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WO2024063540A1 - Multi-layer phase cosmetic composition - Google Patents

Multi-layer phase cosmetic composition Download PDF

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Publication number
WO2024063540A1
WO2024063540A1 PCT/KR2023/014302 KR2023014302W WO2024063540A1 WO 2024063540 A1 WO2024063540 A1 WO 2024063540A1 KR 2023014302 W KR2023014302 W KR 2023014302W WO 2024063540 A1 WO2024063540 A1 WO 2024063540A1
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WO
WIPO (PCT)
Prior art keywords
oil
weight
mixture
polyglyceryl
cosmetic composition
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PCT/KR2023/014302
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French (fr)
Korean (ko)
Inventor
김나래
조주현
Original Assignee
주식회사 에델프라우
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Publication of WO2024063540A1 publication Critical patent/WO2024063540A1/en

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/03—Liquid compositions with two or more distinct layers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37—Esters of carboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin

Definitions

  • the present invention relates to a multi-layered cosmetic composition, and more specifically, to an oil phase comprising a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main ingredients, polyglyceryl-10 laurate, and It consists of an emulsified part containing a mixture of polyglyceryl-10 myristate as the main component, and an aqueous part containing purified water and polyol, so that each layer is stably separated. When sheared, the components of each layer are mixed, and after a certain period of time, the multilayer is again formed. It relates to a multi-layered cosmetic composition that can be separated into phases.
  • the function of basic cosmetics is to help the skin function normally. Therefore, when developing cosmetics, it is desirable to consider the skin's moisturizing mechanism and create a moisturizing environment with an appropriate combination of water-soluble moisturizing substances and oil-soluble oil film, that is, moisture, humectants, and oil, so that skin homeostasis is normally maintained.
  • One of the cosmetic compositions to solve this problem is multilayer cosmetics.
  • they either mix or separate.
  • water with a relatively high specific gravity sinks to the bottom to form the lower layer and oil with a relatively low specific gravity floats to the top to form the upper layer.
  • This mixing and separation is due to the compatibility between liquids.
  • things that are highly compatible with each other are mixed, they mix together, and if the compatibility is low, separation occurs.
  • Patent Document 1 Republic of Korea Patent Publication No. 10-0933551 (announced on December 23, 2009), “Two-layer foundation cosmetic composition”
  • the present invention provides an oil phase containing a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main ingredients, polyglyceryl-10 laurate and polyglyceryl- It consists of an emulsified part containing a mixture of 10 myristate as the main component, and an aqueous part containing purified water and polyol, so that each layer is stably separated, and when sheared, the components of each layer are mixed and separated again into a multilayer phase after a certain period of time.
  • the purpose is to provide a multilayer cosmetic composition.
  • the present invention provides an oil phase containing a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main ingredients, polyglyceryl-10 laurate and polyglyceryl- An emulsified portion containing a mixture of 10 myristate as a main ingredient; and an aqueous phase containing purified water and polyol.
  • oily part further includes one or more selected from the group consisting of meadowfoam seed oil, sunflower seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil.
  • the emulsifying part contains one or more from the group consisting of lecithin, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, polysorbate 20, polysorbate 60, and polysorbate 80. It is characterized by further inclusion by selection.
  • the polyol of the aqueous phase is any of the group consisting of glycerin, butylene glycol, propanediol, 2,3-butanediol, pentylene glycol, sodium hyaluronate, and 1,2-hexanediol. It is characterized by having more than one.
  • the oil phase part is included in an amount of 1.0 to 30.0 parts by weight
  • the emulsified part is included in an amount of 1.0 to 30.0 parts by weight
  • the polyol in the aqueous phase part is included in an amount of 5.0 to 30.0 parts by weight
  • the purified water in the aqueous phase part is included in the remaining amount. It is characterized by being
  • the multilayered cosmetic composition according to the present invention has an oily part containing a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main ingredients, and polyglyceryl-10 laurate and polyglyceryl-10 milliliter. It consists of an emulsified part containing a mixture of states as the main component, and an aqueous part containing purified water and polyol, so that each layer is stably separated, and when sheared, the components of each layer are mixed, and after a certain period of time, they are separated into a multilayer phase again.
  • the multi-layered cosmetic composition according to the present invention can contain different components in each layer and has excellent moisturizing effect.
  • Figure 2 is a photograph of the mixing state of the multilayer cosmetic composition according to the present invention.
  • Figure 3 is a graph relating to an experiment confirming the degree of layer separation for Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 of the present invention.
  • Figure 4 is a graph showing mixing time confirmation experiments for Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 of the present invention.
  • Figure 5 is a graph showing an experiment confirming the degree of dispersion after mixing for Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 of the present invention.
  • Figure 6 is a graph relating to an experiment confirming the layered skin moisturizing effect for Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 of the present invention.
  • the multilayered cosmetic composition according to the present invention has an oily part containing a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as active ingredients, and polyglyceryl-10 laurate and polyglyceryl-10 milliliter. It consists of an emulsified part containing a mixture of states as an active ingredient, and an aqueous phase containing purified water and polyol.
  • the oil phase contains a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as the main active ingredient.
  • the calendula oil (Calendula Officinalis Flower Oil) is an oil obtained by distilling the flowers of calendula (marigold), a native of Mexico. The calendula grows well in the mountains and fields of Korea, and the calendula (calendula) includes marigolds, marigolds, and marigolds. It is also called a tree and has the property of growing well in sunny, sandy soil.
  • the Butylene Glycol Dicaprylate/Dicaprate is a mixture of butylene glycol diester of caprylic and capric acid.
  • the butylene glycol dicaprylate/dicaprate is a raw material mainly used as a skin conditioning agent (moisture blocker) and solvent.
  • calendula oil and butylene glycol dicaprylate/dicaprate may be mixed at a weight ratio of 0.01:99.99 to 99.99:0.01.
  • the components of the oil phase are not limited to this, and the components of the oil phase may include any polar oil. Accordingly, the oily part may further include one or more selected from the group consisting of meadowfoam seed oil, sunflower seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil.
  • Limnanthes Alba (Meadowfoam) Seed Oil refers to oil extracted from the seeds of Limnanthes alba.
  • the sunflower seed oil (Helianthus Annuus (Sunflower) Seed Oil) refers to oil obtained by pressing the seeds of sunflower (Helianthus annuus).
  • the caprylic/capric triglyceride refers to a mixed triester of caprylic, capric acid, and glycerin.
