CN102674981A - Preparation and application of compound chemical fertilizer capable of promoting growth and health of plants - Google Patents
Preparation and application of compound chemical fertilizer capable of promoting growth and health of plants Download PDFInfo
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Abstract
The invention provides preparation and an application of a compound chemical fertilizer capable of promoting growth and health of plants. The compound chemical fertilizer capable of promoting growth and health of plants is composed of a natural organic plant nutrient liquid, a plant extract liquid having bactericidal activity, a macroelement fertilizer and/or a secondary-element fertilizer and/or a microelement fertilizer and/or a plant growth regulator, and auxiliaries, and an efficiency low-toxic bactericide if necessary. The compound chemical fertilizer capable of promoting growth and health of plants is mainly in the form of a water-based preparation, and has an obvious control effect for some common diseases of crops without causing a residue problem. The compound chemical fertilizer capable of promoting growth and health of plants provided by the invention is safe for utilization, friendly to the environment, and capable of effectively improving the yield of agricultural products and improving the quality of the agricultural products. Besides, the compound chemical fertilizer is high in popularization and application values, and has good comprehensive economic benefits and social benefits.
Description
Technical field
The present invention relates to a kind ofly promote plant-growth fertile with healthy compound medicines, particularly be with fertile preparation and application thereof of the organic medicine that is composited of component such as the plant milk extract that contains Fungicidal active substance and other natural organic plant nutritive elements.The present invention is used for agricultural produce and prevents and treats disease, belongs to the fertile production technical field of medicine.
Background technology
The enforcement of vegetable basket project has guaranteed that the resident has the supply of fresh vegetables throughout the year.And vegetable variety is many, and growth cycle is short, easy introduced disease, and especially the facility vegetable plot is even more serious.And some peasant households devote exclusive attention to output unilaterally, excessive blindly use chemical fertilizer, agricultural chemicals, and existing market apply fertilizer, pesticide species are various in addition, and quality is uneven, and some high malicious persistent pesticide have been buried hidden danger to agricultural product quality.Therefore agricultural product quality and safety comes into one's own day by day, seems particularly important and develop some efficient, environmentally friendly agricultural material products for producing non-polluted farm product, green agricultural product and even organic farm products, has great importance to ensuring food safety.
Big quantity research in decades proves that humic acids is " preserver " in carbon cycle " snubber ", biosphere, " cleaner " of ecotope.The plant nutrition product that with the humic acids is staple has acquired application and approval more and more widely.
For solving the pesticide residue problem, some countries develop botanical pesticide in active research.Since after using, botanical pesticide is prone to be decomposed into non-toxic substance, environmentally safe, and component diversification in addition makes insect give birth to characteristics such as resistance than difficult labour, has attracted a lot of experts and scholars to put in the middle of the research of botanical pesticide.Seal chinaberry (Azadirachta india A.Juss) is the most well-known in the world pesticide plant, and nineteen sixty-eight Butterworth separates with Morgan and obtains wherein topmost activeconstituents---nimbin (azadirachtin).The thirties in 20th century, China just carried out extensive studies to plants such as tobacco, trifoliate jewelvine, crotons, the tubers of stemona.The research contents of the relevant botanical pesticide of China relates to the various plants that sections such as Meliaceae, Celastraceae, Cupressaceae, thymelaeceae, pulse family, composite family belong at present.
Matrine is the alkaloid that from plants such as kuh-seng, Herba Sophorae alopecuroidis, extracts, and on agricultural, obtains widespread use in recent years.Isolate vegeto-alkali in 27 altogether from radix sophorae, stem, leaf and spending at present, be mainly quinolizine pyridine (quinolizidin) Alkaloid, only a few is Bispiperidines (dipiperidine-typ) vegeto-alkali.Wherein matrine, Oxymatyine, sophor-anol, sophocarpine, Sophocarpidin etc. are the more vegeto-alkali of content.From existing 34 kinds of the isolating flavonoid compound of matrine root, majority is flavanone and flavanonol, and minority is flavones, NOVASOY 400, phenyl styryl ketone and alcohol thereof, wherein has only 3 kinds to be former times.These flavonoid compounds have bacteriostatic activity mostly.
Acetone extracts such as kuh-seng have the obvious suppression effect to wheat scab (Gibberella zeae), apple anthracnose (Clomerella cingulata), graw mold of tomato (Botrvtis cinerea) mycelial growth and germ spore germination; Through measuring Cytisine, sophoramine, matrine, sophocarpine and sophorine bacteriostatic activity is arranged all; Wherein sophocarpine and sophorine bacteriostatic activity are stronger; Far above m-tetrachlorophthalodinitrile, matrine is active not to be had than big difference with m-tetrachlorophthalodinitrile, and is higher than thiophanate methyl.Report in addition that in addition ethyl acetate extracts such as kuh-seng are to causing the sharp sickle spore bacterium of plant blight; Cause the rhizoctonia of damping-off; The 7 kinds of fungies such as Botrytis cinerea bacterium that cause leaf spot all have significant bacteriostatic action, isolating flavonoid compound Vexibinol from kuh-seng, kurarinone, kuh-seng alcohol, the new pure C of methyl kuh-seng; L-Koryo element and trifolirhizin are mould to Solanum rhizoctonia, hard handle skin umbrella, the special Bo Lishi corruption of model, and standing grain is given birth to the rotten lawn pathogenic bacterium such as mould of rotten mould, melon and fruit has certain restraining effect.In addition, Radix Sophorae Flavescentis extract is inhibited to multiple diseases such as the oidium on the vegetables, Powdery Mildew, gray mold and eqpidemic diseases.The separation from radix sophorae of Ma Zhigang report obtains a kind of 32KD agglutinant protein (SFL); Mycelia is suppressed cotton-wilt fusarium when SFL is 31 μ g (Fusarium oxysporum f.sp.vas-in fectum); SFL be 93 μ g when above zoon to the cotton-wilt fusarium mycelia stop; This agglutinant protein also has the obvious suppression effect to the growth of wheat scab (Gibberella zeae) and Pyricularia oryzae Cav bacterium (Piricularia oryzae), can find out that from above-mentioned the fungicidal activity property composition of kuh-seng can suppress the biosynthesizing of thalline; Can influence mycelial biological oxidation process again, and fungicidal spectrum is wider.
