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KR102245847B1 - Pla mask pack and preparing method thereof - Google Patents

Pla mask pack and preparing method thereof Download PDF

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KR102245847B1
KR102245847B1 KR1020190044818A KR20190044818A KR102245847B1 KR 102245847 B1 KR102245847 B1 KR 102245847B1 KR 1020190044818 A KR1020190044818 A KR 1020190044818A KR 20190044818 A KR20190044818 A KR 20190044818A KR 102245847 B1 KR102245847 B1 KR 102245847B1
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nonwoven fabric
pla
biodegradable pla
weight
mask pack
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KR20200122045A (en
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이광용
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에콜그린텍(주)
이광용
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    • AHUMAN NECESSITIES
    • A45HAND OR TRAVELLING ARTICLES
    • A45DHAIRDRESSING OR SHAVING EQUIPMENT; EQUIPMENT FOR COSMETICS OR COSMETIC TREATMENTS, e.g. FOR MANICURING OR PEDICURING
    • A45D44/00Other cosmetic or toiletry articles, e.g. for hairdressers' rooms
    • A45D44/002Masks for cosmetic treatment of the face
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212Face masks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4326Condensation or reaction polymers
    • D04H1/435Polyesters
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/44Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2401/00Physical properties
    • D10B2401/12Physical properties biodegradable

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
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  • Textile Engineering (AREA)
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  • Biotechnology (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Cosmetics (AREA)

Abstract

본 발명은 생분해성 PLA 마스크팩에 관한 것으로, 더욱 상세하게는 인체 및 환경에 해롭지 않은 식물유래 PLA(Poly Lactic Acid) 소재를 활용하면서 PLA 시트지에 함침된 각종 성분들이 피부층으로 이행되어 미백, 주름개선, 보습 등의 효과가 우수하고 폐기 시 자연분해되는 이행 효과가 우수한 건식 생분해성 PLA 마스크팩 제조방법 및 그 제품에 관한 것이다.
본 발명의 이행 효과가 우수한 건식 생분해성 PLA 마스크팩 제조방법은 엠보싱롤은 140℃ ~ 150℃, 나머지 롤은 50℃ ~ 60℃로 이루어진 압착롤에 수분 흡수율이 0.15중량% 이하의 PLA 레진을 통과시켜 비결정성 생분해성 PLA 부직포를 생산하는 단계; 각종 성분이 함유된 정제수를 생산하는 단계; 생분해성 PLA 부직포를 각종 성분이 함유된 정제수에 디핑한 후 2개의 포리싱롤로 압착하여 강제 침투되도록 하는 단계; 순차적으로 온도가 낮아지는 열풍챔버를 통해 생분해성 PLA 부직포를 건조하는 단계; 건조된 생분해성 PLA 부직포를 프레스로 컷팅하는 단계; 를 포함한다.
The present invention relates to a biodegradable PLA mask pack, and more particularly, while utilizing a plant-derived PLA (Poly Lactic Acid) material that is not harmful to the human body and the environment, various ingredients impregnated on the PLA sheet are transferred to the skin layer to improve whitening and wrinkles. It relates to a method of manufacturing a dry biodegradable PLA mask pack, which has excellent effects such as moisturizing, and has excellent transfer effects that are naturally degraded upon disposal, and its products.
In the method of manufacturing a dry biodegradable PLA mask pack with excellent implementation effect of the present invention, the embossing roll is 140℃ ~ 150℃, and the remaining rolls pass through PLA resin having a moisture absorption rate of 0.15% by weight or less in a compression roll consisting of 50℃ ~ 60℃. To produce an amorphous biodegradable PLA nonwoven fabric; Producing purified water containing various components; Dipping the biodegradable PLA nonwoven fabric in purified water containing various components and then compressing it with two polishing rolls to force penetration; Drying the biodegradable PLA nonwoven fabric through a hot air chamber in which the temperature is sequentially lowered; Cutting the dried biodegradable PLA nonwoven fabric with a press; Includes.