  • the grape seed oil (Vitis Vinifera (Grape) Seed Oil) refers to a non-volatile oil obtained by pressing the seeds of grapes (Vitis vinifera).
  • the avocado oil refers to the oil obtained from avocado (Persea gratissima).
  • the oil phase may be included in an amount of 1.0 to 30.0 parts by weight based on 100 parts by weight of the total cosmetic composition.
  • the oil phase does not contain non-polar oil or silicone oil, and preferably contains only polar oil.
  • the oily part may additionally contain a preservative or the like.
  • the emulsification part contains a mixture of polyglyceryl-10 laurate and polyglyceryl-10 myristate as the main active ingredient.
  • the polyglyceryl-10 laurate is an ester of lauric acid and polyglycerin-10.
  • the polyglyceryl-10 laurate is a raw material mainly used as a skin conditioning agent and surfactant-emulsifier.
  • the polyglyceryl-10 myristate is an ester of myristic acid and polyglycerin-10.
  • the polyglyceryl-10 myristate is a raw material mainly used as a skin conditioning agent and surfactant-emulsifier.
  • the ingredients of the emulsified part are not limited to this, and the emulsified part includes lecithin, polyglyceryl-10 stearate, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, and polysorbate 20. , polysorbate 60, and polysorbate 80 may be further included by selecting any one or more from the group consisting of.
  • the lecithin is a naturally occurring diglyceride mixture of stearic acid, palmitic acid, and oleic acid, and is bound to the choline ester of phosphoric acid and is found in living animals and plants.
  • the polyglyceryl-10 stearate is an ester of stearic acid and polyglycerin-10.
  • the PEG-40 Hydrogenated Castor Oil is a polyethylene glycol derivative of hydrogenated castor oil containing an average of 40 moles of ethylene oxide.
  • the PEG-60 Hydrogenated Castor Oil is a polyethylene glycol derivative of hydrogenated castor oil containing an average of 60 moles of ethylene oxide.
  • Polysorbate 20 is mainly composed of monoesters and is a mixture of sorbitol anhydride and sorbitol laurate ester condensed with about 20 moles of ethylene oxide.
  • Polysorbate 60 is mainly composed of monoesters and is a mixture of sorbitol anhydride and sorbitol stearate ester condensed with about 60 moles of ethylene oxide.
  • Polysorbate 80 is mainly composed of monoesters and is a mixture of sorbitol anhydride and sorbitol oleate ester condensed with about 80 moles of ethylene oxide, and has the following structure.
  • the emulsifying part may be included in an amount of 1.0 to 30.0 parts by weight based on 100 parts by weight of the total cosmetic composition.
  • the aqueous phase contains purified water and polyol as main active ingredients.
  • the moisturizing agent for the aqueous phase may be any one or more from the group consisting of glycerin, butylene glycol, propanediol, 2,3-butanediol, pentylene glycol, sodium hyaluronate, and 1,2-hexanediol. You can.
  • Glycerin is polyhydric alcohol and is an ingredient used as a denaturant, flavoring agent, hair conditioning agent, moisturizing agent, skin protection agent, skin conditioning agent (moisturizer), and viscosity reducer.
  • Butylene Glycol is an aliphatic diol and is an ingredient used as a flavoring agent, skin conditioning agent, solvent, and viscosity reducer.
  • the propanediol is a type of organic compound and is used as a solvent and viscosity reducer.
  • the 2,3-butanediol is a type of organic compound and is used as a flavoring agent, moisturizer, skin conditioning agent (moisturizer), and solvent.
  • Pentylene Glycol is a type of organic compound and is used as a skin conditioning agent and solvent.
  • Sodium Hyaluronate is the sodium salt of hyaluronic acid and is an ingredient used as a skin conditioning agent.
  • the 1,2-hexanediol is a type of organic compound and is used as a solvent.
  • the polyol in the aqueous phase may be included in an amount of 5.0 to 30.0 parts by weight based on 100 parts by weight of the total cosmetic composition, and the purified water in the aqueous phase may be included in the remaining amount.
  • the water phase may further include other conditioning agents useful for the skin in addition to the ingredients listed above.
  • other conditioning agents useful for the skin in addition to the ingredients listed above.
  • carbomer it would be appropriate not to include carbomer in the aqueous phase.
  • the method for producing a multilayer cosmetic composition according to the present invention includes a first mixture preparation step (S10) of mixing purified water and polyol to form a first mixture and heating to 50 to 80°C; A second mixture preparation step (S20) of mixing each component of the emulsified portion and each component of the oil phase to form a second mixture and heating to 50 to 80°C; A multi-layer cosmetic composition manufacturing step of mixing the first mixture being heated in the first mixture preparation step (S10) and the second mixture being heated in the second mixture preparation step (S20) to produce a multi-layer cosmetic composition. (S30); includes.
  • the first mixture preparation step (S10) is performed.
  • the first mixture in the first mixture preparation step (S10) is formed by mixing purified water and polyol, and is preferably heated to 50 to 80°C.
  • the polyol in the first mixture preparation step (S10) is glycerin, butylene glycol, propanediol, 2,3-butanediol, pentylene glycol, sodium hyaluronate, and 1,2-hexane. It may be any one or more selected from the group consisting of diol.
  • the second mixture in the second mixture preparation step (S20) is formed by mixing each component of the emulsified portion and each component of the oil phase portion, and is preferably heated to 50 to 80°C.
  • the emulsifying part in the second mixture preparation step (S20) is preferably polyglyceryl-10 laurate and polyglyceryl-10 myristate, and in addition, lecithin, polyglyceryl-10 stearate, PEG- It may include 40 Hydrogenated Castor Oil, PEG-60 Hydrogenated Castor Oil, Polysorbate 20, Polysorbate 60, Polysorbate 80, etc.
  • the oil phase in the second mixture preparation step (S20) is preferably calendula oil and butylene glycol dicaprylate/dicaprate, and in addition, meadowfoam seed oil, sunflower seed oil, and caprylic oil. / May include capric triglyceride, grape seed oil, avocado oil, etc.
  • the multilayered cosmetic composition in the multilayered cosmetic composition manufacturing step (S30) is a first mixture being heated to 50 to 80° C. in the first mixture manufacturing step (S10), and a second mixture manufacturing step (S20). It is preferably prepared by mixing the second mixture, which is heated at 50 to 80°C.
  • the multi-layered cosmetic according to the present invention is manufactured.