Berberine is the alkaloid from extracted form natural plant such as the coptis, golden cypresses, and its has a broad antifungal spectrum is external to multiple gram-positive and the equal tool bacteriostatic action of negative bacterium.Berberine distributes very wide at occurring in nature, as the Stem of Mountain Dragon of coptis root genus and the Thalictrum of Ranunculaceae, Menispermaceae belong to, the golden cypress genus of Rutaceae, various plants such as the Berberis of Berberidaceae and Mahonia all contain Berberine.
With matrine etc. is that the botanical pesticide of main active ingredient has a lot of bibliographical informations; Some disclosed patents are also arranged; Like CN02125973, its main method is to be that starting material carry out alcohol extracting, concentrate the back and add emulsifying agent and process product with kuh-seng, black false hellebore and cluster redpepper etc.Some patents such as CN02148559, CN200810052326, CN200510123043, CN03156785, CN01144671, CN02113257, CN200310109705, CN01130605 have also reported with kuh-seng and other different herbal medicine to be that starting material extract, being mixed forms some disinfectant use in agriculture.Yet the botanical pesticide ubiquity drug effect of producing with these methods is lower, and it is slower to take effect, and the perhaps relative more high defective of consumption, and the herbal medicine of using in some compatibility belongs to scarce resource, is unfavorable for suitability for industrialized production.On the other hand owing to use chemical pesticide to make a lot of controlling objects produce resistance for many years,, make ecotope face immense pressure in order to keep preventive effect to have to strengthening the consumption of chemical pesticide.And in some facility vegetable plots, it is more or less freely that peasant household satisfies the nutrition of plant growth needs, but the most headache be the disease problem of preventing and treating, the resistance of some disease strengthens gradually, is difficult to control with conventional medicament.For overcoming the above problems; The nutrient for plants of environmental protection and botanical pesticide and suitable chemical pesticide rationally are mixed; Also control simultaneously the generation of disease satisfying the plant-growth desired nutritional like this, reduced the consumption of chemical pesticide again greatly, slowed down pest resistance to insecticide; Reduce toxicity, preserve the ecological environment.
Main purpose of the present invention is rationally to be mixed (suitably adding the environmental type chemical pesticide in case of necessity) through natural organic plant nutrient substance and botanical pesticide; Reach the disease-resistant purpose of raising the output; Reduce the chemical pesticide consumption simultaneously, reduce toxicity, delay the drug-fast development of disease; Reduce pesticidal contamination, preserve the ecological environment.
Summary of the invention
The technical issues that need to address of the present invention just are to provide a kind of preparation and application that promotes that plant-growth is fertile with healthy compound medicines; The present invention with green organic plant nutrient substance with have the plant milk extract reasonable compatibility of fungicidal activity, suitably add efficient, environmentally friendly chemical pesticide in case of necessity and add the regulator that promotes plant-growth, synergistic agent etc. based on this again.Through the reasonable assembly of several plant source fungicide active ingredient; The characteristics of many target spots effect make mixture when preventing and treating disease, also delay the development of germ resistance, are aided with the natural phant nutrient substance simultaneously, can promote the absorption that plant reaches necessary nutritive element effectively; And then the healthy growth of promotion plant; Further the disease resistance of enhancement of plant makes and urgees to grow and prevent and treat disease to complement each other, and reaches a kind of good synergy; Make product of the present invention reach short long raising the output, the environment amenable again effect of efficient sterilizing, finally improve crop yield and quality.Product stability of the present invention is good, and result of use is good, and is easy to use, and saving of work and time is saved peasant household's planting cost, is for producing the effective agrotechnique of green safety agricultural-food, the market outlook broadness.
The objective of the invention is to realize through following technical scheme:
A kind of preparation and application that promotes that plant-growth is fertile with healthy compound medicines, it is made up of following raw materials by weight percent:
Natural organic plant nutritive medium 10-50%
Bactericidal plant extraction liquid 3-30%
High-efficiency low-toxicity sterilant 0.1-8%
Big-and-middle trace element fertilizer 20-40%
Growth regulator 0.05-2%
Sequestrant 0.1-8%
Auxiliary 1-20%
Described natural organic plant nutritive medium is for containing the humic acid plants nutritive medium.
Described bactericidal plant extraction liquid is one or both or two kinds or the mixture of said any combination thereof extracting solution in the plant extraction liquids such as kuh-seng, Herba Sophorae alopecuroidis, wide beans, Root of Chinese Barberry, golden cypress, rheum officinale, garlic, the tuber of stemona, giant knotweed, the bark of eucommia, Pink Plumepoppy Herb, Flower of Aztec Marigold root, grass of meadow rue.
