured by Nippon Aerosil Co., Ltd.) Etc.
  • Examples of commercially available octylsiloxylated silicic acid include “AEROSIL R805” (manufactured by Nippon Aerosil Co., Ltd.) and the like.
  • Commercially available products of silicone oil-treated silicic anhydride include, for example, trade name “AEROSIL R202”, trade name “AEROSIL RY200”, trade name “AEROSIL RY200S”, trade name “AEROSIL RY300” (above, manufactured by Nippon Aerosil Co., Ltd.) Etc.
  • methacrylsiloxy silicic anhydride a brand name "AEROSIL R711" (made by Nippon Aerosil Co., Ltd.) etc. are mentioned, for example.
  • silica Commercially available products of the above-mentioned easily disintegrating silica include, for example, a trade name “Silica Beads SB-705” (manufactured by Miyoshi Kasei Co., Ltd.), a trade name “God Ball SF-16C”, a trade name “God Ball AF-6C”, The product name “Godball AF-16C” (manufactured by Suzuki Oil & Fat Co., Ltd.) and the like can be mentioned.
  • the talc is represented by the INCI name “TALK”.
  • the oil absorption amount of the talc is not particularly limited, but is preferably 18 to 50 mL / 100 g.
  • the average particle size of the talc is not particularly limited, but is preferably 0.5 to 25 ⁇ m. Only one type of talc may be used, or two or more types may be used. As a commercial item of the said talc, brand name "Crown talc PP" (made by Matsumura Sangyo Co., Ltd.) etc. are mentioned, for example.
  • the titanium oxide is represented by the INCI name “TITANIUM DIOXIDE”.
  • the titanium oxide is not particularly limited, and may be fine particle titanium oxide or pigment titanium, for example.
  • the titanium oxide may be used alone or in combination of two or more. Examples of commercially available titanium oxide include trade name “TTO-55 (A)”, trade name “CR-50” (above, manufactured by Ishihara Sangyo Co., Ltd.), and the like.
  • the above mica is represented by the INCI name “MICA”.
  • the oil absorption of the mica is not particularly limited, but is preferably 50 to 150 mL / 100 g.
  • the average particle diameter of the mica is not particularly limited, but is preferably 0.5 to 50 ⁇ m.
  • the said mica may use only 1 type and may use 2 or more types. Examples of the mica commercially available product include “PDM-8W” (manufactured by Topy Industries Co., Ltd.).
  • the content of the component (A) in the hairdressing composition of the present invention is 0.5 to 5.0% by mass, preferably 0.8 to 100% by mass with respect to 100% by mass of the hairdressing composition of the present invention. It is 4.0 mass%. When the content is within the above range, the effect of using the component (A) is sufficiently obtained, the glossiness after hair styling is suppressed, and a fine hair bundle can be formed.
  • the content of the component (A) is the total content of all the components (A) in the hairdressing composition of the present invention.
  • silica is preferable from the viewpoint of further improving the touch and further suppressing white floatation (current state in which the powder appears white on the hair).
  • the content of silica in the hairdressing composition of the present invention is not particularly limited, but is preferably 0.5 to 5.0% by mass, more preferably 0.8 to 4.0% by mass.
  • Component (B) is polyoxyethylene hydrogenated castor oil, and component (B1) (polyoxyethylene hydrogenated castor oil having an average addition mole number of oxyethylene of 45 to 65) and component (B2) (average addition mole of oxyethylene) 75 to 125 polyoxyethylene hydrogenated castor oil).
  • the hair styling composition of the present invention contains such a component (B), has a sufficient arrangement power and characteristics of raising hair from the root, can form a fine hair bundle, and has a hairstyle For a long time.
  • the blending of the component (B1) gives the hairdressing composition a certain degree of hardness and tackiness, makes it easy to form hair bundles by combining the hairs, and further raises the arrangement power and hair from the roots.
  • component (B2) imparts hardness to the hairdressing composition and improves the property of maintaining the hairstyle after hairdressing for a long time.
  • component (B) and component (C) is thought to increase the cohesive force due to the hydrophobic group interaction, but after scraping the hairdressing composition from the container, the hair conditioning in the container over time Since the surface of the agent composition is naturally smooth and the scratch marks are repaired, it is excellent in aesthetics.
