JP5562038B2 - 鉄元素を酸化された形で含む、多元素酸化物材料の製造方法 - Google Patents
鉄元素を酸化された形で含む、多元素酸化物材料の製造方法 Download PDFInfo
- Publication number
- JP5562038B2 JP5562038B2 JP2009545195A JP2009545195A JP5562038B2 JP 5562038 B2 JP5562038 B2 JP 5562038B2 JP 2009545195 A JP2009545195 A JP 2009545195A JP 2009545195 A JP2009545195 A JP 2009545195A JP 5562038 B2 JP5562038 B2 JP 5562038B2
- Authority
- JP
- Japan
- Prior art keywords
- iron nitrate
- iron
- oxide material
- element oxide
- elemental
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 title claims description 58
- 239000000463 material Substances 0.000 title claims description 47
- 238000004519 manufacturing process Methods 0.000 title claims description 11
- MVFCKEFYUDZOCX-UHFFFAOYSA-N iron(2+);dinitrate Chemical compound [Fe+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O MVFCKEFYUDZOCX-UHFFFAOYSA-N 0.000 claims description 32
- 238000000034 method Methods 0.000 claims description 29
- 239000000203 mixture Substances 0.000 claims description 26
- 229910052760 oxygen Inorganic materials 0.000 claims description 22
- 239000002243 precursor Substances 0.000 claims description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 239000007864 aqueous solution Substances 0.000 claims description 18
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 18
- 229910052742 iron Inorganic materials 0.000 claims description 18
- 230000003647 oxidation Effects 0.000 claims description 18
- 238000007254 oxidation reaction Methods 0.000 claims description 18
- 239000001301 oxygen Substances 0.000 claims description 18
- 239000000243 solution Substances 0.000 claims description 17
- 239000007789 gas Substances 0.000 claims description 16
- NEOOEFDJRSCWOU-UHFFFAOYSA-N iron(2+);dinitrate;hydrate Chemical compound O.[Fe+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O NEOOEFDJRSCWOU-UHFFFAOYSA-N 0.000 claims description 16
- 238000002844 melting Methods 0.000 claims description 16
- 230000008018 melting Effects 0.000 claims description 16
- VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical compound CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 claims description 10
- 150000002894 organic compounds Chemical class 0.000 claims description 10
- 239000007787 solid Substances 0.000 claims description 10
- 229910000608 Fe(NO3)3.9H2O Inorganic materials 0.000 claims description 8
- 239000013543 active substance Substances 0.000 claims description 8
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims description 7
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims description 7
- 238000002360 preparation method Methods 0.000 claims description 6
- 239000000155 melt Substances 0.000 claims description 5
- 239000003054 catalyst Substances 0.000 description 13
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 description 10
- 238000001354 calcination Methods 0.000 description 9
- 238000010438 heat treatment Methods 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- 230000003197 catalytic effect Effects 0.000 description 5
- 239000011261 inert gas Substances 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- VCJMYUPGQJHHFU-UHFFFAOYSA-N iron(3+);trinitrate Chemical compound [Fe+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O VCJMYUPGQJHHFU-UHFFFAOYSA-N 0.000 description 4
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 4
- 229910044991 metal oxide Inorganic materials 0.000 description 4
- 229910052698 phosphorus Inorganic materials 0.000 description 4
- 229910052700 potassium Inorganic materials 0.000 description 4
- 229910052708 sodium Inorganic materials 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- STNJBCKSHOAVAJ-UHFFFAOYSA-N Methacrolein Chemical compound CC(=C)C=O STNJBCKSHOAVAJ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 239000011149 active material Substances 0.000 description 3
- 229910052796 boron Inorganic materials 0.000 description 3
- 229910052792 caesium Inorganic materials 0.000 description 3
- 239000010439 graphite Substances 0.000 description 3
- 229910002804 graphite Inorganic materials 0.000 description 3
- 238000000465 moulding Methods 0.000 description 3
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 3
