CN111686065A - Anti-aging moisturizing mask and preparation method thereof - Google Patents
Anti-aging moisturizing mask and preparation method thereof Download PDFInfo
- Publication number
- CN111686065A CN111686065A CN202010664412.0A CN202010664412A CN111686065A CN 111686065 A CN111686065 A CN 111686065A CN 202010664412 A CN202010664412 A CN 202010664412A CN 111686065 A CN111686065 A CN 111686065A
- Authority
- CN
- China
- Prior art keywords
- parts
- mask
- purple sweet
- sweet potato
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Images
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/14—Liposomes; Vesicles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
- A61K8/986—Milk; Derivatives thereof, e.g. butter
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Zoology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses an anti-aging moisturizing mask and a preparation method thereof, wherein the mask is prepared from the following components in parts by weight: 5-15 parts of purple sweet potato anthocyanin nano liposome freeze-dried powder, 2-5 parts of pearl powder, 4-10 parts of milk, 2-4 parts of honey, 3-6 parts of aloe extract, 2-5 parts of hyaluronic acid, 10-20 parts of sweet almond oil, 0.3-0.5 part of bitter orange flower essential oil, 0.05-0.5 part of pH regulator and 50-75 parts of deionized water; weighing raw materials in proportion, preparing into water phase and oil phase, mixing, emulsifying with water, adjusting pH, soaking non-woven fabric film in the mixed solution, vacuumizing to completely combine the mixed solution with the non-woven fabric film, performing sampling inspection, and packaging. The purple sweet potato anthocyanin nano liposome freeze-dried powder is safe in raw material source, and is matched with pure natural pearl powder, sweet almond oil, bitter orange flower essential oil, milk, honey, aloe extract, hyaluronic acid and other auxiliary materials, so that the mask is mild in performance and free of damage to the skin, and the purposes of resisting skin oxidation, deeply replenishing water and delaying aging are achieved.
Description
Technical Field
The invention relates to a mask, in particular to an anti-aging moisturizing mask and a preparation method thereof, and belongs to the field of skin care products and cosmetics.
Background
The anthocyanin is a water-soluble natural pigment widely existing in plants in the nature, belongs to flavonoid compounds, and is also a main color substance in plant petals. Anthocyanins are purely natural anti-aging nutritional supplements. The purple sweet potato anthocyanin is a natural anthocyanin extracted from root tuber, stem leaf and leaves of purple sweet potato, and researches show that the oxidation resistance of the anthocyanin is 3.2 times of that of blueberry anthocyanin, and the expressed free radical scavenging capacity is 20 times and 50 times of that of vitamin C and vitamin E respectively.
The purple sweet potato can be planted in a large scale, has low processing cost, few links and no pollution, and is environment-friendly, so the method is very suitable for industrialized production of anthocyanin. The phenolic hydroxyl contained in the anthocyanins of the purple sweet potatoes is a main active factor with antioxidation, can achieve the effect of preventing peroxidation by combining with protein, can effectively inhibit the generation of peroxide generated by ultraviolet irradiation, promotes blood circulation, accelerates metabolism of a human body, and further achieves the purposes of slowing down the aging of the human body skin, increasing the elasticity of the skin and whitening the skin. The anthocyanins from purple sweet potato are more stable than anthocyanins from other sources, but are still easily affected by external conditions, such as easy oxidation, sensitivity to light, temperature and pH value, and the anthocyanins have the advantages of large molecular weight, complex structure and large particle size, and are not easy to be absorbed by human tissues.
The facial mask is a carrier of a beauty and health care product, temporarily isolates outside air and pollution by using a short time of covering the facial mask on the face, improves the temperature of the skin, expands pores of the skin, promotes secretion and metabolism of sweat glands, increases the oxygen content of the skin, is beneficial to the skin to remove products of metabolism of epidermal cells and accumulated grease substances, and ensures that water in the facial mask permeates into the cuticle of the epidermis, the skin becomes soft, and the skin is naturally bright and elastic. Various whitening and moisturizing masks in the existing market are not numerous, but the functions and effects are general, and many masks contain irritant components such as alcohol and the like, so that the masks cannot be accepted by consumers, and facial allergy and the like are very easy to occur.
Disclosure of Invention
The invention aims to provide an anti-aging moisturizing mask, which utilizes active ingredients in purple sweet potato anthocyanin nano-liposomes to improve the skin care effect of the mask, and has the effects of enhancing oxidation resistance and deeply moisturizing skin.
The invention also aims to provide a preparation method of the anti-aging moisturizing mask, which is simple in industry and can be produced industrially.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
an anti-aging moisturizing mask is prepared from the following components in parts by weight: 5-15 parts of purple sweet potato anthocyanin nano liposome freeze-dried powder, 2-5 parts of pearl powder, 4-10 parts of milk, 2-4 parts of honey, 3-6 parts of aloe extract, 2-5 parts of hyaluronic acid, 10-20 parts of sweet almond oil, 0.3-0.5 part of bitter orange flower essential oil, 0.05-0.5 part of pH regulator and 50-75 parts of deionized water.
