CN107629900A - A kind of preparation method of cape jasmine whitening anti-acne type craft cold process soap - Google Patents
A kind of preparation method of cape jasmine whitening anti-acne type craft cold process soap Download PDFInfo
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Abstract
The invention discloses a kind of preparation method of cape jasmine whitening anti-acne type craft cold process soap.A certain amount of coconut oil, palm oil, olive oil, rice bran oil, plant white oil, wheat-germ oil, grape-kernel oil, cera flava are weighed in beaker, heating water bath.Weigh a certain amount of NaOH and water simultaneously, sodium hydroxide is poured slowly into water, stirring becomes clear to solution and is completely dissolved, it is identical with grease to treat that it is cooled to, it is slowly added into, and quickly stir, treat that soap lye becomes sticky, cape jasmine oil, cape jasmine shell extract, gardenia pollen, cape jasmine flower essential oil, aloe extract, mulberry-leaf extract, green-tea extract, pearl powder, micro food coloring and other additives can be added, 8 words can be drawn by, which being stirred to, terminates, and pours into mould, is stripped after isothermal solidifying immediately, it is placed at shady and cool ventilation and preserves, treats that it is ripe.
Description
Technical field
The present invention relates to articles for daily use technical field, is related to a kind of preparation side of cape jasmine whitening anti-acne type craft cold process soap
Method.
Background technology
Cape jasmine (Garadenia jasminoides), also known as Yellow Fructus Gardeniae, mountain Cape jasmine, Fructus Gardeniae etc., are rubiaceous one
Kind evergreen shrubs, main product is in Jiangxi, Zhejiang, Hunan and other places.Cape jasmine fruit system traditional Chinese medicine, also fall within Ministry of Public Health's promulgation first
Medicine-food two-purpose resource, effect are clearing heat and promoting diuresis, and purging intense heat dehumidifies, removing pattogenic heat from the blood and toxic material from the body, externally used detumescence analgesic.Modern pharmacological research shows Cape jasmine
Son has the effect such as anti-oxidant, anti-inflammatory and antalgic, antimicrobial, hepatic cholagogic, hypoglycemic.Research shows that cape jasmine ethyl acetate extracts
Thing and 90% ethanol extract can suppress mouse auricular concha swelling caused by dimethylbenzene and formaldehyde-caused toes swelling, acetic acid
The antiinflammatory action of ethyl ester extract is not so good as ethanol extract;Meanwhile both have treatment to make mouse and rabbit soft tissue injury
With, and the therapeutic action of ethyl acetate extract is better than ethanol extract.Cape jasmine is to staphylococcus aureus, hemolytic hammer
Bacterium, micrococcus catarrhalis, corynebacterium diphtheriae, human-like combination bacillus etc. have moderate strength antibacterial action.Cape jasmine fruit decocting liquid energy is in body
Outer kill Leptospira and blood fluke, and there is anti-echovirus;Water logging liquid energy suppresses various skins in vitro
Fungi.The aqueous extract of cape jasmine fruit has inhibitory action to a variety of fungies, thus play the role of to skin it is certain clean, health
, bacterium is acted on without this.Gardenia Yellow is yellow to yellowish-brown, does not influence with special odor but the fragrance of cosmetics,
Dissolution velocity is fast in water, and can be formed as clear as crystal, and bright-coloured pleasing bright yellow also has pharmacological action concurrently, and it is applied
Mainly determined in the feasibility of cosmetics by its physicochemical properties.Gardenia essential oil containing cape jasmine, it is to refine gardenia compound
Primary raw material.The chemical composition of cape jasmine flower essential oil is mainly linalool (21.09%), amphene (7.25%), α-carypohyllene
(6.49%), geraniol (5.72%), α-farnesene (5.35%) etc..Wherein linalool has typical Rose Essentielle
Fragrance, geraniol have hesperidium fragrance, α-farnesene, with the fragrance of a flower with stronger oxidation resistance.