Description

이행 효과가 우수한 건식 생분해성 PLA 마스크팩 제조방법 및 그 제품{PLA MASK PACK AND PREPARING METHOD THEREOF}Dry biodegradable PLA mask pack manufacturing method with excellent transfer effect and its products {PLA MASK PACK AND PREPARING METHOD THEREOF}

본 발명은 생분해성 PLA 마스크팩에 관한 것으로, 더욱 상세하게는 인체 및 환경에 해롭지 않은 식물유래 PLA(Poly Lactic Acid) 소재를 활용하면서 PLA 시트지에 함침된 각종 성분들이 피부층으로 이행되어 미백, 주름개선, 보습 등의 효과가 우수하고 폐기 시 자연분해되는 이행 효과가 우수한 건식 생분해성 PLA 마스크팩 제조방법 및 그 제품에 관한 것이다.The present invention relates to a biodegradable PLA mask pack, and more particularly, while utilizing a plant-derived PLA (Poly Lactic Acid) material that is not harmful to the human body and the environment, various components impregnated in PLA sheet paper are transferred to the skin layer to improve whitening and wrinkles. It relates to a method of manufacturing a dry biodegradable PLA mask pack, which has excellent effects such as moisturizing, and has excellent transfer effects that are naturally degraded upon disposal, and its products.

일반적으로 일회용 마스크팩은 화장수가 적셔져 있는 거즈나 부직포를 얼굴에 붙인 뒤 일정 시간 후에 떼어 냄으로써 보습, 각질 제거, 영양 공급을 하는 미용 팩으로 널리 사용되고 있다.In general, disposable mask packs are widely used as cosmetic packs that moisturize, remove dead skin cells, and supply nutrients by attaching gauze or nonwoven fabric moistened with lotion to the face and removing them after a certain period of time.

최근 들어 환경오염 및 온실가스(CO2) 저감 정책에 따라 유럽 및 국내에서 일회용품 사용규제가 가속화되고 있는데, 대부분의 마스크팩 시트는 화학 합성계 부직포 또는 면, 한지 등에 화학 합성계 단섬유를 함유한 제품으로 이루어진다. Recently, regulations on the use of disposable products are accelerating in Europe and Korea in accordance with policies to reduce environmental pollution and greenhouse gas (CO2), and most mask pack sheets are made of chemically synthetic nonwoven fabrics or products containing chemically synthesized short fibers such as cotton and Korean paper. .

그리고 식물계 셀룰로오스 시트로 제조되는 경우 셀룰로오스 또는 펄프 시트는 제조 시 화학약품과 제조 공정이 까다로워 가격이 비싼 문제점이 있다.In addition, in the case of manufacturing a plant-based cellulose sheet, the cellulose or pulp sheet has a problem in that the price is expensive due to the difficult chemicals and manufacturing process during manufacturing.

이러한 종래의 마스크팩은 습식 방식으로 제조되므로 제조 공정이 까다롭고 보관상에 어려움이 있다. 또한, 수분으로 인해 각종 균이 발생할 수 있으므로 방부제 등과 같은 첨가물을 함유할 수밖에 없다.Since such a conventional mask pack is manufactured by a wet method, a manufacturing process is difficult and storage is difficult. In addition, since moisture can cause various bacteria, it is bound to contain additives such as preservatives.

또한, 펄프, 면, 셀룰로오스 등의 시트지는 수분 흡수율이 높아서 각종 원료를 시트지가 흡수하고 있어 피부층으로 이행되기 어렵고, 오일 성분으로 인해 얼굴에 번들거림이 발생하여 마스크팩 사용 후 메이크업이 어려운 문제점이 있다.In addition, sheet paper such as pulp, cotton, and cellulose has a high moisture absorption rate, so it is difficult to transfer to the skin layer because the sheet paper absorbs various raw materials, and there is a problem in that it is difficult to make makeup after using a mask pack due to oiliness on the face due to the oil component.

