CN104107151A - Dendrobium candidum paste mask and preparation method thereof - Google Patents
Dendrobium candidum paste mask and preparation method thereof Download PDFInfo
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Abstract
The invention relates to a dendrobium candidum paste mask and a preparation method of the dendrobium candidum paste mask, aiming at providing a dendrobium candidum paste mask which can be used for keeping effective components of dendrobium candidum and the preparation method of the dendrobium candidum paste mask. The dendrobium candidum paste mask comprises 4-6 parts by weight of dendrobium candidum ultra-micro powder, wherein the dendrobium candidum ultra-micro powder contains polysaccharide, chlorophyll, vitamins and proteins. The preparation method of the dendrobium candidum paste mask sequentially comprises the following processes: A, a pre-treatment process; B, a freeze-drying process; C, a low-temperature ultra-micro airflow crushing process: screening by using a 100-mesh sieve, and performing low-temperature ultra-micro airflow crushing to obtain dendrobium candidum ultra-micro powder of which the average particle size is 5.5-6.5 microns; D, an emulsification process; and E, a filling process. The dendrobium candidum paste mask disclosed by the invention performs freeze-drying and low-temperature ultra-micro crushing by adopting a dendrobium candidum fresh product as a raw material, and can be used for reserving the effective components of dendrobium candidum to the highest extent; and an obtained product is high in content of polysaccharide, vitamins, chlorophyll and free amino acids.
Description
Technical field
The present invention relates to a kind of mud facial film and preparation method thereof, especially relate to a kind of Herba Dendrobii mud facial film and preparation method thereof, belong to medicinal plants manufacture field.
Background technology
Herba Dendrobii is the fresh stem of orchid Herba Dendrobii (Dendrobium officinale Kimura et Migo), belongs to state guarantee plant, has precious health preserving and medical value.Because its epidermis is, ferrum is green gains the name Herba Dendrobii, successive dynasties Chinese medicine ancient books and records are all on the books, the discussions of classical works to Herba Dendrobii such as comprehensive Shennong's Herbal, Compendium of Material Medica, " detailed outline is picked up any lost article from the road " and " not Lu ", its main effect is reinforcing YIN-essence benefit essence, and clearing away heat and promoting production of body fluid can tonifying five ZANG-organs asthenia, thick the intestines and stomach, strong muscles and bones, the arresting convulsion of calming the nerves, makes light of one's life by commiting suicide and prolongs life.Taoist school's health preserving classical works " Taoist Scriptures " are by Fu desert (Poria and Herba Cistanches), remote mountains Ganoderma, seabed Margarita and the Cordyceps of Herba Dendrobii, Herba Saussureae Involueratae, three double Radix Ginsengs, the hundred vicennial Radixs Polygoni Multiflori, cycle of sixty years and be called China's nine large Herba mesonae chinensis, and Herba Dendrobii ranks first.Herba Dendrobii nature and flavor: sweet, be slightly cold, enter stomach, kidney channel; Property belong to clear and rich, have benefit in clear, invigorating middle warmer has clearly.
The efficacy effect of Herba Dendrobii, successive dynasties well-known doctor respectively has discussion, specific as follows:
" explaining abstruseness of the canon of materia medica " cloud: " Herba Dendrobii, sweet energy is pleased spleen, salty can kidney tonifying, therefore many merits are dirty in water and soil two: but gas is wide slow, the merit of playing without victory, ancients with this tea, on very clear diaphragm in generation.”
Supplementary Amplifications of the Compendium of Materia Medica cloud: " Herba Dendrobii clearing stomach except deficiency-heat, promote the production of body fluid and strain, with for tea, merit with ginseng stilbene.”
" for tea, promote the production of body fluid and wet one's whistle summer, and reinforcing YIN-essence is good for sufficient power in " property of medicine ", to record Herba Dendrobii." visible, Herba Dendrobii is long-standing as the high tonic being of illnesses and fitness.The traditional Chinese medical science thinks, Herba Dendrobii can extensive use in the disease treatments such as atrophic gastritis, tumor, diabetes, pharyngolaryngitis and cataract.Herba Dendrobii has multiple pharmacological effect, and as the immunocompetence of enhancing body, antioxidation, defying age, reduce blood glucose, YIN nourishing and the production of body fluid promoting etc.The traditional Chinese medical science is thought, " YIN and YANG in a relative equilibrium, life activities being normally maintained." as cloudy body fluid deficiency void, can not contain sun, sun is floating, and without system, equilibrium between yin and yang is destroyed, and all diseases are grown thickly.”
" a Ling Shu Miraculous Pivot or Divine Axis Benshen section " said: " the main store essential substances person of the five internal organs also, can not hinder, and wound is fallen into enemy hands and the deficiency of YIN, depletion of QI of the deficiency of YIN, and depletion of QI is dead." Herba Dendrobii Yin-nourishing and body fluid promoting key medicine just, between old friend, be referred to as " help Herba mesonae chinensis ".
Shennong's Herbal: main damaging the spleen and stomach, eliminating impediment, the therapeutic method to keep the adverse QI flowing downwards, tonifying five ZANG-organs asthenia weakness and emaciation, reinforcing YIN-essence, take thick the intestines and stomach for a long time.
Compendium of Material Medica: reinforcing YIN-essence benefit essence.Clothes for a long time, thick the intestines and stomach, never sufficient in benefit, flat gastric qi, longue meat, by skin pathogenic heat miliaria gas, a little less than foot knee joint aches cold numbness, determines intelligence except frightened, makes light of one's life by commiting suicide and prolongs life.
" detailed outline is picked up any lost article from the road ": clearing stomach is except deficiency-heat, the strain in the sixth of the twelve Earthly Branches of promoting the production of body fluid, with for tea, appetite promoting and the spleen strengthening.Wind is treated in arresting convulsion, energy town saliva expectorant, sweet fragrant sending down the abnormal ascending QI.
" medicine justice ": control lung qi prolonged deficiency, cough is more than.
" not Lu ": benefit essence is never sufficient in mending, flat gastric qi, longue meat, by skin pathogenic heat gas, foot knee joint pain is weak, strong sun, the long-pending essence of the kidney invigorating.
" Japan hanako materia medica ": control deficient bad weak strengthening bone and muscle, warming the kidney, Fructus Alpiniae Oxyphyllae, flat gastric qi, by exogenous pathogen.
" book on Chinese herbal medicine is new again ": reason gastric qi, clearing stomach fire.Remove excessive thirst in the heart, treat kidney channel deficiency-heat, the arresting convulsion of calming the nerves, separates night sweat, and summer-heat can fall apart.
Herba Dendrobii also has external efficacy, modern scientific research shows, Herba Dendrobii is rich in polysaccharide, dendrobine, free amino acid, vitamin (vitamin A, vitamin C, vitamin E), chlorophyll and various enzyme, not only can pass through oral absorption, Herba Dendrobii can also stop blooding, promote wound healing, can be outward for repairing damaged skin.