Cold process soap refers to handmade soap in the narrow sense, refers to and is obtained at 45 DEG C using grease with saponification that alkali lye is carried out
Handmade soap.Formula is：Oil+alkali（It is dissolved in the sodium hydroxide or potassium hydroxide of water）=soap+natural glycerin.Due to soapmaking process
In avoid high temperature, therefore contain natural complex and nutritional ingredient in remaining vegetable oil and other additives to greatest extent,
Therefore it is the best skin care products of skin.Skin is also required to absorb nutrition by contacting, and is maintained in shower, is most fast, most
Effective method, when whole body pore all diastoles, skin is set easily to absorb, loosen with plant soap, it is not tight.All cold process soaps
About 20% natural glycerin will be produced naturally during saponification, be the optimal natural moisture preserving agent of skin, formed on skin
One layer of natural diaphragm.Have a large amount of nutriments for being not involved in saponification in vegetable oil, these it is precious into branch when in use
In being penetrated to the skin through pore, so as to reach cleaning, maintenance while the effect carried out.Manual perfumed soap can be directed to oneself
Skin quality makes, therefore oneself understands and what material is with the addition of in perfumed soap, strange into branch's injury skin without worrying, can feel at ease to make
With；Manual perfumed soap is not only gently non-stimulated to skin, and also helps environmental protection；Manual perfumed soap is " natural face cleaning activating agent ",
Grease can be effectively cleaned, and will not at all destroy the cuticula of skin；Add olive oil in handmade soap, and with other oil with
Different proportion mixes, and the handmade soap for making to make washes sense and function with unique.
Olive oil is added in the present invention, and it, can rich in polyphenoils such as monounsaturated fatty acids and vitamins
Anti-wrinkle and anti-aging, it is commonly used in fatty acid monoglyceride/olive oil organogel for containing in the cosmetic formulations of skin care
Ratio is being continuously increased；Squalene and skin affinity in olive oil is strong, can effectively be absorbed by skin, keeps skin gloss
It is flexible；The polyphenol compound contained in olive oil has higher bioactivity, energy antibacterial, anti-oxidant, uvioresistant etc.；Can
Make skin soft flexible containing moisturizing, protection and the function of curing skin.Wheat-germ oil, containing protein, mineral matter, dimension
His life, pantothenic acid, niacin and unrighted acid, eczema, chronic eczema, aged skin can be improved, promote skin regeneration, to blackspot,
Striae of pregnancy and scar have nourishes effect；Grape-kernel oil, containing vitamin, mineral matter, chlorophyll, fructose, glucose, vine polyphenol with
Protein, it is adapted to dark sore, acne oily skin, prevention melanin deposition etc..
In addition, also add the natural plant extracts with whitening and anti-acne effect, such as reed in the handmade soap of the present invention
Luxuriant growth extract, mulberry-leaf extract, green-tea extract and pearl powder.The anthraquinone analog compound of aloe has and makes skin contraction, soft
Softening, moisturizing, anti-inflammatory, bleaching performance, also release hardening, angling, improvement scar effect, can not only prevent small wrinkle,
Pouch, cutis laxa, moreover it is possible to skin wet, tender and lovely is kept, at the same time it can also treat scytitis, to acne, freckle, acne
And scald, knife wound, insect bite etc. also have the effect of fine.Mulberry leaf also have good beautifying skin effect, particularly to face
Acne, moth patch have the effect of relatively good.Green-tea extract also can be as cosmetics and the excellent additive of household chemicals, its
There are very strong antibacterial action and Inhibitory activity, skin disease, allergic effect can be prevented and treated, go skin pigment pearl powder that there is whitening
Anti-wrinkle nti-freckle, for facial lines, color spot, pearl contains the growth that a variety of protein hydrolysate promote cell, adsorbable in dry
The preferable film of water-retaining property is formed on skin, there is good nutrition and protection skin, local blood can be promoted again
Circulation, effective pre- anti-wrinkle and color spot.Therefore, this money handmade soap not only has disappearing for cape jasmine series of elements and plant extracts
The effect such as scorching, antibacterial also has superior white-skinned face function, is prepared by hand plus pure, makes the performance of this money handmade soap more prominent.
The content of the invention
It is an object of the invention to provide a kind of preparation method of cape jasmine whitening anti-acne type craft cold process soap, and cape jasmine oil is applied
Into handmade soap, and essential oil is added, realize that the pure of cold process soap prepares by hand.
It is a further object to provide the preparation method of above-mentioned cape jasmine whitening anti-acne type craft cold process soap.