  • the multilayer cosmetic composition of Example 1 was prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
  • First mixture preparation step (S10) Purified water and polyol containing glycerin were mixed, colorant was added, and the mixture was heated to 65°C to prepare the first mixture.
  • the oil phase components were mixed, colorant and preservative were added, and then heated to 65°C to prepare a second mixture.
  • the comparative composition of Comparative Example 1 was prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
  • First mixture preparation step (S10) Pigment was added to purified water and then heated to 65°C to prepare the first mixture.
  • the oil phase components were mixed, colorant and preservative were added, and then heated to 65°C to prepare a second mixture.
  • the comparative composition of Comparative Example 2 was prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
  • First mixture preparation step (S10) Purified water and polyol containing glycerin were mixed, colorant was added, and the mixture was heated to 65°C to prepare the first mixture.
  • the comparative composition of Comparative Example 3 was prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
  • First mixture preparation step (S10) Purified water and polyol containing glycerin were mixed, colorant was added, and the mixture was heated to 65°C to prepare the first mixture.
  • the comparative composition of Comparative Example 4 was prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
  • First mixture preparation step (S10) Purified water and polyol containing glycerin were mixed, colorant was added, and the mixture was heated to 65°C to prepare the first mixture.
  • the comparative composition of Comparative Example 5 was prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
  • First mixture preparation step (S10) Purified water and polyol containing glycerin were mixed, colorant was added, and the mixture was heated to 65°C to prepare the first mixture.
  • the multilayered cosmetic compositions of Examples 2 to 4 were prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
  • First mixture preparation step (S10) purified water, glycerin, and glycerin, butylene glycol, propanediol, 2,3-butanediol, pentylene glycol, and sodium hyaluron as shown in Tables 7 to 9 below.
  • a first mixture was prepared by mixing at least one polyol of ronate and 1,2-hexanediol, adding pigment, and heating to 65°C.
  • the oil phase components were mixed, colorant and preservative were added, and then heated to 65°C to prepare a second mixture.
  • Example 2 glycerin and butylene glycol were used as polyols, and in Example 3, propanediol and 2,3-butanediol were used as polyols. In Example 4, pentylene glycol, sodium hyaluronate, and 1,2-hexanediol were applied as polyols.
  • Example 2 division ingredient content A Purified water remaining amount glycerin 5.0% by weight Butylene glycol 10.0% by weight Pigment 1 Appropriate amount B Polyglyceryl-10 Laurate 9.5% by weight Polyglyceryl-10 myristate 9.5% by weight Calendula oil 10.0% by weight Butylene Glycol Dicaprylate/Dicaprate 10.0% by weight Pigment 2 Appropriate amount preservative Appropriate amount
  • Example 3 division ingredient content A Purified water remaining amount Propanediol 5.0% by weight 2,3-Butanediol 10.0% by weight Pigment 1 Appropriate amount B Polyglyceryl-10 Laurate 9.5% by weight Polyglyceryl-10 myristate 9.5% by weight Calendula oil 10.0% by weight Butylene Glycol Dicaprylate/Dicaprate 10.0% by weight Pigment 2 Appropriate amount preservative Appropriate amount
  • Example 4 division ingredient content A Purified water remaining amount Pentylene glycol 5.0% by weight Sodium Hyaluronate 5.0% by weight 1,2-hexanediol 5.0% by weight Pigment 1 Appropriate amount B Polyglyceryl-10 Laurate 9.5% by weight Polyglyceryl-10 myristate 9.5% by weight Calendula oil 10.0% by weight Butylene Glycol Dicaprylate/Dicaprate 10.0% by weight Pigment 2 Appropriate amount preservative Appropriate amount
  • the multilayered cosmetic compositions of Examples 5 to 11 were prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
  • First mixture preparation step (S10) Purified water and polyol containing glycerin and butylene glycol were mixed, colorant was added, and the mixture was heated to 65°C to prepare the first mixture.
  • -Emulsifying component further comprising one or more of 40 Hydrogenated Castor Oil, PEG-60 Hydrogenated Castor Oil, Polysorbate 20, Polysorbate 60, and Polysorbate 80, calendula oil, and butyl
  • the oil phase components including len glycol dicaprylate/dicaprate were mixed, colorant and preservative were added, and then heated to 65°C to prepare a second mixture.
  • Example 5 is lecithin
  • Example 6 is polyglyceryl-10 stearate
  • Example 7 is PEG-40 hydrogenated castor oil
  • Example 8 PEG-60 hydrogenated castor oil
  • Example 9 further included polysorbate 20
  • Example 10 contained polysorbate 60
  • Example 11 further included polysorbate 80 as an emulsifying component.
