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CN107739670A - A kind of Eucommia Oil perfumed soap and preparation method thereof - Google Patents

A kind of Eucommia Oil perfumed soap and preparation method thereof Download PDF

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Publication number
CN107739670A
CN107739670A CN201711118921.8A CN201711118921A CN107739670A CN 107739670 A CN107739670 A CN 107739670A CN 201711118921 A CN201711118921 A CN 201711118921A CN 107739670 A CN107739670 A CN 107739670A
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CN
China
Prior art keywords
eucommia
oil
perfumed soap
soap
weight
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711118921.8A
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Chinese (zh)
Inventor
杜庆鑫
王璐
冯延芝
刘攀峰
杜红岩
杜兰英
朱景乐
孙志强
李铁柱
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PAULOWNIA RESEARCH AND DEVELOPMENT CENTRE STATE FOREST BUREAU
Original Assignee
PAULOWNIA RESEARCH AND DEVELOPMENT CENTRE STATE FOREST BUREAU
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Priority to CN201711118921.8A priority Critical patent/CN107739670A/en
Publication of CN107739670A publication Critical patent/CN107739670A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/02Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/005Synthetic soaps
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/44Perfumes; Colouring materials; Brightening agents ; Bleaching agents
    • C11D9/442Perfumes

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention discloses a kind of Eucommia Oil perfumed soap and preparation method thereof, the Eucommia Oil perfumed soap includes by weight:The Eucommia Oil of 30 50 parts by weight, the olive oil of 5 20 parts by weight, the eucommia leaf extract of 5 20 parts by weight, the aloe extract of 2 15 parts by weight, the Lavender of 1 10 parts by weight, the deionized water of the sodium hydroxide of 5 15 parts by weight and 20 30 parts by weight.The Eucommia Oil perfumed soap of the present invention is using the pure plants such as Eucommia Oil, olive oil oil, saponification is made by low temperature, completely remain the active ingredient of each grease, add Lavender and eucommia leaf extract, aloe extract rich in various active composition simultaneously, without any chemical addition agent, do not stimulate gently, easily absorb, can be with deep clean skin;Each active ingredient is mutually coordinated, and excitant is low, and anti-microbial property is good, and the foaming power and foam stability of perfumed soap are good, has moist skin, oil-control moisturizing, desalinates color spot, prevents the multi-efficiencies such as skin senescence.

Description

A kind of Eucommia Oil perfumed soap and preparation method thereof
Technical field
The invention belongs to commodity technical field, more particularly to a kind of Eucommia Oil perfumed soap and preparation method thereof.
Background technology
Perfumed soap is washing and nursing article essential in people's daily life, is generally lived with sodium soap and other surfaces Property agent be primary raw material, adding quality improver and appearance modifying agents is made, and not only face cleaning and mask effect are undesirable, Er Qiepi The fragile people of skin can have very big stimulation after to face, the problems such as causing skin allergy, drying, pore obstruction, cause flesh Skin damages.As the improvement of people's living standards, the variation of consumer demand, there is higher want to washing and nursing article Ask, be more likely to select natural, green, functional washing product.Therefore, there is an urgent need to a kind of modulation of natural materials Into novel toilet soap, both without chemical addition agent, have no toxic side effect, and can Glycerin, there is good face cleaning and mask effect.
The bark of eucommia also known as think of are celestial, belong to the peculiar section's Eucommiaceae in China, are distributed mainly on Shaanxi, Henan, Guizhou, Zhejiang, Gansu etc. Save, the bark of eucommia has filling liver kidney, strengthening the bones and muscles, hypotensive and other effects.To eucommia composition studies have shown that, bark of eucommia free amino acid Seldom, a small amount of protein contained, be with adequate proteins as most foodstuffs, can hydrolyze detection to needed by human 8 kinds of amino acid.Mineral element contained by the bark of eucommia includes the trace elements such as zinc, copper, iron, and the macroelement such as calcium, phosphorus, potassium, magnesium;This Outside, the bark of eucommia also composition containing various active, there is the effect such as hypotensive, diuresis, antibacterial, anti-inflammatory, calmness, hemostasis, analgesia.