Polysaccharide in A, Herba Dendrobii effect to skin.
That Dendrobium officinale polysaccharide has is antibacterial, the function of anti-inflammatory effect, enhancing Cell-mediated Immunity, and external can be resisted the infringement to skin such as dirt demodicid mite, antibacterial; Dendrobium officinale polysaccharide external can be stopped blooding, and can promote the growth of skin fiber albumen, thereby promotes wound healing, repairs damaged skin tissue.Theory of Chinese medical science is thought, Herba Dendrobii cold nature is the holy product of YIN nourishing, and skin is grown skin sore, acne, small pox etc. and mostly is due to hyperactivity of fire caused by deficiency of YIN, therefore Herba Dendrobii can be used for above-mentioned skin problem.
Free amino acid in B, Herba Dendrobii effect to skin.
Free amino acid can provide skin immune function controlling, regulates moisture, soda acid, Sage Extract, is improved the antiallergic ability of sensitive skin, prevents the generation of wrinkle; Activate the activity of Skin Cell superoxide dismutase peroxide, the free radical of dispelling Skin Cell surplus, effectively delay skin aging; The phagocytic function of activating macrophage, once strong lymphoid toxin expelling, function of detoxification, effectively blocks the infringement of extraneous harmful substance to skin; Improve resisting skin allergy ability, and harmful substance in body and aged cells are decomposed to excretion.Can with bivalent metal ion generation chelatropic reaction in wheat bran, stop the collagen protein generation crosslinked action in too much bivalent metal ion and skin, maintain enough collagen fiber and elastic fibers, make soft and smooth, the fine and smooth high resilience of skin.
The major function of the vitamin A in C, Herba Dendrobii.
Vitamin A, in vivo from the oxidative damage of different link antagonism radical pair cells, is strengthened the oxidation resistance of health, the harm that alleviates free radical; Contribute to keep skin soft and plentiful, improve the lock water function of skin; There is significantly anti-cornified effect, and energy delay skin aging, regulating action had in division and the development of Skin Cell; Help acne carried out to topical therapeutic, and prevent that pachylosis from chapping, chilblain and dandruff etc.; Contribute to strengthen metabolism, make skin keep younger state.
Vitamin C in D, Herba Dendrobii and vitamin E effect to skin.
Vitamin C, the effect of E aspect beauty and skin care are very important especially.Because the Oxidation of human body sebum is the one of the main reasons of skin aging, and vitamin E has antioxidation, thereby protect the moisture in sebum and cell membrane protein and skin; It can also promote regeneration and the vigor of human body cell, postpones the ageing process of cell.In addition, can also promote the utilization of human body to vitamin A; Can play synergism with vitamin C, the health of protection skin, reduces occurrence of skin infections; Collagen fiber in skin and elastic fibers are had to " moistening " effect, thereby improve and safeguard the elasticity of skin; Can promote the blood circulation in skin, make skin obtain sufficient nutrition and moisture, to maintain the tender and gloss of skin; Also can suppress the formation of pigmented spots, senile plaque, reduce facial wrinkles and pure white skin, prevent and treat acne.
Now also have the effective ingredient in Herba Dendrobii is applied on skin and is recorded, if open day is on 08 14th, 2013, publication number is in the Chinese patent of CN103239471A, a kind of skin moistening external preparation is disclosed, this skin moistening external preparation is made up of effective ingredient and medically acceptable adjuvant, described effective ingredient is that molecular weight is the Dendrobium officinale polysaccharide of 85-90KDa, only utilize the polysaccharide in Herba Dendrobii, the utilization rate of Herba Dendrobii is low, in addition, extract polysaccharide from Herba Dendrobii time, adopt to decoct and extracted, these three kinds of methods of supersound extraction and enzymolysis and extraction at 50 DEG C, these extracting method are for the vitamin of Herba Dendrobii, aminoacid, the destruction of the effective ingredient such as organized enzyme is comparatively serious.
Conventionally adopt at present the method decocting to extract the effective ingredient in Herba Dendrobii, traditional decoction extracting method can cause the destruction of the effective ingredient such as polysaccharide in Herba Dendrobii, vitamin, aminoacid, organized enzyme, polysaccharide in products obtained therefrom, vitamin, chlorophyll, free amino acid equal size are lower, greatly reduce the utilization rate of Herba Dendrobii.Now also there is no a kind of Herba Dendrobii mud facial film that can retain effective ingredient in Herba Dendrobii and preparation method thereof.
Summary of the invention
The object of the invention is to overcome above shortcomings in prior art, and provide one to retain as much as possible Herba Dendrobii effective ingredient, expand Herba Dendrobii application, give full play to Herba Dendrobii mud facial film of Herba Dendrobii value and preparation method thereof, this Herba Dendrobii mud facial film and preparation method thereof carries out lyophilization and superfine comminution at low temperature taking iron-sheet dendrobe fresh product as raw material, save the baking operation of traditional Herba Dendrobii, effective ingredient is difficult for destroyed, and the polysaccharide in products obtained therefrom, vitamin, chlorophyll, free amino acid equal size are high.
The present invention addresses the above problem adopted technical scheme: the feature of this Herba Dendrobii mud facial film is: this Herba Dendrobii mud facial film comprises that parts by weight are the water of 38～43 parts; Parts by weight are the dendrobium candidum ultrafine powder of 4～6 parts, contain polysaccharide, chlorophyll, vitamin and protein in this dendrobium candidum ultrafine powder; Parts by weight are the glycerol of 6～9 parts; Parts by weight are the Kaolin of 4～6 parts; Parts by weight are the cetearyl glucoside of 1～2 part; Parts by weight are the cetearyl alcohol of 3～5 parts; Parts by weight are the Dormant oils of 3～5 parts; Parts by weight are the mixture of the sad and tricaprin of 2～4 parts, and this sad and weight ratio tricaprin is 1:2; Parts by weight are polymethyl acid glyceride, propylene glycol and the Gantrez AN-119 of 2～4 parts, and the weight ratio of this polymethyl acid glyceride, propylene glycol and Gantrez AN-119 is 3:2:1; Parts by weight are the polydimethylsiloxane of 2～4 parts; Parts by weight are the spermol of 2～4 parts and the mixture of spermol polyethers-20, and the weight ratio of this spermol and spermol polyethers-20 is 1:1; Parts by weight are the Butyrospermum parkii (BUTYROSPERMUM PARKII) of 4～6 parts; Parts by weight are the mixture of PEG-75 stearate, spermol polyethers-20 and stearyl alcohol polyethers-20 of 3～5 parts, and the weight ratio of this PEG-75 stearate, spermol polyethers-20 and stearyl alcohol polyethers-20 is 1:1:2; Parts by weight are Aloe vulgaris (ALOE BARBADENSIS) leaf extract of 4～6 parts; Parts by weight are the xanthan gum of 0.2～0.4 part; Parts by weight are the glycyrrhizic acid dipotassium of 0.4～0.6 part; Parts by weight are the allantoin of 0.3～0.5 part; Parts by weight are the CI77492 of 0.3～0.5 part; Parts by weight are the CI77499 of 0.1～0.3 part; Parts by weight are the methyl hydroxybenzoate of 0.1～0.2 part; Parts by weight are the propyl hydroxybenzoate of 0.05～0.1 part; Parts by weight are the IPBC of 0.2～0.4 part and the mixture of dihydroxymethyl dimethyl hydantoin, and the weight ratio of this IPBC and dihydroxymethyl dimethyl hydantoin is 3:2.Make thus the scientific formulation of Herba Dendrobii mud facial film in the present invention, between composition, can produce synergism, the effect that contains polysaccharide, chlorophyll, vitamin and protein in Herba Dendrobii extract be can more effectively give play to, and the polysaccharide, chlorophyll, vitamin and the protein that in skin absorption Herba Dendrobii extract, contain have more been conducive to.