  • Component (B) preferably contains polyoxyethylene hydrogenated castor oil having an average addition mole number of oxyethylene of 5 or more and less than 45, in addition to component (B1) and component (B2).
  • the polyoxyethylene hydrogenated castor oil having an average addition mole number of oxyethylene of 5 or more and less than 45 may be referred to as “component (B3)”.
  • component (B3) the polyoxyethylene hydrogenated castor oil having an average addition mole number of oxyethylene of 5 or more and less than 45
  • the hairdressing composition of the present invention contains the component (B3) in addition to the component (B1) and the component (B2) as the component (B), it is excellent in ease of squeezing and the formation of fine hair bundles.
  • each of the above components (B1) to (B3) may be used alone or in combination of two or more.
  • the average added mole number of oxyethylene in the component (B1) is 45 to 65, preferably 50 to 60, from the viewpoint of imparting appropriate hardness and tackiness to the hairdressing composition.
  • the average added mole number of oxyethylene in the component (B2) is 75 to 125, preferably 80 to 120, from the viewpoint of imparting hardness to the hairdressing composition.
  • the average number of moles of oxyethylene added in the component (B3) is 5 or more and less than 45, preferably 10 to 40.
  • Examples of commercially available components (B1) include, for example, trade name “Brownon RCW-50”, trade name “Brownon RCW-60” (above, manufactured by Aoki Oil & Fat Co., Ltd.), trade name “EMALEX HC-50”, product The name “EMALEX HC-60”, the trade name “EMALEX RWIS-150”, the trade name “EMALEX RWIS-350”, the trade name “EMALEX RWIS-360” (above, manufactured by Nippon Emulsion Co., Ltd.), and the like.
  • Examples of commercially available components (B2) include, for example, trade name “Brownon RCW-80”, trade name “Brownon RCW-100”, trade name “Brownon CW-100” (above, manufactured by Aoki Oil & Fat Co., Ltd.), product The name “EMALEX HC-80”, the trade name “EMALEX HC-100” (manufactured by Nippon Emulsion Co., Ltd.), and the like.
  • Examples of commercially available components (B3) include, for example, trade name “Brownon RCW-20”, trade name “Brownon RCW-40”, trade name “Brownon CW-10”, trade name “Brownon CW-25”, trade name. "Brownon CW-40" (Aoki Yushi Kogyo Co., Ltd.), trade name "EMALEX HC-5”, trade name “EMALEX HC-7”, trade name “EMALEX HC-10", trade name “EMALEX HC- 20 ”, trade name“ EMALEX HC-30 ”, trade name“ EMALEX HC-40 ”, trade name“ EMALEX RWIS-105 ”, trade name“ EMALEX RWIS-105EX ”, trade name“ EMALEX RWIS-110 ”, trade name “EMALEX RWIS-110EX”, product name “EMALEX RWIS- 15 ”, trade name“ EMALEX RWIS-115EX ”, trade name“ EMALEX RWIS-120 ”, trade
  • the mass ratio of the content of the component (B1) to the total content of the component (B1) and the component (B2) [(B1) / ⁇ (B1) + (B2) ⁇ ] Is 0.1 to 0.9, preferably 0.2 to 0.8.
  • the mass ratio is within the above range, all of the characteristics of ease of arrangement (arrangement force), the property of raising the hair bundle from the root, the formability of fine hair bundles, and the property of maintaining the hairstyle for a long time Excellent.
  • [(B1) / ⁇ (B1) + (B2) ⁇ ] is more preferably 0.25 to 0.5 from the viewpoint of further improving the property of holding the hairstyle for a long time.
  • content of the said component (B1) is content of the sum total of all the components (B1) in the hairdressing composition of this invention
  • content of the said component (B2) is It is total content of all the components (B2) in the hairdressing composition of this invention.
  • the total content of component (B1) and component (B2) in component (B) is not particularly limited, but is 50.0% by mass or more (for example, 50.0 to 100 mass%) is preferable, more preferably 70.0 mass% or more, and still more preferably 80.0 mass% or more.
  • the content is 50.0% by mass or more, the effect of using the component (B1) and the component (B2) is sufficiently obtained, and in particular, the property of raising the hair bundle from the root, the fine hair bundle The formability and the property of holding the hairstyle for a long time are improved.
  • the total content of the component (B1) and the component (B2) in the hairdressing composition of the present invention is 3.0 to 25.0 mass% with respect to 100 mass% of the hairdressing composition of the present invention.