KR 등록특허공보 제10-0992398호KR Registered Patent Publication No. 10-0992398

본 발명은 종래와 같은 문제점을 해결하기 위해 창안한 것으로, 인체 및 환경에 해롭지 않은 식물유래 PLA(Poly Lactic Acid) 소재를 활용하면서 PLA 시트지에 함침된 각종 성분들이 피부층으로 이행되어 미백, 주름개선, 보습 등의 효과가 우수하고 폐기 시 자연분해되는 이행 효과가 우수한 건식 생분해성 PLA 마스크팩 제조방법 및 그 제품을 제공하는데 그 목적이 있다.The present invention was invented to solve the problems as in the prior art, while utilizing a plant-derived PLA (Poly Lactic Acid) material that is not harmful to the human body and the environment, various ingredients impregnated in PLA sheet are transferred to the skin layer to whiten, improve wrinkles, Its purpose is to provide a dry biodegradable PLA mask pack manufacturing method and its products with excellent moisturizing effects and excellent transitional effects that are naturally degraded upon disposal.

상기 목적을 달성하기 위한 본 발명에 따른 이행 효과가 우수한 건식 생분해성 PLA 마스크팩 제조방법은,The method of manufacturing a dry biodegradable PLA mask pack having excellent transition effect according to the present invention for achieving the above object,

엠보싱 롤 140℃ ~ 150℃, 나머지 롤 50℃ ~ 60℃로 이루어진 압착롤을 통과시켜 비결정성 생분해성 PLA 부직포를 생산하는 단계;Producing an amorphous biodegradable PLA nonwoven fabric by passing through a pressing roll consisting of an embossing roll of 140°C to 150°C and the remaining rolls of 50°C to 60°C;

각종 성분이 함유된 정제수를 생산하는 단계;Producing purified water containing various components;

생분해성 PLA 부직포를 각종 성분이 함유된 정제수에 디핑한 후 2개의 포리싱롤로 압착하여 강제 침투되도록 하는 단계;Dipping the biodegradable PLA nonwoven fabric in purified water containing various components and then compressing it with two polishing rolls to force penetration;

순차적으로 온도가 낮아지는 열풍챔버를 통해 생분해성 PLA 부직포를 건조하는 단계; 및Drying the biodegradable PLA nonwoven fabric through a hot air chamber in which the temperature is sequentially lowered; And

건조된 생분해성 PLA 부직포를 프레스로 컷팅하는 단계; 를 포함함을 특징으로 한다.Cutting the dried biodegradable PLA nonwoven fabric with a press; It characterized in that it includes.

또한, 상기 비결정성 생분해성 PLA 부직포 생산 단계는,In addition, the amorphous biodegradable PLA nonwoven production step,

스크류 온도는 230℃이며, 압착롤을 통과한 부직포는 20 ~ 40g/㎡임을 특징으로 한다.The screw temperature is 230°C, and the nonwoven fabric passing through the pressing roll is characterized by 20 to 40 g/m 2.

또한, 상기 각종 성분은 허브추출물, 야채, 과일, 곡물류, 약용식물, 수산물, 콩, 두유, 화장품 원료 중 2종 이상의 혼합물임을 특징으로 한다.In addition, the various ingredients are characterized by being a mixture of two or more of herbal extracts, vegetables, fruits, grains, medicinal plants, aquatic products, soybeans, soy milk, and cosmetic ingredients.

또한, 상기 각종 성분이 함유된 정제수를 생산하는 단계는,In addition, the step of producing purified water containing the various components,

정제수 90 ~ 95중량%, 각종 성분 5 ~ 10중량%의 비율로 혼합하고, 정제수 온도 40 ~ 50℃에서 RPM 20 ~ 30의 속도로 60 ~ 80분(10kg 기준) 교반하여 혼합함을 특징으로 한다.It is characterized by mixing in a ratio of 90 to 95% by weight of purified water and 5 to 10% by weight of various components, and mixing by stirring for 60 to 80 minutes (based on 10 kg) at a rate of 20 to 30 RPM at a temperature of 40 to 50°C of purified water. .

또한, 상기 각종 성분에 잔탄검 0.05 ~ 0.5 중량%가 첨가됨을 특징으로 한다.In addition, it is characterized in that 0.05 to 0.5% by weight of xanthan gum is added to the various components.