- -1 polyoxy Polymers 0.000 description 3
- 239000012495 reaction gas Substances 0.000 description 3
- 229910052701 rubidium Inorganic materials 0.000 description 3
- 229910052710 silicon Inorganic materials 0.000 description 3
- 229910052725 zinc Inorganic materials 0.000 description 3
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 229910002554 Fe(NO3)3·9H2O Inorganic materials 0.000 description 2
- GYCMBHHDWRMZGG-UHFFFAOYSA-N Methylacrylonitrile Chemical compound CC(=C)C#N GYCMBHHDWRMZGG-UHFFFAOYSA-N 0.000 description 2
- 229920001410 Microfiber Polymers 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 235000021355 Stearic acid Nutrition 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 229910052787 antimony Inorganic materials 0.000 description 2
- 229910052785 arsenic Inorganic materials 0.000 description 2
- 239000010425 asbestos Substances 0.000 description 2
- UFMZWBIQTDUYBN-UHFFFAOYSA-N cobalt dinitrate Chemical compound [Co+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O UFMZWBIQTDUYBN-UHFFFAOYSA-N 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- NJLLQSBAHIKGKF-UHFFFAOYSA-N dipotassium dioxido(oxo)titanium Chemical compound [K+].[K+].[O-][Ti]([O-])=O NJLLQSBAHIKGKF-UHFFFAOYSA-N 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 235000011187 glycerol Nutrition 0.000 description 2
- 238000009776 industrial production Methods 0.000 description 2
- NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 description 2
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 description 2
- 229910052748 manganese Inorganic materials 0.000 description 2
- 239000003658 microfiber Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 2
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000010298 pulverizing process Methods 0.000 description 2
- 229910052895 riebeckite Inorganic materials 0.000 description 2
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 2
- 229910010271 silicon carbide Inorganic materials 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 239000008117 stearic acid Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 229910052718 tin Inorganic materials 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- 238000004448 titration Methods 0.000 description 2
- 229910052726 zirconium Inorganic materials 0.000 description 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 229910052582 BN Inorganic materials 0.000 description 1
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical class [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 229910052684 Cerium Inorganic materials 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 229920002125 Sokalan® Polymers 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 150000001242 acetic acid derivatives Chemical class 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- VBIXEXWLHSRNKB-UHFFFAOYSA-N ammonium oxalate Chemical compound [NH4+].[NH4+].[O-]C(=O)C([O-])=O VBIXEXWLHSRNKB-UHFFFAOYSA-N 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 229910052797 bismuth Inorganic materials 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 229910002090 carbon oxide Inorganic materials 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 239000012018 catalyst precursor Substances 0.000 description 1
- 229920003086 cellulose ether Polymers 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 150000001860 citric acid derivatives Chemical class 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 150000004675 formic acid derivatives Chemical class 0.000 description 1
- 125000002485 formyl group Chemical group [H]C(*)=O 0.000 description 1
- 238000004108 freeze drying Methods 0.000 description 1
- 229910052735 hafnium Inorganic materials 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 239000008241 heterogeneous mixture Substances 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 150000004677 hydrates Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- RXPAJWPEYBDXOG-UHFFFAOYSA-N hydron;methyl 4-methoxypyridine-2-carboxylate;chloride Chemical compound Cl.COC(=O)C1=CC(OC)=CC=N1 RXPAJWPEYBDXOG-UHFFFAOYSA-N 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 239000003701 inert diluent Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- SZQUEWJRBJDHSM-UHFFFAOYSA-N iron(3+);trinitrate;nonahydrate Chemical compound O.O.O.O.O.O.O.O.O.[Fe+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O SZQUEWJRBJDHSM-UHFFFAOYSA-N 0.000 description 1