Preferably, the purple sweet potato anthocyanin nano liposome freeze-dried powder comprises 10 parts of pearl powder, 7 parts of milk, 3 parts of honey, 5 parts of aloe extract, 4 parts of hyaluronic acid, 15 parts of natural sweet almond oil, 0.5 part of bitter orange flower essential oil and 65 parts of deionized water.
Further, the purple sweet potato anthocyanin nano liposome freeze-dried powder is prepared by adopting an ethanol injection-dynamic high-pressure micro-jet method.
Further, the ethanol injection-dynamic high pressure micro-jet method comprises the following specific steps: dissolving 10-100 parts by weight of purple sweet potato anthocyanin in 5000-9000 parts by weight of phosphate buffer solution with pH value of 6.0, adding 5000-9000 parts by weight of cholesterol, 700-1200 parts by weight of phospholipid and 1-5 parts by weight of tween-80, and fully mixing to obtain a mixed solution; injecting 1000-5000 parts by weight of absolute ethyl alcohol into the mixed solution under the condition of rapid stirring, homogenizing at a high speed, removing the absolute ethyl alcohol through vacuum rotary evaporation, and performing constant volume by using a phosphate buffer solution with the pH value of 6.0 to obtain the purple sweet potato anthocyanin crude liposome; then adding the mixture into a high-pressure micro-jet homogenizer, and treating for 3-30 times under the pressure of 800-1000 bar to obtain purple sweet potato anthocyanin nano liposome emulsion; adding a freeze-drying protective agent, pre-freezing for 24 hours at-60 ℃, and then putting the mixture into a freeze dryer for freeze drying, wherein the temperature is controlled between-62 ℃ and-60 ℃, so as to obtain the freeze-dried powder of the anthocyanidin nanoliposome of the purple sweet potatoes.
Preferably, the phospholipid is soybean lecithin.
Preferably, the pH adjusting agent is citric acid.
The preparation method of the anti-aging moisturizing mask specifically comprises the following steps:
(1) mixing purple sweet potato anthocyanin nano liposome lyophilized powder, pearl powder, aloe extract, hyaluronic acid, honey and milk uniformly according to a proportion to prepare a water phase;
(2) mixing sweet almond oil and bitter orange flower essential oil uniformly according to a proportion to prepare an oil phase;
(3) mixing the oil phase and the water phase, adding deionized water in proportion, and emulsifying at room temperature to obtain a facial mask mixed solution;
(4) adjusting the pH value to 6.0-6.5 by using a pH regulator;
(6) soaking the non-woven fabric film in the mask mixed solution, then transferring the non-woven fabric film into a vacuum box, and vacuumizing for 5-10 min to completely combine the mask mixed solution with the non-woven fabric film;
(7) randomly performing spot inspection, subpackaging, sealing and labeling after the inspection is qualified.
Preferably, the soaking time of the non-woven fabric film is 20-30 min.
Preferably, the non-woven fabric film is made of natural chitosan, and is good in air permeability and strong in repairing function.
The purple sweet potato anthocyanin has strong functions of resisting oxidation and scavenging free radicals, enables the skin to be smooth and elastic through inhibiting elastase and collagenase, and can prevent the skin from being damaged due to excessive sunshine from the inside and the outside.
The pearl powder in the invention has the functions of whitening, controlling oil and the like, and can effectively solve the problems of face oil, dead skin and the like; and has anti-aging effect by enhancing SOD activity.
The aloe extract is extracted from aloe vera, contains natural physiological water, mineral substances and lignin, has extremely strong permeability, can form a thin breathable film on the surface layer of the skin while permeating to the deep layer of the skin, prevents the evaporation of skin moisture, simultaneously enables the moisture to permeate into the skin, and can help to recover the original smoothness, softness and good elasticity of the skin; the whitening cream is rich in various amino acids and natural whitening and moisturizing factors, can be directly absorbed by skin, and can decompose and convert pigmentation to achieve natural moisturizing and whitening; is rich in monosaccharide, polysaccharide, vitamins and minerals, has antioxidant effect, and has obvious effect in treating cell aging and reducing wrinkle.
The hyaluronic acid in the invention is a natural biomolecule widely existing in skin and other tissues, has excellent moisturizing effect, and is known as an "ideal natural moisturizing factor". The hyaluronic acid aqueous solution has very high viscosity, can thicken the water phase, is uniform and fine with the paste after the mailbox emulsification, and has stable emulsification; hyaluronic acid can promote proliferation and differentiation of epidermal cells, remove oxygen free radicals, and delay skin aging.
The sweet almond oil has good skin-friendly property, contains high nutrient, and is good moistening and mixed oil. Is suitable for infants, dry skin, wrinkle, acne and sensitive skin.
The bitter orange flower essential oil is extracted from bitter orange white petals and has the nerve calming effect. The whitening cream is rich in various whitening active ingredients, can lead out melanin formed in skin layer by layer under the mediation of aromatic factors, and is discharged along with the metabolism of aged cutin, thereby achieving the purposes of whitening and spot fading.