  • Example 5 division ingredient content A Purified water remaining amount glycerin 5.0% by weight Butylene glycol 10.0% by weight Pigment 1 Appropriate amount B Polyglyceryl-10 Laurate 7.0% by weight Polyglyceryl-10 myristate 7.0% by weight lecithin 5.0% by weight Calendula oil 10.0% by weight Butylene Glycol Dicaprylate/Dicaprate 10.0% by weight Pigment 2 Appropriate amount preservative Appropriate amount
  • Example 6 division ingredient content A Purified water remaining amount glycerin 5.0% by weight Butylene glycol 10.0% by weight Pigment 1 Appropriate amount B Polyglyceryl-10 Laurate 7.0% by weight Polyglyceryl-10 myristate 7.0% by weight Polyglyceryl-10 Stearate 5.0% by weight Calendula oil 10.0% by weight Butylene Glycol Dicaprylate/Dicaprate 10.0% by weight Pigment 2 Appropriate amount preservative Appropriate amount
  • Example 7 division ingredient content A Purified water remaining amount glycerin 5.0% by weight Butylene glycol 10.0% by weight Pigment 1 Appropriate amount B Polyglyceryl-10 Laurate 7.0% by weight Polyglyceryl-10 myristate 7.0% by weight PEG-40 Hydrogenated Castor Oil 5.0% by weight Calendula oil 10.0% by weight Butylene Glycol Dicaprylate/Dicaprate 10.0% by weight Pigment 2 Appropriate amount preservative Appropriate amount
  • Example 8 division ingredient content A Purified water remaining amount glycerin 5.0% by weight Butylene glycol 10.0% by weight Pigment 1 Appropriate amount B Polyglyceryl-10 Laurate 7.0% by weight Polyglyceryl-10 myristate 7.0% by weight PEG-60 Hydrogenated Castor Oil 5.0% by weight Calendula oil 10.0% by weight Butylene Glycol Dicaprylate/Dicaprate 10.0% by weight Pigment 2 Appropriate amount preservative Appropriate amount
  • Example 9 division ingredient content A Purified water remaining amount glycerin 5.0% by weight Butylene glycol 10.0% by weight Pigment 1 Appropriate amount B Polyglyceryl-10 Laurate 7.0% by weight Polyglyceryl-10 myristate 7.0% by weight Polysorbate 20 5.0% by weight Calendula oil 10.0% by weight Butylene Glycol Dicaprylate/Dicaprate 10.0% by weight Pigment 2 Appropriate amount preservative Appropriate amount
  • Example 10 division ingredient content A Purified water remaining amount glycerin 5.0% by weight Butylene glycol 10.0% by weight Pigment 1 Appropriate amount B Polyglyceryl-10 Laurate 7.0% by weight Polyglyceryl-10 myristate 7.0% by weight Polysorbate 60 5.0% by weight Calendula oil 10.0% by weight Butylene Glycol Dicaprylate/Dicaprate 10.0% by weight Pigment 2 Appropriate amount preservative Appropriate amount
  • Example 11 division ingredient content A Purified water remaining amount glycerin 5.0% by weight Butylene glycol 10.0% by weight Pigment 1 Appropriate amount B Polyglyceryl-10 Laurate 7.0% by weight Polyglyceryl-10 myristate 7.0% by weight Polysorbate 80 5.0% by weight Calendula oil 10.0% by weight Butylene Glycol Dicaprylate/Dicaprate 10.0% by weight Pigment 2 Appropriate amount preservative Appropriate amount
  • the multilayered cosmetic compositions of Examples 12 to 16 were prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
  • First mixture preparation step (S10) Purified water and polyol containing glycerin were mixed, colorant was added, and the mixture was heated to 65°C to prepare the first mixture.
  • Emulsifying component including polyglyceryl-10 laurate and polyglyceryl-10 myristate, calendula oil, and butylene glycol dicaprylate/dicaprate.
  • oily components further containing one or more of meadowfoam seed oil, sunflower seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil are mixed, and coloring is added. and a preservative were added and then heated to 65°C to prepare a second mixture.
  • Example 12 is meadowfoam seed oil
  • Example 13 is sunflower seed oil
  • Example 14 is caprylic/capric triglyceride
  • Example 15 is grape seed.
  • Example 16 included avocado oil as an oil phase component.
  • Example 12 division ingredient content A Purified water remaining amount glycerin 5.0% by weight Butylene glycol 10.0% by weight Pigment 1 Appropriate amount B Polyglyceryl-10 Laurate 9.5% by weight Polyglyceryl-10 myristate 9.5% by weight Calendula oil 7.0% by weight Butylene Glycol Dicaprylate/Dicaprate 7.0% by weight Meadowfoam seed oil 6.0% by weight Pigment 2 Appropriate amount preservative Appropriate amount
  • Example 13 division ingredient content A Purified water remaining amount glycerin 5.0% by weight Butylene glycol 10.0% by weight Pigment 1 Appropriate amount B Polyglyceryl-10 Laurate 9.5% by weight Polyglyceryl-10 myristate 9.5% by weight Calendula oil 7.0% by weight Butylene Glycol Dicaprylate/Dicaprate 7.0% by weight sunflower seed oil 6.0% by weight Pigment 2 Appropriate amount preservative Appropriate amount
  • Example 14 division ingredient content A Purified water remaining amount glycerin 5.0% by weight Butylene glycol 10.0% by weight Pigment 1 Appropriate amount B Polyglyceryl-10 Laurate 9.5% by weight Polyglyceryl-10 myristate 9.5% by weight Calendula oil 7.0% by weight Butylene Glycol Dicaprylate/Dicaprate 7.0% by weight Caprylic/Capric Triglyceride 6.0% by weight Pigment 2 Appropriate amount preservative Appropriate amount
  • Example 15 division ingredient content A Purified water remaining amount glycerin 5.0% by weight Butylene glycol 10.0% by weight Pigment 1 Appropriate amount B Polyglyceryl-10 Laurate 9.5% by weight Polyglyceryl-10 myristate 9.5% by weight Calendula oil 7.0% by weight Butylene Glycol Dicaprylate/Dicaprate 7.0% by weight grape seed oil 6.0% by weight Pigment 2 Appropriate amount preservative Appropriate amount
  • Example 16 division ingredient content A Purified water remaining amount glycerin 5.0% by weight Butylene glycol 10.0% by weight Pigment 1 Appropriate amount B Polyglyceryl-10 Laurate 9.5% by weight Polyglyceryl-10 myristate 9.5% by weight Calendula oil 7.0% by weight Butylene Glycol Dicaprylate/Dicaprate 7.0% by weight avocado oil 6.0% by weight Pigment 2 Appropriate amount preservative Appropriate amount
  • the multilayered cosmetic composition of Preparation Example 1 was prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
  • First mixture preparation step (S10) Purified water, glycerin, butylene glycol, propanediol, 2,3-butanediol, pentylene glycol, sodium hyaluronate, and 1,2-hexanediol.
  • the first mixture was prepared by mixing the polyol containing the mixture, adding a pigment, and heating to 65°C.
  • Emulsifying components including generated castor oil, polysorbate 20, polysorbate 60, and polysorbate 80, calendula oil, butylene glycol dicaprylate/dicaprate, meadowfoam seed oil, and sunflower
  • the oil phase components including seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil were mixed, colorant and preservative were added, and then heated to 65°C to prepare a second mixture.
  • Example 1 4.4 Comparative Example 1 1.5 Comparative example 2 3.3 Comparative Example 3 3.5 Comparative example 4 3.4 Comparative Example 5 3.4 Example 2 4.4 Example 3 4.4 Example 4 4.4 Example 5 4.6 Example 6 4.5 Example 7 4.7 Example 8 4.6 Example 9 4.7 Example 10 4.6 Example 11 4.5 Example 12 4.6 Example 13 4.7 Example 14 4.6 Example 15 4.5 Example 16 4.6 Manufacturing Example 1 4.8
  • the oil phase contains a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main ingredients, and the oil phase contains a mixture of polyglyceryl-10 laurate and polyglyceryl-10 myristate as main ingredients.