The present invention is implemented according to following scheme：
The base oil of handmade soap of the present invention has：
The base oil of the handmade soap of table 1
| Grease | Sodium hydroxide saponification valency | INS values |
| Coconut oil | 0.19 | 258 |
| Palm oil | 0.141 | 145 |
| Olive oil | 0.134 | 109 |
| Rice bran oil | 0.128 | 70 |
| Castor oil | 0.1286 | 95 |
| Plant white oil | 0.136 | 115 |
| Wheat-germ oil | 0.131 | 58 |
| Grape-kernel oil | 0.1265 | 66 |
| Cera flava | 0.069 | 84 |
The INS values 125 ~ 150 of the grease of the present invention are appropriate.
Step 1, the g of coconut oil 20 ~ 100, the g of palm oil 15 ~ 75, the g of olive oil 35 ~ 100, rice bran oil are weighed on balance
10 ~ 50 g, castor oil 10 ~ 50, the g of plant white oil 5 ~ 25, the g of grape-kernel oil 15 ~ 75, the g of cera flava 3 ~ 25 are placed in 1000 mL's
In beaker；Weigh the g of NaOH 17 ~ 70 respectively to be placed in 250 mL beaker, the g of water 34 ~ 140 is placed in 1000 mL beaker.
Step 2, the sodium hydroxide weighed up is slowly poured into water, while slowly stirs and become clear to solution and be
Only, that is, it is completely dissolved, stands, treat that its temperature is down to 45 ~ 50 DEG C.
Step 3, grease is placed in water-bath and heated, and with its temperature of thermometer measure, when temperature rises to 40 ~ 50 DEG C
Beaker is taken out from water-bath.
Step 4, the sodium hydroxide solution after cooling slowly poured into grease, side edged quickly stirs, at 40 ~ 50 DEG C
Under water bath condition, continue the h of stirring 0.5 ~ 1.0.
Step 5, stirring start to become sticky to solution, then add 5 ~ 25 mL cape jasmine oil, 5 ~ 25 mL cape jasmine
Shell extract, 5 ~ 25 g gardenia pollen, 5 ~ 25 mL cape jasmine flower essential oil, 5 ~ 25 g aloe extract, 5 ~ 25 g
Mulberry-leaf extract, 5 ~ 25 g green-tea extract, can be write after stirring on soap lye and 20 ~ 30 s do not disappear
I.e. stirring terminates, and pours into immediately in mould, rests in 30 ~ 35 DEG C of incubators, be stripped after 2 ~ 5 days.
Step 6, preservation at shady and cool ventilation is placed on, 25 ~ 35 DEG C of temperature, humidity is below 60, after 30 ~ 45 days, surveys its pH value 7
It is ripe when ~ 8.
The preparation method of the cape jasmine whitening anti-acne type craft cold process soap of the present invention also resides in：
The wet concentration used of the cape jasmine whitening anti-acne type craft cold process soap of the present invention selects distilled water or pure water.
The cape jasmine added before soap lye enters mould the oil of the cape jasmine whitening anti-acne type craft cold process soap of the present invention, by fresh cape jasmine fruit
Extract and obtain through ultrasonic assistant, condition is solid-liquid ratio 5:1~15:1, the min of extraction time 30 ~ 60,30 ~ 50 DEG C of Extracting temperature,
Extraction time 2 ~ 5 times, Extraction solvent are the one or several kinds such as petroleum ether, ethyl acetate, ethanol.
The cape jasmine shell extract added before soap lye enters mould of the cape jasmine whitening anti-acne type craft cold process soap of the present invention, by doing
Cape jasmine shell after dry is extracted and obtained through soxhlet extraction, and condition is solid-liquid ratio 5:1~15:1, the min of extraction time 45 ~ 60, extraction
60 ~ 80 DEG C of temperature, extraction time 2 ~ 4 times, Extraction solvent are the one or several kinds such as petroleum ether, ethyl acetate, ethanol.
The gardenia pollen added before soap lye enters mould of the cape jasmine whitening anti-acne type craft cold process soap of the present invention, it is to have newly
It is pollen that particle diameter is 200 ~ 300 mesh that fresh gardenia is crushed after drying in the shade naturally with pulverizer, sieving for standby.
The cape jasmine flower essential oil added before soap lye enters mould of the cape jasmine whitening anti-acne type craft cold process soap of the present invention, it is to utilize
Fresh gardenia is prepared by the method for supercritical carbon dioxide, and method is 40 ~ 50 W ultra violet lamps, gardenia percentage of water loss
When 70 ~ 90%, it is put into constant temperature oven, nitrogen protection is lower 30 ~ 40 DEG C, dries 2 ~ 3 h, then rapid cooling, and temperature is -10 ~ -20
40 ~ 50 s are freeze-dried at DEG C, places into and dries 8 ~ 9h in constant temperature oven at 70 ~ 80 DEG C of temperature, then will be dried
In the static water with 4 ~ 5 times of quality of gardenia, after supersound washing, the gardenia after remaining drying process is carried out Soxhlet extraction 6 ~
8 h, it is concentrated under reduced pressure and produces pure gardenia essential oil.
