CN101792353A - Multifunctional compound fertilizer capable of killing pests, preventing diseases and increasing yield - Google Patents
Multifunctional compound fertilizer capable of killing pests, preventing diseases and increasing yield Download PDFInfo
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Abstract
The invention relates to a multifunctional compound fertilizer capable of killing pests, preventing diseases and increasing yield. The preparation method of the multifunctional compound fertilizer comprises the following steps: firstly, respectively preparing a component A, a component B and a component C, wherein the component A is a vegetable insecticide, thecomponent B is a vegetable bactericide, and the component C is a vegetable growth promoting and yield increasing agent; after the three components are prepared, adding the finished product of the component C into a synthesis kettle for heating; then, sequentially adding the liquid medicine of the component A and the liquid medicine of the component B for continuously stirring, and keeping constant temperature; adding a penetrating agent JFC and polyethylene glycol into the synthesis kettle for stirring; and finally, adding a buffering agent for stirring and mixing uniformly, and homogenizing the mixture by a high-pressure homogenizer to obtain the finished product of the multifunctional compound fertilizer. The multifunctional compound fertilizer of the invention has very high insecticidal and bactericidal efficiencies, smaller toxic side effects and safety to people and livestock, promotes the growth and the development of plants, increases the chlorophyll content, and greatly improves the crop yield.
Description
Technical field
The invention discloses a kind of fertilizer, especially a kind of multifunctional compound fertilizer.
Background technology
Multifunctional compound fertilizer is a kind of new-type fertilizer.At present, the desinsection that uses in the domestic plant husbandry, diseases prevention, production-increasing preparation is the simple function product mostly; The production overall efficiency is low; Desinsection, diseases prevention agent are also in the majority with artificial chemosynthesis, and high malicious high residue is unfavorable for the exploitation and the production of green food.
Summary of the invention
The objective of the invention is to make a kind of new fertilizer, it has the dual nature of sterilant and fertilizer, and the raw material that wherein plays insecticidal action is with the preparation of the extract of natural thallophyta.
The present invention is achieved in that a kind of multifunctional compound fertilizer capable of killing pests, preventing diseases and increasing yield, makes by following method:
Step 1: prepare following three kinds of components respectively---A component vegetable insecticide, B component bactericide and C component plant growing volume increase agent
1) preparation A component vegetable insecticide
Get following raw material: the root of langdu; Tobacco rods; Black false hellebore; Trifoliate jewelvine; Kuh-seng; The tuber of stemona; Fructus Cnidii; The Fruit of Belveder; Cortex meliae; Pericarpium zanthoxyli.
After above-mentioned raw materials cleaned, dries, cuts into slices, pulverizes, adopt totally-enclosed, thermal backflow, twice circulation to extract again, distillation concentrates extraction process by water: the first step, earlier the medicinal material after the above-mentioned pulverizing is added and extract still, add medicinal material amount 5-6 water (quality multiple) doubly then, keep thermal backflow and extract 80-100 ℃ of temperature, 60 minutes extraction times.From extract still, extract and be delivered to soup out still kettle with the vacuum filtration machine; Second step, continue in extracting still, to add medicinal material amount 5-6 water (quality multiple) doubly, keep thermal backflow and extract 80-100 ℃ of temperature, 60 minutes extraction times.With the soup vacuum filtration to still kettle.Distill concentratedly after the soup that extracted twice is obtained mixes, keep 100 ℃ of temperature.The water of condensation that produces in the still-process reclaims, and as the solvent of later extraction, at last soup is concentrated into mass concentration and is 35% soup, and promptly A component vegetable insecticide is standby.
2) preparation B component bactericide
Get following raw material: the common vetch dish; Honeysuckle; The capsule of weeping forsythia; Pyroligneous liquor; Natural propolis.
The back is cleaned, dries, cuts into slices, pulverized to common vetch dish, honeysuckle and capsule of weeping forsythia process by after being same as the extraction of A component similarity condition, filtration, concentration technology processing, soup with the mass concentration 35% that obtains, be mixed by 44: 5: 1 (mass ratio) with pyroligneous liquor (mass concentration 98%) and natural propolis again, promptly make B component bactericide, standby.
3) preparation C component plant growing volume increase agent
Get following raw material: amino acid; Potassium fulvate solution; Citric acid; Organic nutrient aganic nutrient agent; Urea; Phosphoric acid; Saltpetre; Trace element 1-2; Poly-aspartic potassium; Rare earth element; Sodium nitrophenolate; DA-6; The EDTA disodium salt.