- WKPSFPXMYGFAQW-UHFFFAOYSA-N iron;hydrate Chemical compound O.[Fe] WKPSFPXMYGFAQW-UHFFFAOYSA-N 0.000 description 1
- 239000001282 iso-butane Substances 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- 238000010309 melting process Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000002480 mineral oil Substances 0.000 description 1
- 235000010446 mineral oil Nutrition 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 125000000896 monocarboxylic acid group Chemical group 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 229910052758 niobium Inorganic materials 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229910052756 noble gas Inorganic materials 0.000 description 1
- 150000003891 oxalate salts Chemical class 0.000 description 1
- 125000004430 oxygen atom Chemical group O* 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 239000006069 physical mixture Substances 0.000 description 1
- 239000004584 polyacrylic acid Substances 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000012744 reinforcing agent Substances 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229910052716 thallium Inorganic materials 0.000 description 1
- BKVIYDNLLOSFOA-UHFFFAOYSA-N thallium Chemical compound [Tl] BKVIYDNLLOSFOA-UHFFFAOYSA-N 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- FAQYAMRNWDIXMY-UHFFFAOYSA-N trichloroborane Chemical compound ClB(Cl)Cl FAQYAMRNWDIXMY-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 229910052720 vanadium Inorganic materials 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G49/00—Compounds of iron
- C01G49/009—Compounds containing iron, with or without oxygen or hydrogen, and containing two or more other elements
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G49/00—Compounds of iron
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Compounds Of Iron (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US88503707P | 2007-01-16 | 2007-01-16 | |
| DE102007003076.4 | 2007-01-16 | ||
| US60/885,037 | 2007-01-16 | ||
| DE102007003076A DE102007003076A1 (de) | 2007-01-16 | 2007-01-16 | Verfahren zur Herstellung einer das Element Eisen in oxidischer Form enthaltenden Multielementoxidmasse |
| PCT/EP2008/050341 WO2008087115A2 (de) | 2007-01-16 | 2008-01-14 | Verfahren zur herstellung einer das element eisen in oxidischer form enthaltenden multielementoxidmasse |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2010515564A JP2010515564A (ja) | 2010-05-13 |
| JP2010515564A5 JP2010515564A5 (ko) | 2013-06-06 |
| JP5562038B2 true JP5562038B2 (ja) | 2014-07-30 |
Family
ID=39509952
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009545195A Active JP5562038B2 (ja) | 2007-01-16 | 2008-01-14 | 鉄元素を酸化された形で含む、多元素酸化物材料の製造方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US8128904B2 (ko) |
| EP (1) | EP2104646B1 (ko) |
| JP (1) | JP5562038B2 (ko) |
| KR (1) | KR101465279B1 (ko) |
| CN (1) | CN101583569B (ko) |
| BR (1) | BRPI0806241A2 (ko) |
| DE (1) | DE102007003076A1 (ko) |
| WO (1) | WO2008087115A2 (ko) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102008040094A1 (de) | 2008-07-02 | 2009-01-29 | Basf Se | Verfahren zur Herstellung eines oxidischen geometrischen Formkörpers |
| DE102008040093A1 (de) | 2008-07-02 | 2008-12-18 | Basf Se | Verfahren zur Herstellung eines ringähnlichen oxidischen Formkörpers |
| DE102008054586A1 (de) * | 2008-12-12 | 2010-06-17 | Basf Se | Verfahren zur kontinuierlichen Herstellung von geometrischen Katalysatorformkörpern K |
| DE102009047291A1 (de) | 2009-11-30 | 2010-09-23 | Basf Se | Verfahren zur Herstellung von (Meth)acrolein durch heterogen katalysierte Gasphasen-Partialoxidation |
| DE102010048405A1 (de) | 2010-10-15 | 2011-05-19 | Basf Se | Verfahren zum Langzeitbetrieb einer heterogen katalysierten partiellen Gasphasenoxidation von Proben zu Acrolein |
| DE102011079035A1 (de) | 2011-07-12 | 2013-01-17 | Basf Se | Mo, Bi und Fe enthaltende Multimetalloxidmassen |