  • the content is 5.0 to 20.0% by mass, and more preferably 6.0 to 15.0% by mass.
  • the content is within the above range, it is excellent in all of the ease of kneading, the property of raising the hair bundle from the root, the formability of a fine hair bundle, and the property of maintaining the hairstyle for a long time.
  • the content of the component (B3) in the hairdressing composition of the present invention is not particularly limited, but is preferably 0.5 to 10.0% by weight with respect to 100% by weight of the hairdressing composition of the present invention, and more Preferably, the content is 0.8 to 5.0% by mass.
  • the arranging power can be further improved while suppressing the gloss and weight of the hair. Moreover, it can suppress that a hairdressing agent composition becomes too hard, and can improve operativity further.
  • the content of the component (B) in the hairdressing composition of the present invention is not particularly limited, but is preferably 3.0 to 30.0 mass% with respect to 100 mass% of the hairdressing composition of the present invention, and more Preferably it is 5.0 to 25.0 mass%, more preferably 6.0 to 20.0 mass%. When the content is within the above range, it is excellent in all of the easiness of squeezing, the property of raising the hair bundle from the root, the formability of a fine hair bundle, and the property of maintaining the hairstyle for a long time.
  • the content of the component (B) is the total content of all the components (B) in the hairdressing composition of the present invention.
  • the component (C) is a polymer obtained by using (meth) acrylic acid and / or (meth) acrylic acid alkyl ester and (meth) acrylic acid polyoxyethylene alkyl ether as essential monomer components.
  • “(meth) acryl” means “acryl” and / or “methacryl”, that is, both or one of “acryl” and “methacryl”.
  • Component (C) has the effect of thickening the hairdressing composition. Furthermore, by using the component (B) and the component (C) in combination, the elasticity of the hairdressing composition is increased, and the decrease in viscosity under shearing can be suppressed. Therefore, when the hairdressing composition is scraped from the container, etc.
  • the use of the component (C) further improves the property of maintaining the hairstyle of the hairdressing composition for a long time. Only 1 type may be used for a component (C), and 2 or more types may be used for it.
  • the monomer component used to obtain the polymer of component (C) is at least one monomer component [monomer component (c1)] selected from the group consisting of (meth) acrylic acid and (meth) acrylic acid alkyl ester; (Meth) acrylic acid polyoxyethylene alkyl ether [monomer component (c2)]. Furthermore, other monomer components may be included. That is, the component (C) is a polymer including at least a structural unit derived from the monomer component (c1) and a structural unit derived from the monomer component (c2). As a monomer component (c1) and a monomer component (c2), only 1 type may be used, respectively, and 2 or more types may be used.
  • INCI name International Cosmetic Ingredient Dictionary and Handbook, 15th edition, Volume 1, 2014, p.72
  • ACRYLATES / STEARETTH-20 METHACRYLATE COPOLY relay “ACRYLATES / STEARETH-20 METHACRYLATE” (INCI name: International Cosmetic Ingredient Dictionary and Handbook, 15th Edition, Volume 1, 2014, p. 73)
  • Acrelants “ACRYLATES / BEHENETH-25R METHACRYLA 25 METHACRYLA METHACRYLA” in the INCI name (International Cosmetic Ingredient Dictionary and Handbook, 15th edition, volume 1, 2014, p. 62)
  • a compound represented by ((Acrylates / Beheneth-25 methacrylate) copolymer) is preferred.
  • (acrylates / Beheneth-25 methacrylate) copolymer is preferable.
  • an (acrylates / Beheneth-25 methacrylate) copolymer is used as component (C)
  • the spinnability of the hairdressing composition is reduced, and the operability is further improved.
  • Commercially available products of (Acrylates / Beheneth-25 Methacrylate) copolymer include, for example, trade name “Aculin 28” (manufactured by Dow Chemical Company).
  • Component (C) is not particularly limited, but is preferably neutralized with a basic substance or neutralized with a basic substance.
  • the basic substance include alkanolamines such as triethanolamine and monoethanolamine, inorganic bases such as ammonia, sodium hydroxide and potassium hydroxide, and basic amino acids such as arginine.
