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CN105616286A - Formula of wild-relative dendrobium officinale fresh juice facial mask and preparation method thereof - Google Patents

Formula of wild-relative dendrobium officinale fresh juice facial mask and preparation method thereof Download PDF

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Publication number
CN105616286A
CN105616286A CN201610016644.9A CN201610016644A CN105616286A CN 105616286 A CN105616286 A CN 105616286A CN 201610016644 A CN201610016644 A CN 201610016644A CN 105616286 A CN105616286 A CN 105616286A
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herba dendrobii
dendrobium officinale
parts
nearly
fresh
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方玉占
王升贵
蒋正剑
魏明泽
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Hangzhou Tai Rentang Biological Polytron Technologies Inc
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Hangzhou Tai Rentang Biological Polytron Technologies Inc
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    • AHUMAN NECESSITIES
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    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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    • A61K8/55Phosphorus compounds
    • A61K8/553Phospholipids, e.g. lecithin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
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Abstract

The invention provides a formula of a wild-relative dendrobium officinale fresh juice facial mask and a preparation method thereof. The preparation method comprises the steps of extracting fresh materials, namely steaming and sterilizing wild-relative dendrobium officinale, carrying out ultra-fine grinding with a grinder, carrying out pumping filtration with a 200-mesh screen, and mixing and emulsifying filtrate and other components. The invention has remarkable advantages in raw material selection, formula compatibility, processing technology, product preparation and other fields in comparison with similar products in the market, and has excellent market prospects.

Description

A kind of nearly fresh juice facial mask formula of dendrobium officinale and method for making thereof
Technical field
The invention belongs to medicinal plants manufacture field, be specifically related to a kind of nearly fresh juice facial mask formula of dendrobium officinale and method for making thereof.
Background technology
1.1 Herba Dendrobii summaries
Herba Dendrobii, perennial the orchid family herbaceous plant, it is divided into Herba Dendrobii, Dendrobium nobile, dendrobium loddigesii Rolfe, HERBA DENDROBII, Herba Dendrobii oculati etc. more than 70 to plant by kind preciousness degree, wherein Herba Dendrobii is come out top. Herba Dendrobii (DendrobiumofficinaleKimuraetMigo) is Chinese Second Class Key Protected Plant, has extraordinary health preserving and medical value. In the culture of health preserving that China is long, Herba Dendrobii, because of its outstanding effect, becomes ancient Chinese medicine doctor and the health preserving superfine product of nobility's high praise.
In the Shennong's Herbal in Eastern Han Dynasty's last years of a dynasty or reign, in connection with in the record of Herba Dendrobii. Product above are all included wherein, are claimed its " tonifying five ZANG-organs asthenia, manages gastric qi, controls deficient labor weak, and clothes are made light of one's life by commiting suicide for a long time, prolongs life, and sedate is except frightened " by successive dynasties famous doctor's allusion quotations such as the Chinese " Mingyi Bielu ", bright Compendium of Material Medica and clear essentials of Matea Medica.
Taoist school doctor's allusion quotation " Taoist Scriptures " between Katyuan year the Tang Dynasty, iron sheet stone is pushed into the first place of " nine big Herba mesonae chinensis ", before being listed in Herba Saussureae Involueratae, three double Radix Ginsengs, the hundred vicennial Radixs Polygoni Multiflori, the Poria of cycle of sixty years, Herba Cistanches, remote mountains Ganoderma, seabed Margarita, Cordyceps, it is seen that medicinal effects is extraordinary. Successive dynasties well-known doctor such as Huatuo, Zhang Zhongjing, Sun Simiao, Li Shizhen (1518-1593 A.D.) etc. are considered as " in medicine celestial product " it especially, are used for curing critical patient.
Since the Tang and Song Dynasty, Herba Dendrobii is just listed in tribute, for royalty's life lengthening, becomes health preserving superfine product the most honorable. According to Historical Data Data About, Wu Tse-tien took the party for 50 years, and year still preserves agerasia to old age; Qianrong Supreme Being's group minister of often feting must drink Herba Dendrobii soup, 60 years in place, becomes the emperor that the time is the longest, the longevity in year is the highest that holds power on Chinese history, and effect of Herba Dendrobii life prolonging is as can be seen here.
Herba Dendrobii nature and flavor: sweet, are slightly cold, and enter stomach, kidney channel. Property belong to clear and rich, have benefit in clear, invigorating middle warmer has clearly.
The efficacy effect of Herba Dendrobii, the successive dynasties, well-known doctor was respectively arranged with discussion:
" explaining abstruseness of the canon of materia medica " cloud: " Herba Dendrobii, sweet energy pleases spleen, salty energy kidney tonifying, therefore many merits are dirty in water and soil two: but gas width delays, and without the merit that victory is played, ancients are with this generation tea, on very clear diaphragm. "
Supplementary Amplifications of the Compendium of Materia Medica cloud: " Herba Dendrobii clearing stomach except deficiency-heat, promote the production of body fluid and strain, with for tea, merit is with joining stilbene. "
In " property of medicine ", load Herba Dendrobii " for tea, promote the production of body fluid and wet one's whistle, reinforcing YIN-essence strong foot power by summer. " visible, Herba Dendrobii is long-standing as the high tonic being of illnesses and fitness. The traditional Chinese medical science is thought, Herba Dendrobii can extensive use in the disease treatments such as atrophic gastritis, tumor, diabetes, pharyngolaryngitis and cataract. Herba Dendrobii has multiple pharmacological effect, such as the immunocompetence of enhancing body, antioxidation, defying age, reduction blood glucose, YIN nourishing and the production of body fluid promoting etc. The traditional Chinese medical science is thought, " YIN and YANG in a relative equilibrium, life activities being normally maintained. " as empty in cloudy body fluid deficiency, it is impossible to containing sun, sun is floating without system, and equilibrium between yin and yang is destroyed, then all diseases are grown thickly. "
" Ling Shu Miraculous Pivot or Divine Axis Benshen's section " is said: " the main store essential substances person of the five internal organs also, can not hinder, and wound is then fallen into enemy hands and the deficiency of YIN, the deficiency of YIN then depletion of QI, and depletion of QI is then dead. " Herba Dendrobii Yin-nourishing and body fluid promoting key medicine just, the human world thus be referred to as " help Herba mesonae chinensis ".