Compared with the prior art, the invention has the following beneficial effects:
1. the anti-aging moisturizing mask disclosed by the invention is added with the purple sweet potato anthocyanin nano liposome freeze-dried powder, and the special purple sweet potato anthocyanin which is wide in source and encapsulated by the nano liposome is adopted, so that the influence of the external operating environment on the purple sweet potato anthocyanin is reduced, the stability of the anthocyanin is effectively improved, the loss of the anthocyanin in the processing process is reduced, the effective content of the anthocyanin in the product is greatly improved, the granularity is greatly reduced, the nutritional ingredients are easily absorbed by the skin, the anti-aging moisturizing mask has higher bioavailability, and the effect of the product is greatly improved.
2. The purple sweet potato anthocyanin nano liposome freeze-dried powder is safe in raw material source, and is matched with pure natural pearl powder, sweet almond oil, bitter orange flower essential oil, milk, honey, aloe extract, hyaluronic acid and other auxiliary materials, so that the mask is mild in performance and does not harm to skin; and the purple sweet potato anthocyanin nano liposome freeze-dried powder, the pearl powder, the aloe extract, the hyaluronic acid, the sweet almond oil and the bitter orange flower essential oil are combined together, have a synergistic effect, can remarkably enhance the whitening effect, and achieve the purposes of preventing the aging of horny layer, deeply replenishing water and delaying aging.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings used in the description of the embodiments will be briefly introduced below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art that other drawings can be obtained according to the drawings without creative efforts.
FIG. 1 is a process flow chart of the preparation of purple sweet potato anthocyanin nano-liposome freeze-dried powder of the invention;
fig. 2 is a process flow chart of the anti-aging moisturizing mask prepared by the invention.
Detailed Description
In order to facilitate a better understanding of the invention, the following examples are given to illustrate, but not to limit the scope of the invention. The invention is described in further detail below with reference to the figures and specific examples.
The lyophilized powder of anthocyanidin nanoliposome of purple sweet potato in the following examples is prepared by ethanol injection-dynamic high pressure micro-jet method.
As shown in fig. 1, the specific steps are: dissolving 10-100 parts by weight of purple sweet potato anthocyanin in 5000-9000 parts by weight of phosphate buffer solution with pH value of 6.0, adding 5000-9000 parts by weight of cholesterol, 700-1200 parts by weight of soybean lecithin and 1-5 parts by weight of tween-80, and fully mixing to obtain a mixed solution; injecting 1000-5000 parts by weight of absolute ethyl alcohol into the mixed solution under the condition of rapid stirring, homogenizing at a high speed, removing the absolute ethyl alcohol through vacuum rotary evaporation, and performing constant volume by using a phosphate buffer solution with the pH value of 6.0 to obtain the purple sweet potato anthocyanin crude liposome; then adding the mixture into a high-pressure micro-jet homogenizer, and treating for 3-30 times under the pressure of 800-1000 bar to obtain purple sweet potato anthocyanin nano liposome emulsion; adding a freeze-drying protective agent, pre-freezing for 24 hours at-60 ℃, and then putting the mixture into a freeze dryer for freeze drying, wherein the temperature is controlled between-62 ℃ and-60 ℃, so as to obtain the freeze-dried powder of the anthocyanidin nanoliposome of the purple sweet potatoes.
The facial mask prepared in the examples was subjected to a moisturizing performance test and a liquid absorption test, respectively, to further illustrate the efficacy of the facial mask.
1. Water supplement performance test
(1) Laying multiple layers of filter paper in a glass dish, cutting the first layer cowhide into 6cm × 6cm, laying on the multiple layers of filter paper, and naming the combination of glass dish, filter paper and first layer cowhide as simulated skin, and weighting as A0。
(2) The mask base cloth was cut into 5cm × 5cm samples, weighed and recorded as m0. And then, soaking the mask base cloth in the mask mixed solution, vacuumizing, taking out, standing vertically until no liquid drops, weighing, and recording as m.
(3) The moist mask was laid flat on the simulated skin and the timer was started. Every 1min, the mask was peeled off the simulated skin, the simulated skin weight was weighed and recorded as At。
(4) With the increase of time, the concentration difference of the moisture or the essence in the simulated skin and the facial mask is smaller and smaller, the simulated skin can not absorb the moisture or the essence any more, and the time at this moment is recorded as T.
2. Liquid absorption amount test
(1) Taking a certain amount of facial mask base cloth, weighing, and recording as M0. Fully mixing the weighed mask base cloth with the mask mixed solution, vacuumizing, taking out, standing vertically, weighing after no liquid drops, and recording as M1
(2) Loading the liquid-absorbed facial mask base cloth into a centrifugal sleeve with small holes at the bottom, centrifuging at 3000r/min for 10min, taking out the non-woven cloth, weighing, and recording as M2. The liquid absorption amount of the sample was calculated according to the following formula:
example 1
An anti-aging moisturizing mask is prepared from the following components in parts by weight: 10 parts of purple sweet potato anthocyanin nano liposome freeze-dried powder, 4 parts of pearl powder, 7 parts of milk, 3 parts of honey, 5 parts of aloe extract, 4 parts of hyaluronic acid, 15 parts of natural sweet almond oil, 0.5 part of bitter orange flower essential oil, 0.25 part of citric acid and 65 parts of deionized water.