  • oil painting department and, in the case of Example 1, which included both purified water and an aqueous phase containing polyol, it was confirmed that layer separation occurred well. On the other hand, in the case of Comparative Examples 1 to 5 lacking some components, it was confirmed that the degree of layer separation was significantly reduced.
  • Example 2 Example 3, and Example 4 in which only the type of polyol was changed from Example 1, similar values to Example 1 appeared, indicating that the type of polyol may be arbitrarily changed within the types described in the present invention. .
  • the oily part further includes any one or more from the group consisting of meadowfoam seed oil, sunflower seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil, and the emulsified part In the group consisting of lecithin, polyglyceryl-10 stearate, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, polysorbate 20, polysorbate 60, and polysorbate 80. When more than one was included, it was confirmed that the evaluation score regarding the degree of layer separation was somewhat high. The most excellent one was Preparation Example 1.
  • the test was repeated 5 times for each sample, and the average was calculated.
  • Example 1 6.7 Comparative Example 1 27.3 Comparative example 2 14.7 Comparative Example 3 16.4 Comparative Example 4 15.6 Comparative Example 5 17.3 Example 2 6.7 Example 3 6.6 Example 4 6.7 Example 5 5.5 Example 6 5.3 Example 7 5.5 Example 8 5.4 Example 9 5.6 Example 10 5.5 Example 11 5.3 Example 12 5.4 Example 13 5.5 Example 14 5.7 Example 15 5.5 Example 16 5.4 Manufacturing Example 1 3.2
  • the oil phase contains a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main components, and the oil phase contains a mixture of polyglyceryl-10 laurate and polyglyceryl-10 myristate as main components.
  • oil painting department in the case of Example 1, which includes both purified water and an aqueous phase containing polyol, it was confirmed that the mixing speed was fast and mixing was easily accomplished within a short time. On the other hand, in the case of Comparative Examples 1 to 5 lacking some components, it was confirmed that mixing was significantly slow.
  • Example 2 in which only the type of polyol was changed from Example 1, a similar time was consumed as Example 1, and the type of polyol may be arbitrarily changed within the types described in the present invention. represents.
  • the oily part further includes any one or more from the group consisting of meadowfoam seed oil, sunflower seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil, and the emulsified part In the group consisting of lecithin, polyglyceryl-10 stearate, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, polysorbate 20, polysorbate 60, and polysorbate 80. It was confirmed that when more than one was included, the mixing speed appeared somewhat faster. The fastest one was Preparation Example 1.
  • the test is shaken for the same amount of time and visually checked by 20 cosmetic ingredient experts using a 5-point scale (1 point if it is not mixed uniformly and large oil droplets are formed; 2 points if it is not mixed uniformly and oil droplets are formed normally; 2 points if it is mixed to an average degree) It was evaluated as 3 points if oil droplets were formed in small sizes, 4 points if they were uniformly mixed but the properties of each component were vaguely distinguished, and 5 points if they were uniformly dispersed and mixed like a single component), and this was calculated as the average.
  • Example 1 Degree of dispersion after mixing (evaluation score) Example 1 4.6 Comparative Example 1 1.8 Comparative example 2 3.5 Comparative example 3 3.3 Comparative example 4 3.6 Comparative Example 5 3.4 Example 2 4.6 Example 3 4.6 Example 4 4.6 Example 5 4.7 Example 6 4.8 Example 7 4.7 Example 8 4.7 Example 9 4.8 Example 10 4.8 Example 11 4.7 Example 12 4.7 Example 13 4.8 Example 14 4.8 Example 15 4.7 Example 16 4.8 Manufacturing example 1 4.9
  • the oil phase contains a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main ingredients, and the oil phase contains a mixture of polyglyceryl-10 laurate and polyglyceryl-10 myristate as main ingredients.
  • oil painting department and, in the case of Example 1, which includes both purified water and an aqueous phase containing polyol, it was confirmed that the evaluation score for the degree of dispersion after mixing was high. On the other hand, Comparative Examples 1 to 5 lacking some components showed significantly lower values.
  • Example 2 Example 3, and Example 4 in which only the type of polyol was changed from Example 1, evaluation scores similar to Example 1 were shown, and the type of polyol could be arbitrarily changed within the types described in the present invention. It indicates freedom.
  • the oily part further includes any one or more from the group consisting of meadowfoam seed oil, sunflower seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil, and the emulsified part In the group consisting of lecithin, polyglyceryl-10 stearate, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, polysorbate 20, polysorbate 60, and polysorbate 80. When more than one was included, it was confirmed that the evaluation score for the degree of dispersion after mixing was somewhat high. The most excellent one was Preparation Example 1.
  • compositions prepared in Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 were applied to 30 test subjects (men and women aged 20 to 45 years) on both sides of the face twice a day for 4 weeks.
  • the compositions prepared in Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 were applied to the first half, respectively, and the improvement in skin moisture was measured before application, after 30 minutes, and after 1 hour, using a skin moisture meter Corneometer CM 820. It was measured using (Courage + Khazaka, Germany), and the unit is expressed in an arbitrary unit (AU) given by the device. The higher the measured value, the higher the moisture content on the skin surface.
  • the oil phase contains a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main components, and the oil phase contains a mixture of polyglyceryl-10 laurate and polyglyceryl-10 myristate as main components.
  • oil painting department And, in the case of Example 1, which included both purified water and an aqueous phase containing polyol, it was confirmed that the moisturizing effect was excellent. On the other hand, Comparative Examples 1 to 5 lacking some components showed significantly lower values.
  • the oily part further includes any one or more from the group consisting of meadowfoam seed oil, sunflower seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil, and the emulsified part In the group consisting of lecithin, polyglyceryl-10 stearate, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, polysorbate 20, polysorbate 60, and polysorbate 80. When more than one was included, it was confirmed that the moisturizing effect was somewhat high. The most excellent one was Preparation Example 1.
  • the multilayer cosmetic composition according to the present invention has a high degree of multilayer separation, a quick mixing time, and , it was confirmed that not only was the degree of dispersion excellent after mixing, but also the moisturizing effect was excellent after application to the skin. That is, it can be confirmed that the multilayer cosmetic composition according to the present invention has excellent layer separation effect, ease of mixing, dispersibility after mixing, and skin moisturizing effect.