A kind of former extraction healthy soap of bark of eucommia and its preparation side are disclosed in the patent application of Application No. 201610401536.3 Method, including bark of eucommia stoste working substance and soap stock working substance, bark of eucommia stoste working substance include the bark of eucommia, the fleece-flower root, peppermint and gleditsia sinensis, soap Expect that working substance includes aliphatic alcohol polyethenoxy sodium sulphate, sodium laurate, Sodium myristate, sodium cocoyl methyl sodium taurocholate, hard Resin acid sodium and fatty acid potassium soap.The former extraction healthy soap of the bark of eucommia can accelerate the metabolism of collagen, recover skin bullet Property, prevent that skin from wrinkling, increase skin gloss, there is preferable beautification function.
The content of the invention
In view of the shortcomings of the prior art, it is described it is an object of the invention to provide a kind of Eucommia Oil perfumed soap and preparation method thereof Preparation method is simple, used containing a variety of natural materials, and is free of chemical addition agent, has no side effect, does not stimulate gently, prepare and Into Eucommia Oil perfumed soap can depth face cleaning, oil-control moisturizing, anti-inflammation, desalination color spot, it is anti-ageing wait for a long time, there is multi-efficiency.
Therefore, technical solution of the present invention is as follows:
In a first aspect, the present invention provides a kind of Eucommia Oil perfumed soap, the Eucommia Oil perfumed soap includes following components by weight:
Eucommia Oil:30-50
Olive oil:5-20
Eucommia leaf extract:5-20
Aloe extract:2-15
Lavender:1-10
Sodium hydroxide:5-15
Deionized water:20-30;
Wherein, the parts by weight of Eucommia Oil can be 30,31,32,33,34,35,36,37,38,39,40,41,42,43, 44th, 45,46,47,48,49 or 50;The parts by weight of olive oil can be 5,6,7,8,9,10,11,12,13,14,15,16,17, 18th, 19 or 20;The parts by weight of eucommia leaf extract can be 5,6,7,8,9,10,11,12,13,14,15,16,17,18,19 or 20;The parts by weight of aloe extract can be 2,3,4,5,6,7,8,9,10,11,12,13,14 or 15;The weight of Lavender It can be 1,2,3,4,5,6,7,8,9 or 10 to measure part;The parts by weight of sodium hydroxide can be 5,6,7,8,9,10,11,12,13, 14 or 15;The parts by weight of deionized water can be 20,21,22,23,24,25,26,27,28,29 or 30.
Eucommia Oil is derived from bark of eucommia seed, and rich in aliphatic acid, (unsaturated fatty acid content is up to 91%, wherein linolenic acid content About 67%, oleic acid about 15%), the active ingredient such as amino acid, aucubin, have very high nutritive value and health care valency Value.Alpha-linolenic acid content in Eucommia Oil is high, has anticancer, anti-oxidant, suppression aging, drop " three high " and other effects, is health care The important source material of the industry such as product, medicine, cosmetics.Olive oil is formed by fresh olive fruit cold press, rich in oleic acid, dimension Raw element and polyphenoils, have good alimentary health-care function, can moisten beauty skin.Eucommia leaf extract is by molten The extracts active ingredients dried in folium cortex eucommiae, filtering are made agent extraction method, have anti-inflammation, anti-oxidant, raising immunity Deng effect.Aloe extract is made by fresh Aloe Barbadensis Miller enzymolysis, centrifugation, rich in anthraquinone analog compound, protein And vitamin etc., having makes skin convergence, replenishing water and preserving moisture, desalination color spot and other effects.The Lavender of the present invention is to pass through water Steam distillation method refines extraction gained, can be with cleaning skin, oil-control, freckle removing and whitening, tender skin.
Preferably, the Eucommia Oil perfumed soap includes following components by weight:
Eucommia Oil:32-42
Olive oil:5-15
Eucommia leaf extract:8-18
Aloe extract:2-12
Lavender:1-5
Sodium hydroxide:8-10
Deionized water:20-25.
Preferably, the Eucommia Oil perfumed soap includes following components by weight:
Eucommia Oil:34-42
Olive oil:7-15
Eucommia leaf extract:8-16
Aloe extract:4-12
Lavender:1-5
Sodium hydroxide:8-10
Deionized water:20-25.