As shown in fig. 2, the preparation method comprises the following steps:
(1) mixing purple sweet potato anthocyanin nano liposome lyophilized powder, pearl powder, aloe extract, hyaluronic acid, honey and milk uniformly according to a proportion to prepare a water phase;
(2) mixing sweet almond oil and bitter orange flower essential oil uniformly according to a proportion to prepare an oil phase;
(3) mixing the oil phase and the water phase, adding deionized water in proportion, and performing emulsification treatment at room temperature of 25 ℃ to obtain a facial mask mixed solution;
(4) adjusting the pH value to 6.0 by using citric acid;
(6) soaking the natural chitosan non-woven fabric film in the facial mask mixed solution for 25min, then transferring the natural chitosan non-woven fabric film into a vacuum box, and vacuumizing for 10min to completely combine the facial mask mixed solution with the non-woven fabric film;
(7) randomly performing spot inspection, subpackaging, sealing and labeling after the inspection is qualified.
The using method comprises the following steps: and taking out the mask paper, unfolding the mask paper, pasting the mask paper on the face to avoid the nose, eyes and mouth parts, completely pasting the mask and the face, taking down the mask after static application for 10-20 min, and cleaning the mask with clear water.
Through tests, the liquid absorption of the facial mask prepared in the embodiment reaches 29.41, and the liquid supplementing rate reaches the maximum value of 91.38% when T is 9 min.
Example 2
An anti-aging moisturizing mask is prepared from the following components in parts by weight: 5 parts of purple sweet potato anthocyanin nano liposome freeze-dried powder, 2 parts of pearl powder, 4 parts of milk, 2 parts of honey, 3 parts of aloe extract, 2 parts of hyaluronic acid, 10 parts of sweet almond oil, 0.3 part of bitter orange flower essential oil, 0.05 part of citric acid and 50 parts of deionized water.
The preparation steps are as follows:
(1) mixing purple sweet potato anthocyanin nano liposome lyophilized powder, pearl powder, aloe extract, hyaluronic acid, honey and milk uniformly according to a proportion to prepare a water phase;
(2) mixing sweet almond oil and bitter orange flower essential oil uniformly according to a proportion to prepare an oil phase;
(3) mixing the oil phase and the water phase, adding deionized water in proportion, and performing emulsification treatment at room temperature of 25 ℃ to obtain a facial mask mixed solution;
(4) adjusting the pH value to 6.0 by using citric acid;
(6) soaking the natural chitosan non-woven fabric film in the facial mask mixed solution for 20min, then transferring the natural chitosan non-woven fabric film into a vacuum box, and vacuumizing for 5min to completely combine the facial mask mixed solution with the non-woven fabric film;
(7) randomly performing spot inspection, subpackaging, sealing and labeling after the inspection is qualified.
The using method comprises the following steps: and taking out the mask paper, unfolding the mask paper, pasting the mask paper on the face to avoid the nose, eyes and mouth parts, completely pasting the mask and the face, taking down the mask after static application for 10-20 min, and cleaning the mask with clear water.
Through tests, the liquid absorption of the facial mask prepared in the embodiment reaches 19.66, and the liquid supplement rate reaches the maximum value of 84.25% when T is 13 min.
Example 3
An anti-aging moisturizing mask is prepared from the following components in parts by weight: 15 parts of purple sweet potato anthocyanin nano liposome freeze-dried powder, 5 parts of pearl powder, 10 parts of milk, 4 parts of honey, 6 parts of aloe extract, 5 parts of hyaluronic acid, 20 parts of sweet almond oil, 0.5 part of bitter orange flower essential oil, 0.5 part of citric acid and 75 parts of deionized water.
The preparation steps are as follows:
(1) mixing purple sweet potato anthocyanin nano liposome lyophilized powder, pearl powder, aloe extract, hyaluronic acid, honey and milk uniformly according to a proportion to prepare a water phase;
(2) mixing sweet almond oil and bitter orange flower essential oil uniformly according to a proportion to prepare an oil phase;
(3) mixing the oil phase and the water phase, adding deionized water in proportion, and performing emulsification treatment at room temperature of 25 ℃ to obtain a facial mask mixed solution;
(4) adjusting the pH value to 6.5 by using citric acid;
(6) soaking the natural chitosan non-woven fabric film in the facial mask mixed solution for 30min, then transferring the natural chitosan non-woven fabric film into a vacuum box, and vacuumizing for 10min to completely combine the facial mask mixed solution with the non-woven fabric film;
(7) randomly performing spot inspection, subpackaging, sealing and labeling after the inspection is qualified.