Describedly can suitably increase the high-efficiency low-toxicity sterilant as required, one or both or the said material that can be selected from the sterilant such as disliking mould spirit, tebuconazole, fenarimol, triazolone, Wocosin 50TK, ICIA 5504, difenoconazole, antimycoin 120, nitrile bacterium azoles, white urea cyanogen, SYP-L190, SN 39744 hydrochloric acid, fluzilazol, ethylicin, prochloraz are planted mixture arbitrarily.
Described big secondary nutrients is divided into: macroelement fertilizer and weight unit fertilizer, and wherein macroelement fertilizer is urea, sulphur ammonium, an ammonium nitrate, saltpetre, vitriolate of tartar, Repone K, monoammonium phosphate, diammonium phosphate, potassium primary phosphate, Ureaphil, one or both or the said raw material that contain in the mineral acid/alkali/salt of ammonium phosphate nitrate, nitric acid ammonia calcium and nitrogenous phosphorus potassium plant mixture arbitrarily; In trace element fertilizer one or both or the said raw material that are selected from boric acid, borax, four water eight borate two sodium, calcium chloride, magnesium chloride, sal epsom, zinc sulfate, copper sulfate, ferric sulfate, manganous sulfate, ammonium molybdate, the microelement chelate plant mixture arbitrarily.
Described growth regulator is that one or both or the said raw material in the bright fat of triacontanol price quote, potassium para-nitrophenate, sodium nitrophenolate, methyl piperidine, amine, Plant hormones regulators,gibberellins, 6-BA, forchlorfenuron, indolebutyric acid sodium, brassinolide, the indolebutyric acid potassium planted mixture arbitrarily.
Described sequestrant is YD 30/salt, Hydrocerol A/salt, ethylenediamine triacetic acid/salt, the big acetate/salt of quadrol two salicyls, hydroxyethylethylene diamine tri-acetic acid/salt, diethyl pentetic acid/salt, 1, and one or both in 2-cyclohexanediaminetetraacetic acid/salt, ethyleneglycolbis(2-aminoethylether)tetraacetic acid/salt, the diethylene triamine pentacetic acid (DTPA)/salt or said raw material are planted mixture arbitrarily.
Described auxiliary is a toluene; YLENE; Isopropylcarbinol; Butylacetate; Propyl alcohol; THF; ETHYLE ACETATE; Virahol; Dioxane; Acetone; Formic acid; Acetate; N; Ethanol; Methyl alcohol; Terepthaloyl moietie; Sodium hydroxide; Pottasium Hydroxide; Methyl-sulphoxide; Hydrogen peroxide; Ucar 35; Youxiaolin; TX10 Succinic Acid sodium sulfonate; The dibutyl naphthalenesulfonate; Succinic Acid half ester sulphonate fatty amide; The N methyl taurine sodium salt; Polyoxyethylenated alcohol sodium sulfate; Methylene-bis bitter edible plant sodium sulfonate; The alkyl biphenyl sodium naphthalene sulfonate; Polyoxyethylene stearic acid ester; The alkylnaphthalene formaldehyde condensation products; The styrenated phenol Soxylat A 25-7; Sulfonated alkylbenzene; Sulfonated alkyl naphathalene; Alkyl-sulphate; The alkyl sulfonates material; Alkylphosphonic; Metaphosphate; Pyrophosphate salt; Draw back powder; Lauryl alcohol; Alkene sulfonate; Petroleum sodium sulfonate; Alkylsulphonic acid an alkali metal salt and ammonium salt; TX10; Alkylphenol-polyethenoxy base vitriol; TX10 vitriol; AEO; Sulfonated lignin; Castor oil polyoxyethylene ether; The Viscotrol C ethylene oxide condensate; Polyoxyethylene sorbitan monooleate; In the organosilicon auxiliary agent one or both or said material are planted mixture arbitrarily.
A kind of preparation and application that promotes that plant-growth is fertile with healthy compound medicines, its production craft step and process method are following:
(1) natural organic plant is sought the preparation of liquid.Get an amount of high-quality mineral source humate (humic acids>=40%) in 1: the ratio of 2-5 is dissolved in the deionized water, fully dissolving, guarantee water insoluble matter content≤7% after, add the 0.1%-8 sequestrant, fully stir, this is an A liquid.
(2) contain the preparation of fungicidal activity plant milk extract, comprise raw material processing, lixiviate, concentrate, be mixed etc.Working method of the present invention is: with one or more cut-outs (like needs), the pulverizing in kuh-seng, Herba Sophorae alopecuroidis, wide beans, Root of Chinese Barberry, golden cypress, rheum officinale, garlic, the tuber of stemona, giant knotweed, the bark of eucommia, Pink Plumepoppy Herb, Flower of Aztec Marigold root, the grass of meadow rue; To pulverize raw material and 60%-90% aqueous ethanolic solution mixed soaking then 10-36 hour, blending ratio is 1: 2-6; Refluxing extraction is carried out in interlayer heating then, continues 6-12 hour, collects liquid concentrator at last, makes relative density of medicine liquid remain on 1.1-1.2; Also can carry out after the soaking and extracting required plant extraction liquid being mixed to starting material respectively.The plant extraction liquid for preparing is left standstill, filters, and it is for use to detect qualified importing reaction kettle, and this is a B liquid.
(3) B liquid is imported A liquid and mix, stir, will select big-and-middle trace element, sterilant and plant-growth regulator, auxiliary agent reaches processing condition in proportion and adds people's hybrid reactor and be mixed, and detects to be finished product after qualified, can pack.