  • This effect is achieved by an oily part containing a mixture of calendula oil and butylene glycol dicaprylate/dicaprate, an emulsified part containing a mixture of polyglyceryl-10 laurate and polyglyceryl-10 myristate, and ,
  • This is a characteristic that can be confirmed only when the aqueous phase consists of a multi-layered phase containing purified water and polyol, and if any one of these components is lacking, the layer separation effect according to the present invention, ease of mixing, dispersibility after mixing, and skin moisturization It was confirmed through a comparative example lacking some ingredients that the effect was difficult to appear, and it was confirmed that the multilayer cosmetic composition according to the present invention brought about unexpected effects depending on the combination of each ingredient.
  • the present invention is a mixture of an oil phase containing a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main ingredients, and a mixture of polyglyceryl-10 laurate and polyglyceryl-10 myristate. It is stated that a multi-layered cosmetic composition has been developed as a novel composition consisting of an emulsified part containing as the main ingredient and an aqueous part containing purified water and polyol, and has a layer separation effect, ease of mixing, dispersibility after mixing, and skin moisturizing effect. .

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Abstract

The present invention relates to a multi-layer phase cosmetic composition comprising: an oil phase part containing a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main components; an emulsified part containing a mixture of polyglyceryl-10 laurate, polyglyceryl-10 myristate, and polyglyceryl-10 stearate as main components; and an aqueous part containing purified water and polyols, wherein each layer is stably separated, and upon application, the components of each layer mix together and then re-separate into multiple layers after a certain period of time.

Description

다층상 화장료 조성물Multilayer cosmetic composition
본 발명은 다층상의 화장료 조성물에 관한 것으로, 더 자세하게는, 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트의 혼합물을 주 성분으로 포함하는 유상부와, 폴리글리세릴-10라우레이트 및 폴리글리세릴-10미리스테이트의 혼합물을 주성분으로 포함하는 유화부, 정제수 및 폴리올을 포함하는 수상부로 이루어져, 각 층이 안정적으로 구분되며, 전단 시 각층의 성분이 혼합되고, 일정 시간 경과 후 다시 다층상으로 분리되도록 한 다층상 화장료 조성물에 관한 것이다. The present invention relates to a multi-layered cosmetic composition, and more specifically, to an oil phase comprising a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main ingredients, polyglyceryl-10 laurate, and It consists of an emulsified part containing a mixture of polyglyceryl-10 myristate as the main component, and an aqueous part containing purified water and polyol, so that each layer is stably separated. When sheared, the components of each layer are mixed, and after a certain period of time, the multilayer is again formed. It relates to a multi-layered cosmetic composition that can be separated into phases.
기초화장품의 기능은 피부 본래가 가지고 있는 기능을 정상적으로 작용하도록 도와주는 것이다. 따라서 화장품을 개발할 때 피부의 보습 메커니즘을 고려하여 수용성 보습물질과 유용성 오일막, 즉 수분 및 보습제와 유분의 적절한 배합으로 보습환경을 조성하여 피부의 항상성이 정상적으로 유지되도록 하는 것이 바람직하다.The function of basic cosmetics is to help the skin function normally. Therefore, when developing cosmetics, it is desirable to consider the skin's moisturizing mechanism and create a moisturizing environment with an appropriate combination of water-soluble moisturizing substances and oil-soluble oil film, that is, moisture, humectants, and oil, so that skin homeostasis is normally maintained.
환경오염과 노화 진행에 따라 항상성 유지 기능이 충분하지 못하여 점점 건조해지고 피부 표면이 거칠어지면 유분 및 수분을 모두 공급할 수 있는 화장품을 사용하여 피부의 모이스처 밸런스를 유지하고 피부 상태를 개선할 필요가 있다.As environmental pollution and aging progress, the homeostasis function is not sufficient, and the skin becomes increasingly dry and rough, so it is necessary to maintain the moisture balance of the skin and improve the skin condition by using cosmetics that can supply both oil and moisture.
이와 같은 과제를 해결하기 위한 화장료 조성물 중 하나로 다층상의 화장품이 있다. 일반적으로 서로 다른 액체를 혼합하면 섞이거나 분리가 일어난다. 예를 들면, 물과 기름을 혼합하면 비중이 상대적으로 높은 물이 아래로 가라앉아 하층부를 형성하고, 비중이 상대적으로 낮은 기름은 위로 뜨게 되어 상층부를 형성하게 된다. 이러한 혼합과 분리는 액체간의 상용성에 기인하는데, 서로 상용성이 높은 것끼리 혼합되면 서로 섞이고 상용성이 낮으면 분리가 일어난다.One of the cosmetic compositions to solve this problem is multilayer cosmetics. Generally, when different liquids are mixed, they either mix or separate. For example, when water and oil are mixed, water with a relatively high specific gravity sinks to the bottom to form the lower layer, and oil with a relatively low specific gravity floats to the top to form the upper layer. This mixing and separation is due to the compatibility between liquids. When things that are highly compatible with each other are mixed, they mix together, and if the compatibility is low, separation occurs.
기존 층상 구조의 화장료 조성물은 수상과 오일 사이의 2층상 구조의 화장료 조성물, 또는 수상과 파우더 사이의 비중차이를 이용한 2층상 구조가 대부분이었다. 이 중에서, 종래의 2층상 구조의 경우, 기본적인 파우더를 포함하는 화장료 조성물이 가져야 하는 3요소인 파우더, 유상, 수상을 모두 가지고 있지 않기 때문에 사용감이나 효과적인 면에서 한계가 발생할 수 밖에 없다.Most existing cosmetic compositions with a layered structure had a two-layer structure between the water phase and oil, or a two-layer structure using the difference in specific gravity between the water phase and the powder. Among these, in the case of the conventional two-layer structure, it does not have all three elements that a cosmetic composition containing basic powder must have, namely powder, oil phase, and water phase, so it inevitably has limitations in terms of feeling of use and effectiveness.
따라서, 적절한 유화제를 적용하여, 수상과 오일 상의 사이에 유화층을 형성하도록 하는 방법에 대한 연구가 늘어나고 있으며, 이와 같은 방법을 통해 사용자의 심미적인 욕구를 충족시킴은 물론, 각 층에 피부에 유용한 성분을 각기 다르게 적용할 수 있어, 화장료 조성물에 대해 새로운 접근을 시도할 수 있을 것이다. Therefore, research is increasing on methods to form an emulsified layer between the water phase and the oil phase by applying an appropriate emulsifier. This method not only satisfies the user's aesthetic needs, but also provides benefits to the skin in each layer. Since the ingredients can be applied differently, it will be possible to try a new approach to cosmetic compositions.