  • the addition amount of the basic substance is an amount that becomes a sufficiently neutralized component (C), or an amount sufficient to neutralize the component (C), and the component (C) and What is necessary is just to mix
  • the content of the component (C) in the hairdressing composition of the present invention is 0.1 to 1.5% by mass, preferably 0.3 to 0.1% by mass with respect to 100% by mass of the hairdressing composition of the present invention. 1.2% by mass.
  • the content of the component (C) is the total content of all the components (C) in the hairdressing composition of the present invention.
  • the component (D) is a carboxyvinyl polymer and / or an alkyl-modified carboxyvinyl polymer, that is, a carboxyvinyl polymer and / or an alkyl-modified carboxyvinyl polymer.
  • Component (D) mainly has the effect of thickening the system.
  • Component (D) has the effect of thickening the hairdressing composition. Furthermore, by using the component (D) in combination with the component (C), the deterioration of the scraping property from the container due to excessive elasticity of the hairdressing composition is suppressed, and the hairdressing composition can be removed from the container.
  • the component (C) and the component (D) in combination it becomes easy to use in an appropriate amount, handling property is improved, and operability of the hairdressing composition is improved. Further, by using the component (C) and the component (D) in combination, it is possible to suppress the stickiness at the time of application and sufficiently increase the viscosity while keeping the washability good. In addition, it is preferable to increase the viscosity using the component (D), since the stretchability at the time of application of the hairdressing composition is improved and the applicability is improved. As the component (D), only one type may be used, or two or more types may be used.
  • the carboxyvinyl polymer is mainly a polymer of acrylic acid, and the alkyl-modified carboxyvinyl polymer is a copolymer of mainly acrylic acid and alkyl methacrylate (for example, a total carbon number of 10 to 30 (C10 to C30)). It is. Although it does not specifically limit as said carboxy vinyl polymer, It describes with the INCI name (International Cosmetic Ingredient Dictionary and Handbook, the 15th edition, the 1st volume, 2014, p.582-583). Compounds.
  • alkyl-modified carboxyvinyl polymer is not particularly limited, but it is “ACRYLATES / C10-30 ALKYL ACRYLATE” under the INCI name (International Cosmetic Ingredient Dictionary and Handbook, 15th Edition, Volume 1, 2014, p. 63-64).
  • CROSSPOLYMER ((acrylates / alkyl acrylate (C10-30)) crosspolymer) ”.
  • Examples of commercially available products of the carboxyvinyl polymer include a trade name “Carbopol 934”, a trade name “Carbopol 940”, a trade name “Carbopol 941”, a trade name “Carbopol 980”, and a trade name “Carbopol 981”.
  • Component (D) is not particularly limited, but is preferably neutralized with a basic substance or used after being neutralized with a basic substance.
  • the basic substance include alkanolamines such as triethanolamine and monoethanolamine, inorganic bases such as ammonia, sodium hydroxide and potassium hydroxide, and basic amino acids such as arginine.
  • the addition amount of the basic substance is an amount that becomes a sufficiently neutralized component (D) or an amount sufficient to neutralize the component (D), and the component (D) and What is necessary is just to mix
  • the content of component (D) in the hairdressing composition of the present invention is 0.05 to 1.5% by mass, preferably 0.2 to 0.1% by mass with respect to 100% by mass of the hairdressing composition of the present invention. 0.8% by mass. When the content is within the above range, the viscoelasticity of the hairdressing composition is adjusted to an appropriate range, and the operability is improved.
  • the content of the component (D) is the total content of all the components (D) in the hairdressing composition of the present invention.
  • Component (E) is water and is not particularly limited, but purified water is preferred.
  • Ingredient (E) has the effect of improving the spreadability by improving the spreadability of the hairdressing composition of the present invention as a grease-like aqueous hairdressing composition, with a clean feel without oiliness.
  • the content of the component (E) in the hairdressing composition of the present invention is not particularly limited, but is preferably 40.0 to 95.0 mass% with respect to 100 mass% of the hairdressing composition of the present invention, and more Preferably it is 50.0-85.0 mass%.
  • the hairdressing composition of the present invention may further contain a film-forming polymer (sometimes referred to as “component (F)”).
  • Component (F) is a polymer that can form a film on the hair after being applied to the hair, for example.
  • component (F) is a polymer that can form a film on the hair after being applied to the hair, for example.
  • a component (F) For example, an anionic film forming polymer, a cationic film forming polymer, an amphoteric film forming polymer, a nonionic film forming polymer etc. are mentioned.