Second aspect, the present invention provide a kind of preparation method of Eucommia Oil perfumed soap as described in relation to the first aspect, including following Step:
1) after mixing Eucommia Oil and olive oil, heat and be stirred continuously in a water bath, obtain solution A;
2) another extracting container adds deionized water, is slowly added to sodium hydroxide and is stirred continuously, is completely dissolved to sodium hydroxide Afterwards, cooling obtains solution B;
3) solution B is slowly added to carry out saponification in solution A, soap base solution is made;
4) eucommia leaf extract, aloe extract and Lavender are added in soap base solution, and is stirred continuously, is obtained Soap lye;
5) soap lye is poured into mould, after standing 1-7d in incubator after sealing, dries the demoulding, be packaged into product.
Preferably, 35-65 DEG C is heated in step 1), for example, can be 35 DEG C, 36 DEG C, 37 DEG C, 38 DEG C, 39 DEG C, 40 ℃、41℃、42℃、43℃、44℃、45℃、46℃、47℃、48℃、49℃、50℃、 51℃、52℃、53℃、54℃、55 DEG C, 56 DEG C, 57 DEG C, 58 DEG C, 59 DEG C, 60 DEG C, 61 DEG C, 62 DEG C, 63 DEG C, 64 DEG C or 65 DEG C.
Preferably, 35-55 DEG C is cooled in step 2), for example, can be 35 DEG C, 36 DEG C, 37 DEG C, 38 DEG C, 39 DEG C, 40 DEG C, 41 DEG C, 42 DEG C, 43 DEG C, 44 DEG C, 45 DEG C, 46 DEG C, 47 DEG C, 48 DEG C, 49 DEG C, 50 DEG C, 51 DEG C, 52 DEG C, 53 DEG C, 54 DEG C or 55 ℃。
Preferably, the time of saponification is 30-50min in step 3), for example, can be 30min, 31min, 32min, 33min、34min、35min、36min、37min、38min、39min、40min、41 min、42min、43min、44min、 45min, 46min, 47min, 48min, 49min or 50min.
Preferably, the pH of soap base solution is 7.2-8.2 in step 3), for example, can be 7.2,7.3,7.4,7.5,7.6, 7.7th, 7.8,7.9,8.0,8.1 or 8.2.
Preferably, step 5) further comprises the steps:
51) palm oil is smeared in mould inner wall, soap lye is poured into mould, then mould sealed with plastic sheeting, Stood in 36-46 DEG C of incubator 1-7d (temperature of incubator can be 36 DEG C, 37 DEG C, 38 DEG C, 39 DEG C, 40 DEG C, 41 DEG C, 42 DEG C, 43 DEG C, 44 DEG C, 45 DEG C or 46 DEG C);
52) mould is subjected to the natural drying demoulding, then normal temperature stands 5-7 weeks, is packaged into product as ventilation.
As optimal technical scheme, the preparation method comprises the following steps:
1) Eucommia Oil, olive oil are mixed by above-mentioned weight proportion and be put into heatproof container, heating water bath, while use glass Rod is stirred continuously, and is maintained the temperature at 35 DEG C -65 DEG C, is obtained solution A;
2) deionized water is added in alkali-proof glass container, then according to the amount of required sodium hydroxide, be slowly added into, side Edged stirs, until sodium hydroxide is completely dissolved, is cooled to 35 DEG C -55 DEG C, obtains solution B;
3) solution B is slowly added into the container equipped with solution A and carries out saponification, stirring while adding, 30-50min Mixed liquor is presented thick afterwards, and saponification is completed, and soap base solution is made, and adjust pH to 7.2-8.2;
4) toward add eucommia leaf extract according to required ratio while stirring in soap base solution made from step 3), aloe carries Thing and Lavender are taken, is stirred, obtains soap lye;
5) a small amount of palm oil is applied in mould inner wall, the soap lye being stirred is poured into mould, mould sealed with plastic sheeting It is good, 1-7d is stood in 36-46 DEG C of incubator;
6) it is placed in ventilation after soap lye solidification and spontaneously dries the demoulding, is then placed within normal temperature 5-7 weeks, is packaged into product.
Compared with prior art, Eucommia Oil perfumed soap provided by the invention is oily using pure plants such as Eucommia Oil, olive oil, Saponification is made by low temperature, completely remains the active ingredient of each grease, while adds Lavender and rich in various active Eucommia leaf extract, the aloe extract of composition, without any chemical addition agent, are not stimulated gently, are easily absorbed, can be clear with depth Clean skin;Each active ingredient is mutually coordinated, and excitant is low, and anti-microbial property is good, and the foaming power and foam stability of perfumed soap are good, has profit Damp skin, oil-control moisturizing, desalinate color spot, prevent the multi-efficiencies such as skin senescence.