The using method comprises the following steps: and taking out the mask paper, unfolding the mask paper, pasting the mask paper on the face to avoid the nose, eyes and mouth parts, completely pasting the mask and the face, taking down the mask after static application for 10-20 min, and cleaning the mask with clear water.
Through tests, the liquid absorption of the facial mask prepared in the embodiment reaches 24.58, and the liquid supplement rate reaches the maximum value of 85.22% when T is 10 min.
Comparative example 1
An anti-aging moisturizing mask is prepared from the following components in parts by weight: 10 parts of purple sweet potato anthocyanin nano liposome freeze-dried powder, 7 parts of milk, 3 parts of honey, 15 parts of natural sweet almond oil, 0.5 part of bitter orange flower essential oil, 0.25 part of citric acid and 65 parts of deionized water.
The procedure was as in example 1.
Comparative example 2
An anti-aging moisturizing mask is prepared from the following components in parts by weight: 10 parts of purple sweet potato anthocyanin nano liposome freeze-dried powder, 4 parts of pearl powder, 7 parts of milk, 3 parts of honey, 15 parts of natural sweet almond oil, 0.5 part of bitter orange flower essential oil, 0.25 part of citric acid and 65 parts of deionized water.
The procedure was as in example 1.
Comparative example 3
An anti-aging moisturizing mask is prepared from the following components in parts by weight: 10 parts of purple sweet potato anthocyanin nano liposome freeze-dried powder, 7 parts of milk, 3 parts of honey, 5 parts of aloe extract, 15 parts of natural sweet almond oil, 0.5 part of bitter orange flower essential oil, 0.25 part of citric acid and 65 parts of deionized water.
The procedure was as in example 1.
Comparative example 4
An anti-aging moisturizing mask is prepared from the following components in parts by weight: 10 parts of purple sweet potato anthocyanin nano liposome freeze-dried powder, 7 parts of milk, 3 parts of honey, 4 parts of hyaluronic acid, 15 parts of natural sweet almond oil, 0.5 part of bitter orange flower essential oil, 0.25 part of citric acid and 65 parts of deionized water.
The procedure was as in example 1.
Comparative example 5
An anti-aging moisturizing mask is prepared from the following components in parts by weight: 10 parts of purple sweet potato anthocyanin nano liposome freeze-dried powder, 7 parts of milk, 3 parts of honey, 5 parts of aloe extract, 4 parts of hyaluronic acid, 15 parts of natural sweet almond oil, 0.5 part of bitter orange flower essential oil, 0.25 part of citric acid and 65 parts of deionized water.
The procedure was as in example 1.
The facial masks prepared in comparative examples 1 to 5 were subjected to moisturizing performance tests, and the results are shown in table 1:
TABLE 1 evaluation of Water supplement Performance test Effect
As can be seen from table 1, comparative example 1 does not contain an active ingredient having high moisture retention, and thus the moisturizing effect is the worst; the pearl powder, the aloe extract and the hyaluronic acid are respectively added in the comparative example 2, the comparative example 3 and the comparative example 4, so that the water replenishing effect is improved. The comparison shows that the comparative example 2 with the pearl powder is poorer in water replenishing effect than the comparative example 5 with the aloe extract and the hyaluronic acid, while the comparative example 1 with the pearl powder, the aloe extract and the hyaluronic acid is better than the comparative example 5.
The whitening effect evaluation (namely the detection of melanin content) of the facial masks prepared in the example 1 and the comparative examples 1 to 5 is carried out, and the specific steps are as follows:
140 healthy women aged 25-50 years and having dark or dark skin color were selected and divided into a blank group, a control group (comparative examples 1-5) and an experimental group (example 1), and 20 persons were each selected. The cheek color and skin color were measured and the test mask was delivered. The subject continuously used a whitening mask. The control group and the experimental group are used 1 time a day and applied after face cleaning every night. Blank group, no whitening cosmetics were used.
The using method comprises the following steps: and taking out the mask paper, unfolding the mask paper, pasting the mask paper on the face to avoid the nose, eyes and mouth parts, completely pasting the mask and the face, taking down the mask after static application for 15-20 min, and cleaning the mask with clear water. Other whitening cosmetics were discontinued during the experiment. After the continuous use of 7d, 14d, 21d and 28d, each efficacy index is measured. Meanwhile, the volunteers are asked to feel and whether or not there is an allergy phenomenon after using the test sample, and the comparison before and after the volunteers use the test sample is recorded. The skin melanin content was measured using a MeXAMETER MXI 8 skin pigment instrument 1d before and 7d, 14d, 21d, and 28d after application of the cosmetic, and the skin melanin content was measured 3 times continuously and averaged. And the data processing adopts sigmastat statistical software to carry out pairing t test, and has significance when P is less than 0.05.
The results showed that no irritation or allergic phenomenon was found during the use. As can be seen from the data in Table 1, the melanin content in the experimental groups at 7d, 14d, 21d and 28d after the application of the samples was reduced compared with that before the application (P < 0.05).