Shennong's Herbal: main damaging the spleen and stomach, eliminating impediment, the therapeutic method to keep the adverse QI flowing downwards, tonifying five ZANG-organs asthenia weakness and emaciation, the thick the intestines and stomach of reinforcing YIN-essence, for a long time clothes.
Compendium of Material Medica: reinforcing YIN-essence benefit essence. Clothes for a long time, thick the intestines and stomach, never sufficient in benefit, flat gastric qi, longue meat, by skin pathogenic heat miliaria gas, it is weak that foot knee joint aches cold numbness, determines intelligence except frightened, makes light of one's life by commiting suicide and prolong life.
" detailed outline is picked up any lost article from the road ": clearing stomach remove deficiency-heat, promote the production of body fluid the sixth of the twelve Earthly Branches strain, with for tea, appetite promoting and the spleen strengthening. Wind, energy town saliva expectorant, sweet virtue sending down the abnormal ascending QI are treated in arresting convulsion.
" medicineization justice ": controlling lung qi prolonged deficiency, cough is more than.
" not Lu ": benefit essence is never sufficient in mending, flat gastric qi, longue meat, by skin pathogenic heat gas, foot knee joint pain weakness, strong sun, the long-pending essence of the kidney invigorating.
" Japan hanako materia medica ": controlling deficient bad weak strengthening bone and muscle, warming the kidney, Fructus Alpiniae Oxyphyllae, flat gastric qi, by exogenous pathogen.
" book on Chinese herbal medicine is new again ": reason gastric qi, clearing stomach fire. Except excessive thirst, treatment kidney channel deficiency-heat, arresting convulsion of calming the nerves in the heart, solve night sweat, summer-heat can be dissipated.
1.2 Herba Dendrobii efficacy studies
Modern medicine study shows, Herba Dendrobii has Yin-nourishing and body fluid promoting, health invigorating, strengthens the spleen and stomach, hepatoprotective function of gallbladder promoting, bone and muscle strengthening, reduction blood glucose, suppress tumor, promote circulation, bright eyes, nourish the effects such as skin. Suitable at the beginning of daily health caring, prolonged illness more, impairment of YIN of staying up late, dinner party drink, fatigue of driving.
1.2.1 tonify Qi of the kidney
Qing Dynasty's " property of medicine opinion " says that essence, nourishing stomach-YIN, physical strength profiting are amassed in Herba Dendrobii energy the kidney invigorating. Modern medicine shows, Herba Dendrobii takes a tonic or nourishing food to build up one's health renal system, carries nutrition for systemic circulation, makes QI and blood, spirit sufficient, indefatigability.
1.2.2 lung heat clearing toxin expelling
Qing Dynasty's well-known doctor's ZHAO Xue-Min records Herba Dendrobii " strain in the sixth of the twelve Earthly Branches of promoting the production of body fluid " in supplementary Amplifications of the Compendium of Materia Medica. Be meant to Herba Dendrobii and can promote the generation of internal water liquid, conditioning weakness caused by the five internal organs fatigue, have promote the production of body fluid, lung moistening, toxin expelling effect.
1.2.3 hepatoprotective function of gallbladder promoting
Ancient Chinese medicine doctor all thinks that " Herba Dendrobii " has the effect of nourishing hepatic yin, is the rare medicinal herbs treating various liver-gallbladder disease, and the treatment being beneficial to the liver and gall diseases such as hepatitis, cholecystitis, cholelithiasis recovers. The antioxidation of Herba Dendrobii can reduce the damage of internal liver function, simultaneously by the function of hepatoprotective, clearing heat secreting bile, the preventing and treating of liver-gallbladder disease is had unique auxiliary curative effect.
1.2.4 tumor is suppressed
Some cell of the malignant tumor such as pulmonary carcinoma, ovarian cancer and promyelocytic leukemia is had killing action by Herba Dendrobii, has stronger anti-tumor activity. Clinical experiment shows, Herba Dendrobii, for the auxiliary treatment of malignant tumor, can improve the symptom of tumor patient, alleviates the side effect of Radiotherapy chemotherapy, enhancing immunity, improves life quality, extends life span.
1.2.5 bright eyes
The traditional Chinese medical science is thought, the vital essence of the vital organs of the human body is all passed through on arteries and veins, notes in eyes, and whether vigorous the physiological and pathological of liver " having one's ideas straightened out in order " eyes is in close relations in the cloudy essence of liver, and Herba Dendrobii has YIN nourishing to support purpose function, by the ancient Chinese medicine doctor good merchantable brand as eye-protecting. Modern pharmacology research confirms: Herba Dendrobii does not only have retarding action to preventing and treating senile cataract, it is possible to keep lenticular transparency 36.8%, and the enzymatic activity ANOMALOUS VARIATIONS caused by galactose has suppression or role of correcting.
1.2.6 blood glucose is reduced
The traditional Chinese medical science is thought, the generation of diabetes (diabetes), and mainly with deficiency of the kidney yin, lung stomach early heat is basic pathogenesis, and with deficiency of both QI and YIN for its pathological characteristic, Herba Dendrobii replenishing YIN and removing heat is moisturized, and treats the medicine dedicated of diabetes since ancient times exactly. Clinical research shows, Herba Dendrobii is possible not only to strengthen insulin active, can significantly reduce blood sugar level simultaneously, make blood sugar recovery normal.
