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ES2165214T3 - Procedimiento para la vaporizacion de una solucion de hidrato de hidrazina. - Google Patents

Procedimiento para la vaporizacion de una solucion de hidrato de hidrazina.

Info

Publication number
ES2165214T3
ES2165214T3 ES99111127T ES99111127T ES2165214T3 ES 2165214 T3 ES2165214 T3 ES 2165214T3 ES 99111127 T ES99111127 T ES 99111127T ES 99111127 T ES99111127 T ES 99111127T ES 2165214 T3 ES2165214 T3 ES 2165214T3
Authority
ES
Spain
Prior art keywords
vaporization
hydrazine hydrate
solution
procedure
azine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES99111127T
Other languages
English (en)
Inventor
Gerard Krempf
Bertrand Collier
Pierre Tellier
Jean-Pierre Pleuvry
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Atofina SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Atofina SA filed Critical Atofina SA
Application granted granted Critical
Publication of ES2165214T3 publication Critical patent/ES2165214T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C243/00Compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
    • C07C243/10Hydrazines
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28FDETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F21/00Constructions of heat-exchange apparatus characterised by the selection of particular materials
    • F28F21/08Constructions of heat-exchange apparatus characterised by the selection of particular materials of metal
    • F28F21/081Heat exchange elements made from metals or metal alloys
    • F28F21/082Heat exchange elements made from metals or metal alloys from steel or ferrous alloys
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00Nitrogen; Compounds thereof
    • C01B21/082Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/16Hydrazine; Salts thereof
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00Distillation: processes, separatory
    • Y10S203/06Reactor-distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • General Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Investigating Or Analyzing Materials By The Use Of Ultrasonic Waves (AREA)
  • Measuring Fluid Pressure (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)

Abstract

LA INVENCION SE REFIERE A UN PROCEDIMIENTO DE VAPORIZACION DE UNA SOLUCION DE HIDRATO DE HIDRACINA QUE CONSISTE EN CALENTAR ESTA SOLUCION EN FASE LIQUIDA Y A CONTINUACION EN EXPANDIRLA PARA PROVOCAR LA VAPORIZACION. SE HA DESCUBIERTO QUE ESTE PROCEDIMIENTO PERMITE EVITAR LA DESCOMPOSICION DEL HIDRATO DE HIDRACINA.LA INVENCION ES PARTICULARMENTE UTIL PARA EL HERVIDOR DE UNA COLUMNA EN LA QUE SE EFECTUA LA HIDROLISIS DE UNA AZINA R 1 R 2 C=N.N=CR 1 R 2 (EN LA QUE R 1 Y R 2 SON ALQUILOS QUE TIENEN HASTA 12 ATOMOS DE CARBONO) CON RECUPERACION DE HIDRATO DE HIDRACINA EN EL PIE Y DE CETONA R 1 R 2 C=0 EN LA CABEZA.
ES99111127T 1989-12-04 1990-11-16 Procedimiento para la vaporizacion de una solucion de hidrato de hidrazina. Expired - Lifetime ES2165214T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR8915968A FR2655336B1 (fr) 1989-12-04 1989-12-04 Procede de vaporisation d'une solution d'hydrate d'hydrazine.

Publications (1)

Publication Number Publication Date
ES2165214T3 true ES2165214T3 (es) 2002-03-01

Family

ID=9388103

Family Applications (2)

Application Number Title Priority Date Filing Date
ES99111127T Expired - Lifetime ES2165214T3 (es) 1989-12-04 1990-11-16 Procedimiento para la vaporizacion de una solucion de hidrato de hidrazina.
ES90403246T Expired - Lifetime ES2157195T3 (es) 1989-12-04 1990-11-16 Procedimiento para la vaporizacion de una solucion de hidrato de hidrazina.

Family Applications After (1)

Application Number Title Priority Date Filing Date
ES90403246T Expired - Lifetime ES2157195T3 (es) 1989-12-04 1990-11-16 Procedimiento para la vaporizacion de una solucion de hidrato de hidrazina.