Embodiment
With reference to specific embodiment, the present invention is described further, but following embodiments absolutely not to the present invention have appoint What is limited.
Embodiment 1
Data according to embodiment 1 corresponding to table 1 weigh each raw material, then operate in the steps below:
1) Eucommia Oil, olive oil are mixed and be put into heatproof container, heating water bath, while be stirred continuously with glass bar, protect Temperature is held at 35 DEG C, obtains solution A;
2) deionized water is added in alkali-proof glass container, then according to the amount of required sodium hydroxide, be slowly added into, side Edged stirs, until sodium hydroxide is completely dissolved, is cooled to 35 DEG C, obtains solution B;
3) solution B is slowly added into the container equipped with solution A and carries out saponification, it is stirring while adding, after 30min Thick, saponification completion, obtained soap base solution is presented in mixed liquor, and adjusts pH to 7.2;
4) toward add eucommia leaf extract according to required ratio while stirring in soap base solution made from step 3), aloe carries Thing and Lavender are taken, is stirred, obtains soap lye;
5) a small amount of palm oil is applied in mould inner wall, the soap lye being stirred is poured into mould, mould sealed with plastic sheeting It is good, 1d is stood in 36 DEG C of incubator;
6) it is placed in ventilation after soap lye solidification and spontaneously dries the demoulding, is then placed within normal temperature 5 weeks, is packaged into product.
Embodiment 2
Data according to embodiment 2 corresponding to table 1 weigh each raw material, then operate in the steps below:
1) Eucommia Oil, olive oil are mixed by above-mentioned weight proportion and be put into heatproof container, heating water bath, while use glass Rod is stirred continuously, and is maintained the temperature at 65 DEG C, is obtained solution A;
2) deionized water is added in alkali-proof glass container, then according to the amount of required sodium hydroxide, be slowly added into, side Edged stirs, until sodium hydroxide is completely dissolved, is cooled to 55 DEG C, obtains solution B;
3) solution B is slowly added into the container equipped with solution A and carries out saponification, it is stirring while adding, after 50min Thick, saponification completion, obtained soap base solution is presented in mixed liquor, and adjusts pH to 8.2;
4) toward add eucommia leaf extract according to required ratio while stirring in soap base solution made from step 3), aloe carries Thing and Lavender are taken, is stirred, obtains soap lye;
5) a small amount of palm oil is applied in mould inner wall, the soap lye being stirred is poured into mould, mould sealed with plastic sheeting It is good, 7d is stood in 46 DEG C of incubator;
6) it is placed in ventilation after soap lye solidification and spontaneously dries the demoulding, is then placed within normal temperature 7 weeks, is packaged into product.
Embodiment 3
Data according to embodiment 3 corresponding to table 1 weigh each raw material, then operate in the steps below:
1) Eucommia Oil, olive oil are mixed by above-mentioned weight proportion and be put into heatproof container, heating water bath, while use glass Rod is stirred continuously, and is maintained the temperature at 50 DEG C, is obtained solution A;
2) deionized water is added in alkali-proof glass container, then according to the amount of required sodium hydroxide, be slowly added into, side Edged stirs, until sodium hydroxide is completely dissolved, is cooled to 45 DEG C, obtains solution B;
3) solution B is slowly added into the container equipped with solution A and carries out saponification, it is stirring while adding, after 40min Thick, saponification completion, obtained soap base solution is presented in mixed liquor, and adjusts pH to 7.7;
4) toward add eucommia leaf extract according to required ratio while stirring in soap base solution made from step 3), aloe carries Thing and Lavender are taken, is stirred, obtains soap lye;
5) a small amount of palm oil is applied in mould inner wall, the soap lye being stirred is poured into mould, mould sealed with plastic sheeting It is good, 4d is stood in 42 DEG C of incubator;
6) it is placed in ventilation after soap lye solidification and spontaneously dries the demoulding, is then placed within normal temperature 6 weeks, is packaged into product.