본 발명에 따른 이행 효과가 우수한 건식 생분해성 PLA 마스크팩 제조방법 및 그 제품은 인체 및 환경에 해롭지 않고 일회용품 규제 대상에서 제외될 수 있으며, 수분흡수율이 0.15중량% 이하에 PLA 시트지를 활용해 각종 성분들이 피부층으로 이행되어 효능을 상승시킬 수 있는 효과가 있다.The method of manufacturing a dry biodegradable PLA mask pack with excellent transition effect according to the present invention and its products are not harmful to the human body and the environment, and can be excluded from the regulation of disposable products, and various ingredients using PLA sheet paper with a moisture absorption rate of 0.15% by weight or less. It has an effect that can increase the efficacy by transferring to the skin layer.

도 1은 본 발명에 따른 이행 효과가 우수한 건식 생분해성 PLA 마스크팩 제조과정을 도시한 공정도.1 is a flow chart showing a process of manufacturing a dry biodegradable PLA mask pack having excellent transition effect according to the present invention.

이하, 본 발명에 따른 이행 효과가 우수한 건식 생분해성 PLA 마스크팩 제조방법의 바람직한 실시 예를 첨부된 도면을 참조하여 상세히 설명한다.Hereinafter, a preferred embodiment of a method for manufacturing a dry biodegradable PLA mask pack having excellent transition effect according to the present invention will be described in detail with reference to the accompanying drawings.

도 1은 본 발명에 따른 이행 효과가 우수한 건식 생분해성 PLA 마스크팩 제조과정을 도시한 것으로, 도면에 도시된 바와 같이 비결정성 생분해성 PLA 부직포를 생산하는 단계; 각종 성분이 함유된 정제수를 생산하는 단계; 포리싱롤을 이용하여 압착시켜 강제 침투시키는 단계; 열풍챔버를 통해 건조하는 단계; 컷팅하는 단계; 로 이루어진다.1 is a diagram showing a process of manufacturing a dry biodegradable PLA mask pack having an excellent transition effect according to the present invention, the steps of producing an amorphous biodegradable PLA nonwoven fabric as shown in the drawings; Producing purified water containing various components; Compressing using a polishing roll and forcibly penetrating it; Drying through a hot air chamber; Cutting; Consists of

[비결정성 생분해성 PLA 부직포를 생산하는 단계][Step of producing amorphous biodegradable PLA nonwoven fabric]

PLA 소재는 브리틀(brittle) 한 특성으로 인해 깨지거나 인장강도가 약하여 저중량(40g/㎡) 생산이 어렵고 결정화(Crystallization)가 되면 하드(Hard)한 특성으로 인해 마스크팩으로 사용할 시 얼굴에 밀착력 및 부착력이 약하여 떨어질 수 있다. 이러한 문제를 해결하기 위해 PLA 스판본딩 부직포 생산시 스크류 온도를 230℃로 하여 생산하되 비결정화가 되도록 2개의 압착롤을 통과시켜 40g/㎡ 이하의 비결정성 생분해성 PLA 부직포를 생산한다.PLA material is brittle due to its brittle properties, and it is difficult to produce low weight (40g/㎡) due to its weak tensile strength. It may fall off due to weak adhesion. In order to solve this problem, when producing PLA spunbonding nonwoven fabric, the screw temperature is set to 230℃, but amorphous biodegradable PLA nonwoven fabric of 40g/m² or less is produced by passing two pressing rolls to make it amorphous.

상기 압착롤 중 엠보싱 롤은 140℃ ~ 150℃로 하고, 나머지 롤은 50℃ ~ 60℃가 되도록 한다. 여기서 방사된 장섬유 PLA 화이버의 강도 보강을 위해 압착롤 중 엠보싱 롤의 온도가 140℃ 이하가 되면 PLA 레진이 용융되지 않아 스판본딩 부직포에 인장강도가 약해지고, 150℃ 이상이면 PLA 화이버에 열이 전달되어 결정화가 될 수 있으며, 나머지 일반 롤의 온도가 60℃ 이상이면 PLA 화이버가 결정화될 수 있다.Among the pressing rolls, the embossing roll is 140°C to 150°C, and the remaining rolls are 50°C to 60°C. In order to reinforce the strength of the long-fiber PLA fiber spun here, if the temperature of the embossing roll among the pressing rolls is below 140℃, the PLA resin does not melt and the tensile strength of the spunbonded nonwoven fabric is weakened. It can be crystallized, and PLA fibers can be crystallized if the temperature of the rest of the general rolls is 60°C or higher.