Earlier potassium fulvate solution is injected synthesis reactor, be heated to 50-55 ℃, add amino acid then successively. citric acid .EDTA disodium salt. constantly stirred 10 minutes, keep 50-55 ℃ of constant temperature, after the dissolving, again trace element is added fully, constantly stirring reaction is 10 minutes, keeps 50-55 ℃ of constant temperature; Again saltpetre, potassium primary phosphate, rare earth element, sodium nitrophenolate, DA-6, organic nutrient aganic nutrient agent, poly-aspartic potassium are added synthesis reactor successively, constantly stirred 30 minutes, keep 50-55 ℃ of temperature; At last urea is added synthesis reactor and constantly stirred 10 minutes,, both obtained C component plant growing volume increase agent finished product with the liquid filtering that obtains and with behind the filtrate glue mill, standby.
Step 2: preparation multifunctional compound fertilizer
Get the A component; The B component; The C component; Get penetrating agent JFC again; Polyoxyethylene glycol; Buffer reagent.
Earlier C component finished product is added synthesis reactor, be heated to 50-55 ℃, then A component soup, B component soup are added successively, constantly stirred 30 minutes, keep 50-55 ℃ of constant temperature, again with penetrating agent JFC, polyoxyethylene glycol adds synthesis reactor, constantly stirs 10 minutes; Add buffer reagent at last, after constantly mixing, behind the high pressure homogenizer homogeneous, both obtained the multifunctional compound fertilizer finished product.
Multifunctional compound fertilizer desinsection of the present invention, germ-resistant efficient are high, and toxic side effect is less, to the person poultry safety; Promote growth and development of plants, increase chlorophyll content, improve crop yield greatly.
Embodiment
In above-mentioned step 1:
The raw material of preparation A component vegetable insecticide by total mass per-cent is: root of langdu 30-45; Tobacco rods 15-35; Black false hellebore 2-5; Trifoliate jewelvine 2-5; Kuh-seng 8-12; Tuber of stemona 5-10; Fructus Cnidii 3-5; Fruit of Belveder 3-5; Cortex meliae 5-10; Pericarpium zanthoxyli 1-3.
The raw material of preparation B component bactericide by total mass per-cent is: common vetch dish 40-55; Honeysuckle 15-25; Capsule of weeping forsythia 15-25; Pyroligneous liquor (mass concentration 98%) 10-15; Natural propolis 1-2.
The raw material of preparation C component plant growing volume increase agent by total mass per-cent is: amino acid (40% quality solid content) 6-8; Potassium fulvate solution (mass concentration 4%) 40-50; Citric acid 2-4; Organic nutrient aganic nutrient agent (yellow humic acid) 5-8; Urea 10-15; Potassium primary phosphate 8-10; Saltpetre 7-9; Trace element H3BO3, (NH4) 6Mo7O24 4H2O, MnSO4H2O, ZnSO4 and MgSO4 1-2; Poly-aspartic potassium (46% solid content) 1-2; Rare earth element 0.2-0.3; Sodium nitrophenolate 0.1-0.5; DA-6 0.1-0.5; EDTA disodium salt 0.5-1.Wherein: contained each constituent mass is identical in the trace element; Rare earth element is any one or any several and any proportioning in its 17 kinds of elements, that is, so long as rare earth element, no matter its moiety all can be used.
In above-mentioned steps two:
Get A component 10-15; B component 5-10; C component 55-60; Penetrating agent JFC 10-15; Polyoxyethylene glycol 8-10; Buffer reagent 5-10.
Wherein: penetrating agent JFC is the condenses of low-carbon (LC) alkanol and oxyethane, is the commercially available prod, and the great Chemical Industry Science Co., Ltd, sky, Jingzhou City of closing closes scientific and technological chemical industry company limited and have this product to sell as Shanghai.Buffer reagent is the mixture of SODIUM PHOSPHATE, MONOBASIC and Sodium phosphate dibasic, and wherein, the mass ratio of SODIUM PHOSPHATE, MONOBASIC and Sodium phosphate dibasic is 1: 2.
Below be the practicality experiment situation of product of the present invention on crop:
One, the experiment of the practicality on soybean (2008 year)
(1) materials and methods:
Experiment is located at Raohe County, Heilongjiang Province agricultural technology spread experiment centre, is smolmitza for examination soil.
1, for trying fertilizer: disinsection prophylaxis yield-increasing multifunctional composite liquid fertilizer
2, experimental cultivar: " closing rich 35 ". provide by county seeds company
3, one mu of experiment area, one mu of contrast area
4, experiment is handled
1. begin in the soybean initial bloom stage, twice of foliage-spray (15 days at interval), mu consumption 50 grams are converted 15 kilograms in water.