As preferably, dendrobium candidum ultrafine powder of the present invention is adopted with the following method and is made: the fresh Herba Dendrobii after cleaning is placed in to the boiling water 3～5min that sterilizes, takes out and be placed in water coolingly, then cut off, set drying chamber pressure 55～65Pa, putting dish, to put the fresh Herba Dendrobii amount of cut-out be 8～10kg/m
2, cold-trap circulation pipe Temperature Setting is-50 DEG C, pre-freeze Temperature Setting is-35～-50 DEG C, freeze-off time 8～9h, 40～42 DEG C of temperature of heating plate, 0.27～0.31 DEG C/min of rate of temperature fall, dry initial stage Temperature Setting is at 40～45 DEG C, and the later stage of drying Temperature Setting, at 35～40 DEG C, is dried 9h, after lyophilizing finishes, abolish vacuum toward nitrogen injection in hothouse or dry air, then shift out immediately material at relative humidity below 50% and discharging in the closed environment of 22～25 DEG C of temperature, the Herba Dendrobii of above-mentioned lyophilizing was pulverized to 100 eye mesh screens, obtained Herba Dendrobii powder, next carry out low temperature ultra micro comminution by gas stream, first ensure that the temperature of comminution by gas stream operation room is below 25 DEG C, relative humidity is below 50%, open air compressor and freezer dryer, compressed air is dewatered, after oil removing, deliver to air accumulator, in the time that air accumulator compressed air pressure reaches 0.8MPa, open pulverizing airflow line, make from air accumulator compressed air out through dedusting, filtration enters comminution by gas stream chamber, and make to pulverize stream pressure and reach 0.6～0.7MPa, then open feed stream pipeline, and make the pressure in feed stream pipeline reach 0.65～0.7MPa, after two strands of stream pressures are stable, open and adjust vibrations feeder, make Herba Dendrobii powder enter continuously pulverizing chamber, the superfine powder of pulverizing after up to standard enters in cyclone separator with air-flow, through separating to obtain dendrobium candidum ultrafine powder, the mean diameter of this dendrobium candidum ultrafine powder is 5.5～6.5 μ m, particle size distribution is between 0.87～15.27 μ m, pulverize yield 95～98%.
A preparation method for Herba Dendrobii mud facial film, its feature is: comprise successively following operation:
A pretreatment procedure,
A Herba Dendrobii ingredient requirement,
The Herba Dendrobii of gathering before blooming;
B sterilization,
Fresh Herba Dendrobii after cleaning is placed in the boiling water 3～5min that sterilizes, take out be placed in water cooling;
C cutting,
By Herba Dendrobii cutting;
B lyophilization operation,
Set drying chamber pressure 55～65Pa, putting dish, to put the fresh Herba Dendrobii amount of cut-out be 8～10kg/m
2, cold-trap circulation pipe Temperature Setting is-50 DEG C, pre-freeze Temperature Setting is-35～-50 DEG C, freeze-off time 8～9h, 40～42 DEG C of temperature of heating plate, 0.27～0.31 DEG C/min of rate of temperature fall; Dry initial stage Temperature Setting is at 40～45 DEG C, and the later stage of drying Temperature Setting, at 35～40 DEG C, is dried 9h;
C low temperature ultra micro comminution by gas stream operation,
After lyophilizing finishes, abolish vacuum toward nitrogen injection in hothouse or dry air, then shift out immediately material at relative humidity below 50% and discharging in the closed environment of 22～25 DEG C of temperature, the Herba Dendrobii of above-mentioned lyophilizing was pulverized to 100 eye mesh screens, obtained Herba Dendrobii powder, next carry out low temperature ultra micro comminution by gas stream, first ensure that the temperature of comminution by gas stream operation room is below 25 DEG C, relative humidity is below 50%, open air compressor and freezer dryer, compressed air is dewatered, after oil removing, deliver to air accumulator, in the time that air accumulator compressed air pressure reaches 0.8MPa, open pulverizing airflow line, make from air accumulator compressed air out through dedusting, filtration enters comminution by gas stream chamber, and make to pulverize stream pressure and reach 0.6～0.7MPa, then open feed stream pipeline, and make the pressure in feed stream pipeline reach 0.65～0.7MPa, after two strands of stream pressures are stable, open and adjust vibrations feeder, make Herba Dendrobii powder enter continuously pulverizing chamber, the superfine powder of pulverizing after up to standard enters in cyclone separator with air-flow, through separating to obtain dendrobium candidum ultrafine powder, the mean diameter of this dendrobium candidum ultrafine powder is 5.5～6.5 μ m, particle size distribution is between 0.87～15.27 μ m, pulverize yield 95～98%,
D emulsification process,
The oil phase of formula ratio is heated to 85 DEG C, maintains 30min sterilizing; The water of formula ratio is added to the water, is heated with stirring to 90～100 DEG C, maintain 30min sterilizing, be cooled to 85 DEG C; Oil phase is slowly added to stirring and emulsifying in water, obtains base material; In the time that the temperature of base material drops to 40～45 DEG C, dendrobium candidum ultrafine powder, CI77492, CI77499, methyl hydroxybenzoate, propyl hydroxybenzoate and IPBC/dihydroxymethyl dimethyl hydantoin are joined in base material, continue stirring and emulsifying 20min, carry out emulsifying 5min with homogenizer, leave standstill cooling 12～24 hours and become cream, stop stirring, cooling, obtains Herba Dendrobii mud facial film;
E fill operation,
Herba Dendrobii mud facial film is carried out to fill.
Make thus the course of processing of the whole dendrobium candidum ultrafine powder of the present invention, except instantaneously sterilising, all complete below at 30 DEG C, even if in the course of processing of Herba Dendrobii mud facial film, its temperature is also controlled at below 45 DEG C, has fully retained the various effective ingredient in Herba Dendrobii.
As preferably, in a Herba Dendrobii ingredient requirement of A pretreatment procedure of the present invention, Herba Dendrobii raw material is the Herba Dendrobii of 3 years trophophases.