Embodiment 4
Data according to embodiment 4 corresponding to table 1 weigh each raw material, then operate in the steps below:
1) Eucommia Oil, olive oil are mixed by above-mentioned weight proportion and be put into heatproof container, heating water bath, while use glass Rod is stirred continuously, and is maintained the temperature at 45 DEG C, is obtained solution A;
2) deionized water is added in alkali-proof glass container, then according to the amount of required sodium hydroxide, be slowly added into, side Edged stirs, until sodium hydroxide is completely dissolved, is cooled to 45 DEG C, obtains solution B;
3) solution B is slowly added into the container equipped with solution A and carries out saponification, it is stirring while adding, after 45min Thick, saponification completion, obtained soap base solution is presented in mixed liquor, and adjusts pH to 7.5;
4) toward add eucommia leaf extract according to required ratio while stirring in soap base solution made from step 3), aloe carries Thing and Lavender are taken, is stirred, obtains soap lye;
5) a small amount of palm oil is applied in mould inner wall, the soap lye being stirred is poured into mould, mould sealed with plastic sheeting It is good, 6d is stood in 40 DEG C of incubator;
6) it is placed in ventilation after soap lye solidification and spontaneously dries the demoulding, is then placed within normal temperature 5 weeks, is packaged into product.
Embodiment 5
Data according to embodiment 5 corresponding to table 1 weigh each raw material, then operate in the steps below:
1) Eucommia Oil, olive oil are mixed by above-mentioned weight proportion and be put into heatproof container, heating water bath, while use glass Rod is stirred continuously, and is maintained the temperature at 55 DEG C, is obtained solution A;
2) deionized water is added in alkali-proof glass container, then according to the amount of required sodium hydroxide, be slowly added into, side Edged stirs, until sodium hydroxide is completely dissolved, is cooled to 39 DEG C, obtains solution B;
3) solution B is slowly added into the container equipped with solution A and carries out saponification, it is stirring while adding, after 38min Thick, saponification completion, obtained soap base solution is presented in mixed liquor, and adjusts pH to 7.7;
4) toward add eucommia leaf extract according to required ratio while stirring in soap base solution made from step 3), aloe carries Thing and Lavender are taken, is stirred, obtains soap lye;
5) a small amount of palm oil is applied in mould inner wall, the soap lye being stirred is poured into mould, mould sealed with plastic sheeting It is good, 3d is stood in 39 DEG C of incubator;
6) it is placed in ventilation after soap lye solidification and spontaneously dries the demoulding, is then placed within normal temperature 7 weeks, is packaged into product.
Embodiment 6
Data according to embodiment 6 corresponding to table 1 weigh each raw material, then operate in the steps below:
1) Eucommia Oil, olive oil are mixed by above-mentioned weight proportion and be put into heatproof container, heating water bath, while use glass Rod is stirred continuously, and is maintained the temperature at 43 DEG C, is obtained solution A;
2) deionized water is added in alkali-proof glass container, then according to the amount of required sodium hydroxide, be slowly added into, side Edged stirs, until sodium hydroxide is completely dissolved, is cooled to 47 DEG C, obtains solution B;
3) solution B is slowly added into the container equipped with solution A and carries out saponification, it is stirring while adding, after 38min Thick, saponification completion, obtained soap base solution is presented in mixed liquor, and adjusts pH to 8.1;
4) toward add eucommia leaf extract according to required ratio while stirring in soap base solution made from step 3), aloe carries Thing and Lavender are taken, is stirred, obtains soap lye;
5) a small amount of palm oil is applied in mould inner wall, the soap lye being stirred is poured into mould, mould sealed with plastic sheeting It is good, 5d is stood in 43 DEG C of incubator;
6) it is placed in ventilation after soap lye solidification and spontaneously dries the demoulding, is then placed within normal temperature 5 weeks, is packaged into product.
Embodiment 7
Data according to embodiment 7 corresponding to table 1 weigh each raw material, then operate in the steps below:
1) Eucommia Oil, olive oil are mixed by above-mentioned weight proportion and be put into heatproof container, heating water bath, while use glass Rod is stirred continuously, and is maintained the temperature at 57 DEG C, is obtained solution A;
2) deionized water is added in alkali-proof glass container, then according to the amount of required sodium hydroxide, be slowly added into, side Edged stirs, until sodium hydroxide is completely dissolved, is cooled to 48 DEG C, obtains solution B;
3) solution B is slowly added into the container equipped with solution A and carries out saponification, it is stirring while adding, after 48min Thick, saponification completion, obtained soap base solution is presented in mixed liquor, and adjusts pH to 7.4;
4) toward add eucommia leaf extract according to required ratio while stirring in soap base solution made from step 3), aloe carries Thing and Lavender are taken, is stirred, obtains soap lye;
5) a small amount of palm oil is applied in mould inner wall, the soap lye being stirred is poured into mould, mould sealed with plastic sheeting It is good, 5d is stood in 44 DEG C of incubator;
6) it is placed in ventilation after soap lye solidification and spontaneously dries the demoulding, is then placed within normal temperature 7 weeks, is packaged into product.