The utilization of product of the present invention on multiple diseases such as various crop especially melon vegetables can be used to prevent and treat by Alternariaspp Alternaria.sp, dry thread Pyrenomycetes Rhizoctonia solani, parasitica Phytophthora sp, anthrax bacteria Colletotrichum sp, sickle-like bacteria Fusarium sp, Botrytis cinerea Botrytis cinerea, stem and put the plurality of plant diseases that mould Phoma sp, Verticillium Verticillium sp, ustilago Ustilago sp cause.Particularly be fit to the control of some common disease such as Powdery Mildews (sphaerothrca fuliginea), late blight (Phytophthora infestans), oidium (Pseudoperonospora cubensis), target spot (Corynespora cassiicola), leaf spot diseases such as (Cercospora citrullina).Especially product of the present invention is suitable for using on the crop of susceptible disease evil under the facility planting conditions such as booth, and some disease that produces resistance is had good control effect, improves the yield and quality of crop simultaneously.
Beneficial effect of the present invention is:
1, obvious effect of increasing production.Test shows that product of the present invention comparison is according to nearly increasing production 20%.
2, good to disease-controlling effect.Test shows that product of the present invention has good control effect to multiple diseases such as melon vegetables, such as Powdery Mildew, oidium, blight etc.
3, polynary short plant health growth compound medicines fertilizer of the present invention is safe in utilization, environmentally friendly, can effectively improve agricultural output, improves fruit-vegetable quality.Popularization, using value height have overall economic efficiency and social benefit preferably.
Description of drawings:
Fig. 1 promotes plant-growth and the preparation of the compound medicines fertilizer of health and preparing method's schema of application for the present invention is a kind of.
Embodiment
In order better to understand the present invention, adopt embodiment that utilization the present invention is done further explain below, but embodiment of the present invention are not limited to these instances.
A kind of preparation and application that promotes that plant-growth is fertile with healthy compound medicines, it is made up of following raw materials by weight percent:
Natural organic plant nutritive medium 10-50%
Bactericidal plant extraction liquid 3-30%
High-efficiency low-toxicity sterilant 0.1-8%
Big-and-middle trace element fertilizer 20-40%
Growth regulator 0.05-2%
Sequestrant 0.1-8%
Auxiliary 1-20%
Described natural organic plant nutritive medium is for containing the humic acid plants nutritive medium.
Described bactericidal plant extraction liquid is one or both or two kinds or the mixture of said any combination thereof extracting solution in the plant extraction liquids such as kuh-seng, Herba Sophorae alopecuroidis, wide beans, Root of Chinese Barberry, golden cypress, rheum officinale, garlic, the tuber of stemona, giant knotweed, the bark of eucommia, Pink Plumepoppy Herb, Flower of Aztec Marigold root, grass of meadow rue.
Describedly can suitably increase the high-efficiency low-toxicity sterilant as required, one or both or the said material that can be selected from the sterilant such as disliking mould spirit, tebuconazole, fenarimol, triazolone, Wocosin 50TK, ICIA 5504, difenoconazole, antimycoin 120, nitrile bacterium azoles, white urea cyanogen, SYP-L190, SN 39744 hydrochloric acid, fluzilazol, ethylicin, prochloraz are planted mixture arbitrarily.
Described big secondary nutrients is divided into: macroelement fertilizer and weight unit fertilizer, and wherein macroelement fertilizer is urea, sulphur ammonium, an ammonium nitrate, saltpetre, vitriolate of tartar, Repone K, monoammonium phosphate, diammonium phosphate, potassium primary phosphate, Ureaphil, one or both or the said raw material that contain in the mineral acid/alkali/salt of ammonium phosphate nitrate, nitric acid ammonia calcium and nitrogenous phosphorus potassium plant mixture arbitrarily; In trace element fertilizer one or both or the said raw material that are selected from boric acid, borax, four water eight borate two sodium, calcium chloride, magnesium chloride, sal epsom, zinc sulfate, copper sulfate, ferric sulfate, manganous sulfate, ammonium molybdate, the microelement chelate plant mixture arbitrarily.
Described growth regulator is that one or both or the said raw material in the bright fat of triacontanol price quote, potassium para-nitrophenate, sodium nitrophenolate, methyl piperidine, amine, Plant hormones regulators,gibberellins, 6-BA, forchlorfenuron, indolebutyric acid sodium, brassinolide, the indolebutyric acid potassium planted mixture arbitrarily.
Described sequestrant is YD 30/salt, Hydrocerol A/salt, ethylenediamine triacetic acid/salt, the big acetate/salt of quadrol two salicyls, hydroxyethylethylene diamine tri-acetic acid/salt, diethyl pentetic acid/salt, 1, and one or both in 2-cyclohexanediaminetetraacetic acid/salt, ethyleneglycolbis(2-aminoethylether)tetraacetic acid/salt, the diethylene triamine pentacetic acid (DTPA)/salt or said raw material are planted mixture arbitrarily.