  • the component (F) does not include the polymer corresponding to the component (C) and the polymer corresponding to the component (D).
  • the component (F) only one type may be used, or two or more types may be used.
  • anionic film-forming polymer examples include acrylic resin alkanolamine, methyl vinyl ether / maleic ester copolymer, vinyl acetate / crotonic acid copolymer, vinyl acetate / crotonic acid / vinyl neodecanoate copolymer, vinyl acetate.
  • Examples of the cationic film-forming polymer include vinylpyrrolidone / N, N-dimethylaminoethyl methacrylic acid copolymer diethyl sulfate, ⁇ - [2-hydroxy-3- (trimethylammonio) propyl] hydroxyethylcellulose, Vinyl imidazolium trichloride / vinyl pyrrolidone copolymer, hydroxyethyl cellulose / dimethyl diallylammonium chloride, polyvinyl pyrrolidone / alkylamino acrylate / vinyl caprolactam copolymer, methyl vinyl imidazolium chloride / vinyl pyrrolidone copolymer, (vinyl pyrrolidone / dimethyl Aminopropylmethacrylamide / lauryldimethylaminopropylmethacrylamide) copolymer and the like.
  • amphoteric film-forming polymer examples include N-methacryloyloxyethyl N, N-dimethylammonium- ⁇ -N-methylcarboxybetaine / alkyl methacrylate ester copolymer [(methacryloyloxyethylcarboxybetaine / alkyl methacrylate) copolymer.
  • nonionic film-forming polymer examples include polyvinyl pyrrolidone, vinyl pyrrolidone / vinyl acetate copolymer [(vinyl pyrrolidone / VA) copolymer], vinyl pyrrolidone / methacrylamide / vinyl imidazole copolymer, vinyl methyl ether / maleic acid.
  • Ethyl copolymer polyvinyl alcohol, polyvinyl caprolactam, dimethylacrylamide / hydroxyethyl acrylate / methoxyethyl acrylate copolymer, hydroxyethyl acrylate / methoxyethyl acrylate copolymer [(hydroxyethyl acrylate / methoxyethyl acrylate) ) Copolymer] and the like.
  • nonionic film-forming polymers are preferred from the viewpoint of better properties for raising hair bundles from the roots and properties for maintaining hairstyles for a long time.
  • a (hydroxyethyl acrylate / methoxyethyl acrylate) copolymer is more preferable.
  • the (hydroxyethyl acrylate / methoxyethyl acrylate) copolymer is a copolymer in which a structural unit derived from hydroxyethyl acrylate and a structural unit derived from methoxyethyl acrylate are essential structural units.
  • the above-mentioned (hydroxyethyl acrylate / methoxyethyl acrylate) copolymer is a compound represented by, for example, the INCI name: HYDROXYETHYL ACRYLATE / METHOXYETHYL ACRYLATE COPOLYMER.
  • Commercially available products of the above (hydroxyethyl acrylate / methoxyethyl acrylate) copolymer include trade name “Plus Size L-2200” (manufactured by Kyoyo Chemical Co., Ltd.) and the like.
  • the content of the component (F) in 100% by mass of the hairdressing composition of the present invention is not particularly limited, but is 0.1 to 7.0. % By mass is preferable, and 0.2 to 5.0% by mass is more preferable.
  • the content is 0.1% by mass or more, the properties of starting up the hair bundle from the root and the property of maintaining the hairstyle for a long time are more excellent. Moreover, operativity and re-styling property improve that it is 7.0 mass% or less.
  • the content of the component (F) is the total content of all the components (F) in the hairdressing composition of the present invention.
  • the hairdressing composition of the present invention may contain components (other components) other than the components (A) to (F) within a range not impairing the effects of the present invention.
  • the other components are not particularly limited, and examples include components usually used for cosmetics and quasi drugs.