Also lemon, clove oil, jasmine essence can be separately added in the cape jasmine whitening anti-acne type craft cold process soap of the present invention
Oil, Rosa Damascana, Lavender are one or several kinds of.
The cape jasmine whitening anti-acne type craft cold process soap of the present invention carries out adding micro food coloring, dimension before soap lye enters mould
Raw plain E, pearl powder are one or several kinds of.
Total free alkali of the cape jasmine whitening anti-acne type craft cold process soap of the present invention is 0.07 ~ 0.10%（In terms of NaOH）.
The free causticity alkali content of the cape jasmine whitening anti-acne type craft cold process soap of the present invention is 0.06 ~ 0.10%（With NaOH
Meter）.
The moisture and volatile matter of the cape jasmine whitening anti-acne type craft cold process soap of the present invention are 20 ~ 24%（Temperature is 60 DEG C ± 2 DEG C）.
The content of the chloride of the cape jasmine whitening anti-acne type craft cold process soap of the present invention is 0.1 ~ 0.9%（In terms of NaCl）.
The phosphatic content of the cape jasmine whitening anti-acne type craft cold process soap of the present invention is 0.001 ~ 0.01%（With P2O5
Meter）.
Experimental implementation of the present invention is easy, and Lipid use rate is high, and can be changed according to the hobby of oneself and the requirement to function
The species of the ratio of grease, essential oil and pigment.
Embodiment
Following examples are some citings of the present invention, should not be seen as limitation of the invention.
Embodiment 1
Weigh the g of coconut oil 25, the g of palm oil 15, the g of olive oil 35 on balance, the g of rice bran oil 10, the g of castor oil 10, plant is white
10 g of oil, the g of wheat-germ oil 6, the g of grape-kernel oil 10, the g of cera flava 3, are placed in 500 mL beaker；NaOH is weighed respectively
17.75 g are placed in 250 mL beaker, and the g of water 35.5 is placed in 1000 mL beaker.
The sodium hydroxide weighed up is slowly poured into water, while slowly stirred untill solution becomes clear, i.e., it is complete
Fully dissolved, stand, treat that its temperature is down to 45 DEG C, grease is placed in water-bath and heated, and with its temperature of thermometer measure, work as temperature
Degree takes out beaker when rising to 45 DEG C from water-bath.
Sodium hydroxide solution is slowly poured into grease, side edged quickly stirs, at 45 DEG C water-bath and continue stir 1 h
Until soap lye starts to become thick, 10 mL cape jasmine oil, 10 mL cape jasmine shell extract, 10 g gardenia are then added
Powder, 10 mL cape jasmine flower essential oil, 5 g aloe extract, 5 g mulberry-leaf extract, 5 g green-tea extract, stir
After can be write on soap lye and 20 ~ 30 s do not disappear i.e. stirring terminate, pour into immediately in mould, rest on 30 DEG C of incubators
It is interior, it is stripped after 2 days.
The cape jasmine added before soap lye enters mould the oil of cape jasmine whitening anti-acne type craft cold process soap, by fresh cape jasmine fruit through ultrasonic wave
Assisted extraction and obtain, condition is solid-liquid ratio 5:1, extraction time 30min, 30 DEG C of Extracting temperature, extraction time 2 times, Extraction solvent
For petroleum ether.
The cape jasmine shell extract added before soap lye enters mould of cape jasmine whitening anti-acne type craft cold process soap, by dried Cape jasmine
Sub- shell is extracted and obtained through soxhlet extraction, and condition is solid-liquid ratio 5:1, the min of extraction time 45,80 DEG C of Extracting temperature, extraction time
2 times, Extraction solvent is petroleum ether.
The gardenia pollen added before soap lye enters mould of cape jasmine whitening anti-acne type craft cold process soap, is to have fresh cape jasmine
It is pollen that particle diameter is 300 mesh to spend nature to be crushed after drying in the shade with pulverizer.