1.2.7 strong muscle blood fat reducing
After people enters the middle age, cloudy Tianjin of " people's half of YIN QI consumed " human body starts weak, and muscles and bones function is faded, Herba Dendrobii energy vital essence replenishing, lubricating joint, thus reaching strengthening the tendons and bones, fluent joint, strengthening antiheumatic effect. Modern pharmacological research shows, Herba Dendrobii can improve stress ability, has good resisting fatigue, resisting oxygen lack; Can be made moist sering, expands blood vessel, thus blood circulation promoting, significantly improves blood stasis symptom, reduces cholesterolemia and triglyceride, it is provided that high density lipoprotein sterol levels, it is possible to treatment blood cerebrovascular disease.
1.2.8 reinforcing stomach reg fluid
Herba Dendrobii reinforcing stomach reg fluid, all on the books in Shennong's Herbal, " book on Chinese herbal medicine is new again ", it is called " medicine for enterogastritis ". Modern medicine confirms, pathogenic bacterium helicobacter pylori common in the spleen-stomach disease is had good inhibiting effect by Herba Dendrobii, contributes to the disease of the Helicobacter pyloris such as treatment atrophic gastritis, superficial gastritis, duodenal ulcer; Oral Herba Dendrobii decocting liquid can promote the secretion of gastric juice simultaneously, strengthens the emptying ability of stomach, helps digest.
1.2.9 slow down aging
Herba Dendrobii is classified as by Shennong's Herbal has the panacea that " make light of one's life by commiting suicide and prolong life " acts on. After human body enters the middle age, internal cloudy liquid reduces day by day, and skin is aging rapidly. Herba Dendrobii can promote the generation of blood of human body, body fluid, body fluid, nourishes rough skin. Modern pharmacology research confirms: Herba Dendrobii contains various trace elements, and the good health and a long life for human body have close relationship, to the anti-aging effects of human body than general medicine more extensively, more comprehensively.
1.2.10 sleep is improved
The traditional Chinese medical science thinks that the cause of disease of chronic insomnia is that yin and yang imbalance, the deficiency of YIN can not suppress yang hyperactivity fire to move to cause. Herba Dendrobii just has the magical effect of " tonifying five ZANG-organs asthenia ", by YIN nourishing qi-restoratives, fundamentally solves solidity insomnia problem.
1.3 nearly dendrobium officinale
The planting patterns of Herba Dendrobii is varied, has potted plant growth, the plantation of booth seedbed, basswood plantation, attached tree planting etc. Yueqing City Herba Dendrobii association is declaring of specification Herba Dendrobii planting patterns, the planting patterns imitating dendrobium officinale growing environment is referred to as " nearly wild planting ", utilizes the Herba Dendrobii that this planting patterns is planted to become nearly dendrobium officinale. Dendrobium officinale is often grown in, on the overhanging cliff away from signs of human habitation or old trees that reach into the skies, growing in its natural state. Nearly dendrobium officinale alleged by this patent is exactly simulate environment and the growth pattern of dendrobium officinale, planting base selects in the mountain region luxuriant with concentrating residential block (guaranteeing that water quality, air, soil are not contaminated), vegetation away from industrial occupancy or forest land, Herba Dendrobii is directly planted on the live body tree in field, and has passed through GAP (GAP) and organic products certification. Herba Dendrobii planting process in the present invention does not use chemical fertilizer and pesticide, polysaccharide content of dendrobium candidum is up to 39.6% (States Pharmacopoeia specifications polysaccharide content of dendrobium candidum standard is 25%), EN that is rare and that be referred to as " anticancer factor " can also be detected, be the upper product in Herba Dendrobii.
2 Herba Dendrobii external efficacies
Modern scientific research shows, Herba Dendrobii is rich in polysaccharide, dendrobine, free amino acid, vitamin (vitamin A, vitamin C, vitamin E), chlorophyll and various enzyme, not only by oral absorption, Herba Dendrobii can also stop blooding, promote wound healing, can be used for outward repairing damaged skin. Traditional decoction extracting method can cause the destruction of the compositions such as vitamin in Herba Dendrobii, aminoacid, organized enzyme; Gu Benfamingte adopts low-temperature extraction technology; Dendrobium officinale polysaccharide, dendrobine, aminoacid are at utmost extracted, protects the compositions such as Herba Dendrobii Determination of Chlorophyll, vitamin and organized enzyme from high temperature simultaneously. And owing to Herba Dendrobii product is many to take orally, the present invention has expanded its application, substantially more play it and be worth.
2.1 Dendrobium officinale polysaccharides effect to skin
Dendrobium officinale polysaccharide has function antibacterial, anti-inflammatory effect, enhancing Cell-mediated Immunity, and external can resist the infringement to skin such as dust mite, antibacterial; Dendrobium officinale polysaccharide external can be stopped blooding, and can promote the growth of skin fiber albumen, thus promoting wound healing, repairs damaged skin tissue. Theory of Chinese medical science is thought, Herba Dendrobii cold nature, is YIN nourishing sage's product, and skin is grown skin sore, acne, small pox etc. and mostly is caused by hyperactivity of fire caused by deficiency of YIN, therefore Herba Dendrobii can be used for above-mentioned skin problem.