  • surfactants other than component (B) nonionic surfactants other than component (B), anionic surfactants, cationic surfactants, amphoteric surfactants); lower alcohols such as ethanol; Oily components such as polyhydric alcohols, higher alcohols, silicone oils, ester oils, waxes, vegetable oils, hydrocarbon waxes, hydrocarbon oils, oils and fats, higher fatty acids; thickeners other than component (C) and component (D) (hydroxy Methyl cellulose, hydroxypropyl methyl cellulose, xanthan gum, etc.); fragrances; ultraviolet absorbers; antioxidants; sequestering agents; powders other than component (A); pigments; pigments; dyes; Agents; animal and plant extracts; pH adjusters; preservatives; solvents; acids;
  • the hairdressing composition of the present invention does not substantially contain diglycerin, polyglycerin, and dipropylene glycol. That is, the hairdressing composition of the present invention does not contain diglycerin, polyglycerin, and dipropylene glycol, or the total of diglycerin, polyglycerin, and dipropylene glycol in the hairdressing composition of the present invention. It is preferable that content is less than 5.0 mass% with respect to 100 mass% of hairdressing composition of this invention.
  • the total content of diglycerin, polyglycerin, and dipropylene glycol in the hairdressing composition of the present invention is more preferably 1.0% by mass or less, and still more preferably 0.1% by mass or less.
  • the hair styling composition of the present invention preferably has a viscosity (25 ° C.) of 5000 mPa ⁇ s or more from the viewpoint that it is difficult to sag from the hand when applied to hair and is excellent in handleability.
  • the “viscosity (25 ° C.)” can be measured at 25 ° C. using a Brookfield rotary viscometer, for example.
  • the consistency (25 ° C.) of the hairdressing composition of the present invention is preferably 50 gf or less, more preferably 30 gf or less, from the viewpoint of easy scooping when the finger is scooped from the container and excellent handleability.
  • the “consistency (25 ° C.)” can be measured, for example, using a consistency meter equipped with a 17 ⁇ flat adapter at 25 ° C., a speed of 60 mm / min, and a stroke of 20 mm.
  • Examples of the consistency meter include “RHEO METER” manufactured by Sun Kagaku Co., Ltd.
  • the properties of the hairdressing composition of the present invention are preferably in the form of a gel or a grease from the viewpoint that it is difficult to sag from the hand when applied to the hair and is excellent in handleability, and is filled in a jar container or the like. From the viewpoint of taking an appropriate amount with a finger from a container and using it, a grease shape is particularly preferable. That is, the hair styling composition of the present invention is preferably a gel-like hair styling composition or a grease-like hair styling composition (referred to as hair grease, water grease, water-soluble pomade, etc.), particularly preferably grease. Hair-styling composition.
  • the hair styling composition of the present invention is not particularly limited and can be produced by a known or conventional method.
  • it can be produced by a method of stirring and homogenizing the above components with a disper mixer, paddle mixer or the like.
  • the hair styling composition of the present invention is not particularly limited, but can be used, for example, in a form filled in a container.
  • the container include a bottle container, a jar container, and a tube container.
  • the hairdressing composition of the present invention is in a gel form, a bottle container, a tube container, or a jar container is preferable, and the hairdressing composition of the present invention is in the form of a grease. In some cases, jars are preferred.
  • the hair styling composition of the present invention is an aqueous hair styling composition containing component (E) and is excellent in coatability. And as a main hair-styling component, a component (B1) and a component (B2) are used as a component (B).
  • the composition (B1) has the property of raising the hair bundle from the roots, while being able to be sufficiently eliminated, and the component (B2) has the characteristic of maintaining the hairstyle after styling for a long time.
  • the hairdressing composition of this invention uses a combination of a component (C) and a component (D) as a thickener.
  • the component (C) is considered to be due to the interaction with the component (B) while increasing the viscosity of the hairdressing composition, but it increases the elasticity of the hairdressing composition and suppresses the decrease in viscosity under shear. it can.
  • the stickiness increases, the wash-out property is deteriorated, and the elasticity of the hairdressing composition becomes too high, so that the finger from the container is removed. There arises a problem that the operability is lowered such as which one is lowered.
  • the hairdressing composition is moderately thickened while suppressing an excessive increase in elasticity due to the component (C). .
  • the hairdressing composition is moderately thickened while suppressing an excessive increase in elasticity due to the component (C).
  • the component (A) is a thickening component
  • the adhesion between the hairs is appropriately dispersed, so that it is moderately fine due to the synergistic effect with the component (B1) that has a certain degree of hardness while having tackiness. Hair bundles can be formed, and glossiness is suppressed.
  • the stickiness of the hair mainly due to the component (C) is suppressed, and the wash-off property is improved.
  • the hairdressing composition when taken from the container with a finger, the trace remains on the surface of the hairdressing composition. Disappears, the surface of the hairdressing composition in the container is naturally smooth, and the aesthetics are excellent.