그러나, 종래의 다층상 화장료 조성물은, 아직 연구가 부족하여, 어떠한 성분이 어떤 층에 포함되어야 하는지, 이들의 조합에 따른 특성에 대한 연구가 부족하여, 층 분리가 뚜렷하지 않고, 혼합이 용이하지 않으며, 혼합 후 분산이 제대로 이루어지지 않는다던가, 피부 보습에 대한 보습효과 등을 충분히 충족하기 어려운 문제점이 있었다. However, conventional multi-layered cosmetic compositions are still lacking in research into which ingredients should be included in which layer and the characteristics of their combination, so the layer separation is not clear and mixing is not easy. However, there were problems such as poor dispersion after mixing and difficulty in satisfying the moisturizing effect on the skin.
[선행기술문헌][Prior art literature]
[특허문헌][Patent Document]
(특허문헌 1) 대한민국 등록특허공보 제10-0933551호(2009.12.23.공고), "2층상 파운데이션 화장료 조성물" (Patent Document 1) Republic of Korea Patent Publication No. 10-0933551 (announced on December 23, 2009), “Two-layer foundation cosmetic composition”
상기와 같은 문제점을 해결하기 위하여 본 발명은 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트의 혼합물을 주 성분으로 포함하는 유상부와, 폴리글리세릴-10라우레이트 및 폴리글리세릴-10미리스테이트의 혼합물을 주성분으로 포함하는 유화부, 정제수 및 폴리올을 포함하는 수상부로 이루어져, 각 층이 안정적으로 구분되며, 전단 시 각층의 성분이 혼합되고, 일정 시간 경과 후 다시 다층상으로 분리되도록 한 다층상 화장료 조성물을 제공하는데 그 목적이 있다. In order to solve the above problems, the present invention provides an oil phase containing a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main ingredients, polyglyceryl-10 laurate and polyglyceryl- It consists of an emulsified part containing a mixture of 10 myristate as the main component, and an aqueous part containing purified water and polyol, so that each layer is stably separated, and when sheared, the components of each layer are mixed and separated again into a multilayer phase after a certain period of time. The purpose is to provide a multilayer cosmetic composition.
상기와 같은 목적을 달성하기 위하여 본 발명은, 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트의 혼합물을 주 성분으로 포함하는 유상부, 폴리글리세릴-10라우레이트 및 폴리글리세릴-10미리스테이트의 혼합물을 주성분으로 포함하는 유화부; 및, 정제수 및 폴리올을 포함하는 수상부;의 다층상으로 이루어지는 것을 특징으로 하는 화장료 조성물을 제공한다. In order to achieve the above object, the present invention provides an oil phase containing a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main ingredients, polyglyceryl-10 laurate and polyglyceryl- An emulsified portion containing a mixture of 10 myristate as a main ingredient; and an aqueous phase containing purified water and polyol.
또한, 상기 유상부는 메도우폼씨오일, 해바라기씨오일, 카프릴릭/카프릭트라이글리세라이드, 포도씨오일, 아보카도오일로 구성된 군에서 어느 하나 이상을 선택하여 더 포함하는 것을 특징으로 한다. In addition, the oily part further includes one or more selected from the group consisting of meadowfoam seed oil, sunflower seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil.
또한, 상기 유화부는 레시틴, 피이지-40하이드로제네이티드캐스터오일, 피이지-60하이드로제네이티드캐스터오일, 폴리소르베이트 20, 폴리소르베이트 60, 폴리소르베이트 80으로 구성되는 군에서 어느 하나 이상을 선택하여 더 포함하는 것을 특징으로 한다. In addition, the emulsifying part contains one or more from the group consisting of lecithin, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, polysorbate 20, polysorbate 60, and polysorbate 80. It is characterized by further inclusion by selection.
또한, 상기 수상부의 폴리올은 글리세린, 부틸렌글라이콜, 프로판다이올, 2,3-부탄다이올, 펜틸렌글라이콜, 소듐하이알루로네이트, 1,2-헥산다이올로 구성되는 군에서 어느 하나 이상인 것을 특징으로 한다. In addition, the polyol of the aqueous phase is any of the group consisting of glycerin, butylene glycol, propanediol, 2,3-butanediol, pentylene glycol, sodium hyaluronate, and 1,2-hexanediol. It is characterized by having more than one.
전체 화장료 조성물 100 중량부에 대해, 상기 유상부는 1.0 ~ 30.0 중량부로 포함되며, 상기 유화부는 1.0 ~ 30.0 중량부로 포함되고, 상기 수상부의 폴리올은 5.0 ~ 30.0 중량부, 상기 수상부의 정제수는 잔량으로 포함되는 것을 특징으로 한다.With respect to 100 parts by weight of the total cosmetic composition, the oil phase part is included in an amount of 1.0 to 30.0 parts by weight, the emulsified part is included in an amount of 1.0 to 30.0 parts by weight, the polyol in the aqueous phase part is included in an amount of 5.0 to 30.0 parts by weight, and the purified water in the aqueous phase part is included in the remaining amount. It is characterized by being
본 발명에 따른 다층상 화장료 조성물은 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트의 혼합물을 주 성분으로 포함하는 유상부와, 폴리글리세릴-10라우레이트 및 폴리글리세릴-10미리스테이트의 혼합물을 주성분으로 포함하는 유화부, 정제수 및 폴리올을 포함하는 수상부로 이루어져, 각 층이 안정적으로 구분되며, 전단 시 각층의 성분이 혼합되고, 일정 시간 경과 후 다시 다층상으로 분리되는 효과를 갖는다. 또한, 본 발명에 따른 다층상 화장료 조성물은 각 층에 성분을 달리하여 수용할 수 있으며, 보습 효과가 우수하다. The multilayered cosmetic composition according to the present invention has an oily part containing a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main ingredients, and polyglyceryl-10 laurate and polyglyceryl-10 milliliter. It consists of an emulsified part containing a mixture of states as the main component, and an aqueous part containing purified water and polyol, so that each layer is stably separated, and when sheared, the components of each layer are mixed, and after a certain period of time, they are separated into a multilayer phase again. have In addition, the multi-layered cosmetic composition according to the present invention can contain different components in each layer and has excellent moisturizing effect.
도 1은 본 발명에 따른 다층상 화장료 조성물의 층분리 상태를 촬영한 사진1 is a photograph of the layer separation state of the multilayer cosmetic composition according to the present invention.