Embodiment 8
Data according to embodiment 8 corresponding to table 1 weigh each raw material, then operate in the steps below:
1) Eucommia Oil, olive oil are mixed by above-mentioned weight proportion and be put into heatproof container, heating water bath, while use glass Rod is stirred continuously, and is maintained the temperature at 42 DEG C, is obtained solution A;
2) deionized water is added in alkali-proof glass container, then according to the amount of required sodium hydroxide, be slowly added into, side Edged stirs, until sodium hydroxide is completely dissolved, is cooled to 43 DEG C, obtains solution B;
3) solution B is slowly added into the container equipped with solution A and carries out saponification, it is stirring while adding, after 48min Thick, saponification completion, obtained soap base solution is presented in mixed liquor, and adjusts pH to 7.4;
4) toward add eucommia leaf extract according to required ratio while stirring in soap base solution made from step 3), aloe carries Thing and Lavender are taken, is stirred, obtains soap lye;
5) a small amount of palm oil is applied in mould inner wall, the soap lye being stirred is poured into mould, mould sealed with plastic sheeting It is good, 3d is stood in 45 DEG C of incubator;
6) it is placed in ventilation after soap lye solidification and spontaneously dries the demoulding, is then placed within normal temperature 7 weeks, is packaged into product.
Comparative example 1
Each raw material and operating procedure of comparative example 1 are same as Example 1, and Eucommia Oil is only substituted for 10g, remaining and implementation The all same of example 1.
Comparative example 2
Each raw material and operating procedure of comparative example 2 are same as Example 1, and eucommia leaf extract is only substituted for 2g, remaining With all same of embodiment 1.
Comparative example 3
Each raw material and operating procedure of comparative example 3 are same as Example 1, and olive oil is only substituted for 1g, remaining and implementation The all same of example 1.
Comparative example 4
Each raw material and operating procedure of comparative example 4 are same as Example 1, and aloe extract is only substituted for 32g, remaining with The all same of embodiment 1.
Comparative example 5
Each raw material and operating procedure of comparative example 5 are same as Example 1, and Lavender is only substituted for 42g, remaining with The all same of embodiment 1.
Comparative example 6
Each raw material and operating procedure of comparative example 6 are same as Example 1, and sodium hydroxide is only substituted for 1.5g, remaining with The all same of embodiment 1.
Comparative example 7
Each raw material and operating procedure of comparative example 7 are same as Example 1, and eucommia leaf extract is only substituted for 52g, its The remaining and all same of embodiment 1.
Comparative example 8
Each raw material and operating procedure of comparative example 8 are same as Example 1, and Eucommia Oil is only substituted for 100g, remaining and reality Apply all same of example 1.
Comparative example 9
Each raw material and operating procedure of comparative example 9 are same as Example 1, and the temperature of step 1) is only maintained at 20 DEG C, its The remaining and all same of embodiment 1.
Comparative example 10
Each raw material and operating procedure of comparative example 10 are same as Example 1, and the temperature of step 1) is only maintained at 80 DEG C, Remaining and all same of embodiment 1.
Comparative example 11
Each raw material and operating procedure of comparative example 11 are same as Example 1, and the temperature of step 2) is only maintained at 20 DEG C, Remaining and all same of embodiment 1.
Comparative example 12
Each raw material and operating procedure of comparative example 12 are same as Example 1, and the temperature of step 2) is only maintained at 70 DEG C, Remaining and all same of embodiment 1.
Comparative example 13
Each raw material and operating procedure of comparative example 13 are same as Example 1, and the pH of step 3) is only maintained at 6.5, remaining With all same of embodiment 1.
Comparative example 14
Each raw material and operating procedure of comparative example 14 are same as Example 1, and the pH of step 3) is only maintained at 9.0, remaining With all same of embodiment 1.
Each embodiment composition of raw materials (unit of table 1:g)
The excitant of embodiment 9 is tested
Perfumed soap prepared by all embodiments and comparative example is dissolved into soap lye, each soap lye concentration is adjusted to 5wt%, works as dosage For 0.3mL when, by HET VAM measurements determinations dermoreaction classification (relative values be classified), intense stimulus > 2.0, stimulation 1.2-2.0, medium stimulation 0.8-1.2, minimal irritation 0.0-0.8.Test result is as shown in table 2, test result indicates that, utilize this Perfumed soap prepared by the formula and method of invention is low with respect to values, because using pure plant oil and various plants extract, Without any chemical addition agent, moderate performance, suitable for sensitive group;In addition, whole use low temperature preparation, plant group is not damaged Active material in point.And the relative values in comparative example more belong to medium stimulation, illustrate beyond formula once beyond The value that the present invention limits, excitant can be substantially increased, and cost also rises in addition, and cost performance reduces.
The excitant test result of table 2
The foaming properties test of embodiment 10
Foaming properties test is carried out using Roche foam meter, the soap lye concentration of each embodiment and comparative example is adjusted to 2.5wt%, the foam height of 0 minute, 3 minutes and 6 minutes is tested respectively.Test result is as shown in table 3, from table 3 it can be seen that The foaming power and foam stability energy of the perfumed soap prepared using the formula and method of the present invention are preferable, under the foam height after 6min Depreciation is obvious compared with comparative example to be reduced, and illustrates having good stability for foam.
The foaming properties test result of table 3
The bacteriostasis property of embodiment 11 is tested
Choose Escherichia coli (Escherichia coli, ATCC24752), staphylococcus aureus (Staphylocouus Aureus, ATGC6538) and Candida albicans (Monilia albican, ATGC10231) conduct test strain, by above-mentioned bacterium Kind recovered, cultivate to exponential phase, 105-106CFU/mL is diluted to culture medium, using spreader by the bacterium of dilution Liquid is uniformly coated on solid medium.By Oxford cup as on solid medium, every part of sample controls 3, and set it is negative right According to, by solid medium be placed in 37 DEG C culture about 20h.Then vernier caliper measurement antibacterial circle diameter is used, experiment is repeated 3 times. Test result is as shown in table 4, it can be seen that perfumed soap bacteriostasis property of the invention is good, and bacteria-eliminating efficacy is obvious, and suppresses bacterium Grow.
The bacteriostasis property of table 4 tests table
Note:"+" represents that part is antibacterial, it can be seen that antibacterial ring size, but still have part colony growth in ring;" ++ " represents obvious suppression Bacterium, there is an obvious antibacterial ring size, without bacterium colony in ring.
It should be noted that and understand, the feelings of the spirit and scope of the present invention required by appended claims are not departed from Under condition, various modifications and improvements can be made to the present invention of foregoing detailed description.It is therefore desirable to the model of the technical scheme of protection Enclose and do not limited by given any specific exemplary teachings.
Applicant states, above content is that to combine specific preferred embodiment made for the present invention further specifically It is bright, it is impossible to assert that the specific implementation of the present invention is confined to these explanations.For the ordinary skill of the technical field of the invention For personnel, without departing from the inventive concept of the premise, some simple deduction or replace can also be made, should all be considered as category In protection scope of the present invention.

Claims (9)

1. a kind of Eucommia Oil perfumed soap, it is characterised in that the Eucommia Oil perfumed soap includes following components by weight:
Eucommia Oil:30-50
Olive oil:5-20
Eucommia leaf extract:5-20
Aloe extract:2-15
Lavender:1-10
Sodium hydroxide:5-15
Deionized water:20-30.
2. Eucommia Oil perfumed soap according to claim 1, it is characterised in that the Eucommia Oil perfumed soap includes following by weight Component:
Eucommia Oil:32-42
Olive oil:5-15
Eucommia leaf extract:8-18
Aloe extract:2-12
Lavender:1-5
Sodium hydroxide:8-10
Deionized water:20-25.
3. Eucommia Oil perfumed soap according to claim 1, it is characterised in that the Eucommia Oil perfumed soap includes following by weight Component:
Eucommia Oil:34-42
Olive oil:7-15
Eucommia leaf extract:8-16
Aloe extract:4-12
Lavender:1-5
Sodium hydroxide:8-10
Deionized water:20-25.
4. the preparation method of the Eucommia Oil perfumed soap according to one of claim 1-3, it is characterised in that comprise the following steps:
1) after mixing Eucommia Oil and olive oil, heat and be stirred continuously in a water bath, obtain solution A;
2) another extracting container adds deionized water, is slowly added to sodium hydroxide and is stirred continuously, cold after being completely dissolved to sodium hydroxide But solution B is obtained;
3) solution B is slowly added to carry out saponification in solution A, soap base solution is made;
4) eucommia leaf extract, aloe extract and Lavender are added in soap base solution, and is stirred continuously, obtains soap Liquid;
5) soap lye is poured into mould, after standing 1-7d in incubator after sealing, dries the demoulding, be packaged into product.
5. the preparation method of Eucommia Oil perfumed soap according to claim 4, it is characterised in that 35-65 is heated in step 1) ℃。
6. the preparation method of the Eucommia Oil perfumed soap according to claim 4 or 5, it is characterised in that 35- is cooled in step 2) 55℃。
7. the preparation method of the Eucommia Oil perfumed soap according to claim 4 or 5, it is characterised in that saponification in step 3) Time be 30-50min.
8. the preparation method of the Eucommia Oil perfumed soap according to claim 4 or 5, it is characterised in that soap base solution in step 3) PH be 7.2-8.2.
9. the preparation method of the Eucommia Oil perfumed soap according to claim 4 or 5, it is characterised in that step 5) further comprises Following steps:
51) palm oil is smeared in mould inner wall, soap lye is poured into mould, then mould sealed with plastic sheeting, in 36-46 DEG C incubator in stand 1-7d;
52) mould is subjected to the natural drying demoulding, then normal temperature stands 5-7 weeks, is packaged into product as ventilation.
CN201711118921.8A 2017-11-14 2017-11-14 A kind of Eucommia Oil perfumed soap and preparation method thereof Pending CN107739670A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110408486A (en) * 2018-04-26 2019-11-05 北京化工大学 A kind of Cortex Eucommiae soap and preparation method thereof
CN111440680A (en) * 2020-04-24 2020-07-24 山东贝隆杜仲生物工程有限公司 Acne-removing soap prepared from byproduct in eucommia oil refining and preparation method thereof
CN112300877A (en) * 2020-10-30 2021-02-02 广东宇通医药生物科技有限公司 Formula and preparation method of traditional Chinese medicine soap
CN115700275A (en) * 2022-11-30 2023-02-07 汉中天泽嘉源农林科技有限公司 Eucommia seed oil handmade soap and preparation method thereof

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Publication number Priority date Publication date Assignee Title
CN106047538A (en) * 2016-06-11 2016-10-26 张家界茶坤缘生物科技开发有限公司 Healthy soap containing original eucommia ulmoide extract and preparation method of healthy soap
CN106350312A (en) * 2016-08-18 2017-01-25 河南中医学院 Traditional Chinese medicine anti-wrinkle handmade soap

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106047538A (en) * 2016-06-11 2016-10-26 张家界茶坤缘生物科技开发有限公司 Healthy soap containing original eucommia ulmoide extract and preparation method of healthy soap
CN106350312A (en) * 2016-08-18 2017-01-25 河南中医学院 Traditional Chinese medicine anti-wrinkle handmade soap

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110408486A (en) * 2018-04-26 2019-11-05 北京化工大学 A kind of Cortex Eucommiae soap and preparation method thereof
CN111440680A (en) * 2020-04-24 2020-07-24 山东贝隆杜仲生物工程有限公司 Acne-removing soap prepared from byproduct in eucommia oil refining and preparation method thereof
CN112662491A (en) * 2020-04-24 2021-04-16 山东贝隆杜仲生物工程有限公司 Acne-removing soap prepared from byproduct in eucommia oil refining and preparation method thereof
CN112300877A (en) * 2020-10-30 2021-02-02 广东宇通医药生物科技有限公司 Formula and preparation method of traditional Chinese medicine soap
CN115700275A (en) * 2022-11-30 2023-02-07 汉中天泽嘉源农林科技有限公司 Eucommia seed oil handmade soap and preparation method thereof

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