TABLE 2 Melanin changes at the test sites during the use of the mask
As can be seen from table 1, the control group 1 had the least content of active whitening ingredients and thus had the least whitening effect; the pearl powder is added into the control group 2, and the aloe extract is added into the control group 3, so that the better whitening effect is shown; hyaluronic acid was added to the control group 4, and the whitening effect was not significantly enhanced. The comparison shows that the control group 5 added with the aloe extract and the hyaluronic acid has more remarkable whitening effect than the control group 2 added with the pearl powder; the experimental group added with the pearl powder, the aloe extract and the hyaluronic acid has the best whitening effect, so that the pearl powder, the aloe extract and the hyaluronic acid have the synergistic whitening effect, and the whitening effect is optimal, namely the pearl powder, the aloe extract and the hyaluronic acid belong to a whole body, and the expected whitening effect cannot be achieved due to the lack of one.
The above description should not be taken as limiting the invention to the embodiments, but rather, as will be apparent to those skilled in the art to which the invention pertains, numerous simplifications or substitutions may be made without departing from the spirit of the invention, which shall be deemed to fall within the scope of the invention as defined by the claims appended hereto.
Claims (9)
1. The anti-aging moisturizing mask is characterized by being prepared from the following components in parts by weight: 5-15 parts of purple sweet potato anthocyanin nano liposome freeze-dried powder, 2-5 parts of pearl powder, 4-10 parts of milk, 2-4 parts of honey, 3-6 parts of aloe extract, 2-5 parts of hyaluronic acid, 10-20 parts of sweet almond oil, 0.3-0.5 part of bitter orange flower essential oil, 0.05-0.5 part of pH regulator and 50-75 parts of deionized water.
2. The anti-aging hydrating mask as claimed in claim 1, which is prepared from the following components in parts by weight: 10 parts of purple sweet potato anthocyanin nano liposome freeze-dried powder, 4 parts of pearl powder, 7 parts of milk, 3 parts of honey, 5 parts of aloe extract, 4 parts of hyaluronic acid, 15 parts of natural sweet almond oil, 0.5 part of bitter orange flower essential oil, 0.25 part of pH regulator and 65 parts of deionized water.
3. The anti-aging hydrating mask as claimed in claim 1 or 2, wherein the lyophilized powder of purple sweet potato anthocyanin nanoliposome is prepared by ethanol infusion-dynamic high pressure microfluidization method.
4. The anti-aging hydrating mask as claimed in claim 3, wherein the ethanol infusion-dynamic high pressure micro-jet method comprises the specific steps of:
(1) dissolving 10-100 parts by weight of purple sweet potato anthocyanin in 5000-9000 parts by weight of pH6.0 phosphate buffer solution, adding 5000-9000 parts by weight of cholesterol, 1200 parts by weight of phospholipid and 1-5 parts by weight of Tween 80, and fully mixing to obtain a mixed solution;
(2) injecting 1000-5000 parts by weight of absolute ethyl alcohol into the mixed solution under the condition of rapid stirring, homogenizing at a high speed, removing the absolute ethyl alcohol through vacuum rotary evaporation, and performing constant volume by using a phosphate buffer solution with the pH value of 6.0 to obtain the purple sweet potato anthocyanin crude liposome;
(3) then adding the mixture into a high-pressure micro-jet homogenizer, and treating for 3-30 times under the pressure of 800-1000 bar to obtain purple sweet potato anthocyanin nano liposome emulsion;
(4) adding a freeze-drying protective agent, pre-freezing for 24 hours at-60 ℃, and then putting the mixture into a freeze dryer for freeze drying, wherein the temperature is controlled between-62 ℃ and-60 ℃, so as to obtain the freeze-dried powder of the anthocyanidin nanoliposome of the purple sweet potatoes.
5. The anti-aging hydrating mask of claim 4, wherein the phospholipid is soy lecithin.
6. The mask according to claim 1 or 2, wherein the pH regulator is citric acid.
7. The preparation method of the anti-aging hydrating mask as set forth in claim 1 or 2, comprising the steps of:
(1) mixing purple sweet potato anthocyanin nano liposome lyophilized powder, pearl powder, aloe extract, hyaluronic acid, honey and milk uniformly according to a proportion to prepare a water phase;
(2) mixing sweet almond oil and bitter orange flower essential oil uniformly according to a proportion to prepare an oil phase;
(3) mixing the oil phase and the water phase, adding deionized water in proportion, and emulsifying at room temperature to obtain a facial mask mixed solution;
(4) adjusting the pH value to 6.0-6.5 by using a pH regulator;
(6) soaking the non-woven fabric film in the mask mixed solution, then transferring the non-woven fabric film into a vacuum box, and vacuumizing for 5-10 min to completely combine the mask mixed solution with the non-woven fabric film;
(7) randomly performing spot inspection, subpackaging, sealing and labeling after the inspection is qualified.