The cape jasmine flower essential oil added before soap lye enters mould of cape jasmine whitening anti-acne type craft cold process soap, it is using fresh
Gardenia is prepared by the method for supercritical carbon dioxide, and method is 50 W ultra violet lamps, during gardenia percentage of water loss 90%, is put
Enter in constant temperature oven, lower 40 DEG C of nitrogen protection, dry 3 h, then rapid cooling, temperature is to be freeze-dried 50s at -10 DEG C, then is put
Enter and dry 9h in constant temperature oven at 80 DEG C of temperature, then by dried gardenia it is static with the water of 5 times of quality, ultrasound
After washing, the h of Soxhlet extraction 8 is carried out to the gardenia after remaining drying process, is concentrated under reduced pressure and produces pure cape jasmine flower essential oil
Liquid.
Cape jasmine whitening anti-acne type craft cold process soap can also be separately added into 2 mL lemons, cloves essence before soap lye enters mould
Oil, refined jasmine oil, Rosa Damascana.
Cape jasmine whitening anti-acne type craft cold process soap can add micro food coloring, appropriate vitamin before soap lye enters mould
E, pearl powder.
INS values calculate
INS values are used for representing the hardness of soap.The ratio of soap base shared by the INS value * greases of grease=after the completion of soap hardness.INS
Value is lower, and the perfumed soap after the completion of representative is softer；On the contrary, INS values are higher, the perfumed soap after the completion of expression is harder.INS values between 120 ~
160 be all to belong to appropriate hardness.
The measure of total free alkali
Dissolve soap in ethanol solution, with known excessive concentration be 0.5 mol/L sulfuric acid solution in and free alkali, then
With the excessive acid of the potassium hydroxide-ethanol solution residual titration that concentration is 0.5 mol/L.Specific method refers to QB/T 2623.2-2003.
The measure of free causticity alkali content
Soap is dissolved in neutral alcohol, then titrates trip with the acidic alcohol standard titration solution that concentration is 0.5 mol/L
From caustic alkali.Specific method refers to QB/T 2623.1-2003.
The measure of moisture and volatile matter
At an established temperature, by a certain amount of sample drying to constant weight, weigh and reduce.Specific method refers to QB-T 2623.4-
2003。
The measure of chloride content
Decomposition experiment part and after being separated by filtration aliphatic acid, silver consuming amount method determines the content of chloride.Specific method refers to QB/T
2623.6-2003。
The measure of phosphate content
After sample is acidified, with petroleum ether extraction aliphatic acid not soluble in water, certain raffinate solution is taken to add ammonium molybdate-sulfuric acid molten
Liquid and ascorbic acid solution, 45min is heated in boiling water bath, Quadrafos is hydrolyzed into phosphate and generates P-Mo blue, with light splitting
Photometer determines absorbance A under wavelength 650nm, by the phosphorus pentoxide that corresponding absorbance is obtained on standard curve（P2O5）
Amount, calculate the content of relative sample.Specific method refers to QB-T 2623.8-2003.
There is soap powder generation on the soap surface that this scheme is worked it out, partially firmly；Possible cause saponification is incomplete, and the few water of alkali is more.
The soap INS values that this scheme is worked it out are 133.06, and total free alkali is 0.07%, and the caustic alkali that dissociates is 0.07%, moisture
It is 20% with volatile matter, chloride content 0.65%, phosphate content 0.008%.
Embodiment 2
Weigh the g of coconut oil 20, the g of palm oil 15, the g of olive oil 20 on balance, the g of rice bran oil 10, the g of castor oil 10, plant is white
5 g of oil, the g of wheat-germ oil 6, the g of grape-kernel oil 10, the g of cera flava 4, are placed in 500 mL beaker；Weigh NaOH 14.18
G, the g of water 28.36 are placed in 250 mL beaker.Operating process such as embodiment 1.
The soap body that this scheme is worked it out is softer, and there is soap powder on soap surface, and water outlet is fuel-displaced, occurs oil mark, easily quilt in maturation
Air oxidation.
The soap INS values that this scheme is worked it out are 125.55, and total free alkali is 0.08%, and the caustic alkali that dissociates is 0.06%, moisture
It is 22% with volatile matter, chloride content 0.66%, phosphate content 0.007%.