상기와 같이 비결정성 PLA 스판본딩 부직포를 생산하되 마스크팩에 상용되는 중량은 20 ~ 40g/㎡로 바람직하게는 25g/㎡를 사용한다. 여기서 중량이 20g/㎡ 이하일 경우 각종 성분을 함침할 때 문제가 될 수 있고, 40g/㎡ 이상일 경우 얼굴에 부착시 밀착력이 떨어질 수 있다.As described above, an amorphous PLA spunbonding nonwoven fabric is produced, but the weight used in the mask pack is 20 to 40g/m2, preferably 25g/m2. Here, if the weight is less than 20g/m2, it may be a problem when impregnating various components, and if it is more than 40g/m2, adhesion to the face may decrease.

[각종 성분이 함유된 정제수를 생산하는 단계][Step of producing purified water containing various ingredients]

각종 성분은 식품의약품 안전처 규정에 준하는 성분을 사용할 수 있고, 허브추출물, 야채, 과일, 곡물류, 약용식물, 수산물 등과 같은 추출물과 콩, 두유와 같이 발효된 식품 및 화장품 원료 등의 2종 이상 혼합물을 사용한다.Various ingredients can use ingredients that comply with the regulations of the Ministry of Food and Drug Safety, and a mixture of two or more such as extracts such as herbal extracts, vegetables, fruits, grains, medicinal plants, aquatic products, and fermented food and cosmetic ingredients such as soybeans and soy milk. Use.

여기서 각종 성분은 멜라노사이트 내의 멜라닌 생성 억제와 이미 생겨 침착된 멜라닌을 제거하여 뽀얗고 투명한 잡티 없는 피부를 만드는 화이트닝 에센스, 피부 보호를 통해 탄력을 되찾고 주름을 완화하는 안티에이징 에센스, 피지 분비를 억제하고 염증을 완화하며 피부 결점 생성을 방지해 번들거리지 않고 뽀송뽀송한 피부를 유지하는 피지 정상화 에센스, 수분공급 에센스, 민감한 피부를 진정시키는 민감성 에센스, 아침에 피부를 깨우고 수분과 비타민을 공급하며 밤에는 진정시켜 메인 트리트먼트의 흡수력을 높여주는 부스터 에센스 등이 이용된다.Here, various ingredients are whitening essence that suppresses the production of melanin in melanocytes and removes melanin that has already formed and deposited to make the skin white and transparent and blemishes, an anti-aging essence that restores elasticity and relieves wrinkles through skin protection, and suppresses sebum secretion and inflammation. The sebum normalizing essence that keeps the skin dry and smooth by preventing the creation of skin blemishes, moisturizing essence, sensitive essence that soothes sensitive skin, wakes up the skin in the morning, supplies moisture and vitamins, and soothes at night. Booster essences are used to increase the absorption power of the main treatment.

각종 성분의 비율은 정제수 95 ~ 90중량%에 각종 성분 5 ~ 10중량%의 비율로 혼합한 후 정제수 온도 40 ~ 50℃에서 회전속도 20 ~ 30 RPM으로 10kg 기준 60 ~ 80분 교반하여 혼합한다. 여기서 각종 성분의 함량이 5중량% 이하면 효능이 떨어질 수 있고, 10중량% 이상이면 분산성이 떨어지거나 겔화되어 PLA 부직포에 함침시 문제가 발생할 수 있다. 또한, 정제수 온도가 40℃ 이하이면 분산성이 떨어지고, 50℃ 이상이면 각종 원료가 반응하여 겔화될 수 있다.The ratio of various components is mixed with 95 to 90% by weight of purified water in a ratio of 5 to 10% by weight of various components, and then stirred for 60 to 80 minutes based on 10 kg at a rotation speed of 20 to 30 RPM at a temperature of 40 to 50°C of purified water and mixed. Here, if the content of various components is 5% by weight or less, the efficacy may be reduced, and if the content is 10% by weight or more, the dispersibility may decrease or gelation may cause problems when impregnating the PLA nonwoven fabric. In addition, when the purified water temperature is 40°C or less, dispersibility is inferior, and when the purified water temperature is 50°C or more, various raw materials may react and gel.