8. The preparation method of the anti-aging hydrating mask as claimed in claim 7, wherein the soaking time of the non-woven fabric mask is 20-30 min.
9. The method for preparing the anti-aging hydrating mask as claimed in claim 7 or 8, wherein the non-woven fabric mask is made of natural chitosan.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010664412.0A CN111686065A (en) | 2020-07-10 | 2020-07-10 | Anti-aging moisturizing mask and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010664412.0A CN111686065A (en) | 2020-07-10 | 2020-07-10 | Anti-aging moisturizing mask and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN111686065A true CN111686065A (en) | 2020-09-22 |
Family
ID=72485406
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202010664412.0A Withdrawn CN111686065A (en) | 2020-07-10 | 2020-07-10 | Anti-aging moisturizing mask and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN111686065A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113208991A (en) * | 2021-04-23 | 2021-08-06 | 刘生仁 | Mask powder with beauty maintaining and young keeping functions and preparation method thereof |
| CN113262176A (en) * | 2021-04-22 | 2021-08-17 | 江苏师范大学 | Anti-aging moisturizing mask essence based on anthocyanin liposome and preparation method thereof |
| CN114469840A (en) * | 2022-03-21 | 2022-05-13 | 英中再生医学(山东)有限公司 | Product with scald relieving and oxidation resisting capabilities and preparation method and application thereof |
Citations (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102871947A (en) * | 2012-10-29 | 2013-01-16 | 杨军 | Natural powdery facial mask |
| CN103070814A (en) * | 2012-12-14 | 2013-05-01 | 北海黑珍珠海洋生物科技有限公司 | Moisturizing and water locking mask liquid and its making technology |
| CN103494760A (en) * | 2013-09-29 | 2014-01-08 | 黄珍珍 | Moistening and whitening facial mask and preparation method thereof |
| CN103919710A (en) * | 2014-03-31 | 2014-07-16 | 韩雁如 | Facial mask capable of improving sleeping and preparation method thereof |
| CN104644518A (en) * | 2014-12-19 | 2015-05-27 | 王大明 | Whitening rose sleeping mask and preparation method thereof |
| CN104940106A (en) * | 2015-06-25 | 2015-09-30 | 青岛克立克信息技术有限公司 | Mask capable of performing deep water supplement and moisture retention |
| CN105411926A (en) * | 2015-12-03 | 2016-03-23 | 青蛙王子(中国)日化有限公司 | Skin-tendering essence rich in anthocyanin and preparation method of skin-tendering essence |
| CN106265419A (en) * | 2016-08-17 | 2017-01-04 | 倪娟形 | Whitening moisturizing face masque liquid and preparation method thereof |
| CN106474025A (en) * | 2015-08-27 | 2017-03-08 | 李尧 | Moisture saver mask |
| CN106821944A (en) * | 2017-04-12 | 2017-06-13 | 广州海梦科化妆品有限公司 | A kind of composite factor synthesizes Transdermal absorption facial mask and preparation method |
| CN106852821A (en) * | 2015-12-03 | 2017-06-16 | 刘泽华 | Sleep above film |
| CN107773508A (en) * | 2016-08-24 | 2018-03-09 | 张文闻 | A kind of facial mask and preparation method thereof |
| CN108078904A (en) * | 2018-02-05 | 2018-05-29 | 云南瑞宝生物科技股份有限公司 | One kind contains anthocyanidin and Bee Pollen facial mask and preparation method thereof |
| CN108078894A (en) * | 2018-01-04 | 2018-05-29 | 湖北瑞晟生物有限责任公司 | A kind of ferment essential oil face pack and its preparation process |
| CN108851072A (en) * | 2018-04-18 | 2018-11-23 | 江苏师范大学 | A kind of purple sweet potato cyanidin nano liposomes and preparation method thereof |
| CN109172497A (en) * | 2018-11-30 | 2019-01-11 | 广东澳元健集团有限公司 | A kind of whitening mask |
-
2020
- 2020-07-10 CN CN202010664412.0A patent/CN111686065A/en not_active Withdrawn
Patent Citations (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102871947A (en) * | 2012-10-29 | 2013-01-16 | 杨军 | Natural powdery facial mask |
| CN103070814A (en) * | 2012-12-14 | 2013-05-01 | 北海黑珍珠海洋生物科技有限公司 | Moisturizing and water locking mask liquid and its making technology |
| CN103494760A (en) * | 2013-09-29 | 2014-01-08 | 黄珍珍 | Moistening and whitening facial mask and preparation method thereof |
| CN103919710A (en) * | 2014-03-31 | 2014-07-16 | 韩雁如 | Facial mask capable of improving sleeping and preparation method thereof |
| CN104644518A (en) * | 2014-12-19 | 2015-05-27 | 王大明 | Whitening rose sleeping mask and preparation method thereof |
| CN104940106A (en) * | 2015-06-25 | 2015-09-30 | 青岛克立克信息技术有限公司 | Mask capable of performing deep water supplement and moisture retention |
| CN106474025A (en) * | 2015-08-27 | 2017-03-08 | 李尧 | Moisture saver mask |
| CN105411926A (en) * | 2015-12-03 | 2016-03-23 | 青蛙王子(中国)日化有限公司 | Skin-tendering essence rich in anthocyanin and preparation method of skin-tendering essence |