As preferably, in the b sterilization of A pretreatment procedure of the present invention, in 200L caldron, add 150L purified water, heated and boiled, Herba Dendrobii first rinses 3 times with tap water, rinse 2 times by purified water again, by stainless steel clamp, Herba Dendrobii is put to the 3～5min that " quenches " in boiling water, take out in rearmounted purified water cooling.
As preferably, in B lyophilization operation of the present invention, for shortening drying time, need effectively supply with the ice crystal needed heat that distils, in single heating mode, the temperature of drying plate is controlled at 40～45 DEG C at the vigorous dry initial stage of distillation, is controlled at 60 DEG C dry mid-term, and the later stage of drying is controlled at 35～40 DEG C.
As preferably, in D emulsification process of the present invention, described oil phase comprises Kaolin, cetearyl glucoside, cetearyl alcohol, Dormant oils, caprylic/capric triglyceride, polymethyl acid glyceride and propylene glycol and Gantrez AN-119, polydimethylsiloxane, spermol and spermol polyethers-20, Butyrospermum parkii and allantoin.
As preferably, in D emulsification process of the present invention, described water comprises glycerol, xanthan gum, glycyrrhizic acid dipotassium and Aloe vulgaris.
As preferably, in E fill operation of the present invention, get the packaging material that disinfect, the Herba Dendrobii mud facial film being up to the standards is carried out to fill with mastic automatic filling machine, the loading amount of pouring process control product, overgauge is in 7.5%.
A kind of Herba Dendrobii mud facial film, its feature is: this Herba Dendrobii mud facial film adopts above-mentioned preparation method to be prepared from.
The present invention compared with prior art, has the following advantages and effect: can retain as much as possible the effective ingredient of Herba Dendrobii, expand its application, give full play to its value.The present invention carries out lyophilization and superfine comminution at low temperature taking iron-sheet dendrobe fresh product as raw material, save the baking operation of traditional Herba Dendrobii, effective ingredient is difficult for destroyed, products obtained therefrom polysaccharide, vitamin, chlorophyll, free amino acid equal size are high, and therefore the present invention has obvious advantage than traditional handicraft.
Preparation method in the present invention than the advantage of traditional disintegrating process is: sterilize taking iron-sheet dendrobe fresh product as raw material, section, lyophilization, coarse pulverization and low-temperature airflow super-micro wall-broken, gained superfine powder average particle size distribution between 5.5～6.5 μ m, i.e. 2000～2500 orders.According to the literature, Herba Dendrobii cell dia is 10～200 μ m, shows that the preparation method in the present invention breaks the cell wall of Herba Dendrobii substantially, and the utmost point is beneficial to the wherein release of effective ingredient and the absorption of human body.In the whole course of processing of dendrobium candidum ultrafine powder, except moment of sterilization process is high temperature, other techniques have all been followed low temperature principle, Dendrobium officinale polysaccharide can be fully preserved and 38～41% (" Chinese Pharmacopoeia " regulation Dendrobium officinale polysaccharide content is not less than 25%) can be reached, traditional processing technique (hot-air seasoning, pulverizing) gained fine powder particle diameter mostly is 38～75 μ m, and polyoses content is 30～35%.In addition, the Vitamin C content of gained dendrobium candidum ultrafine powder of the present invention reaches 34mg/100g (be traditional handicraft 15～20 times), chlorophyll content reaches 10mg/100g (traditional decoction extraction process almost make chlorophyll composition all destroyed), in sum, the present invention is with the obvious advantage.
The compositions such as polysaccharide in Herba Dendrobii of the present invention, chlorophyll, vitamin, aminoacid can absorb by skin, can be skin very abundant nutrition is provided, and its effect is above being set forth.Herba Dendrobii is many is at present widely used in health food and medicine as product for oral administration, and the present invention has opened up the application of Herba Dendrobii, has boundless market prospect.
Brief description of the drawings
Fig. 1 is the schematic flow sheet of the preparation method of Herba Dendrobii mud facial film in the embodiment of the present invention.
Fig. 2 is the schematic flow sheet of Herba Dendrobii extract preparation technology in the embodiment of the present invention.
Detailed description of the invention
Below in conjunction with accompanying drawing and by embodiment, the present invention is described in further detail, and following examples are explanation of the invention and the present invention is not limited to following examples.
Embodiment.
Referring to Fig. 1 to Fig. 2,
Table one dendrobium candidum ultrafine powder production technology and major parameter
Table two Herba Dendrobii mud face pack prescription
Remarks: in table two, " CN Translation " hurdle ratio used is weight ratio.
Finally determine preparation technology and the parameter of Herba Dendrobii mud facial film.
In the present embodiment, the preparation method of Herba Dendrobii mud facial film comprises following operation successively.
(1) pre-treatment.
1, Herba Dendrobii ingredient requirement.
Select the Herba Dendrobii of 3 years trophophases, and gathered when (April～June) before blooming.The experiment proved that, be the most vigorous period of Growth of Dendrobium candidum before florescence, Dendrobium officinale polysaccharide, vitamin, free amino acid, chlorophyll and other organized enzyme content are the highest in the whole year, and its epidermis and stem are all ferrum green, fiber content is low, is beneficial to and improves product extraction yield.
2, sterilization.
In 200L caldron, add 150L purified water, heated and boiled, rinses tap water for Herba Dendrobii 3 times, then rinses 2 times by purified water, puts the boiling water 3～5min that " quenches " with the appropriate Herba Dendrobii of rustless steel gripping, and taking-up is put in purified water cooling.
3, cutting.
Get the complete Herba Dendrobii of sterilization, cut into slices with medicine cutter, the speed control system of cutting is 150～180 times/min, and every segment length is controlled at 0.5～0.8cm, and the Herba Dendrobii section cutting is collected with the stainless steel cask of sterilizing, for subsequent use.
(2) freeze drying process and parameter.
Material choice → arrangement → prefreezing → sublimation drying → post processing → packaging, storage.
1, prefreezing.
Prefreezing is that premenstrual raw material after treatment is carried out to freezing processing, and it is the important procedure of lyophilizing.Due to biochemical change and the physicochemical change of Herba Dendrobii meeting generation series of complex in refrigerating process, therefore the quality of pre-freeze will directly have influence on the quality of lyophilizing.Set drying chamber pressure 55～65Pa, putting dish, to put fresh Herba Dendrobii amount be 8～10kg/m
2, cold-trap circulation pipe Temperature Setting is-50 DEG C, pre-freeze Temperature Setting is-35～-50 DEG C, freeze-off time 8～9h, 40～42 DEG C of temperature of heating plate, 0.27～0.31 DEG C/min of rate of temperature fall.
2, sublimation drying.
Sublimation drying is the core process in lyophylized food production process.Dry initial stage Temperature Setting is at 40～45 DEG C, and the later stage of drying Temperature Setting, at 35～40 DEG C, is dried 9h.When lyophilization, for shortening drying time, must effectively supply with the ice crystal needed heat that distils, in single heating mode, the temperature of drying plate should be controlled at 40～45 DEG C at the vigorous dry initial stage of distillation, is controlled at 60 DEG C dry mid-term, and the later stage of drying is controlled at 35～40 DEG C.