Embodiment 3
Weigh the g of coconut oil 25, the g of palm oil 15, the g of olive oil 10 on balance, the g of rice bran oil 10, the g of castor oil 10, plant is white
5 g of oil, the g of wheat-germ oil 10, the g of grape-kernel oil 10, the g of cera flava 5, are placed in 500 mL beaker；Weigh NaOH 14.38
G, the g of water 28.76 are placed in 250 mL beaker.Operating process such as embodiment 1.
There is soap powder on the soap surface that this scheme is worked it out, easily fuel-displaced, and possible cause stirring is insufficient, and soap body is harder.
The soap INS values that this scheme is worked it out are 136, and total free alkali is 0.08%, and the caustic alkali that dissociates is 0.07%, moisture and is waved
Stimulating food is 24%, chloride content 0.75%, phosphate content 0.006%.
Embodiment 4
Weigh the g of coconut oil 25, the g of palm oil 10, the g of olive oil 15 on balance, the g of rice bran oil 5, the g of castor oil 10, plant is white
5 g of oil, the g of wheat-germ oil 10, the g of grape-kernel oil 15, the g of wasp 5, are placed in 500 mL beaker；Weigh NaOH 14.34
G, the g of water 28.68 are placed in 250 mL beaker.Operating process such as embodiment 1.
The soap hardness that this scheme is worked it out is moderate, the smooth no soap powder in surface.
The soap INS values that this scheme is worked it out are 134, and total free alkali is 0.08%, and the caustic alkali that dissociates is 0.06%, moisture and is waved
Stimulating food is 23%, chloride content 0.81%, phosphate content 0.003%.
The suitable INS values of handmade soap are 125 ~ 160 in national sector standard, total free alkali, free caustic alkali, moisture and are waved
Stimulating food, chloride content, phosphate content national sector standard be respectively≤0.1 ,≤0.1,20 ~ 25 ,≤1.0 ,≤1.1,
Therefore these four schemes are all satisfactory in theory.
Claims (14)
1. a kind of preparation method of cape jasmine whitening anti-acne type craft cold process soap, its step are as follows：
The first step, weighs the g of coconut oil 20 ~ 100, the g of palm oil 15 ~ 75, the g of olive oil 35 ~ 100 on balance, and rice bran oil 10 ~
50 g, castor oil 10 ~ 50, the g of plant white oil 5 ~ 25, the g of grape-kernel oil 15 ~ 75, the g of cera flava 3 ~ 25 are placed in 1000 mL beaker
In；Weigh the g of NaOH 17 ~ 70 respectively to be placed in 250 mL beaker, the g of water 34 ~ 140 is placed in 1000 mL beaker；
Second step, the sodium hydroxide weighed up is slowly poured into water, while slowly stirred untill solution becomes clear, i.e.,
It is completely dissolved, stands, treat that its temperature is down to 45 ~ 50 DEG C；
3rd step, grease is placed in water-bath and heated, and with its temperature of thermometer measure；Will when temperature rises to 40 ~ 50 DEG C
Beaker is taken out from water-bath；
4th step, the sodium hydroxide solution after cooling is slowly poured into base oil, side edged quickly stirs, at 40 ~ 50 DEG C
Under water bath condition, continue the h of stirring 0.5 ~ 1.0；
5th step, stir to solution and start to become sticky, then add 5 ~ 25 mL cape jasmine oil, 5 ~ 25 mL cape jasmine shell carries
Take thing, 5 ~ 25 g gardenia pollen, 5 ~ 25 mL cape jasmine flower essential oil, 5 ~ 25 g aloe extract, 5 ~ 25 g mulberry
The green-tea extract of leaf extract, 5 ~ 25 g, can write after stirring on soap lye and 20 ~ 30 s do not disappear and stirred
End is mixed, is poured into immediately in mould, rests in 30 ~ 35 DEG C of incubators, is stripped after 2 ~ 5 days；
6th step, it is placed at shady and cool ventilation and preserves, 25 ~ 35 DEG C of temperature, humidity is below 60, after 30 ~ 45 days, surveys its pH value 7 ~ 8
When it is ripe.
2. the preparation method of cape jasmine whitening anti-acne type craft cold process soap according to claim 1, it is characterised in that the first step
Distilled water or pure water are selected with wet concentration used in second step.
3. the preparation method of cape jasmine whitening anti-acne type craft cold process soap according to claim 1, it is characterised in that the first step
The appropriate INS values of middle grease are 125 ~ 150.