| CN106852821A (en) * | 2015-12-03 | 2017-06-16 | 刘泽华 | Sleep above film |
| CN106265419A (en) * | 2016-08-17 | 2017-01-04 | 倪娟形 | Whitening moisturizing face masque liquid and preparation method thereof |
| CN107773508A (en) * | 2016-08-24 | 2018-03-09 | 张文闻 | A kind of facial mask and preparation method thereof |
| CN106821944A (en) * | 2017-04-12 | 2017-06-13 | 广州海梦科化妆品有限公司 | A kind of composite factor synthesizes Transdermal absorption facial mask and preparation method |
| CN108078894A (en) * | 2018-01-04 | 2018-05-29 | 湖北瑞晟生物有限责任公司 | A kind of ferment essential oil face pack and its preparation process |
| CN108078904A (en) * | 2018-02-05 | 2018-05-29 | 云南瑞宝生物科技股份有限公司 | One kind contains anthocyanidin and Bee Pollen facial mask and preparation method thereof |
| CN108851072A (en) * | 2018-04-18 | 2018-11-23 | 江苏师范大学 | A kind of purple sweet potato cyanidin nano liposomes and preparation method thereof |
| CN109172497A (en) * | 2018-11-30 | 2019-01-11 | 广东澳元健集团有限公司 | A kind of whitening mask |
Non-Patent Citations (1)
| Title |
|---|
| 马振友等: "《最新皮肤科药物手册》", 30 June 2008, 世界图书出版西安公司 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113262176A (en) * | 2021-04-22 | 2021-08-17 | 江苏师范大学 | Anti-aging moisturizing mask essence based on anthocyanin liposome and preparation method thereof |
| CN113208991A (en) * | 2021-04-23 | 2021-08-06 | 刘生仁 | Mask powder with beauty maintaining and young keeping functions and preparation method thereof |
| CN114469840A (en) * | 2022-03-21 | 2022-05-13 | 英中再生医学(山东)有限公司 | Product with scald relieving and oxidation resisting capabilities and preparation method and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| WO2021088399A1 (en) | Moisturizing and hydrating facial mask composition, facial mask, and preparation method for facial mask composition | |
| CN111686065A (en) | Anti-aging moisturizing mask and preparation method thereof | |
| KR101810231B1 (en) | Cosmetic composition for improving acne containing propolis spicule powder | |
| CN107296764B (en) | Cream and preparation method thereof | |
| CN111053709A (en) | Emulsion for camellia seed oil mask, mask and preparation method of mask | |
| CN110664650A (en) | Multi-effect skin care composition and essence and preparation method thereof | |
| EP3377084A2 (en) | Compositions containing natural extracts and use thereof for skin and hair | |
| CN104958241A (en) | Moisturizing traditional Chinese medicine mask product and preparation method thereof | |
| CN115040461A (en) | Moisturizing and hydrating fresh freeze-dried mask | |
| CN110522655A (en) | A kind of active peptides milk matrix lipid body essence lotion and preparation method thereof with blue-opalescent and Tyndall effect | |
| CN111728924A (en) | Whitening mask and preparation method thereof | |
| KR102242215B1 (en) | Color cosmetic composition comprising color base and extract reacted with enzyme of low temperature and high pressure | |
| CN109276456A (en) | A kind of donkey milk facial mask and its preparation process with skin whitening, moisturizing effect | |
| KR101896563B1 (en) | Cosmetic composition containing Ligustrum lucidum Aiton extract for moisturizing the skin | |
| KR101862039B1 (en) | A cosmetic composition containing spicule powder and natural complex extract stabilized in nanoliposome | |
| CN112675071A (en) | Wool keratin freeze-dried mask and preparation method and application thereof | |
| CN107496286B (en) | Water-replenishing and moistening type water emulsion capable of fading fine wrinkles and preparation method thereof | |
| CN111450031A (en) | Freeze-dried nanofiber invisible mask and preparation method thereof | |
| CN116898766A (en) | A lyophilized liquid, lyophilized film and repairing facial mask containing liposome active substances | |
| CN115475131A (en) | Moisturizing and elastic anti-wrinkle mask and preparation method thereof | |
| CN110946776A (en) | A skin caring cream containing cicada extract and its preparation method | |
| CN107693480B (en) | Whitening and moisturizing hand mask and preparation method thereof | |
| CN111671703A (en) | Oil-control water-replenishing bidirectional-adjustment essence water | |
| KR20100045684A (en) | The manufacturing method of natural cosmetic composition | |
| CN112137927A (en) | Fibronectin essence emulsion with high penetration and light sensation reproduction and tissue regeneration initiation and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20200922 |
|
| WW01 | Invention patent application withdrawn after publication |