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Microstructural, Optical and Magnetic Study of Ni–Zn Nanoferrites

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Abstract

NixZn1-xFe2O4 (x = 0.0, 0.2, 0.4, 0.5, 0.6, 0.8 and 1.0) nanoferrites were synthesized using the citrate precursor method with high-purity metal nitrates and citric acid as synthesis precursors. For a detailed analysis of the structural, optical and magnetic properties of these nanoferrites sintered at 700 °C for 3 h, X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR) and vibrating sample magnetometer (VSM) tests were done. The analysis of XRD patterns of the powdered samples revealed that the nanoferrites have a spinel structure, and the crystallite size of the nanoferrites ranged from 23 to 31 nm. The nanoferrite samples were found with a maximum porosity of 57% at x = 0.5 which indicated the higher adsorption capacity of the materials. The density of these nanoferrites varied from 2.318 to 2.590 g/cm3 with the change in their crystallite size and lattice parameter. FTIR spectroscopy also revealed two prominent peaks between 542–582 and 402–415 cm−1, representing the tetrahedral and octahedral site occupancies, occupied by Ni2+, Zn2+ and Fe3+ ions. These peaks indicated the spinel structure of the nanoferrites. The magnetic behaviour of the nanoferrites was analysed from the hysteresis loop obtained from VSM data. It was observed that the nanoferrites are highly magnetic as the value of specific saturation magnetization varied from 1.31 to 63.31 emu/g with the variation in concentration of Ni2+ metal ions ranging from x = 0.0 to x = 1.0. High values of anisotropic constant were observed, which varied from 0.00147 \(\times\) 105 to 0.16218 \(\times\) 105 erg/g.

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  1. Department of Physics, Guru Jambheshwar University of Science & Technology, Hisar, Haryana, 125001, India

    Pinki Punia & Rakesh Dhar

  2. Nanjing University of Information Science and Technology (NUIST), Nanjing, 210044, China

    Blaise Ravelo

  3. National University of Science and Technology, MISIS, Moscow, 119991, Russia

    Alex V. Trukhanov & Larissa V. Panina

  4. Department of Physics, Amity University Haryana, Gurugram, Haryana, 122413, India

    Preeti Thakur

  5. Amity Institute of Nanotechnology, Amity University Haryana, Gurugram, Haryana, 122413, India

    Atul Thakur

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Punia, P., Dhar, R., Ravelo, B. et al. Microstructural, Optical and Magnetic Study of Ni–Zn Nanoferrites. J Supercond Nov Magn 34, 2131–2140 (2021). https://doi.org/10.1007/s10948-021-05967-y

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