Described auxiliary is a toluene; YLENE; Isopropylcarbinol; Butylacetate; Propyl alcohol; THF; ETHYLE ACETATE; Virahol; Dioxane; Acetone; Formic acid; Acetate; N; Ethanol; Methyl alcohol; Terepthaloyl moietie; Sodium hydroxide; Pottasium Hydroxide; Methyl-sulphoxide; Hydrogen peroxide; Ucar 35; Youxiaolin; TX10 Succinic Acid sodium sulfonate; The dibutyl naphthalenesulfonate; Succinic Acid half ester sulphonate fatty amide; The N methyl taurine sodium salt; Polyoxyethylenated alcohol sodium sulfate; Methylene-bis bitter edible plant sodium sulfonate; The alkyl biphenyl sodium naphthalene sulfonate; Polyoxyethylene stearic acid ester; The alkylnaphthalene formaldehyde condensation products; The styrenated phenol Soxylat A 25-7; Sulfonated alkylbenzene; Sulfonated alkyl naphathalene; Alkyl-sulphate; The alkyl sulfonates material; Alkylphosphonic; Metaphosphate; Pyrophosphate salt; Draw back powder; Lauryl alcohol; Alkene sulfonate; Petroleum sodium sulfonate; Alkylsulphonic acid an alkali metal salt and ammonium salt; TX10; Alkylphenol-polyethenoxy base vitriol; TX10 vitriol; AEO; Sulfonated lignin; Castor oil polyoxyethylene ether; The Viscotrol C ethylene oxide condensate; Polyoxyethylene sorbitan monooleate; In the organosilicon auxiliary agent one or both or said material are planted mixture arbitrarily.
A kind of preparation and application that promotes that plant-growth is fertile with healthy compound medicines, its production craft step and process method are following:
(1) natural organic plant is sought the preparation of liquid.Get an amount of high-quality mineral source humate (humic acids>=40%) in 1: the ratio of 2-5 is dissolved in the deionized water, fully dissolving, guarantee water insoluble matter content≤7% after, add the 0.1%-8 sequestrant, fully stir, this is an A liquid.
(2) contain the preparation of fungicidal activity plant milk extract, comprise raw material processing, lixiviate, concentrate, be mixed etc.Working method of the present invention is: with one or more cut-outs (like needs), the pulverizing in kuh-seng, Herba Sophorae alopecuroidis, wide beans, Root of Chinese Barberry, golden cypress, rheum officinale, garlic, the tuber of stemona, giant knotweed, the bark of eucommia, Pink Plumepoppy Herb, Flower of Aztec Marigold root, the grass of meadow rue; To pulverize raw material and 60%-90% aqueous ethanolic solution mixed soaking then 10-36 hour, blending ratio is 1: 2-6; Refluxing extraction is carried out in interlayer heating then, continues 6-12 hour, collects liquid concentrator at last, makes relative density of medicine liquid remain on 1.1-1.2; Also can carry out after the soaking and extracting required plant extraction liquid being mixed to starting material respectively.The plant extraction liquid for preparing is left standstill, filters, and it is for use to detect qualified importing reaction kettle, and this is a B liquid.
(3) B liquid is imported A liquid and mix, stir, will select big-and-middle trace element, sterilant and plant-growth regulator, auxiliary agent reaches processing condition in proportion and adds people's hybrid reactor and be mixed, and detects to be finished product after qualified, can pack.
Embodiment 1 natural organic plant is sought the preparation of liquid
Get the high-quality mineral source humate of 40kg (humic acids >=60%) and be dissolved in the 120kg deionized water, fully dissolving.In the aqueous solution, add the 4kg disodium edta, fully stir, this is an A liquid.
Embodiment 2 contains the preparation of fungicidal activity plant extraction liquid
(1) gets kuh-seng 300kg, golden cypress 150kg, Folium Eucommiae 100kg, grass of meadow rue 50kg.
(2) above-mentioned starting material are cut off (like needs), pulverize, will pulverize 80% ethanol mixed soaking 24h of 5 times of raw material and above-mentioned raw materials weight then, extract bulk drug effective constituent.
(3) interlayer heating makes ethanol reach boiling point and is distilled recycling, so concentrates while extracting, and continues 8 hours, medicinal ingredient is extracted as far as possible finish, and collect liquid concentrator, makes relative density of medicine liquid remain on 1.1-1.2.
Embodiment 3 contains the preparation of fungicidal activity plant extraction liquid
(1) gets kuh-seng 400kg, Flower of Aztec Marigold root 50kg, golden cypress 200kg, Folium Eucommiae 150kg.
(2) above-mentioned starting material are cut off (like needs), pulverize, will pulverize 85% ethanol mixed soaking 24h of 4 times of raw material and above-mentioned raw materials weight then, extract bulk drug effective constituent.
(3) interlayer heating makes ethanol reach boiling point and is distilled recycling, so concentrates while extracting, and continues 8 hours, medicinal ingredient is extracted as far as possible finish, and collect liquid concentrator, makes relative density of medicine liquid remain on 1.1-1.2.
Embodiment 4 contains the preparation of fungicidal activity plant extraction liquid
(1) gets kuh-seng 250kg, Folium Eucommiae 150kg.
(2) above-mentioned starting material are cut off (like needs), pulverize, will pulverize 85% ethanol mixed soaking 24h of 5 times of raw material and above-mentioned raw materials weight then, extract bulk drug effective constituent.
(3) interlayer heating makes ethanol reach boiling point and is distilled recycling, so concentrates while extracting, and continues 8 hours, medicinal ingredient is extracted as far as possible finish, and collect liquid concentrator, makes relative density of medicine liquid remain on 1.1-1.2.
(4) get Herba Sophorae alopecuroidis 200kg, golden cypress 150kg, grass of meadow rue 50kg.