한편, 각종 성분 5 ~ 10중량% 중 잔탄검에 첨가는 0.05 ~ 0.5중량%가 첨가되어 있으며 건식 마스크팩 사용 시 정제수에 담근 후 얼굴에 부착시 결착력, 밀착력을 향상시킬 수 있도록 한다. 여기서 잔탄검이 0.5중량% 이상이면 겔화될 수 있고, 0.05중량% 이하이면 밀착력이 약화될 수 있다.On the other hand, out of 5 to 10% by weight of various ingredients, 0.05 to 0.5% by weight of xanthan gum is added, and when using a dry mask pack, it is immersed in purified water to improve adhesion and adhesion when attached to the face. Here, if xanthan gum is 0.5% by weight or more, it may be gelled, and if it is less than 0.05% by weight, adhesion may be weakened.

[부직포를 정제수에 디핑 후 포리싱롤로 압착하는 단계][Step of dipping the nonwoven fabric in purified water and then pressing it with a polishing roll]

생분해성 PLA 부직포를 각종 성분이 혼합된 원료에 디핑한 후 2개의 포리싱롤로 압착하여 생분해성 PLA 부직포 화이버 속으로 각종 성분이 강제 침투되도록 한다.After dipping the biodegradable PLA nonwoven fabric into the raw material mixed with various ingredients, it is pressed with two polishing rolls to force various ingredients to penetrate into the biodegradable PLA nonwoven fabric fiber.

생분해성 PLA 부직포는 수분 흡수율이 0.15중량% 이하이기 때문에 디핑 후 압착하지 않고 건조하면 각종 성분이 생분해성 PLA 부직포에 흡수되지 않으므로 압착공정이 필수적으로 이루어져야 한다.Since the biodegradable PLA nonwoven fabric has a water absorption rate of 0.15% by weight or less, various components are not absorbed by the biodegradable PLA nonwoven fabric if it is dried without pressing after dipping, so a compression process must be performed.

[열풍챔버를 통해 건조하는 단계][Drying through a hot air chamber]

각종 성분이 침투된 생분해성 PLA 부직포는 순차적으로 온도가 낮아지는 열풍챔버를 통해 생분해성 PLA 부직포를 건조한다.The biodegradable PLA nonwoven fabric in which various components have penetrated is dried through a hot air chamber in which the temperature is sequentially lowered.

1번 챔버의 온도는 95℃, 2번 챔버의 온도는 85℃, 3번 챔버의 온도는 75℃, 4번 챔버의 온도는 65℃ 순서로 25g/㎡일 때 60초 동안 8m ~ 9m가 생산되도록 건조한다.The temperature of chamber 1 is 95℃, the temperature of chamber 2 is 85℃, the temperature of chamber 3 is 75℃, and the temperature of chamber 4 is 65℃. When the temperature is 25g/㎡, 8m to 9m are produced for 60 seconds. Dry as much as possible.

여기서 열풍챔버의 온도가 95℃ 이상이면 생분해성 PLA 부직포가 결정화되어 브리틀 한 특성으로 얼굴에 밀착력이 떨어질 수 있다. 이때 건조 후 부직포 중량 대비 각종 성분에 함침량은 15 ~ 20중량%가 함침되었다.Here, when the temperature of the hot air chamber is 95℃ or higher, the biodegradable PLA nonwoven fabric is crystallized and the adhesion to the face may decrease due to its brittle characteristic. At this time, after drying, the amount of impregnation in various components relative to the weight of the nonwoven fabric was impregnated in 15 to 20% by weight.