  • surface is the compounding quantity (namely, compounding quantity of the active ingredient in each raw material) of each component, and unless otherwise indicated, it represents with "mass%".
  • “-” in the blending amount indicates that the component is not blended.
  • Test Example 9 Evaluation of surface appearance
  • Test Example 1 after the hairdressing composition was scraped with a finger from the jar, the surface of the hairdressing composition in the jar after 30 minutes was observed.
  • the surface of the hairdressing composition obtained in the examples had a finger scraping mark almost or completely disappeared, and was a smooth surface.
  • the hair styling composition (Example) of the present invention is excellent in the property of starting up the hair bundle from the root and maintaining the hairstyle for a long time, can form a fine hair bundle, and suppresses glossiness after hair styling. Therefore, it was possible to obtain a hairstyle that had a natural finish while being excellently arranged and sufficiently addicted. Moreover, it was excellent in handleability, and also had good applicability to hair and was excellent in operability. On the other hand, when the component (A) was not blended (Comparative Example 1), a fine hair bundle could not be formed, and the hair that had been trimmed had a surface shape. In addition, there was an unnatural luster after hair styling, and the properties of holding the hairstyle for a long time were inferior.
  • the viscosity of the hairdressing composition decreases under shear, so that it is difficult to scrape a sufficient amount of the hairdressing composition from the jar container and the handling property is poor. It was. In addition, the hair could not be sufficiently crushed during hair styling, and the arrangement power and hair bundle properties were poor from the root. Further, when the total content of the component (B1) and the component (B2) is less than 3.0% by mass (Comparative Example 5), the hair is shaped as if the hair is crushed along the shape of the wig, and the hair It was inferior in the properties of raising the bundle from the root, could not form a fine hair bundle, and had a glossy feeling after hair styling.
  • the present invention relates to a hair styling composition used for a hair styling agent for shaping hair.
  • the hair styling composition of the present invention is preferably a gel hair styling composition or a grease-like hair styling composition (referred to as hair grease, water grease, water-soluble pomade, etc.), particularly preferably a grease-like hair styling. Agent composition.

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Abstract

L'invention concerne une composition d'agent de coiffage qui présente une excellente exploitabilité lors du coiffage, peut former des mèches de cheveux fins, qui est excellente en termes de caractéristiques de lissage de mèches de cheveux (capacité d'arrangement), pour amener des mèches de cheveux à se dresser à partir des racines et à maintenir une coiffure pendant une longue période de temps, et pour supprimer la brillance après la coiffure. La composition d'agent de coiffage contient : A, une ou plusieurs poudres choisies dans le groupe constitué par la silice, le talc, l'oxyde de titane et le mica ; B, l'huile de ricin durcie par polyoxyéthylène comprenant B1 (huile de ricin durcie par polyoxyéthylène ayant une moyenne de 45 à 65 moles ajoutées d'EO) et B2 (huile de ricin durcie de polyoxyéthylène ayant une moyenne de 75 à 125 moles ajoutées d'EO) ; C, un polymère obtenu à l'aide d'acide (méth)acrylique et/ou d'un ester alkylique d'acide (méth)acrylique et un acide (méth)acrylique de polyoxyéthylène alkyl éther ; D, un polymère de carboxyvinyle et/ou un polymère de carboxyvinyle modifié par alkyle ; et E, de l'eau. La teneur en composant A est de 0,5 à 5,0 % en masse, la teneur totale des composants B1 et B2 est de 3,0 à 25,0 % en masse, la teneur en composant C est de 0,1 à 1,5 % en masse, la teneur en composant D est de 0,05 à 1,5 % en masse, et le rapport de masse [B1/(B1 + B2)] est de 0,1 à 0,9.
PCT/JP2018/010101 2017-04-27 2018-03-15 Composition d'agent de coiffage WO2018198563A1 (fr)

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JPWO2021186993A1 (fr) * 2020-03-19 2021-09-23
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KR20190091498A (ko) 2019-08-06
JP6793820B2 (ja) 2020-12-02
JP6784834B2 (ja) 2020-11-11
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KR20190091315A (ko) 2019-08-05
JPWO2018198564A1 (ja) 2019-11-07
CN110177538A (zh) 2019-08-27
KR102226577B1 (ko) 2021-03-11
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