(5) above-mentioned starting material are cut off (like needs), pulverize, will pulverize 85% ethanol mixed soaking 24h of 5 times of raw material and above-mentioned raw materials weight then, extract bulk drug effective constituent.
(6) interlayer heating makes ethanol reach boiling point and is distilled recycling, so concentrates while extracting, and continues 8 hours, medicinal ingredient is extracted as far as possible finish, and collect liquid concentrator, makes relative density of medicine liquid remain on 1.1-1.2.
(7) plant extraction liquid of step (3) and step (6) being produced mixes, and is for use.
Embodiment 5 promotes the preparation that plant-growth is fertile with healthy compound medicines
Under the normal temperature, get 24 parts of A liquid, the plant extraction liquid of 20 parts of embodiment 2 preparations; 0.1 part amine DA-6,15 parts of saltpetre, 10 parts of potassium primary phosphates; 8 parts of urea, 3 parts of Virahols, 8 parts of X 2073es; 5 parts of styrenated phenol T 46155 (n30) ether, water polishing to 100 part can be mixed with polynary compound disease-resistant growth-promoting soluble liquid.
Embodiment 6 promotes plant-growth and healthy fertile detection of compound medicines with embodiment 5, and its result is following:
Table 1 embodiment 5 promotes plant-growth and the healthy fertile survey report table of compound medicines
Embodiment 7 promotes the preparation that plant-growth is fertile with healthy compound medicines
Under the normal temperature, get 22 parts of A liquid, the plant extraction liquid of 20 parts of embodiment 3 preparations, 0.08 part of indolebutyric acid potassium; 15 parts of saltpetre, 10 parts of potassium primary phosphates, 8 parts of urea, 5 parts of four water eight borate two sodiums; 3 parts of Virahols, 5 parts of YLENE, 2 parts of triazolones; 4 parts of X 2073es, 4 parts of styrenated phenol T 46155 (n30) ether, water polishing to 100 part.
Embodiment 8 promotes plant-growth and healthy fertile detection of compound medicines with embodiment 7, and its result is following:
Table 2 embodiment 7 promotes plant-growth and the healthy fertile survey report table of compound medicines
Embodiment 9 promotes the preparation that plant-growth is fertile with healthy compound medicines
Under the normal temperature, get 22 parts of A liquid, the plant extraction liquid of 20 parts of embodiment 4 preparations, 0.1 part of potassium para-nitrophenate; 10 parts of zinc sulfate, 10 parts of four water eight borate two sodiums, 6 parts of manganous sulfates, 5 parts of Virahols; 5 parts of methyl-sulphoxides, 3 parts of SN 39744s, 0.5 part of white urea cyanogen, 3 parts of X 2073es; 5 parts of Viscotrol C ethylene oxide condensates, 5 parts of terepthaloyl moietie, water polishing to 100 part.
Embodiment 10 promotes plant-growth and healthy fertile detection of compound medicines with embodiment 9, and its result is following:
Table 3 embodiment 9 promotes plant-growth and the healthy fertile survey report table of compound medicines
The promotion plant-growth of the embodiment 11 use embodiment of the invention 5 and healthy compound medicines fertilizer are to joint cucurbit wilt control effect
Tested in March, 2010-April and carry out in Xinzhou town, Yangdong County, Guangdong.The same day after transplanting executed medicine for the first time by the joint melon, established 3 processing: the embodiment of the invention 5 promotes plant-growth and healthy compound medicines fertile (diluting 800 times), and 30% dislikes 1000 times of mould Lingshui Spring agent, the clear water contrast.Repeat for 4 times, every repetition 30 strains, soup 100ml is drenched in every strain, drenches medicine for the second time after two weeks again.Periodic investigation diseased plant number is till results.Accumulative total is respectively handled total diseased plant number, calculates control effect.
The control effect of table 4 pair joint cucurbit wilt
Test explanation on the joint melon, the compound medicines fertilizer of the embodiment of the invention 5 promotion plant-growths and health reaches 85.37% to the control effect of joint cucurbit wilt, and it is superior that the mould Lingshui Spring agent protection effect of medicament 30% evil is shone in comparison.After investigation also found to use more than 5 yuan of short plant health growth compound medicines fertilizer of inventive embodiments, the joint melon was very large vivid, has production-increasing function preferably.
Embodiment 12 uses the compound medicines fertilizer of the embodiment of the invention 7 promotion plant-growths and health to the powdery mildew of cucumber control effect
Tested in August, 2011 and carry out in cucumber field, Yulin City of Guangxi Zhuang Autonomous Chang Wang village.If 3 processing: the polynary short plant health growth compound medicines fertile (diluting 800 times) of the embodiment of the invention 7,15% triazolone WP1000 times, clear water contrast.Repeat, be divided into 12 sub-districts, every sub-district area 20m for 4 times
2, adopt randomized block design.
Adopt plants stems foliar spray mist to handle.Spouting liquid is evenly to squirt leave dual sides, spouting liquid 900L/hm
2About.Dispenser is 2 times altogether, 7 days at interval.Carry out state of an illness radix investigation before the 1st dispenser, 7 days investigation prevention effects after 7 days and last 1 dispenser are investigated 3 times altogether after the 1st dispenser.Every sub-district is got 4 investigation at random, every some investigation 2 strains, and whole blades are investigated in every strain.Grade scale is following: 0 grade is no scab; 1 grade accounts for below 5% of whole leaf area for lesion area; 3 grades of 6%-10% that account for whole leaf area for lesion area; 5 grades of 11%-20% that account for whole leaf area for lesion area; 7 grades of 21%-40% that account for whole leaf area for lesion area; 9 grades account for more than 40% of whole leaf area for lesion area.