4. the preparation method of cape jasmine whitening anti-acne type craft cold process soap according to claim 1, it is characterised in that the 5th step
The cape jasmine oil added before soap lye enters mould, is extracted by fresh cape jasmine fruit and is obtained through ultrasonic assistant, condition is solid-liquid ratio 5:1~15:1,
The min of extraction time 30 ~ 60,30 ~ 50 DEG C of Extracting temperature, extraction time 2 ~ 5 times, Extraction solvent are petroleum ether, ethyl acetate, second
The one or several kinds such as alcohol.
5. the preparation method of cape jasmine whitening anti-acne type craft cold process soap according to claim 1, it is characterised in that the 5th step
The cape jasmine shell extract added before soap lye enters mould, extracted by dried cape jasmine shell and obtained through soxhlet extraction, condition is material
Liquor ratio 5:1~15:1, the min of extraction time 45 ~ 60,60 ~ 80 DEG C of Extracting temperature, extraction time 2 ~ 4 times, Extraction solvent is oil
The one or several kinds such as ether, ethyl acetate, ethanol.
6. the gardenia added before soap lye enters mould of cape jasmine whitening anti-acne type craft cold process soap according to claim 1
Powder, it is that to have fresh gardenia to be crushed after drying in the shade naturally with pulverizer be pollen that particle diameter is 200 ~ 300 mesh, sieving for standby.
7. the preparation method of cape jasmine whitening anti-acne type craft cold process soap according to claim 1, it is characterised in that the 5th step
The cape jasmine flower essential oil added before soap lye enters mould, it is to be prepared using fresh gardenia by the method for supercritical carbon dioxide,
Method is 40 ~ 50 W ultra violet lamps, during gardenia percentage of water loss 70 ~ 90%, is put into constant temperature oven, and nitrogen protection is lower 30 ~ 40 DEG C,
2 ~ 3 h are dried, then rapid cooling, temperature is that 40 ~ 50s is freeze-dried at -10 ~ -20 DEG C, is placed into constant temperature oven in temperature 70
8 ~ 9h is dried at ~ 80 DEG C, then by the static water with 4 ~ 5 times of quality of dried gardenia, after supersound washing, to surplus
Gardenia after remaining drying process carries out the h of Soxhlet extraction 6 ~ 8, is concentrated under reduced pressure and produces pure gardenia essential oil.
8. the preparation method of cape jasmine whitening anti-acne type craft cold process soap according to claim 1, it is characterised in that the 5th step
It is a kind of or several that lemon, clove oil, refined jasmine oil, Rosa Damascana, Lavender can be also added before soap lye enters mould
Kind.
9. the preparation method of cape jasmine whitening anti-acne type craft cold process soap according to claim 1, it is characterised in that the 5th step
Carry out adding micro food coloring, vitamin E, pearl powder one or several kinds before soap lye enters mould.
10. the preparation method of cape jasmine whitening anti-acne type craft cold process soap according to claim 1, it is characterised in that the present invention
Cape jasmine whitening anti-acne type craft cold process soap total free alkali be 0.05 ~ 0.10%（In terms of NaOH）.
11. the preparation method of cape jasmine whitening anti-acne type craft cold process soap according to claim 1, it is characterised in that the present invention
Cape jasmine whitening anti-acne type craft cold process soap free causticity alkali content be 0.05 ~ 0.10%（In terms of NaOH）.
12. the preparation method of cape jasmine whitening anti-acne type craft cold process soap according to claim 1, it is characterised in that the present invention
Cape jasmine whitening anti-acne type craft cold process soap moisture and volatile matter be 21 ~ 24%（Temperature is 60 DEG C ± 2 DEG C）.
13. the content of the chloride of the cape jasmine whitening anti-acne type craft cold process soap of the present invention is 0.1 ~ 0.9%（In terms of NaCl）.
14. the phosphatic content of the cape jasmine whitening anti-acne type craft cold process soap of the present invention is 0.001 ~ 0.01%（With P2O5Meter）.
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| CN201710887141.3A CN107629900A (en) | 2017-09-27 | 2017-09-27 | A kind of preparation method of cape jasmine whitening anti-acne type craft cold process soap |
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| JP7454355B2 (en) | 2018-12-27 | 2024-03-22 | ロート製薬株式会社 | DKK1 production promoter and method for producing the same, cosmetic composition for promoting DKK1 production and method for producing the same, and method for promoting DKK1 production |
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Application publication date: 20180126 |