3, dry terminal point determining.
Temperature of charge and temperature of heating plate substantially reach unanimity and keep a period of time (normally keeping 20～30min); Pump group (or cold-trap) vacuometer and hothouse vacuometer reach unanimity, and keep a period of time (normally keeping 20～30min); Index when hothouse vacuometer condenser temperature is returned to equipment zero load substantially also keeps a period of time (normally keeping 20～30min).Above three judgment basis, both can be used alone, also use capable of being combined or combine use.
4, post processing.
Post processing comprises that discharging, semi-finished product sort, packaging and other steps.After lyophilizing finishes, abolish vacuum toward nitrogen injection in hothouse or dry air, then shift out immediately material at a relative humidity below 50%, 22～25 DEG C of temperature, discharging in the few closed environment of dust, and in identical environment, carry out half-finishedly sorting and packing.Because the material after lyophilizing has huge surface area, hygroscopicity is very strong, therefore need to, under a comparatively dry environment, complete the operation of these operations.
(3) low temperature ultra micro comminution by gas stream.
1, pretreatment.
Above-mentioned lyophilizing Herba Dendrobii was pulverized to 100 eye mesh screens with Chinese medicine grinder, with the transfer bag collection of sterilizing, for subsequent use.
2, low temperature ultra micro comminution by gas stream.
2.1, comminution by gas stream general introduction.
Compressed air, by after nozzle, produces high velocity air and near nozzle, forms very high velocity gradient, and the high turbulent flow of the supersonic speed producing by nozzle (450～500m/s) is as particulate vector.Material enters jet pipe through the ejector action of negative pressure, high pressure draught is done gyration and is formed powerful swirling eddy in pulverizing chamber with granule, between material particles, not only to clash into, and air-flow also will produce impact shear effect to material particles, simultaneously material also to impact with pulverizing chamber, friction, shear action.If the energy of collision exceedes the energy of granule interior needs, granule just will be pulverized.Pulverize qualified fine particle and shifted onto in cyclone separating chamber by air-flow, thicker granule continues to pulverize in pulverizing chamber, thereby reaches pulverizing object.
2.2, low temperature ultra micro comminution by gas stream general introduction.
Low-temperature airflow is pulverized by compressed air and is removed moisture, oil content, after purification, and be frozen into the dry air of-20～-10 DEG C, press again aforesaid operations procedure operation, the indoor temperature of whole comminution by gas stream is controlled at below 5 DEG C, greatly improves the storage rate of the nutritional labelings such as the interior vitamin of Herba Dendrobii, chlorophyll, enzyme.For food processing, the powder body that generally particle diameter is less than to 10～25 μ m calls superfine powder, therefore this technique is called " low temperature ultra micro comminution by gas stream ".
2.3, technique and parameter.
First ensure that the temperature of comminution by gas stream operation room is below 25 DEG C, relative humidity is below 50%.Open air compressor and freezer dryer, compressed air is dewatered, after oil removing, deliver to air accumulator, in the time that air accumulator compressed air pressure reaches 0.8MPa, open pulverizing airflow line, make from air accumulator compressed air out through dedusting, filtration enters comminution by gas stream chamber, and make to pulverize stream pressure and reach 0.6～0.7MPa, then open feed stream pipeline, and make its pressure reach 0.65～0.7MPa, after two strands of stream pressures are stable, open and adjust vibrations feeder, make Herba Dendrobii powder enter continuously pulverizing chamber, the superfine powder of pulverizing after up to standard enters in cyclone separator with air-flow, after separating, enter respectively elementary catcher and secondary catcher.Dendrobium candidum ultrafine powder mean diameter after low-temperature airflow is pulverized is 5.5～6.5 μ m, and particle size distribution is between 0.87～15.27 μ m, pulverizes yield 95～98%.
(4) emulsifying process and parameter.
By the oil phase of formula ratio (Kaolin, cetearyl glucoside, cetearyl alcohol, Dormant oils, caprylic/capric triglyceride, polymethyl acid glyceride (with) propylene glycol (with) Gantrez AN-119, polydimethylsiloxane, spermol (with) spermol polyethers-20, Butyrospermum parkii, stearyl alcohol polyethers-20, PEG-75 stearate/spermol polyethers-20/, allantoin) be heated to 85 DEG C, maintain 30min sterilizing; The water of formula ratio (glycerol, xanthan gum, glycyrrhizic acid dipotassium, Aloe vulgaris) raw material is joined in deionized water, be heated with stirring to 90～100 DEG C, maintain 30min sterilizing, be cooled to 85 DEG C; Oil phase is slowly added to stirring and emulsifying in water and obtains base material; In the time that the temperature of base material drops to 40～45 DEG C, dendrobium candidum ultrafine powder, CI77492, CI77499, methyl hydroxybenzoate, propyl hydroxybenzoate and IPBC/dihydroxymethyl dimethyl hydantoin are joined in base material, continue stirring and emulsifying 20min, carry out emulsifying 5min with homogenizer, leave standstill cooling 12～24 hours and become cream, stop stirring cooling, then censorship discharging, obtains Herba Dendrobii mud facial film.
The course of processing of whole dendrobium candidum ultrafine powder, except instantaneously sterilising, all completes at 30 DEG C below, even if in the course of processing of Herba Dendrobii mud facial film, its temperature is also controlled at below 45 DEG C, has fully retained the various effective ingredient in Herba Dendrobii.
(5) fill.
Get the packaging material that disinfect, the Herba Dendrobii mud facial film being up to the standards is carried out to fill with mastic automatic filling machine, the loading amount of pouring process control product, overgauge is in 7.5%.
Because current Herba Dendrobii product is main mainly with taking orally, the Herba Dendrobii mud facial film in the present invention has been expanded the application of Herba Dendrobii, brings into play more fully its value.
Embodiment 2.