The control effect of table 5 pair powdery mildew of cucumber
Investigation result shows that embodiment 7 promotes plant-growth and healthy compound medicines fertilizer that powdery mildew of cucumber is had excellent preventive effect; Be superior to contrasting the control effect of medicament 15% triazolone WP; Polynary short plant health simultaneously of the present invention is grown compound medicines fertilizer to cucumber production promoting effect remarkable (seeing table 6), and to cucumber growth safety, with environmental friendliness; Have higher popularization, using value, overall economic efficiency and control effect are remarkable.
Embodiment 13 uses the compound medicines fertilizer of the embodiment of the invention 7 promotion plant-growths and health to the cucumber production promoting effect
Table 6 pair cucumber production promoting effect
Embodiment 14 uses the compound medicines fertilizer of the embodiment of the invention 9 promotion plant-growths and health to the cucumber downy mildew control effect
Test that town Xi Liucun carries out in rice field, Shouguang City in April, 2011, the cultivation condition of all experimental plots, soil type, water and fertilizer management are all consistent, and experimental field fertility is more even.Adopt the processing of spraying of workers and peasants' 16 type atomizers, water consumption 750kg/hm
2At cucumber downy mildew stadium the 1st time spray medicine that starts, carried out the 2nd time at a distance from 8 days and spray medicine.
Randomized block design is adopted in each sub-district, establishes guard rows between the sub-district and separates; Every sub-district area 30m
2, establish chemicals treatment respectively and be: the embodiment of the invention 9 promotes plant-growths and healthy compound medicines fertile (dilute 800 times), 722g/L SN 39744 aqua (dilute 1000 times) adds supernatant water and contrasts and establish 3 processing altogether, each processing repetition 4 times, totally 12 sub-districts.
Every sub-district is got 5 investigation at random, every some investigation 2 strains, and every sub-district is investigated 10 strains altogether, and 10 blades of every strain investigation are added up total number of sheets, the sick number of sheets and corresponding sick progression, calculate disease index and control effect.Control time and number of times: investigation state of an illness radix before the dispenser, respectively investigated drug effect 1 time in 7 days after (preceding 1 day of the 2nd dispenser) in 7 days, the 2nd dispenser after the 1st dispenser, investigate altogether 3 times.
The blade stage division is 0 grade: no scab; 1 grade: lesion area accounts for below 5% of whole leaf area; 3 grades: lesion area accounts for the 6%-25% of whole leaf area; 5 grades: lesion area accounts for the 26%-50% of whole leaf area; 7 grades: lesion area accounts for the 51%-75% of whole leaf area; 9 grades: lesion area accounts for more than 76% of whole leaf area.
Statistical analysis technique
The control effect of table 7 pair cucumber downy mildew
Can find out from test-results; Embodiment 9 promotes plant-growth and healthy compound medicines fertilizer that cucumber downy mildew is had good preventive effect; Comparison exceeds nearly 10 percentage point according to the preventive effect of medicament SN 39744 aqua, is a kind of desirable medicament of control cucumber downy mildew, begins to spray in the cucumber downy mildew their early stage; Look dispenser 2-3 time continuously of PD situation, be advisable with 7-10 days interval.
Above embodiment is only unrestricted in order to technical scheme of the present invention to be described; Although the present invention is specified with reference to preferred embodiment; Those of ordinary skill in the art is to be understood that; Can make amendment or be equal to replacement technical scheme of the present invention, and not break away from the spirit and the scope of technical scheme of the present invention.
Claims (9)
1. a preparation and application that promotes that plant-growth is fertile with healthy compound medicines, it is characterized in that: it is made up of following raw materials by weight percent:
Natural organic plant nutritive medium 10-50%
Bactericidal plant extraction liquid 3-30%
High-efficiency low-toxicity sterilant 0.1-8%
Big-and-middle trace element fertilizer 20-40%
Growth regulator 0.05-2%
Sequestrant 0.1-8%
Auxiliary 1-20%
2. a kind of preparation and application that promotes that plant-growth is fertile with healthy compound medicines according to claim 1, it is characterized in that: described natural organic plant nutritive medium is for containing the humic acid plants nutritive medium.
3. a kind of preparation and application that promotes that plant-growth is fertile with healthy compound medicines according to claim 1 is characterized in that: described bactericidal plant extraction liquid is one or both or two kinds or the mixture of said any combination thereof extracting solution in the plant extraction liquids such as kuh-seng, Herba Sophorae alopecuroidis, wide beans, Root of Chinese Barberry, golden cypress, rheum officinale, garlic, the tuber of stemona, giant knotweed, the bark of eucommia, Pink Plumepoppy Herb, Flower of Aztec Marigold root, grass of meadow rue.
4. a kind of preparation and application that promotes that plant-growth is fertile with healthy compound medicines according to claim 1; It is characterized in that: described high-efficiency low-toxicity sterilant, one or both or the said material that can be selected from the sterilant such as disliking mould spirit, tebuconazole, fenarimol, triazolone, Wocosin 50TK, ICIA 5504, difenoconazole, antimycoin 120, nitrile bacterium azoles, white urea cyanogen, SYP-L190, SN 39744 hydrochloric acid, fluzilazol, ethylicin, prochloraz are planted mixture arbitrarily.