2. the check plot is in identical time spray equivalent clear water
(2) interpretation of result: to soybeans they grow proterties and volume analysis (seeing Table)
Soybeans they grow proterties and volume analysis table
| Project is handled | Plant height (CM) | Stem thick (CM) | Single-strain legumen number | The empty pod number of individual plant | Setting percentage | 100-grain weight (g) | Per mu yield (kg) | Volume increase % |
| Multifunctional compound fertilizer | ??73 | ??0.64 | ??45 | ??6 | ??86.8 | ??27.1 | ??252 | ??16.12 |
| Contrast | ??65 | ??0.50 | ??31 | ??11 | ??65.1 | ??22.4 | ??217 | ??----- |
(3) field investigation result:
Use the soybean of multi-functional composite liquid fertilizer. it is vigorous to grow. and the leaf look dark green, and aphid is not taken place the time of infertility. heart-eating worm harm, no stem rot takes place; And the middle and later periods is being given birth in the check plot, and August 10, discovery had slight aphid, and has 2% stem rot to take place, and it can be said that bright multi-functional compound liquid fertilizer control soybean diseases and insect pests is satisfactory for result and effect of increasing production is obvious.
Two, the in-use testing on Chinese cabbage (2009 year)
Test objective: check multi-functional composite liquid fertilizer to the Chinese cabbage prevention and control of plant diseases, pest control and effect of increasing production.
Test kind: " east farming 905 "
Test soil: smolmitza
Test area: one mu of treatment zone, one mu of check plot
Test site: growing vegetables base, city east, Raohe County, Heilongjiang Province
Test is handled: July 20 applied fertilizer to the subsoil wholely, and check plot and treatment zone all mu are executed 15 kilograms in urea. 10 kilograms of monoammonium phosphates:
Sowing on July 21, field planting on August 6, several 2560 of mu strain.Respectively at seedling stage. the phase in strong sprout. the heading stage, spray multi-functional composite liquid fertilizer, spray altogether 3 times, each consumption 50 grams add 15 kilograms in water; The check plot sprays the equivalent clear water in the identical time.
1, field investigation: treatment zone grows soon than the check plot, and the leaf look dark green, to small white. and cabbage caterpillar, killing rate reach more than 90%, and soft rot does not take place the time of infertility. oidium. diseases such as heartburn disease; Balling is real, output height, and check plot leaf look pale green, and it is relatively slow to grow, and heartburn sick 3.5%. soft rot 4%. strains are short and balling is unreal.
2, output investigation: see Table lattice
The output questionnaire
| Project is handled | Control time | Gross weight/jin | Net weight/jin | A heartburn dish tree | A soft rot tree | Per mu yield/jin | Volume increase per-cent |
| Handle | September 25 | ??5.0 | ??5.2 | ??----- | ??----- | ??12825 | ??31％ |
| Contrast | September 25 | ??3.8 | ??3.6 | ??25 | ??50 | ??9789 |
3, conclusion: multi-functional compound liquid fertilizer, satisfactory for result to the Chinese cabbage prevention and control of plant diseases, pest control, and can promote to grow, increase chlorophyll content, improve quality, improve output, nontoxic to the person poultry safety.
Claims (8)
1. multifunctional compound fertilizer capable of killing pests, preventing diseases and increasing yield, make by following method:
Step 1: prepare following three kinds of components respectively---A component vegetable insecticide, B component bactericide and C component plant growing volume increase agent
1) preparation A component vegetable insecticide
Get following raw material: the root of langdu; Tobacco rods; Black false hellebore; Trifoliate jewelvine; Kuh-seng; The tuber of stemona; Fructus Cnidii; The Fruit of Belveder; Cortex meliae; Pericarpium zanthoxyli;
After above-mentioned raw materials cleaned, dries, cuts into slices, pulverizes, adopt totally-enclosed, thermal backflow, twice circulation to extract again, distillation concentrates extraction process by water: the first step, earlier the medicinal material after the above-mentioned pulverizing is added and extract still, add medicinal material amount 5-6 water (quality multiple) doubly then, keep thermal backflow and extract 80-100 ℃ of temperature, 60 minutes extraction times; From extract still, extract and be delivered to soup out still kettle with the vacuum filtration machine; Second step, continue in extracting still, to add medicinal material amount 5-6 water (quality multiple) doubly, keep thermal backflow and extract 80-100 ℃ of temperature, 60 minutes extraction times; With the soup vacuum filtration to still kettle; Distill concentratedly after the soup that extracted twice is obtained mixes, keep 100 ℃ of temperature; The water of condensation that produces in the still-process reclaims, and as the solvent of later extraction, at last soup is concentrated into mass concentration and is 35% soup, and promptly A component vegetable insecticide is standby;
2) preparation B component bactericide
Get following raw material: the common vetch dish; Honeysuckle; The capsule of weeping forsythia; Pyroligneous liquor; Natural propolis;
The back is cleaned, dries, cuts into slices, pulverized to common vetch dish, honeysuckle and capsule of weeping forsythia process by after being same as the extraction of A component similarity condition, filtration, concentration technology processing, soup with the mass concentration 35% that obtains, be mixed by 44: 5: 1 (mass ratio) with pyroligneous liquor (mass concentration 98%) and natural propolis again, promptly make B component bactericide, standby;
3) preparation C component plant growing volume increase agent
Get following raw material: amino acid; Potassium fulvate solution; Citric acid; Organic nutrient aganic nutrient agent; Urea; Phosphoric acid; Saltpetre; Trace element 1-2; Poly-aspartic potassium; Rare earth element; Sodium nitrophenolate; DA-6; The EDTA disodium salt.