Referring to Fig. 1 to Fig. 2, the Herba Dendrobii mud facial film in the present embodiment comprises that parts by weight are the water of 38～43 parts; Parts by weight are the dendrobium candidum ultrafine powder of 4～6 parts, contain polysaccharide, chlorophyll, vitamin and protein in this dendrobium candidum ultrafine powder; Parts by weight are the glycerol of 6～9 parts; Parts by weight are the Kaolin of 4～6 parts; Parts by weight are the cetearyl glucoside of 1～2 part; Parts by weight are the cetearyl alcohol of 3～5 parts; Parts by weight are the Dormant oils of 3～5 parts; Parts by weight are the mixture of the sad and tricaprin of 2～4 parts, and this sad and weight ratio tricaprin is 1:2; Parts by weight are polymethyl acid glyceride, propylene glycol and the Gantrez AN-119 of 2～4 parts, and the weight ratio of this polymethyl acid glyceride, propylene glycol and Gantrez AN-119 is 3:2:1; Parts by weight are the polydimethylsiloxane of 2～4 parts; Parts by weight are the spermol of 2～4 parts and the mixture of spermol polyethers-20, and the weight ratio of this spermol and spermol polyethers-20 is 1:1; Parts by weight are the Butyrospermum parkii (BUTYROSPERMUM PARKII) of 4～6 parts; Parts by weight are the mixture of PEG-75 stearate, spermol polyethers-20 and stearyl alcohol polyethers-20 of 3～5 parts, and the weight ratio of this PEG-75 stearate, spermol polyethers-20 and stearyl alcohol polyethers-20 is 1:1:2; Parts by weight are Aloe vulgaris (ALOEBARBADENSIS) leaf extract of 4～6 parts; Parts by weight are the xanthan gum of 0.2～0.4 part; Parts by weight are the glycyrrhizic acid dipotassium of 0.4～0.6 part; Parts by weight are the allantoin of 0.3～0.5 part; Parts by weight are the CI77492 of 0.3～0.5 part; Parts by weight are the CI77499 of 0.1～0.3 part; Parts by weight are the methyl hydroxybenzoate of 0.1～0.2 part; Parts by weight are the propyl hydroxybenzoate of 0.05～0.1 part; Parts by weight are the IPBC of 0.2～0.4 part and the mixture of dihydroxymethyl dimethyl hydantoin, and the weight ratio of this IPBC and dihydroxymethyl dimethyl hydantoin is 3:2.
Wherein, dendrobium candidum ultrafine powder is adopted with the following method and is made: the fresh Herba Dendrobii after cleaning is placed in to the boiling water 3～5min that sterilizes, takes out and be placed in water coolingly, then cut off, set drying chamber pressure 55～65Pa, putting dish, to put the fresh Herba Dendrobii amount of cut-out be 8～10kg/m
2, cold-trap circulation pipe Temperature Setting is-50 DEG C, pre-freeze Temperature Setting is-35～-50 DEG C, freeze-off time 8～9h, 40～42 DEG C of temperature of heating plate, 0.27～0.31 DEG C/min of rate of temperature fall, dry initial stage Temperature Setting is at 40～45 DEG C, and the later stage of drying Temperature Setting, at 35～40 DEG C, is dried 9h, after lyophilizing finishes, abolish vacuum toward nitrogen injection in hothouse or dry air, then shift out immediately material at relative humidity below 50% and discharging in the closed environment of 22～25 DEG C of temperature, the Herba Dendrobii of above-mentioned lyophilizing was pulverized to 100 eye mesh screens, obtained Herba Dendrobii powder, next carry out low temperature ultra micro comminution by gas stream, first ensure that the temperature of comminution by gas stream operation room is below 25 DEG C, relative humidity is below 50%, open air compressor and freezer dryer, compressed air is dewatered, after oil removing, deliver to air accumulator, in the time that air accumulator compressed air pressure reaches 0.8MPa, open pulverizing airflow line, make from air accumulator compressed air out through dedusting, filtration enters comminution by gas stream chamber, and make to pulverize stream pressure and reach 0.6～0.7MPa, then open feed stream pipeline, and make the pressure in feed stream pipeline reach 0.65～0.7MPa, after two strands of stream pressures are stable, open and adjust vibrations feeder, make Herba Dendrobii powder enter continuously pulverizing chamber, the superfine powder of pulverizing after up to standard enters in cyclone separator with air-flow, through separating to obtain dendrobium candidum ultrafine powder, the mean diameter of this dendrobium candidum ultrafine powder is 5.5～6.5 μ m, particle size distribution is between 0.87～15.27 μ m, pulverize yield 95～98%.
The scientific formulation of Herba Dendrobii mud facial film, reasonable in the present embodiment, between composition, can produce cooperative effect, effect of polysaccharide in Herba Dendrobii, chlorophyll, vitamin and protein be can more effectively give play to, and polysaccharide, chlorophyll, vitamin and protein in skin absorption Herba Dendrobii extract have more been conducive to.
Below the consumption of each composition in Herba Dendrobii mud facial film of the present invention is illustrated again, referring to table three.
Table three
Remarks: the each material amount used in table three is parts by weight; " title " hurdle ratio used is weight ratio.
In the present embodiment, the preparation method of Herba Dendrobii mud facial film comprises following operation successively:
A pretreatment procedure,
A Herba Dendrobii ingredient requirement,
The Herba Dendrobii of gathering before blooming, this Herba Dendrobii raw material is the Herba Dendrobii of 3 years trophophases.
B sterilization,
In 200L caldron, add 150L purified water, heated and boiled, Herba Dendrobii first rinses 3 times with tap water, then rinses 2 times by purified water, by stainless steel clamp, Herba Dendrobii is put to the 3～5min that " quenches " in boiling water, takes out in rearmounted purified water cooling.
C cutting,
By Herba Dendrobii cutting;
B lyophilization operation,
Set drying chamber pressure 55～65Pa, putting dish, to put the fresh Herba Dendrobii amount of cut-out be 8～10kg/m
2, cold-trap circulation pipe Temperature Setting is-50 DEG C, pre-freeze Temperature Setting is-35～-50 DEG C, freeze-off time 8～9h, 40～42 DEG C of temperature of heating plate, 0.27～0.31 DEG C/min of rate of temperature fall; Dry initial stage Temperature Setting is at 40～45 DEG C, and the later stage of drying Temperature Setting, at 35～40 DEG C, is dried 9h.
For shortening drying time, need effectively supply with the ice crystal needed heat that distils, in single heating mode, the temperature of drying plate is controlled at 40～45 DEG C at the vigorous dry initial stage of distillation, is controlled at 60 DEG C dry mid-term, and the later stage of drying is controlled at 35～40 DEG C.
C low temperature ultra micro comminution by gas stream operation,
After lyophilizing finishes, abolish vacuum toward nitrogen injection in hothouse or dry air, then shift out immediately material at relative humidity below 50% and discharging in the closed environment of 22～25 DEG C of temperature, the Herba Dendrobii of above-mentioned lyophilizing was pulverized to 100 eye mesh screens, obtained Herba Dendrobii powder, next carry out low temperature ultra micro comminution by gas stream, first ensure that the temperature of comminution by gas stream operation room is below 25 DEG C, relative humidity is below 50%, open air compressor and freezer dryer, compressed air is dewatered, after oil removing, deliver to air accumulator, in the time that air accumulator compressed air pressure reaches 0.8MPa, open pulverizing airflow line, make from air accumulator compressed air out through dedusting, filtration enters comminution by gas stream chamber, and make to pulverize stream pressure and reach 0.6～0.7MPa, then open feed stream pipeline, and make the pressure in feed stream pipeline reach 0.65～0.7MPa, after two strands of stream pressures are stable, open and adjust vibrations feeder, make Herba Dendrobii powder enter continuously pulverizing chamber, the superfine powder of pulverizing after up to standard enters in cyclone separator with air-flow, through separating to obtain dendrobium candidum ultrafine powder, the mean diameter of this dendrobium candidum ultrafine powder is 5.5～6.5 μ m, particle size distribution is between 0.87～15.27 μ m, pulverize yield 95～98%.