| EP2731715B1 (de) * | 2011-07-12 | 2019-12-11 | Basf Se | Mo, bi und fe enthaltende multimetalloxidmassen |
| DE102011084040A1 (de) | 2011-10-05 | 2012-01-05 | Basf Se | Mo, Bi und Fe enthaltende Multimetalloxidmasse |
| EP3068754B1 (de) | 2013-11-11 | 2018-01-31 | Basf Se | Verfahren zur herstellung eines ungesättigten aldehyds und/oder einer ungesättigten carbonsäure |
| JP6407278B2 (ja) | 2013-11-11 | 2018-10-17 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | アルケンを気相酸化して不飽和アルデヒド及び／又は不飽和カルボン酸にするための、機械的に安定な中空円筒形触媒成形体 |
| KR102011252B1 (ko) * | 2017-07-13 | 2019-08-16 | 부산대학교 산학협력단 | 이산화탄소의 전기환원반응용 촉매 및 이를 포함하는 전해셀 |
| DE102018200841A1 (de) | 2018-01-19 | 2019-07-25 | Basf Se | Mo, Bi, Fe und Cu enthaltende Multimetalloxidmassen |
| WO2022065116A1 (ja) * | 2020-09-24 | 2022-03-31 | 日本化薬株式会社 | 触媒前駆体、それを用いた触媒、化合物の製造方法及び触媒の製造方法 |
| WO2024037905A1 (de) | 2022-08-16 | 2024-02-22 | Basf Se | Verfahren zur herstellung von vollkatalysatorformkörpern zur gasphasenoxidation eines alkens und/oder eines alkohols zu einem α,β-ungesättigtem aldehyd und/oder einer α,β-ungesättigten carbonsäure |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3218135A (en) * | 1962-01-31 | 1965-11-16 | Du Pont | Powder metal compositions containing dispersed refractory oxide |
| DE2125032C3 (de) | 1970-05-26 | 1979-11-22 | Nippon Catalytic Chem Ind | Verfahren zur Herstellung von (Meth) Acrolein neben geringen Mengen (Meth) Acrylsäure |
| GB1523772A (en) * | 1974-07-22 | 1978-09-06 | Standard Oil Co | Oxidation catalysts |
| US4148757A (en) | 1977-08-10 | 1979-04-10 | The Standard Oil Company | Process for forming multi-component oxide complex catalysts |
| US4212766A (en) * | 1978-04-21 | 1980-07-15 | Standard Oil Company | Process for forming multi-component oxide complex catalysts |
| US4537874A (en) | 1982-10-22 | 1985-08-27 | Nippon Shokubai Kagaku Kogyo Co Ltd | Catalyst for production of unsaturated aldehydes |
| JPS60232245A (ja) | 1984-05-01 | 1985-11-18 | Mitsubishi Heavy Ind Ltd | 一酸化炭素転化用モノリス型触媒の製造法 |
| US4978764A (en) * | 1989-09-25 | 1990-12-18 | The Standard Oil Company | Method for ammoxidation of paraffins |
| DE3932389A1 (de) * | 1989-09-28 | 1991-04-11 | Basf Ag | Verfahren zur herstellung von feinteiligem pulverfoermigem hexagonalem ferrit und seine verwendung zur herstellung von magnetischen aufzeichnungstraegern |
| DE4220859A1 (de) | 1992-06-25 | 1994-01-05 | Basf Ag | Multimetalloxidmassen |
| US5583086A (en) | 1993-03-09 | 1996-12-10 | Basf Aktiengesellschaft | Cesium containing multimetal oxide catalyst compositions for the preparation of methacrolein by gas-phase-catalytic oxidation |
| JP3895527B2 (ja) * | 1999-08-31 | 2007-03-22 | 株式会社日本触媒 | 接触気相酸化方法 |
| ZA200004211B (en) * | 1999-08-31 | 2001-02-14 | Nippon Catalytic Chem Ind | Method for catalytic gas phase oxidation. |
| DE10046957A1 (de) | 2000-09-21 | 2002-04-11 | Basf Ag | Verfahren zur Herstellung eines Multimetalloxid-Katalysators, Verfahren zur Herstellung ungesättigter Aldehyde und/oder Carbonsäuren und Bandcalziniervorrichtung |
| DE10101695A1 (de) | 2001-01-15 | 2002-07-18 | Basf Ag | Verfahren zur heterogen katalysierten Gasphasenpartialoxidation von Vorläuferverbindungen der (Meth)acrylsäure |
| WO2005046870A1 (ja) | 2003-11-14 | 2005-05-26 | Mitsubishi Chemical Corporation | 複合酸化物触媒の製造方法 |
| JP2005161309A (ja) * | 2003-11-14 | 2005-06-23 | Mitsubishi Chemicals Corp | 複合酸化物触媒の製造方法 |
| US20050279966A1 (en) * | 2004-06-16 | 2005-12-22 | Dejneka Matthew J | Nanocrystallite glass-ceramic and method for making same |
| DE102005035978A1 (de) * | 2005-07-28 | 2007-02-01 | Basf Ag | Katalysator und Verfahren zur Herstellung von Maleinsäureanhydrid |
| ATE428497T1 (de) * | 2005-08-05 | 2009-05-15 | Basf Se | Verfahren zur herstellung von katalysatorformkörpern, deren aktivmasse ein mischoxid ist |
| DE102005037678A1 (de) | 2005-08-05 | 2007-02-08 | Basf Ag | Verfahren zur Herstellung von Katalysatorformkörpern, deren Aktivmasse ein Multielementoxid ist |
-
2007
- 2007-01-16 DE DE102007003076A patent/DE102007003076A1/de not_active Withdrawn
-
2008
- 2008-01-14 JP JP2009545195A patent/JP5562038B2/ja active Active