Earlier potassium fulvate solution is injected synthesis reactor, be heated to 50-55 ℃, add amino acid then successively. citric acid .EDTA disodium salt. constantly stirred 10 minutes, keep 50-55 ℃ of constant temperature, after the dissolving, again trace element is added fully, constantly stirring reaction is 10 minutes, keeps 50-55 ℃ of constant temperature; Again saltpetre, potassium primary phosphate, rare earth element, sodium nitrophenolate, DA-6, organic nutrient aganic nutrient agent, poly-aspartic potassium are added synthesis reactor successively, constantly stirred 30 minutes, keep 50-55 ℃ of temperature; At last urea is added synthesis reactor and constantly stirred 10 minutes,, both obtained C component plant growing volume increase agent finished product with the liquid filtering that obtains and with behind the filtrate glue mill, standby.
Step 2: preparation multifunctional compound fertilizer
Get the A component; The B component; The C component; Get penetrating agent JFC again; Polyoxyethylene glycol; Buffer reagent;
Earlier C component finished product is added synthesis reactor, be heated to 50-55 ℃, then A component soup, B component soup are added successively, constantly stirred 30 minutes, keep 50-55 ℃ of constant temperature, again with penetrating agent JFC, polyoxyethylene glycol adds synthesis reactor, constantly stirs 10 minutes; Add buffer reagent at last, after constantly mixing, behind the high pressure homogenizer homogeneous, both obtained the multifunctional compound fertilizer finished product.
2. multifunctional compound fertilizer according to claim 1 is characterized in that, in above-mentioned step 1:
The raw material of preparation A component vegetable insecticide by total mass per-cent is: root of langdu 30-45; Tobacco rods 15-35; Black false hellebore 2-5; Trifoliate jewelvine 2-5; Kuh-seng 8-12; Tuber of stemona 5-10; Fructus Cnidii 3-5; Fruit of Belveder 3-5; Cortex meliae 5-10; Pericarpium zanthoxyli 1-3.
3. multifunctional compound fertilizer according to claim 1 is characterized in that, in above-mentioned step 1:
The raw material of preparation B component bactericide by total mass per-cent is: common vetch dish 40-55; Honeysuckle 15-25; Capsule of weeping forsythia 15-25; Pyroligneous liquor (mass concentration 98%) 10-15; Natural propolis 1-2.
4. multifunctional compound fertilizer according to claim 1 is characterized in that, in above-mentioned step 1:
The raw material of preparation C component plant growing volume increase agent by total mass per-cent is: amino acid (40% quality solid content) 6-8; Potassium fulvate solution (mass concentration 4%) 40-50; Citric acid 2-4; Organic nutrient aganic nutrient agent (yellow humic acid) 5-8; Urea 10-15; Potassium primary phosphate 8-10; Saltpetre 7-9; Trace element H3BO3, (NH4
)6Mo7O24 4H2O, MnSO4H2O, ZnSO4 and MgSO4 1-2; Poly-aspartic potassium (46% solid content) 1-2; Rare earth element 0.2-0.3; Sodium nitrophenolate 0.1-0.5; DA-6 0.1-0.5; EDTA disodium salt 0.5-1.
5. according to claim 1,4 described multifunctional compound fertilizers, it is characterized in that contained each constituent mass is identical in the trace element in the raw material of preparation C component plant growing volume increase agent.
6. according to claim 1,4 described multifunctional compound fertilizers, it is characterized in that the rare earth element in the raw material of preparation C component plant growing volume increase agent is any one or several and any proportioning arbitrarily in its 17 kinds of elements.
7. multifunctional compound fertilizer according to claim 1 is characterized in that, in above-mentioned step 2:
Get A component 10-15; B component 5-10; C component 55-60; Penetrating agent JFC 10-15; Polyoxyethylene glycol 8-10; Buffer reagent 5-10.
8. according to claim 1,7 described multifunctional compound fertilizers, it is characterized in that, in above-mentioned step 2:
Buffer reagent is the mixture of SODIUM PHOSPHATE, MONOBASIC and Sodium phosphate dibasic, and wherein, the mass ratio of SODIUM PHOSPHATE, MONOBASIC and Sodium phosphate dibasic is 1: 2.
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