D emulsification process,
The oil phase of formula ratio is heated to 85 DEG C, maintains 30min sterilizing; The water of formula ratio is added to the water, is heated with stirring to 90～100 DEG C, maintain 30min sterilizing, be cooled to 85 DEG C; Oil phase is slowly added to stirring and emulsifying in water, obtains base material; In the time that the temperature of base material drops to 40～45 DEG C, dendrobium candidum ultrafine powder, CI77492, CI77499, methyl hydroxybenzoate, propyl hydroxybenzoate and IPBC/dihydroxymethyl dimethyl hydantoin are joined in base material, continue stirring and emulsifying 20min, carry out emulsifying 5min with homogenizer, leave standstill cooling 12～24 hours and become cream, stop stirring, cooling, obtains Herba Dendrobii mud facial film.
Oil phase in the present embodiment comprises Kaolin, cetearyl glucoside, cetearyl alcohol, Dormant oils, caprylic/capric triglyceride, polymethyl acid glyceride and propylene glycol and Gantrez AN-119, polydimethylsiloxane, spermol and spermol polyethers-20, Butyrospermum parkii, stearyl alcohol polyethers-20, PEG-75 stearate/spermol polyethers-20/ and allantoin; Water comprises glycerol, xanthan gum, glycyrrhizic acid dipotassium and Aloe vulgaris.
E fill operation,
Get the packaging material that disinfect, the Herba Dendrobii mud facial film being up to the standards is carried out to fill with mastic automatic filling machine, the loading amount of pouring process control product, overgauge is in 7.5%.
The invention still further relates to a kind of Herba Dendrobii mud facial film being made by above-mentioned preparation method, adopt the Herba Dendrobii mud facial film that above-mentioned preparation method makes can be directly used on skin, the compositions such as polysaccharide, chlorophyll, vitamin and protein in Herba Dendrobii can be absorbed by the body by skin, can be skin very abundant nutrition is provided, expand the application of Herba Dendrobii, brought into play more fully its value.
The course of processing of whole dendrobium candidum ultrafine powder in the present embodiment, except instantaneously sterilising, all complete below at 30 DEG C, even if in the course of processing of Herba Dendrobii mud facial film, its temperature is also controlled at below 45 DEG C, has fully retained the various effective ingredient in Herba Dendrobii.The preparation method of this Herba Dendrobii mud facial film retains Herba Dendrobii effective ingredient as much as possible, expands its application, gives full play to its value.The present invention carries out lyophilization and superfine comminution at low temperature taking iron-sheet dendrobe fresh product as raw material, save the baking operation of traditional Herba Dendrobii, effective ingredient is difficult for destroyed, products obtained therefrom polysaccharide, vitamin, chlorophyll, free amino acid equal size are high, and therefore the present invention has obvious advantage than traditional handicraft.
Although the present invention with embodiment openly as above; but it is not in order to limit protection scope of the present invention; any technical staff who is familiar with this technology, not departing from change and the retouching done in the spirit and scope of the present invention, all should belong to protection scope of the present invention.
Claims (10)
1. a Herba Dendrobii mud facial film, is characterized in that: this Herba Dendrobii mud facial film comprises that parts by weight are the water of 38～43 parts; Parts by weight are the dendrobium candidum ultrafine powder of 4～6 parts, contain polysaccharide, chlorophyll, vitamin and protein in this dendrobium candidum ultrafine powder; Parts by weight are the glycerol of 6～9 parts; Parts by weight are the Kaolin of 4～6 parts; Parts by weight are the cetearyl glucoside of 1～2 part; Parts by weight are the cetearyl alcohol of 3～5 parts; Parts by weight are the Dormant oils of 3～5 parts; Parts by weight are the mixture of the sad and tricaprin of 2～4 parts, and this sad and weight ratio tricaprin is 1:2; Parts by weight are polymethyl acid glyceride, propylene glycol and the Gantrez AN-119 of 2～4 parts, and the weight ratio of this polymethyl acid glyceride, propylene glycol and Gantrez AN-119 is 3:2:1; Parts by weight are the polydimethylsiloxane of 2～4 parts; Parts by weight are the spermol of 2～4 parts and the mixture of spermol polyethers-20, and the weight ratio of this spermol and spermol polyethers-20 is 1:1; Parts by weight are the Butyrospermum parkii of 4～6 parts; Parts by weight are the mixture of PEG-75 stearate, spermol polyethers-20 and stearyl alcohol polyethers-20 of 3～5 parts, and the weight ratio of this PEG-75 stearate, spermol polyethers-20 and stearyl alcohol polyethers-20 is 1:1:2; Parts by weight are the Aloe vulgaris leaf extract of 4～6 parts; Parts by weight are the xanthan gum of 0.2～0.4 part; Parts by weight are the glycyrrhizic acid dipotassium of 0.4～0.6 part; Parts by weight are the allantoin of 0.3～0.5 part; Parts by weight are the CI77492 of 0.3～0.5 part; Parts by weight are the CI77499 of 0.1～0.3 part; Parts by weight are the methyl hydroxybenzoate of 0.1～0.2 part; Parts by weight are the propyl hydroxybenzoate of 0.05～0.1 part; Parts by weight are the IPBC of 0.2～0.4 part and the mixture of dihydroxymethyl dimethyl hydantoin, and the weight ratio of this IPBC and dihydroxymethyl dimethyl hydantoin is 3:2.
2. Herba Dendrobii mud facial film according to claim 1, it is characterized in that: described dendrobium candidum ultrafine powder is adopted with the following method and made: the fresh Herba Dendrobii after cleaning is placed in to the boiling water 3～5min that sterilizes, taking-up is placed in water cooling, then cuts off, set drying chamber pressure 55～65Pa, putting dish, to put the fresh Herba Dendrobii amount of cut-out be 8～10kg/m
2, cold-trap circulation pipe Temperature Setting is-50 DEG C, pre-freeze Temperature Setting is-35～-50 DEG C, freeze-off time 8～9h, 40～42 DEG C of temperature of heating plate, 0.27～0.31 DEG C/min of rate of temperature fall, dry initial stage Temperature Setting is at 40～45 DEG C, and the later stage of drying Temperature Setting, at 35～40 DEG C, is dried 9h, after lyophilizing finishes, abolish vacuum toward nitrogen injection in hothouse or dry air, then shift out immediately material at relative humidity below 50% and discharging in the closed environment of 22～25 DEG C of temperature, the Herba Dendrobii of above-mentioned lyophilizing was pulverized to 100 eye mesh screens, obtained Herba Dendrobii powder, next carry out low temperature ultra micro comminution by gas stream, first ensure that the temperature of comminution by gas stream operation room is below 25 DEG C, relative humidity is below 50%, open air compressor and freezer dryer, compressed air is dewatered, after oil removing, deliver to air accumulator, in the time that air accumulator compressed air pressure reaches 0.8MPa, open pulverizing airflow line, make from air accumulator compressed air out through dedusting, filtration enters comminution by gas stream chamber, and make to pulverize stream pressure and reach 0.6～0.7MPa, then open feed stream pipeline, and make the pressure in feed stream pipeline reach 0.65～0.7MPa, after two strands of stream pressures are stable, open and adjust vibrations feeder, make Herba Dendrobii powder enter continuously pulverizing chamber, the superfine powder of pulverizing after up to standard enters in cyclone separator with air-flow, through separating to obtain dendrobium candidum ultrafine powder, the mean diameter of this dendrobium candidum ultrafine powder is 5.5～6.5 μ m, particle size distribution is between 0.87～15.27 μ m, pulverize yield 95～98%.