Country Status (14)

Country Link
US (1) US5393508A (es)
EP (2) EP0952109B1 (es)
JP (1) JP2607444B2 (es)
KR (1) KR950003334B1 (es)
CN (1) CN1043139C (es)
AT (2) ATE206686T1 (es)
CA (1) CA2031318C (es)
DE (2) DE69033827T2 (es)
ES (2) ES2165214T3 (es)
FI (1) FI114546B (es)
FR (1) FR2655336B1 (es)
IE (1) IE904356A1 (es)
NO (1) NO308840B1 (es)
PT (1) PT96064B (es)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4329599C1 (de) * 1993-09-02 1995-03-16 Bayer Ag Verfahren zur Entfernung von Verunreinigungen aus Hydrazinhydrat
FR2778659B1 (fr) * 1998-05-14 2000-06-23 Atochem Elf Sa Procede de preparation d'hydrate d'hydrazine
FR2787437B1 (fr) * 1998-12-22 2001-02-09 Atochem Elf Sa Procede de fabrication d'hydrazine par hydrolyse d'une azine
CN100333814C (zh) * 2005-03-08 2007-08-29 湖南化工研究院 一种回收利用工业废盐的方法及其设备
CN100389893C (zh) * 2005-10-13 2008-05-28 宜宾天原股份有限公司 一种回收酮连氮法水合肼废盐水中丙酮与氨的方法
CN100389892C (zh) * 2005-10-13 2008-05-28 宜宾天原股份有限公司 尿素法水合肼副产盐碱回收处理方法
CN105384655B (zh) * 2015-10-26 2017-08-25 宜宾海丰和锐有限公司 一种去除酮连氮法水合肼水解系统中杂质的方法
CN108086960B (zh) * 2017-12-12 2020-04-28 大连理工大学 一种水流侵蚀法天然气水合物开采实验模拟方法与装置

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA584845A (en) * 1959-10-13 L. Womer Robert Manufacture of hydrazine
BE509407A (es) * 1952-02-09
US2799631A (en) * 1952-10-07 1957-07-16 Fairmount Chem Process of recovering hydrazine
US2733195A (en) * 1954-09-01 1956-01-31 Process for concentrating aqueous
GB761018A (en) * 1954-10-11 1956-11-07 Fairmount Chem Process for recovering hydrazine
US3230158A (en) * 1961-11-27 1966-01-18 Phillips Petroleum Co Method and apparatus for reboiling a heated system
DE1273503B (de) * 1966-12-17 1968-07-25 Bayer Ag Verfahren zur Aufbereitung von Hydrazin aus waessrigen Ketazinloesungen
GB1207816A (en) * 1966-12-17 1970-10-07 Bayer Ag Preparation of hydrazine hydrate from aqueous hydrazine sulfate
US4036936A (en) * 1975-08-15 1977-07-19 Otsuka Kagaku Yakuhin Kabushiki Kaisha Process for preparing hydrazine hydrate
FR2323635A1 (fr) * 1975-09-10 1977-04-08 Ugine Kuhlmann Procede de preparation de solutions concentrees d'hydrate d'hydrazine
FR2323634A1 (fr) * 1975-09-10 1977-04-08 Ugine Kuhlmann Solutions concentrees d'hydrate d'hydrazine
JPS63295408A (ja) * 1987-05-28 1988-12-01 Mitsubishi Gas Chem Co Inc 水加ヒドラジン水溶液の精製方法

Also Published As

Publication number Publication date
FI114546B (fi) 2004-11-15
NO905169L (no) 1991-06-05
DE69033741T2 (de) 2001-09-13
DE69033741D1 (de) 2001-07-05
FR2655336A1 (fr) 1991-06-07
NO308840B1 (no) 2000-11-06
CN1052304A (zh) 1991-06-19
IE904356A1 (en) 1991-06-05
EP0952109A3 (fr) 1999-11-17
ES2157195T3 (es) 2001-08-16
JPH04104905A (ja) 1992-04-07
FI905951A (fi) 1991-06-05
PT96064B (pt) 1998-06-30
ATE206686T1 (de) 2001-10-15
EP0952109B1 (fr) 2001-10-10
FI905951A0 (fi) 1990-12-03
CA2031318A1 (fr) 1991-06-05
DE69033827T2 (de) 2002-04-25
DE69033827D1 (de) 2001-11-15
NO905169D0 (no) 1990-11-29
CN1043139C (zh) 1999-04-28
CA2031318C (fr) 1998-02-10
FR2655336B1 (fr) 1993-05-21
US5393508A (en) 1995-02-28
EP0431998B1 (fr) 2001-05-30
KR950003334B1 (ko) 1995-04-10
PT96064A (pt) 1991-09-30
EP0431998A1 (fr) 1991-06-12
EP0952109A2 (fr) 1999-10-27
KR910011766A (ko) 1991-08-07
IE20020601A1 (en) 2003-07-23
ATE201657T1 (de) 2001-06-15
JP2607444B2 (ja) 1997-05-07

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