[컷팅하는 단계][Steps to cut]

마지막으로 건조된 생분해성 PLA 부직포를 프레스로 컷팅 한다. Finally, the dried biodegradable PLA nonwoven fabric is cut with a press.

생분해성 PLA 부직포는 얼굴 팩 또는 눈 팩, 코 팩, 손 팩, 미소 팩 등과 같이 사용되는 부위에 맞추어 컷팅하고, 포장하여 완료한다.The biodegradable PLA non-woven fabric is finished by cutting and wrapping according to the areas used such as face packs, eye packs, nose packs, hand packs, and smile packs.

PLA 단섬유를 스판본딩 부직포로 제조하여 사용할 수도 있고, PLA 단섬유와 면, 한지, 펄프 등과 함께 혼합하여 사용할 수도 있음을 밝혀둔다.It should be noted that short PLA fibers can be manufactured and used as spunbonded nonwoven fabrics, or they can be mixed with PLA short fibers and cotton, Korean paper, and pulp.

[실험 1] 피부층 이행 효과[Experiment 1] Skin layer transition effect

A 타입 : 생분해성 PLA 스판본딩 부직포 25g/㎡에 각종 성분이 (건조중량) 20중량%가 함침된 건식 마스크팩Type A: Dry mask pack in which 20% by weight of various ingredients (dry weight) is impregnated with 25g/㎡ of biodegradable PLA spunbonding nonwoven fabric

B 타입 : 생분해성 PLA 단섬유 80중량%, 면 20중량%로 제조된 부직포 25g/㎡에 각종 성분이 (건조중량) 20중량%가 되도록 함침된 건식 마스크팩Type B: A dry mask pack impregnated with 20% by weight of various components (dry weight) in 25g/㎡ of nonwoven fabric made of 80% by weight of biodegradable PLA short fiber and 20% by weight of cotton.

C 타입 : 면 80중량%, PP 단섬유로 제조된 부직포 25g/㎡에 각종 성분이 (건조중량) 20중량%가 되도록 함침된 건식 마스크팩Type C: Dry mask pack impregnated with 80% by weight of cotton and 25g/㎡ of non-woven fabric made of short PP fiber so that various components are 20% by weight (dry weight)

[실험 방법][Experiment method]

① 상기 건식 마스크팩을 정제수 100g에 각각 30초씩 담근 후 얼굴에 부착① Soak the above dry mask pack in 100g of purified water for 30 seconds each and attach it to your face.

② 얼굴에 15분 동안 부착 후 중량 변화 체크② Check the weight change after attaching it to the face for 15 minutes

③ A, B, C 타입 각각에 얼굴 마스크팩 1EA에 부직포 중량은 평균 1.4 중량%이고, 각종 성분이(건조중량) 함침된 중량은 평균 0.028중량g으로 최종 중량은 1.68중량g이다.③ For each of the types A, B, and C, the weight of the nonwoven fabric in 1EA of the face mask pack is 1.4% by weight on average, and the weight of various components (dry weight) impregnated is 0.028% by weight, and the final weight is 1.68% by weight.

④ 각종 성분이 피부층으로 이행되는 중량변화로 15분 후 얼굴에서 마스크팩 제거 후 수분 함량 5중량% 이하가 되도록 건조한 후 중량 변화 체크④ As the weight change in which various ingredients are transferred to the skin layer, remove the mask pack from the face after 15 minutes, dry it so that the moisture content is less than 5% by weight, and check the weight change.

⑤ 1회 사용 후 4번처럼 정제수 50g에 각각 30초씩 담근 후 2회 ~ 3회 반복 사용⑤ After use once, soak in 50g of purified water for 30 seconds, like No. 4, and use 2 to 3 times repeatedly.