3. a preparation method for Herba Dendrobii mud facial film, is characterized in that: comprise successively following operation:
A pretreatment procedure,
A Herba Dendrobii ingredient requirement,
The Herba Dendrobii of gathering before blooming;
B sterilization,
Fresh Herba Dendrobii after cleaning is placed in the boiling water 3～5min that sterilizes, take out be placed in water cooling;
C cutting,
By Herba Dendrobii cutting;
B lyophilization operation,
Set drying chamber pressure 55～65Pa, putting dish, to put the fresh Herba Dendrobii amount of cut-out be 8～10kg/m
2, cold-trap circulation pipe Temperature Setting is-50 DEG C, pre-freeze Temperature Setting is-35～-50 DEG C, freeze-off time 8～9h, 40～42 DEG C of temperature of heating plate, 0.27～0.31 DEG C/min of rate of temperature fall; Dry initial stage Temperature Setting is at 40～45 DEG C, and the later stage of drying Temperature Setting, at 35～40 DEG C, is dried 9h;
C low temperature ultra micro comminution by gas stream operation,
After lyophilizing finishes, abolish vacuum toward nitrogen injection in hothouse or dry air, then shift out immediately material at relative humidity below 50% and discharging in the closed environment of 22～25 DEG C of temperature, the Herba Dendrobii of above-mentioned lyophilizing was pulverized to 100 eye mesh screens, obtained Herba Dendrobii powder, next carry out low temperature ultra micro comminution by gas stream, first ensure that the temperature of comminution by gas stream operation room is below 25 DEG C, relative humidity is below 50%, open air compressor and freezer dryer, compressed air is dewatered, after oil removing, deliver to air accumulator, in the time that air accumulator compressed air pressure reaches 0.8MPa, open pulverizing airflow line, make from air accumulator compressed air out through dedusting, filtration enters comminution by gas stream chamber, and make to pulverize stream pressure and reach 0.6～0.7MPa, then open feed stream pipeline, and make the pressure in feed stream pipeline reach 0.65～0.7MPa, after two strands of stream pressures are stable, open and adjust vibrations feeder, make Herba Dendrobii powder enter continuously pulverizing chamber, the superfine powder of pulverizing after up to standard enters in cyclone separator with air-flow, through separating to obtain dendrobium candidum ultrafine powder, the mean diameter of this dendrobium candidum ultrafine powder is 5.5～6.5 μ m, particle size distribution is between 0.87～15.27 μ m, pulverize yield 95～98%,
D emulsification process,
The oil phase of formula ratio is heated to 85 DEG C, maintains 30min sterilizing; The water of formula ratio is added to the water, is heated with stirring to 90～100 DEG C, maintain 30min sterilizing, be cooled to 85 DEG C; Oil phase is slowly added to stirring and emulsifying in water, obtains base material; In the time that the temperature of base material drops to 40～45 DEG C, dendrobium candidum ultrafine powder, CI77492, CI77499, methyl hydroxybenzoate, propyl hydroxybenzoate and IPBC/dihydroxymethyl dimethyl hydantoin are joined in base material, continue stirring and emulsifying 20min, carry out emulsifying 5min with homogenizer, leave standstill cooling 12～24 hours and become cream, stop stirring, cooling, obtains Herba Dendrobii mud facial film;
E fill operation,
Herba Dendrobii mud facial film is carried out to fill.
4. the preparation method of Herba Dendrobii mud facial film according to claim 3, is characterized in that: in a Herba Dendrobii ingredient requirement of described A pretreatment procedure, Herba Dendrobii raw material is the Herba Dendrobii of 3 years trophophases.
5. the preparation method of Herba Dendrobii mud facial film according to claim 3, it is characterized in that: in the b sterilization of described A pretreatment procedure, in 200L caldron, add 150L purified water, heated and boiled, Herba Dendrobii first rinses 3 times with tap water, rinse 2 times by purified water again, by stainless steel clamp, Herba Dendrobii is put to the 3～5min that " quenches " in boiling water, take out in rearmounted purified water cooling.
6. the preparation method of Herba Dendrobii mud facial film according to claim 3, it is characterized in that: in described B lyophilization operation, for shortening drying time, need effectively supply with the ice crystal needed heat that distils, in single heating mode, the temperature of drying plate is controlled at 40～45 DEG C at the vigorous dry initial stage of distillation, is controlled at 60 DEG C dry mid-term, and the later stage of drying is controlled at 35～40 DEG C.
7. the preparation method of Herba Dendrobii mud facial film according to claim 3, it is characterized in that: in described D emulsification process, described oil phase comprises Kaolin, cetearyl glucoside, cetearyl alcohol, Dormant oils, caprylic/capric triglyceride, polymethyl acid glyceride and propylene glycol and Gantrez AN-119, polydimethylsiloxane, spermol and spermol polyethers-20, Butyrospermum parkii and allantoin.
8. the preparation method of Herba Dendrobii mud facial film according to claim 3, is characterized in that: in described D emulsification process, described water comprises glycerol, xanthan gum, glycyrrhizic acid dipotassium and Aloe vulgaris.
9. the preparation method of Herba Dendrobii mud facial film according to claim 3, it is characterized in that: in described E fill operation, get the packaging material that disinfect, the Herba Dendrobii mud facial film being up to the standards is carried out to fill with mastic automatic filling machine, the loading amount of pouring process control product, overgauge is in 7.5%.
10. a Herba Dendrobii mud facial film, is characterized in that: this Herba Dendrobii mud facial film adopts the preparation method as described in claim 3-9 to be prepared from.
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| CN107157892A (en) * | 2017-06-22 | 2017-09-15 | 西林县大银子铁皮石斛种销农民专业合作社 | It is a kind of to be used to repair dendrobium candidum clay mask of acne print and preparation method thereof |
| CN108785117A (en) * | 2018-07-25 | 2018-11-13 | 广州依露美化妆品有限公司 | A kind of fair-skinned bright white Pure natural mask |
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Application publication date: 20141022 |