5. a kind of preparation and application that promotes that plant-growth is fertile with healthy compound medicines according to claim 1; It is characterized in that: described big secondary nutrients is divided into: macroelement fertilizer and secondary nutrients, and wherein macroelement fertilizer is urea, sulphur ammonium, an ammonium nitrate, saltpetre, vitriolate of tartar, Repone K, monoammonium phosphate, diammonium phosphate, potassium primary phosphate, Ureaphil, one or both or the said raw material that contain in the mineral acid/alkali/salt of ammonium phosphate nitrate, nitric acid ammonia calcium and nitrogenous phosphorus potassium plant mixture arbitrarily; In trace element fertilizer one or both or the said raw material that are selected from boric acid, borax, four water eight borate two sodium, calcium chloride, magnesium chloride, sal epsom, zinc sulfate, copper sulfate, ferric sulfate, manganous sulfate, ammonium molybdate, the microelement chelate plant mixture arbitrarily.
6. a kind of preparation and application that promotes that plant-growth is fertile with healthy compound medicines according to claim 1 is characterized in that: described growth regulator is that one or both or the said raw material in triacontanol price quote, potassium para-nitrophenate, sodium nitrophenolate, methyl piperidine, the bright fat of amine, Plant hormones regulators,gibberellins, 6-BA, forchlorfenuron, indolebutyric acid sodium, brassinolide, the indolebutyric acid potassium planted mixture arbitrarily.
7. a kind of preparation and application that promotes that plant-growth is fertile with healthy compound medicines according to claim 1; It is characterized in that: described sequestrant is YD 30/salt, Hydrocerol A/salt, ethylenediamine triacetic acid/salt, the big acetate/salt of quadrol two salicyls, hydroxyethylethylene diamine tri-acetic acid/salt, diethyl pentetic acid/salt, 1, and one or both in 2-cyclohexanediaminetetraacetic acid/salt, ethyleneglycolbis(2-aminoethylether)tetraacetic acid/salt, the diethylene triamine pentacetic acid (DTPA)/salt or said raw material are planted mixture arbitrarily.
8. a kind of preparation and application that promotes that plant-growth is fertile with healthy compound medicines according to claim 1 is characterized in that: one or both or said material that described auxiliary is toluene, YLENE, isopropylcarbinol, butylacetate, propyl alcohol, THF, ETHYLE ACETATE, Virahol, dioxane, acetone, formic acid, acetate, N, ethanol, methyl alcohol, terepthaloyl moietie, sodium hydroxide, Pottasium Hydroxide, methyl-sulphoxide, hydrogen peroxide, Ucar 35, Youxiaolin, TX10 Succinic Acid sodium sulfonate, dibutyl naphthalenesulfonate, Succinic Acid half ester sulphonate fatty amide, N methyl taurine sodium salt, polyoxyethylenated alcohol sodium sulfate, methylene-bis bitter edible plant sodium sulfonate, alkyl biphenyl sodium naphthalene sulfonate, polyoxyethylene stearic acid ester, alkylnaphthalene formaldehyde condensation products, styrenated phenol Soxylat A 25-7, sulfonated alkylbenzene, sulfonated alkyl naphathalene, alkyl-sulphate, alkyl sulfonates material, alkylphosphonic, metaphosphate, pyrophosphate salt, draw back in powder, lauryl alcohol, alkene sulfonate, petroleum sodium sulfonate, alkylsulphonic acid an alkali metal salt and ammonium salt, TX10, alkylphenol-polyethenoxy base vitriol, TX10 vitriol, AEO, sulfonated lignin, castor oil polyoxyethylene ether, Viscotrol C ethylene oxide condensate, polyoxyethylene sorbitan monooleate, the organosilicon auxiliary agent are planted mixture arbitrarily.
9. a kind of preparation and application that promotes that plant-growth is fertile with healthy compound medicines according to claim 1, it is characterized in that: its production craft step and process method are following:
(1) natural organic plant is sought the preparation of liquid.Get an amount of high-quality mineral source humate (humic acids>=40%) in 1: the ratio of 2-5 is dissolved in the deionized water, fully dissolving, guarantee water insoluble matter content≤7% after, add the 0.1%-8 sequestrant, fully stir, this is an A liquid.
(2) contain the preparation of fungicidal activity plant milk extract, comprise raw material processing, lixiviate, concentrate, be mixed.Working method of the present invention is: with one or more cut-outs (like needs), the pulverizing in kuh-seng, Herba Sophorae alopecuroidis, wide beans, Root of Chinese Barberry, golden cypress, rheum officinale, garlic, the tuber of stemona, giant knotweed, the bark of eucommia, Pink Plumepoppy Herb, Flower of Aztec Marigold root, the grass of meadow rue; To pulverize raw material and 60%-90% aqueous ethanolic solution mixed soaking then 10-36 hour, blending ratio is 1: 2-6; Refluxing extraction is carried out in interlayer heating then, continues 6-12 hour, collects liquid concentrator at last, makes relative density of medicine liquid remain on 1.1-1.2; Also can carry out after the soaking and extracting required plant extraction liquid being mixed to starting material respectively.The plant extraction liquid for preparing is left standstill, filters, and it is for use to detect qualified importing reaction kettle, and this is a B liquid.
(3) B liquid is imported A liquid and mix, stir, will select big-and-middle trace element, sterilant and plant-growth regulator, auxiliary agent reaches processing condition in proportion and adds people's hybrid reactor and be mixed, and detects to be finished product after qualified, can pack.
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Application publication date: 20120919 |