- 2008-01-14 CN CN200880002381XA patent/CN101583569B/zh not_active Expired - Fee Related
- 2008-01-14 BR BRPI0806241-2A patent/BRPI0806241A2/pt not_active IP Right Cessation
- 2008-01-14 WO PCT/EP2008/050341 patent/WO2008087115A2/de active Application Filing
- 2008-01-14 EP EP08701461.9A patent/EP2104646B1/de active Active
- 2008-01-14 US US12/013,693 patent/US8128904B2/en not_active Expired - Fee Related
- 2008-01-14 KR KR1020097016979A patent/KR101465279B1/ko active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| KR20090104104A (ko) | 2009-10-05 |
| US20080171897A1 (en) | 2008-07-17 |
| WO2008087115A2 (de) | 2008-07-24 |
| BRPI0806241A2 (pt) | 2011-09-06 |
| US8128904B2 (en) | 2012-03-06 |
| DE102007003076A1 (de) | 2008-07-17 |
| WO2008087115A3 (de) | 2009-04-09 |
| CN101583569B (zh) | 2013-05-01 |
| CN101583569A (zh) | 2009-11-18 |
| JP2010515564A (ja) | 2010-05-13 |
| KR101465279B1 (ko) | 2014-11-26 |
| EP2104646A2 (de) | 2009-09-30 |
| EP2104646B1 (de) | 2016-12-14 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP5562038B2 (ja) | 鉄元素を酸化された形で含む、多元素酸化物材料の製造方法 | |
| JP3142549B2 (ja) | 鉄・アンチモン・モリブデン含有酸化物触媒組成物およびその製法 | |
| JP4280797B2 (ja) | 複合酸化物触媒の製造方法 | |
| JP4954750B2 (ja) | モリブデン、ビスマス、鉄、シリカ含有複合酸化物触媒の製造方法 | |
| JP2009220008A (ja) | アクリロニトリル合成用触媒およびアクリロニトリルの製造方法 | |
| JPH0441454A (ja) | メタクロレインの製造方法 | |
| KR101735862B1 (ko) | 복합 산화물 촉매의 제조 방법 | |
| JP3995381B2 (ja) | メタクリル酸製造用触媒およびメタクリル酸の製造方法 | |
| JP4356303B2 (ja) | 複合酸化物触媒及びその製造方法 | |
| WO2005056185A1 (ja) | 複合酸化物触媒の製造方法 | |
| JP5378041B2 (ja) | アクリロニトリル合成用複合酸化物触媒の製造方法 | |
| JP2005058909A (ja) | メタクリル酸合成用触媒の製造方法 | |
| JP5042658B2 (ja) | アクリロニトリル製造用触媒の製造方法、およびアクリロニトリルの製造方法 | |
| JP4811977B2 (ja) | メタクリル酸合成用触媒の製造方法 | |
| JP4601420B2 (ja) | メタクリル酸製造用触媒の製造方法 | |
| JP4564317B2 (ja) | メタクリル酸製造用触媒の製造方法 | |
| JP7532841B2 (ja) | 不飽和カルボン酸合成用触媒の製造方法 | |
| JP4951230B2 (ja) | メタクリル酸製造用触媒及びその製造方法、並びにその触媒を用いたメタクリル酸の製造方法 | |
| JP2003205240A (ja) | 複合酸化物触媒の製造方法 | |
| JPH04182449A (ja) | アクロレイン又はメタクロレインの製造方法 | |
| JPS5867643A (ja) | 不飽和酸の製造法 | |
| JP2003190798A (ja) | メタクリル酸製造用触媒の製造方法、この方法により製造される触媒、および、メタクリル酸の製造方法 | |
| WO2021152916A1 (ja) | 触媒の製造方法及びアクリル酸の製造方法 | |
| JP5199044B2 (ja) | メタクロレイン及びメタクリル酸製造用触媒の調製方法 | |
| WO2020203789A1 (ja) | 不飽和カルボン酸合成用触媒の製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RD04 | Notification of resignation of power of attorney |
Free format text: JAPANESE INTERMEDIATE CODE: A7424 Effective date: 20101228 |
|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20110111 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20121019 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20130118 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20130125 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20130219 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20130226 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20130319 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20130327 |
|
| A524 | Written submission of copy of amendment under article 19 pct |
Free format text: JAPANESE INTERMEDIATE CODE: A524 Effective date: 20130416 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20130520 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20130819 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20130826 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20130918 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20130926 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20131018 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20131025 |
|
| A02 | Decision of refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A02 Effective date: 20131209 |
|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20140409 |
|
| A911 | Transfer to examiner for re-examination before appeal (zenchi) |
Free format text: JAPANESE INTERMEDIATE CODE: A911 Effective date: 20140421 |
|
| TRDD | Decision of grant or rejection written | ||
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20140512 |
|
| A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20140610 |
|
| R150 | Certificate of patent or registration of utility model |
Ref document number: 5562038 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |