CN106929230A - A kind of preparation method of olive essential oil cold process soap - Google Patents
A kind of preparation method of olive essential oil cold process soap Download PDFInfo
- Publication number
- CN106929230A CN106929230A CN201710123982.7A CN201710123982A CN106929230A CN 106929230 A CN106929230 A CN 106929230A CN 201710123982 A CN201710123982 A CN 201710123982A CN 106929230 A CN106929230 A CN 106929230A
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- China
- Prior art keywords
- oil
- olive
- essential oil
- water
- soap
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/10—Mixing; Kneading
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of preparation method of olive essential oil cold process soap.Weighed on balance during a certain amount of olive oil, coconut oil, palm oil, castor oil, white oil, cocoa butter be positioned over beaker, and weigh a certain amount of NaOH and water.Then it is completely dissolved the water that will be weighed is poured into NaOH, and stirring becomes clear to solution.Stand, treat that it is down to uniform temperature.Grease is placed in water-bath and is heated, and with its temperature of thermometer measure.Beaker is taken out from water-bath when temperature rises to uniform temperature.Sodium hydroxide solution is poured into base oil, side edged is quickly stirred.Water-bath and continue to stir certain hour at 45 DEG C, while adding micro food coloring and essential oil, stirring to be poured into mould immediately after terminating, be placed at shady and cool ventilation and preserve, treat that its is ripe.Experimental implementation of the present invention is easy, and Lipid use rate is high, can as requested change the species of ratio, essential oil and the pigment of grease.
Description
Technical field
The present invention relates to articles for daily use technical field, it is related to a kind of preparation method of olive essential oil cold process soap.
Background technology
Olive oil rich in the polyphenoils such as monounsaturated fatty acids and vitamin, can anti-wrinkle and anti-aging, it is common
The ratio of the fatty acid monoglyceride/olive oil organogel for containing in the cosmetic formulations of skin care is being continuously increased；Olive
Squalene in oil is strong with skin affinity, can effectively be absorbed by skin, keeps skin gloss flexible；Contain in olive oil
Polyphenol compound there is bioactivity higher, can antibacterial, anti-oxidant, uvioresistant etc..Therefore, olive oil is not only edible
Also can be the cosmetics of " eating " with oil.At present, olive oil is applied to that cosmetic field is more and more extensive, such as by appropriate olive
Olive oil is added to such as mildy wash, shampoo, bath foam in the cosmetics of washing class, does not influence the physicochemical property of product not only, and also
The clean result of product can be strengthened.
Manual perfumed soap contains natural glycerin, and glycerine is the moisturizing ingredient to be lacked in cosmetics and skin care products；By hand
Perfumed soap can be directed to the skin quality of oneself and make, therefore oneself understand what material is with the addition of in perfumed soap, without worrying strange composition
Skin can be injured, can feel at ease to use；Manual perfumed soap is not only gently non-stimulated to skin, and also helps environmental protection；Manual perfumed soap
It is " natural face cleaning activating agent ", can effectively cleans grease, and will not at all destroys the cuticula of skin；Added in handmade soap
Olive oil, and mix in varing proportions with other oil, make the handmade soap made that there is unique washing to feel and function.
The content of the invention
It is an object of the invention to provide a kind of olive essential oil cold process soap, olive oil is applied in handmade soap, and added
Essential oil, realizes that the pure of handmade soap prepares by hand.
It is a further object to provide the preparation method of above-mentioned olive essential oil cold process soap.
The present invention is implemented according to following scheme：
The base oil of handmade soap of the present invention has：
The base oil of the handmade soap of table 1
The INS values 120 ~ 160 of grease of the invention are appropriate.
Step 1, the g of olive oil 40 ~ 140 is weighed on balance, the g of coconut oil 15 ~ 70, the g of palm oil 20 ~ 75, castor oil 7 ~
30 g, the g of white oil 7 ~ 75, the g of cocoa butter 3 ~ 10 is placed in the beaker of 500 mL；The g of NaOH 14 ~ 36 are weighed, the g of water 28 ~ 87 is placed in
In the beaker of 250 mL.
Then it is completely dissolved step 2, Jiang Shui are poured into NaOH, and stirring becomes clear to solution.Stand,
Treat that its temperature is down to 50 DEG C.
Step 3, grease is placed in water-bath and heated, and with its temperature of thermometer measure.When temperature liter, 40 ~ 50 DEG C
Step 4, sodium hydroxide solution is poured into base oil, side edged is quickly stirred.
Step 5, at 40 ~ 50 DEG C water-bath and continue the h of stirring 0.5 ~ 1.0.Stirring is poured into mould immediately after terminating, and is put
Preserved at shady and cool ventilation, wait it ripe.
The preparation method of olive essential oil handmade soap of the invention is also resided in：
The wet concentration used of olive essential oil soap of the invention selects distilled water or pure water.
Olive essential oil soap of the invention adds micro olive essential oil or light component before soap base enters mould, by fresh squeezing
Olive oil is obtained through molecular clock, and condition is the mL/min of charging rate 1.0 ~ 1.5, and 40 ~ 50 DEG C of feeding temperature, molecule steams
Evaporate 100 ~ 120 DEG C of temperature, the Pa of vacuum 100 ~ 200, the r/min of knifing rotating speed 200 ~ 300.
Also clove oil, refined jasmine oil can be added in natural plants essential oil transparent soap of the invention, Rosa Damascana, clothing is smoked
Careless essential oil one or several.
Olive essential oil soap of the invention carries out adding micro food coloring before soap base enters mould.
Total free alkali of olive essential oil soap of the invention is 0.05 ~ 0.10%（In terms of NaOH）.
The free causticity alkali content of olive essential oil soap of the invention is 0.05 ~ 0.10%（In terms of NaOH）.
The moisture and volatile matter of olive essential oil soap of the invention are 21 ~ 24%（Temperature is 60 DEG C ± 2 DEG C）.
Experimental implementation of the present invention is easy, and Lipid use rate is high, and requirement that can be according to the hobby of oneself and to function changes
The species of the ratio, essential oil and pigment of grease.
Specific embodiment
Embodiment 1
The g of olive oil 75, the g of coconut oil 70, the g of palm oil 75 are weighed on balance, is placed in the beaker of 500 mL；Weigh NaOH
36.5 g, the g of water 87.5 is placed in the beaker of 250 mL.
Water is poured into NaOH, and stir become clear to solution be then completely dissolved.Stand, treat its temperature
Degree is down to 50 DEG C.Grease is placed in water-bath and is heated, and with its temperature of thermometer measure.When temperature rises to 50 DEG C by beaker
Taken out from water-bath.
Sodium hydroxide solution is poured into base oil, side edged is quickly stirred.At 45 DEG C water-bath and continue stirring 1 h it is straight
Become thick energy to soap lye and draw 8 words.
Olive essential oil soap adds micro olive essential oil or light component before soap base enters mould, is passed through by the olive oil of fresh squeezing
Molecular clock and obtain, condition is the mL/min of charging rate 1.0,45 DEG C of feeding temperature, 110 DEG C of molecular distillation temperature, vacuum
Spend 150 Pa, the r/min of knifing rotating speed 250.
Olive essential oil soap can also add clove oil, refined jasmine oil, Rosa Damascana before soap base enters mould.
Olive essential oil soap can add micro food coloring before soap base enters mould, continue to stir.
Stirring is poured into mould immediately after terminating, and is placed at shady and cool ventilation and is preserved, and waits it ripe.
INS values are calculated
INS values are used for representing the hardness of soap.The ratio of soap base shared by the INS value * greases of grease=after the completion of soap hardness.INS
Value is lower, and the perfumed soap after the completion of representative is softer；Conversely, INS values are higher, the perfumed soap after the completion of expression is harder.INS values between 120 ~
160 are all belonging to appropriate hardness.
The measure of total free alkali
Dissolving soap in ethanol solution, with the sulfuric acid solution that known excessive concentration is 0.5 mol/L and free alkali, then
With the excessive acid of the potassium hydroxide-ethanol solution residual titration that concentration is 0.5 mol/L.
The measure of free causticity alkali content
Soap is dissolved in neutral alcohol, then trip is titrated with the acidic alcohol standard titration solution that concentration is 0.5 mol/L
From caustic alkali.
The measure of moisture and volatile matter
At an established temperature, by a certain amount of sample drying to constant weight, weigh and reduce.
The soap surface that this scheme is worked it out has soap powder to produce, partially firmly；Not exclusively, the few water of alkali is more for possible cause saponification.
Embodiment 2
The g of olive oil 75, the g of coconut oil 25, the g of palm oil 50 are weighed on balance, is placed in the beaker of 500 mL；Weigh NaOH
21.85 g, the g of water 56.81 is placed in the beaker of 250 mL.Operating process such as embodiment 1.
There is soap powder on the soap surface that this scheme is worked it out, and alkalescence is partially strong；Possible cause stirring is insufficient, and temperature is not enough, preserves
During oxidation by air.
Embodiment 3
The g of olive oil 90, the g of coconut oil 40, the g of palm oil 20, the g of castor oil 30, the g of white oil 20 are weighed on balance, 500 are placed in
In the beaker of mL；The g of NaOH 29 are weighed, the g of water 75.4 is placed in the beaker of 250 mL.Operating process such as embodiment 1.
There is a little fuel-displaced phenomenon on the soap surface that this scheme is worked it out, and hardness is partially soft, but without soap powder, color and luster is preferable；May be former
Because palm oil mass is on the low side, water is on the high side.
Embodiment 4
The g of olive oil 35, the g of coconut oil 15, the g of palm oil 32, the g of castor oil 7, the g of white oil 7, the g of cocoa butter 4 are weighed on balance,
It is placed in the beaker of 500 mL；The g of NaOH 14.4 are weighed, the g of water 28.9 is placed in the beaker of 250 mL.Operating process is as implemented
Example 1.
The soap hardness that this scheme is worked it out is moderate, and surface is smooth without soap powder.
Four kinds of measure of the INS values of embodiment, the measure of total free alkali, free causticity alkali content, moisture and volatile matter
It is as shown in table 2 below.
The index determining result of the experimental program of table 2
| Scheme | Total free alkali（In terms of NaOH）% | Free caustic alkali（In terms of NaOH）% | Moisture and volatile matter（60℃±2℃）% | INS values |
| 1 | 0.09 | 0.09 | 21 | 168.92 |
| 2 | 0.09 | 0.09 | 24 | 146.21 |
| 3 | 0.09 | 0.09 | 24 | 140.90 |
| 4 | 0.08 | 0.08 | 23 | 144.23 |
| National sector standard | ≤0.1 | ≤0.1 | 20~25 | 120~170 |
Claims (9)
1. a kind of preparation method of olive essential oil cold process soap, its step is as follows：
The first step, weighs the g of olive oil 40 ~ 140, the g of coconut oil 15 ~ 70, the g of palm oil 20 ~ 75, castor oil 7 ~ 30 on balance
G, the g of white oil 7 ~ 75, the g of cocoa butter 3 ~ 10 is placed in the beaker of 500 mL；The g of NaOH 14 ~ 36 are weighed, the g of water 28 ~ 87 is placed in 250
In the beaker of mL;
Then it is completely dissolved second step, water is poured into NaOH, and stirring becomes clear to solution, is stood, is treated
Its temperature is down to 40 ~ 50 DEG C;
3rd step, grease is placed in water-bath and is heated, and with its temperature of thermometer measure, when temperature rises to 50 DEG C by beaker
Taken out from water-bath;
4th step, sodium hydroxide solution is poured into base oil, and side edged is quickly stirred;
5th step, water-bath and the h of stirring 0.5 ~ 1.0 is continued at 40 ~ 50 DEG C, and stirring is poured into mould immediately after terminating, and is placed on the moon
Cool ventilation preserves, and waits it ripe.
2. the preparation method of olive essential oil cold process soap according to claim 1, it is characterised in that the first step and second step
In wet concentration used select distilled water or pure water.
3. the preparation method of olive essential oil cold process soap according to claim 1, it is characterised in that in the first step grease compared with
Suitable INS values are 120 ~ 160.
4. the preparation method of olive essential oil cold process soap according to claim 1, it is characterised in that the 5th step enters in soap base
Carry out adding micro olive essential oil or light component before mould, obtained through molecular clock by the olive oil of fresh squeezing, condition
It is the mL/min of charging rate 1.0 ~ 1.5,40 ~ 50 DEG C of feeding temperature, 100 ~ 120 DEG C of molecular distillation temperature, vacuum 100 ~ 200
Pa, the r/min of knifing rotating speed 200 ~ 300.
5. the preparation method of olive essential oil cold process soap according to claim 1, it is characterised in that the 5th step enters in soap base
Can also be added before mould clove oil, refined jasmine oil, Rosa Damascana, Lavender one or several.
6. the preparation method of olive essential oil cold process soap according to claim 1, it is characterised in that the 5th step enters in soap base
Carry out adding micro food coloring before mould.
7. the preparation method of olive essential oil cold process soap according to claim 1, it is characterised in that olive oil of the invention
Total free alkali of essential oil soap is 0.05 ~ 0.10%（In terms of NaOH）.
8. the preparation method of olive essential oil cold process soap according to claim 1, it is characterised in that olive oil of the invention
The free causticity alkali content of essential oil soap is 0.05 ~ 0.10%（In terms of NaOH）.
9. the preparation method of olive essential oil cold process soap according to claim 1, it is characterised in that moisture and volatile matter are
21~24%（Temperature is 60 DEG C ± 2 DEG C）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710123982.7A CN106929230A (en) | 2017-03-03 | 2017-03-03 | A kind of preparation method of olive essential oil cold process soap |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710123982.7A CN106929230A (en) | 2017-03-03 | 2017-03-03 | A kind of preparation method of olive essential oil cold process soap |
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| CN106929230A true CN106929230A (en) | 2017-07-07 |
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ID=59423920
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|---|---|---|---|
| CN201710123982.7A Pending CN106929230A (en) | 2017-03-03 | 2017-03-03 | A kind of preparation method of olive essential oil cold process soap |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107523445A (en) * | 2017-09-27 | 2017-12-29 | 中国林业科学研究院林产化学工业研究所 | A kind of preparation method of cape jasmine humidity-preserving type craft cold process soap |
| CN107629900A (en) * | 2017-09-27 | 2018-01-26 | 中国林业科学研究院林产化学工业研究所 | A kind of preparation method of cape jasmine whitening anti-acne type craft cold process soap |
| CN107760497A (en) * | 2017-09-27 | 2018-03-06 | 中国林业科学研究院林产化学工业研究所 | A kind of preparation method of the crease-resistant type craft cold process soap of cape jasmine |
| CN108456597A (en) * | 2017-10-24 | 2018-08-28 | 浙江康鸿生物科技有限公司 | A kind of preparation method of cape jasmine antiphlogistic craft cold process soap |
| CN109022180A (en) * | 2017-10-24 | 2018-12-18 | 浙江康鸿生物科技有限公司 | A kind of preparation method of cape jasmine skin-protection type craft cold process soap |
| CN109536315A (en) * | 2018-12-28 | 2019-03-29 | 天津金汇药业集团有限公司 | A kind of olive oil cold process soap |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107523445A (en) * | 2017-09-27 | 2017-12-29 | 中国林业科学研究院林产化学工业研究所 | A kind of preparation method of cape jasmine humidity-preserving type craft cold process soap |
| CN107629900A (en) * | 2017-09-27 | 2018-01-26 | 中国林业科学研究院林产化学工业研究所 | A kind of preparation method of cape jasmine whitening anti-acne type craft cold process soap |
| CN107760497A (en) * | 2017-09-27 | 2018-03-06 | 中国林业科学研究院林产化学工业研究所 | A kind of preparation method of the crease-resistant type craft cold process soap of cape jasmine |
| CN108456597A (en) * | 2017-10-24 | 2018-08-28 | 浙江康鸿生物科技有限公司 | A kind of preparation method of cape jasmine antiphlogistic craft cold process soap |
| CN109022180A (en) * | 2017-10-24 | 2018-12-18 | 浙江康鸿生物科技有限公司 | A kind of preparation method of cape jasmine skin-protection type craft cold process soap |
| CN109536315A (en) * | 2018-12-28 | 2019-03-29 | 天津金汇药业集团有限公司 | A kind of olive oil cold process soap |
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Application publication date: 20170707 |