2.2 free amino acids effect to skin
Free amino acid can provide skin immune function controlling, regulates moisture, soda acid, Sage Extract, has the antiallergic ability improving sensitive skin, it is prevented that the generation of wrinkle; Activate the activity of Skin Cell superoxide dismutase peroxide, dispel the free radical that Skin Cell is superfluous, effective delay skin aging; The phagocytic function of activating macrophage, once strong lymphoid toxin expelling, function of detoxification, effectively block the extraneous harmful substance infringement to skin; Improve resisting skin allergy ability, and internal harmful substance and aged cells are decomposed excretion. With bivalent metal ion generation chelatropic reaction in wheat bran, too much bivalent metal ion and the collagen protein generation crosslinked action in skin can be stoped, maintain enough collagen fiber and elastic fiber, make skin slip, fine and smooth high resilience.
The major function of 2.3 vitamin A
Vitamin A from the oxidative damage of different link antagonism radical pair cells, is strengthened the oxidation resistance of health, is alleviated the harm of free radical in vivo; Help maintenance skin emolliency and plentiful, improve the lock water function of skin; Having significantly anti-cornified effect energy delay skin aging, division and development at Skin Cell have adjustment effect; Help and acne carried out local treatment, and prevent pachylosis from chapping, chilblain and dandruff etc.; Contribute to strengthening metabolism, make the state that skin maintenance is younger.
2.4 vitamin Cs and vitamin E effect to skin
Injection Vitamin B_6 effect in beauty and skin care is very important especially. Because the Oxidation of human sebaceous is the one of the main reasons of skin aging, and vitamin E has antioxidation, thus the moisture protected in sebum and cell membrane protein and skin; It can also promote regeneration and the vigor of human body cell, postpones the ageing process of cell. Moreover it is possible to promote the human body utilization to vitamin A; Synergism, the health of protection skin can be played with vitamin C, reduce occurrence of skin infections; " moistening " there are to act on the collagen fiber in skin and elastic fibers, thus improving and safeguard the elasticity of skin; The blood circulation in skin can be promoted, make skin obtain sufficient nutrition and moisture, to maintain the tender of skin and gloss; May also suppress the formation of pigmented spots, senile plaque, reduce facial wrinkles and pure white skin, prevent and treat acne.
Summary of the invention
The purpose of the present invention is precisely in order to overcome the deficiency of above-mentioned technology, and a kind of nearly fresh juice facial mask formula of dendrobium officinale and method for making thereof are provided, apply nearly dendrobium officinale compatibility classics moisturizing, nutrition composition, help Herba Dendrobii active component smoothly, be normally absorbed by the skin.
It is an object of the invention to complete by following technical solution. the fresh juice facial mask formula of this nearly dendrobium officinale, the weight of its each raw material is as follows: nearly wild fresh Herba Dendrobii 15��25 parts, 35��40 parts of water, 1, ammediol 4��8 parts, glycerol 4��8 parts, trehalose 4��7 parts, diglycerol 4��7 parts, Pyrusussuriensis (sugar) alcohol 3��6 parts, rhamnose 3��5 parts, 1, 2-hexanediol 3��5 parts, hyaluronate sodium 2��4 parts, 2��4 parts of carbamide capsule, Fructus Hordei Germinatus widow's glucoside 2��3 parts, xanthan gum 2��3 parts, hydroxyethyl cellulose 2��3 parts, anhydro xylitol 1��3 part, hydrogenated starch hydrolysate 1��3 part, tamarind seed polysaccharide 1��2 part, butanediol 1��2 part, xylitol 1��2 part, Tremella fructification extract 1��2 part, EDETATE SODIUM 0.5��0.8 part, PPG-26-butylol polyether-260.5��0.7 part, PEG-400.5��0.7 part, castor oil hydrogenated 0.3��0.6 part, glucose 0.3��0.5 part, caprylic/capric triglyceride 0.3��0.4 part, Radix Ginseng extract 0.3��0.4 part, hydrogenate soft phosphatidase 0 .2��0.4 part, cholesterol 0.2��0.4 part, parahydroxyacet-ophenone 0.1��0.2 part, 0.05��0.2 part of essence.
The method for making of the fresh juice facial mask formula of this nearly dendrobium officinale, fresh extraction: nearly dendrobium officinale is after steaming blue or green sterilizing, carries out superfine grinding with grinder, then carries out 200 order sucking filtration, filtrate and other component mixing and emulsifyings; Wherein emulsifying process is: formula ratio oil phase includes hydroxyethyl cellulose, PPG-26-butylol polyether-26, PEG-40, castor oil hydrogenated, caprylic/capric triglyceride, the soft phospholipid of hydrogenation, cholesterol, parahydroxyacet-ophenone heating to 95 DEG C, maintain 30min sterilizing, be cooled to 85 DEG C; Aqueous phase is included water, 1, ammediol, glycerol, trehalose, diglycerol, sorbitol, rhamnose, 1,2-hexanediol, hyaluronate sodium, allantoin, Fructus Hordei Germinatus oligose glucoside, Xylitol-based glucoside, xanthan gum, anhydro xylitol, hydrogenated starch hydrolysate, tamarind seed polysaccharide, butanediol, xylitol, Tremella fructification extract, EDETATE SODIUM, glucose, Radix Ginseng extract raw material add in deionized water, it is heated with stirring to 90��100 DEG C, maintain 30min sterilizing, be cooled to 85 DEG C; It is added slowly in aqueous phase by oil phase stirring and emulsifying; When temperature drops to 40��45 DEG C, fresh for Herba Dendrobii extraction liquid, essence are added in base material, continuation stirring 20min, to open homogenizer emulsifying 5min, stand cooling and within 12��24 hours, become cream, discharging is treated in stopping stirring, cooling, then censorship.
Nearly dendrobium officinale cultivating process is as follows:
(1) source screening, is planted: screening Wild Goose and Reed Marsh Mountains dendrobium officinale is as generation kind source;
(2), group training: culture medium: 1/2��1MS, 15��25% Rhizoma Solani tuber osi Aqueous extracts, 6��10% banana puree; Medium sterilization condition: 121 DEG C, 1.1Mpa; Seed asepsis sprouting condition: temperature 25 �� 1 DEG C, 500��1000Lux illumination 12 hour/day;
(3), differentiation, strong sprout: after cultivating 40 days: add 1.0��3.0mg/LBA, 0.1��0.3mg/LNAA; After cultivating 60 days: add 0.1��0.3mg/LBA, 1.0��3.0mg/LNAA;
(4), transplanting processes: fertilizer: Bombyx mori L. 55%��65%, Cortex Cunninghamiae Lanceolatae 45%��55% heap, cover film, natural fermentation 90 days; Booth: temperature 25 �� 3 DEG C, humidity 40%��75%, light application time 8��12 hours; Seedbed: lay fertilizer, thickness 10��20cm; By bottle transplantation of seedlings to taming seedbed, set 5��10min/h automatic watering function;
(5) tree that, lives selects: the jujube tree of diameter 20��40cm or pear tree 100��150/mu;
(6), pluck: the growth selection plant of more than 3 years.
Fresh extraction specifically comprises the following steps that
(1), cleaning: after nearly dendrobium officinale is plucked, defoliation, purified water 1:20��30 rinse 30��60min, then rinse 3 times by purified water;
(2), sterilizing: clean Herba Dendrobii is put in steaming machine, with the steam sterilization 5��10min of 95��105 DEG C, cooling;
(3), cutting: the Herba Dendrobii that sterilizing is good is cut into the segment of 0.5��1.5cm;
(4), grind: Herba Dendrobii section is put in grinder, add purified water by 1:8��12, grind to form the fresh juice that fineness is 250��300 ��m;
(5), filter: the fresh juice of Herba Dendrobii after grinding carries out vacuum filtration, respectively coarse filtration and fine straining, and coarse filtration medium is the nylon gauze of 80��100, and fine straining medium is 200 order nylon gauzes, and filtrate is standby, and filtering residue forwards abstraction process to.
The invention have the benefit that at process aspect, the present invention applies the compositions such as the polysaccharide in " fresh extraction " technology dendrobium officinale nearly, mannose, vitamin, EN, aminoacid and chlorophyll and fully extracts, and is greatly improved the value of rare medicinal herbs Herba Dendrobii; Secondly as directly process with fresh Herba Dendrobii, the provinces and regions cost of Herba Dendrobii dry run, it also avoid Herba Dendrobii and cause the risk of nutrient loss because baking temperature is too high; Again, application " fresh extraction " technique can make the extracts active ingredients yield in Herba Dendrobii be greatly improved, and can retain the color and luster of fresh Herba Dendrobii, abnormal smells from the patient and mouthfeel, more can embody the natural value of product. In conjunction with techniques such as preparation, emulsifying, subpackages, make the facial film skin care item being easy to absorb and carry, be especially suitable for allegro work and the lives such as working, travelling. The present invention all has a clear superiority in from aspects such as the selection of raw material, prescription compatibility, processing technique, product forms than market like product, has good market prospect.
Accompanying drawing explanation
Fig. 1 is nearly dendrobium officinale cultivating technique flow chart;
Fig. 2 is the fresh extraction process chart of nearly dendrobium officinale;
Fig. 3 is nearly dendrobium officinale facial film production technological process.
Fig. 4 is nearly dendrobium officinale emulsifying, subpackage and packaging process flow figure.
Wherein, in Fig. 1: 1* sterilising conditions, sterilization effect control; 2* culture medium and condition of tissue culture control; 3* differentiation condition controls; 4* condition in strong sprout controls; 5* fertilizer substrate, greenhouse-environment control; 6* Tree Species Selection, Planting pattern, disease pest defense controls; 7* plucks the time limit, the picking season controls.
In Fig. 2: 1* sterilising temp, time control; 2* grinds amount of water, fineness controls; 3* filtering accuracy controls.
In Fig. 3: 1* recipe ingredient inventory controls; 2* sterilising temp, time control; 3* oil water phase order by merging controls; 4* chilling temperature controls; 5* homogenizing time, effect control; 6* time of repose controls; 7* loading amount and sealing control.
Detailed description of the invention
Below by detailed description of the invention, the present invention is further elaborated, and embodiment will facilitate a better understanding of the present invention, but the present invention is not limited only to following embodiment.
The content that the present invention relates to includes the cultivation of Herba Dendrobii raw material, formula for a product and preparation technology, and every advantage is as follows:
1 nearly dendrobium officinale source advantage
Market majority Herba Dendrobii derives from greenhouse gardening, and uses chemical fertilizer and pesticide, even auxin in planting process, makes the safety of Herba Dendrobii can not get ensureing. The nearly dendrobium officinale that the present invention uses is by GAP and organic products certification, and polysaccharide content of dendrobium candidum, up to 39.6%, exceeds standards of pharmacopoeia 58.4%, also detected EN (content is 14.2mg/100g), and by organic products certification; Therefore no matter the nearly dendrobium officinale that the present invention applies is quality or safety, is above like product.
Nearly dendrobium officinale cultivates the basis that link is the present invention, and its process includes germplasm screening, group training, differentiation, strong sprout, live tree cultivation, harvesting etc., is specifically shown in table one.
The nearly dendrobium officinale cultivating process of table one and key parameter thereof
2 formula advantage
Inventive formulation is classical moisturizing, the nutritional labeling such as nearly dendrobium officinale compatibility glycerol, trehalose, specifically refers to table two.
The nearly wild fresh Herba Dendrobii granular recipe of table two and proportioning thereof
3 process advantages
" fresh extraction " technique of present invention application is that nearly dendrobium officinale, after steaming blue or green sterilizing (utilizing steaming machine to carry out 5��10min steam sterilization), carries out superfine grinding with grinder, then carries out 200 order sucking filtration, filtrate and other component mixing and emulsifyings. The advantage of this technique is: 1. Dendrobium officinale polysaccharide extracts conversion ratio (actual extracting amount and theoretical content ratio) up to more than 90%, and traditional direct water boiling and extraction conversion ratio is only 60%��70%; 2. the nutritional labeling of Herba Dendrobii at utmost retains, and Vitamin C content is that 85mg/100g (being 28 times of traditional decoction extraction process), chlorophyll content 65mg/100g (chlorophyll of traditional decoction technique is almost all destroyed), protein content also can reach for 9.3% (being about 1.5��1.8 times of traditional decoction extraction process); 3. the product that this technique is made is light green, has the fragrant that Herba Dendrobii is unique, more can embody Herba Dendrobii own characteristic, meet the trend of market natural herb.
(1) nearly dendrobium officinale is cultivated
1 kind of source screening
Wild Goose and Reed Marsh Mountains is the cradle of Herba Dendrobii, " Bencao Congxin " place of production of Herba Dendrobii is also had clear and definite record " Wenzhou is gone up most, takes second place in Guangxi; Guangdong under ", it is domestic that Wild Goose and Reed Marsh Mountains is seated in Wenzhou, is the main producing region of Herba Dendrobii, and its quality receives the high praise of ancient Chinese medicine doctor. Leqing is located in the foot of a hill or mountain, Wild Goose and Reed Marsh Mountains, and local villager excavates Herba Dendrobii centuries history, for the benefit of preservation of Herba Dendrobii, and they are also baked to, and are curled into spring-like, through being handed down from age to age and improving, is also the formation of the Herba Dendrobii in modern times! Produce and be called " genuine medicinal materials " in Herba Dendrobii here or Herba Dendrobii are by industry. The present invention follows the feature of Chinese crude drug Genuine producing area, the wild varieties planting selection Wild Goose and Reed Marsh Mountains, source of Herba Dendrobii.
2 groups of trainings
The growth of Herba Dendrobii is limited mainly by the impact of the factor such as illumination and temperature, is under periodicity of illumination at 12h/d, and now the chlorophyll content of plant and Net Photosynthetic Rate are higher, and growth is stronger with fertility. Select 1/2��1MS, 15��25% Rhizoma Solani tuber osi Aqueous extracts, 6��10% banana puree as culture medium, and 121 DEG C, culture medium is carried out sterilizing under the sterilising conditions of 1.1Mpa.
Select kind of a stem for source Herba Dendrobii, defoliation, Herba Dendrobii stem is carried out surface sterilization with the ethanol of 75% by aseptic operating platform, removes dust then the HgCl with 1%2Sterilizing 5��10min, with aseptic water washing three times, so repeats 3 sterilizings, constantly to rock in sterilization process so that it is fully sterilizing.
By sterilized Radix Stephaniae Tetrandrae stem, being aseptically cut into the stem section with a stipes, be inoculated in inducing culture, temperature 25 �� 1 DEG C, 500��2000Lux illumination 12h/ day, induction is sprouted, and bud induces protocorm again.
3 differentiation, strong sprout
After cultivating 40��43 days, add 1.0��3.0mg/LBA, 0.1��0.3mg/LNAA, after cultivating 58��62 days, add 0.1��0.3mg/LBA, 1.0��3.0mg/LNAA, make protocorm differentiation, strong sprout, just high 5��9cm, 7��9, blade, the healthy and strong plant of root length 3��6cm can be turned out through about time a year and a half.
4 transplant
Owing to the primary growth condition such as temperature and illumination changes, need before transplanting through 1 week seedling exercising. Avoid during transplanting injuring tender tissue, clean the culture medium being attached to root, load kind is on seedbed, fertilizer (Bombyx mori L. 55%��65%, Cortex Cunninghamiae Lanceolatae 45%��55% heap are laid in seedbed, cover film, natural fermentation 90 days, sterilizing), fertilizer to loosen ventilative, laying depth 10��20cm. During transplanting, optimum temperature is 15��30 DEG C, temperature too low or too high be all not suitable for bottle outlet transplant. Greenhouse temperature 25 �� 3 DEG C, humidity 40%��75%, light application time transplant successful Herba Dendrobii in 8��12 hours, water in right amount after 1 week.
5 live sets cultivation
As it was previously stated, the Genuine producing area of Herba Dendrobii is positioned at Wild Goose and Reed Marsh Mountains, also build in the foot of a hill or mountain, Wild Goose and Reed Marsh Mountains for the planting base of Herba Dendrobii in this present invention. After booth seedbed grows 50��70 days, Herba Dendrobii length about 10��15cm, now can transplant to living on tree. The symbiosis of Herba Dendrobii and tree has certain selectivity, its root belongs to aerial root, easily it is attached to the surface of tree, therefore the growth of Herba Dendrobii is had important impact by the moisture of bark and texture thereof, according to experimentation, the present invention selects jujube tree and pear tree as cultivation seeds, trunk diameter 20��40cm jujube tree 100��150/mu, and cultivated areas illumination is fully (light application time 8��12h/ days).
Cultivation: during transplanting, optimum temperature is 15��30 DEG C. Herba Dendrobii is extracted from seedbed, without removing root substrate, directly wrap up root with lichen, then with Caulis et Folium Oryzae rope, the root position of Herba Dendrobii is tied on trunk or thick (diameter >=5cm) branch, minimum altitude 50cm, every 30��40cm plantation one circle. The position that automatic irrigation water pipe is pressed Seedling disposes shower nozzle, and pastes paper and biological insect-catching equipment in tree planting district suspension of living, and pastes paper 3��5/square, biological insect-catching equipment 2��3/10 meters. Automatic spray irrigation system opens auto spraying function, summertime 10��20min/h, winter 5��10min/h in the non-rainy day.
6 pluck
Dendrobium officinale polysaccharide is the significant composition of Herba Dendrobii, shows after deliberation, and the content of Dendrobium officinale polysaccharide is relatively larger by growth year and seasonal effect, is specifically shown in table four.
Table four Dendrobium officinale polysaccharide growth year and seasonal variations (%)
As seen from the above table, the optimal harvest time of Herba Dendrobii is 3��May after growing 3 years, the florescence of Herba Dendrobii is generally for 5��June, feature according to biological heredity, the change of polysaccharide content of dendrobium candidum is limited mainly by the impact bloomed, therefore January after it is generally acknowledged Herba Dendrobii rational 3 years collection period, February, March, April, May and December.
(2) fresh extraction technique and parameter
After nearly dendrobium officinale is plucked, defoliation, purified water 1:20��30 rinse 30��60min, rinse 3 times by purified water again, put in steaming machine, with the steam sterilization 5��10min of 95��105 DEG C, cooling, it is cut into the segment of 0.5��1.5cm, placing in grinder, regulating fineness of grind is 250��350 ��m, adds cryogenic purincation water (2��8 DEG C) by 1:10��20, open grinder, Herba Dendrobii is ground to form fresh juice.
The fresh juice of Herba Dendrobii after grinding carries out vacuum filtration, first carries out coarse filtration, and coarse filtration medium is the nylon gauze of 80��100; Coarse filtration liquid carries out fine straining again, and fine straining medium is 200 order nylon gauzes. Collect filtrate, standby.
(3) emulsifying process and parameter
Formula ratio oil phase (hydroxyethyl cellulose, PPG-26-butylol polyether-26, PEG-40, castor oil hydrogenated, caprylic/capric triglyceride, the soft phospholipid of hydrogenation, cholesterol, parahydroxyacet-ophenone) is heated to 95 DEG C, maintain 30min sterilizing, be cooled to 85 DEG C; By aqueous phase (water, 1, ammediol, glycerol, trehalose, diglycerol, sorbitol, rhamnose, 1,2-hexanediol, hyaluronate sodium, allantoin, Fructus Hordei Germinatus oligose glucoside, Xylitol-based glucoside, xanthan gum, anhydro xylitol, hydrogenated starch hydrolysate, tamarind seed polysaccharide, butanediol, xylitol, Tremella fructification extract, EDETATE SODIUM, glucose, Radix Ginseng extract) raw material adds in deionized water, it is heated with stirring to 90��100 DEG C, maintain 30min sterilizing, be cooled to 85 DEG C; It is added slowly in aqueous phase by oil phase stirring and emulsifying; When temperature drops to 40��45 DEG C, fresh for Herba Dendrobii extraction liquid, (daily) essence are added in base material, continuation stirring 20min, to open homogenizer emulsifying 5min, stand cooling and within 12��24 hours, become cream, discharging is treated in stopping stirring, cooling, then censorship.
(4) subpackage
Take special face pack packaging material, after disinfecting, be transported to workshop, face paper and pearl film are folded, and load in facial film aluminium plastic bag, after the assay was approved, carry out subpackage with mastic racking machine, by the loading amount specifications control loading amount of regulation, seal pressure code after fill, proceed to subsequent processing.
(5) packaging
Packing specification according to regulation carries out outer package.
Finally it is pointed out that above example is only the more representational example of the present invention. Obviously, technical scheme is not limited to examples detailed above, it is also possible to have many deformation, all deformation that those of ordinary skill in the art can directly derive from present disclosure or associate, and is all considered as protection scope of the present invention.

Claims (4)

1. the fresh juice facial mask formula of nearly dendrobium officinale, it is characterized in that: the weight of its each raw material is as follows: nearly wild fresh Herba Dendrobii 15��25 parts, 35��40 parts of water, 1, ammediol 4��8 parts, glycerol 4��8 parts, trehalose 4��7 parts, diglycerol 4��7 parts, Pyrusussuriensis (sugar) alcohol 3��6 parts, rhamnose 3��5 parts, 1, 2-hexanediol 3��5 parts, hyaluronate sodium 2��4 parts, 2��4 parts of carbamide capsule, Fructus Hordei Germinatus widow's glucoside 2��3 parts, xanthan gum 2��3 parts, hydroxyethyl cellulose 2��3 parts, anhydro xylitol 1��3 part, hydrogenated starch hydrolysate 1��3 part, tamarind seed polysaccharide 1��2 part, butanediol 1��2 part, xylitol 1��2 part, Tremella fructification extract 1��2 part, EDETATE SODIUM 0.5��0.8 part, PPG-26-butylol polyether-260.5��0.7 part, PEG-400.5��0.7 part, castor oil hydrogenated 0.3��0.6 part, glucose 0.3��0.5 part, caprylic/capric triglyceride 0.3��0.4 part, Radix Ginseng extract 0.3��0.4 part, hydrogenate soft phosphatidase 0 .2��0.4 part, cholesterol 0.2��0.4 part, parahydroxyacet-ophenone 0.1��0.2 part, 0.05��0.2 part of essence.
2. the method for making of the fresh juice facial mask formula of nearly dendrobium officinale, it is characterised in that: fresh extraction: nearly dendrobium officinale is after steaming blue or green sterilizing, carries out superfine grinding with grinder, then carries out 200 order sucking filtration, filtrate and other component mixing and emulsifyings; Wherein emulsifying process is: formula ratio oil phase includes hydroxyethyl cellulose, PPG-26-butylol polyether-26, PEG-40, castor oil hydrogenated, caprylic/capric triglyceride, the soft phospholipid of hydrogenation, cholesterol, parahydroxyacet-ophenone heating to 95 DEG C, maintain 30min sterilizing, be cooled to 85 DEG C; Aqueous phase is included water, 1, ammediol, glycerol, trehalose, diglycerol, sorbitol, rhamnose, 1,2-hexanediol, hyaluronate sodium, allantoin, Fructus Hordei Germinatus oligose glucoside, Xylitol-based glucoside, xanthan gum, anhydro xylitol, hydrogenated starch hydrolysate, tamarind seed polysaccharide, butanediol, xylitol, Tremella fructification extract, EDETATE SODIUM, glucose, Radix Ginseng extract raw material add in deionized water, it is heated with stirring to 90��100 DEG C, maintain 30min sterilizing, be cooled to 85 DEG C; It is added slowly in aqueous phase by oil phase stirring and emulsifying; When temperature drops to 40��45 DEG C, fresh for Herba Dendrobii extraction liquid, essence are added in base material, continuation stirring 20min, to open homogenizer emulsifying 5min, stand cooling and within 12��24 hours, become cream, discharging is treated in stopping stirring, cooling, then censorship.
3. the method for making of the fresh juice facial mask formula of nearly dendrobium officinale according to claim 2, it is characterised in that: nearly dendrobium officinale cultivating process is as follows:
(1) source screening, is planted: screening Wild Goose and Reed Marsh Mountains dendrobium officinale is as generation kind source;
(2), group training: culture medium: 1/2��1MS, 15��25% Rhizoma Solani tuber osi Aqueous extracts, 6��10% banana puree; Medium sterilization condition: 121 DEG C, 1.1Mpa; Seed asepsis sprouting condition: temperature 25 �� 1 DEG C, 500��1000Lux illumination 12 hour/day;
(3), differentiation, strong sprout: after cultivating 40 days: add 1.0��3.0mg/LBA, 0.1��0.3mg/LNAA; After cultivating 60 days: add 0.1��0.3mg/LBA, 1.0��3.0mg/LNAA;
(4), transplanting processes: fertilizer: Bombyx mori L. 55%��65%, Cortex Cunninghamiae Lanceolatae 45%��55% heap, cover film, natural fermentation 90 days; Booth: temperature 25 �� 3 DEG C, humidity 40%��75%, light application time 8��12 hours; Seedbed: lay fertilizer, thickness 10��20cm; By bottle transplantation of seedlings to taming seedbed, set 5��10min/h automatic watering function;
(5) tree that, lives selects: the jujube tree of diameter 20��40cm or pear tree 100��150/mu;
(6), pluck: the growth selection plant of more than 3 years.
4. the method for making of the fresh juice facial mask formula of nearly dendrobium officinale according to claim 2, it is characterised in that: fresh extraction specifically comprises the following steps that
(1), cleaning: after nearly dendrobium officinale is plucked, defoliation, purified water 1:20��30 rinse 30��60min, then rinse 3 times by purified water;
(2), sterilizing: clean Herba Dendrobii is put in steaming machine, with the steam sterilization 5��10min of 95��105 DEG C, cooling;
(3), cutting: the Herba Dendrobii that sterilizing is good is cut into the segment of 0.5��1.5cm;
(4), grind: Herba Dendrobii section is put in grinder, add purified water by 1:8��12, grind to form the fresh juice that fineness is 250��300 ��m;
(5), filter: the fresh juice of Herba Dendrobii after grinding carries out vacuum filtration, respectively coarse filtration and fine straining, and coarse filtration medium is the nylon gauze of 80��100, and fine straining medium is 200 order nylon gauzes, and filtrate is standby, and filtering residue forwards abstraction process to.
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106265339A (en) * 2016-09-14 2017-01-04 叶树林 A kind of six hours high-efficiency moisturizing compositions and preparation thereof and application
CN106377476A (en) * 2016-10-16 2017-02-08 湖南大围山仙草生物科技有限公司 Dendrobium candidum bio-cellulose mask and manufacturing method
CN107837223A (en) * 2017-11-22 2018-03-27 天津市蓝宝石化妆品有限公司 A kind of facial mask essence containing dendrobium candidum extract and facial mask and preparation method and application
CN108014062A (en) * 2018-01-03 2018-05-11 浙江东来天然生物制品有限公司 Facial mask containing dendrobium candidum active ingredient
CN109157475A (en) * 2018-10-16 2019-01-08 皖西学院 Dendrobium candidum facial mask and preparation method thereof
CN109350578A (en) * 2018-12-26 2019-02-19 广州市科能化妆品科研有限公司 Beautifying liquid and preparation method thereof and tyrosinase inhibitor

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106265339A (en) * 2016-09-14 2017-01-04 叶树林 A kind of six hours high-efficiency moisturizing compositions and preparation thereof and application
CN106377476A (en) * 2016-10-16 2017-02-08 湖南大围山仙草生物科技有限公司 Dendrobium candidum bio-cellulose mask and manufacturing method
CN107837223A (en) * 2017-11-22 2018-03-27 天津市蓝宝石化妆品有限公司 A kind of facial mask essence containing dendrobium candidum extract and facial mask and preparation method and application
CN107837223B (en) * 2017-11-22 2021-05-18 天津市蓝宝石化妆品有限公司 Facial mask essence containing dendrobium officinale extract, facial mask containing dendrobium officinale extract, preparation method of facial mask essence and application of facial mask essence
CN108014062A (en) * 2018-01-03 2018-05-11 浙江东来天然生物制品有限公司 Facial mask containing dendrobium candidum active ingredient
CN109157475A (en) * 2018-10-16 2019-01-08 皖西学院 Dendrobium candidum facial mask and preparation method thereof
CN109350578A (en) * 2018-12-26 2019-02-19 广州市科能化妆品科研有限公司 Beautifying liquid and preparation method thereof and tyrosinase inhibitor

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Application publication date: 20160601