최종 중량Final weight 1회 사용 후 중량Weight after one use 2회 사용 후 중량Weight after 2 use 3회 사용 후 중량Weight after 3 times of use A 타입A type 1.68g1.68g 1.51g1.51g 1.48g1.48g 1.42g1.42g B 타입B type 1.68g1.68g 1.59g1.59g 1.54g1.54g 1.51g1.51g C 타입C type 1.68g1.68g 1.62g1.62g 1.58g1.58g 1.56g1.56g

상기 데이터는 5회 테스트 평균 수치임.The above data are average values of 5 tests.

[결과][result]

상기와 같은 타입의 마스크팩은 각종 성분이 피부층으로 이행되어 우수한 효능이 있었고, 수분 흡수율이 많은 C 타입은 각종 성분이 마스크팩에 흡수되어 피부층으로 이행되는 양이 적어 효능이 떨어지는 결과를 보임.The above type of mask pack has excellent efficacy because various ingredients are transferred to the skin layer, and type C, which has a high moisture absorption rate, shows a result of inferior efficacy because various ingredients are absorbed into the mask pack and the amount transferred to the skin layer is small.

Claims (6)

스크류 온도 230℃, 엠보싱 롤 140℃ ~ 150℃, 나머지 롤 50℃ ~ 60℃로 이루어진 압착롤을 통과시켜 20 ~ 40g/㎡의 비결정성 생분해성 PLA 부직포를 생산하는 단계;
정제수 90 ~ 95중량%, 각종 성분 5 ~ 10중량%의 비율로 혼합하고, 정제수 온도 40 ~ 50℃에서 RPM 20 ~ 30의 속도로 60 ~ 80분(10kg 기준) 교반하여 각종 성분이 함유된 정제수를 생산하는 단계;
생분해성 PLA 부직포를 각종 성분이 함유된 정제수에 디핑한 후 2개의 포리싱롤로 압착하여 강제 침투되도록 하는 단계;
순차적으로 온도가 낮아지는 열풍챔버를 통해 생분해성 PLA 부직포를 건조하는 단계;
건조된 생분해성 PLA 부직포를 프레스로 컷팅하는 단계; 를 포함함을 특징으로 하는 이행 효과가 우수한 건식 생분해성 PLA 마스크팩 제조방법.
Producing an amorphous biodegradable PLA nonwoven fabric of 20 to 40g/m2 by passing through a compression roll consisting of a screw temperature of 230°C, an embossing roll of 140°C to 150°C, and a remaining roll of 50°C to 60°C;
Purified water containing various ingredients by mixing in a ratio of 90 to 95% by weight of purified water and 5 to 10% by weight of various ingredients, and stirring at a rate of 20 to 30 RPM at a temperature of 40 to 50°C for 60 to 80 minutes (10 kg) Producing a;
Dipping the biodegradable PLA nonwoven fabric in purified water containing various components and then compressing it with two polishing rolls to force penetration;
Drying the biodegradable PLA nonwoven fabric through a hot air chamber in which the temperature is sequentially lowered;
Cutting the dried biodegradable PLA nonwoven fabric with a press; Dry biodegradable PLA mask pack manufacturing method having excellent transition effect, characterized in that it comprises a.
제1 항에 있어서, 상기 각종 성분은 허브추출물, 야채, 과일, 곡물류, 약용식물, 수산물, 콩, 두유, 화장품 원료 중 2종 이상의 혼합물임을 특징으로 하는 이행 효과가 우수한 건식 생분해성 PLA 마스크팩 제조방법.
The method of claim 1, wherein the various ingredients are a mixture of two or more of herbal extracts, vegetables, fruits, grains, medicinal plants, aquatic products, soybeans, soy milk, and cosmetic ingredients. Way.
제1 항에 있어서, 각종 성분에 잔탄검 0.05 ~ 0.5 중량%가 첨가됨을 특징으로 하는 이행 효과가 우수한 건식 생분해성 PLA 마스크팩 제조방법.
The method of claim 1, wherein 0.05 to 0.5% by weight of xanthan gum is added to various components.
제1 항 내지 제3 항 중 어느 하나의 항으로 제조된 이행 효과가 우수한 건식 생분해성 PLA 마스크팩.A dry biodegradable PLA mask pack having an excellent transition effect prepared in any one of claims 1 to 3. 삭제delete 삭제delete
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