도 2는 본 발명에 따른 다층상 화장료 조성물의 혼합 상태를 촬영한 사진Figure 2 is a photograph of the mixing state of the multilayer cosmetic composition according to the present invention.
도 3은 본 발명의 실시예 1 내지 16, 비교예 1 내지 5, 제조예 1에 대한 층상 분리 정도 확인 실험에 관한 그래프. Figure 3 is a graph relating to an experiment confirming the degree of layer separation for Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 of the present invention.
도 4는 본 발명의 실시예 1 내지 16, 비교예 1 내지 5, 제조예 1에 대한 혼합 시간 확인 실험에 관한 그래프. Figure 4 is a graph showing mixing time confirmation experiments for Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 of the present invention.
도 5는 본 발명의 실시예 1 내지 16, 비교예 1 내지 5, 제조예 1에 대한 혼합 후 분산 정도 확인 실험에 관한 그래프. Figure 5 is a graph showing an experiment confirming the degree of dispersion after mixing for Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 of the present invention.
도 6은 본 발명의 실시예 1 내지 16, 비교예 1 내지 5, 제조예 1에 대한 층상 피부 보습 효과 확인 실험에 관한 그래프. Figure 6 is a graph relating to an experiment confirming the layered skin moisturizing effect for Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 of the present invention.
이하의 본 발명에 관한 상세한 설명들은 본 발명이 실시될 수 있는 실시 예이고 해당 실시 예의 예시로써 도시된 첨부 도면을 참조한다. 이들 실시 예는 당 업자가 본 발명의 실시에 충분하도록 상세히 설명된다. 본 발명의 다양한 실시 예는 서로 다르지만 상호 배타적일 필요는 없음이 이해되어야 한다. 예를 들어, 여기에 기재되어 있는 특정 형상, 구조 및 특성은 일 실시 예에 관련하여 본 발명의 사상 및 범위를 벗어나지 않으면서 다른 실시 예로 구현될 수 있다. 또한, 각각의 기재된 실시 예 내의 개별 구성요소의 위치 또는 배치는 본 발명의 사상 및 범위를 벗어나지 않으면서 변경될 수 있음이 이해되어야 한다. The following detailed description of the present invention is an embodiment in which the present invention can be practiced and refers to the accompanying drawings, which are shown as examples of the corresponding embodiments. These embodiments are described in sufficient detail to enable any person skilled in the art to practice the invention. It should be understood that the various embodiments of the invention are different from one another but are not necessarily mutually exclusive. For example, specific shapes, structures and characteristics described herein may be implemented in one embodiment without departing from the spirit and scope of the invention. Additionally, it should be understood that the location or arrangement of individual components within each described embodiment may be changed without departing from the spirit and scope of the invention.
따라서 후술되는 상세한 설명은 한정적인 의미로서 취하려는 것이 아니며, 본 발명의 범위는 적절하게 설명된다면 그 청구항들이 주장하는 것과 균등한 모든 범위와 더불어 첨부된 청구항에 의해서만 한정된다. 도면에서 유사한 참조부호는 여러 측면에 걸쳐서 동일하거나 유사한 기능을 지칭한다. Accordingly, the detailed description set forth below is not intended to be taken in a limiting sense, and the scope of the invention is limited only by the appended claims together with all equivalents to what those claims would assert if properly described. Similar reference numbers in the drawings refer to identical or similar functions across various aspects.
본 발명에서 사용되는 용어는 본 발명에서의 기능을 고려하면서 가능한 현재 널리 사용되는 일반적인 용어들을 선택하였으나, 이는 당 분야에 종사하는 기술자의 의도 또는 판례, 새로운 기술의 출현 등에 따라 달라질 수 있다. 또한, 특정한 경우는 출원인이 임의로 선정한 용어도 있으며, 이 경우 해당되는 발명의 설명 부분에서 상세히 그 의미를 기재할 것이다. 따라서 본 발명에서 사용되는 용어는 단순한 용어의 명칭이 아닌, 그 용어가 가지는 의미와 본 발명의 전반에 걸친 내용을 토대로 정의되어야 한다. The terms used in the present invention are general terms that are currently widely used as much as possible while considering the function in the present invention, but this may vary depending on the intention or precedent of a person working in the art, the emergence of new technology, etc. In addition, in certain cases, there are terms arbitrarily selected by the applicant, and in this case, the meaning will be described in detail in the description of the relevant invention. Therefore, the terms used in the present invention should be defined based on the meaning of the term and the overall content of the present invention, rather than simply the name of the term.
본 발명에서 어떤 부분이 어떤 구성요소를 “포함”한다고 할 때, 이는 특별히 반대되는 기재가 없는 한, 다른 구성요소를 제외하는 것이 아니라 다른 구성요소를 더 포함할 수 있음을 의미한다. In the present invention, when a part “includes” a certain component, this means that, unless specifically stated to the contrary, it does not exclude other components but may further include other components.
이하, 본 발명에 따른 다층상 화장료 조성물에 대하여 자세히 설명한다. Hereinafter, the multilayer cosmetic composition according to the present invention will be described in detail.
본 발명에 따른 다층상 화장료 조성물은 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트의 혼합물을 유효성분으로 포함하는 유상부와, 폴리글리세릴-10라우레이트 및 폴리글리세릴-10미리스테이트의 혼합물을 유효성분으로 포함하는 유화부, 그리고, 정제수 및 폴리올을 포함하는 수상부로 이루어진다. The multilayered cosmetic composition according to the present invention has an oily part containing a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as active ingredients, and polyglyceryl-10 laurate and polyglyceryl-10 milliliter. It consists of an emulsified part containing a mixture of states as an active ingredient, and an aqueous phase containing purified water and polyol.
상기 유상부는 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트의 혼합물을 주 유효성분으로 포함한다. The oil phase contains a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as the main active ingredient.
상기 카렌둘라오일(Calendula Officinalis Flower Oil)은 멕시코 원산인 카렌둘라(금잔화)의 꽃을 증류하여 얻은 오일로 상기 카렌듈라는 대한민국 산야에서도 잘 자라며, 상기 카렌둘라(카렌듈라)는 금잔화, 메리골드, 홍황초 등으로 불리며, 양지 바른 모래흙에서 잘 자라는 성질을 갖는다. The calendula oil (Calendula Officinalis Flower Oil) is an oil obtained by distilling the flowers of calendula (marigold), a native of Mexico. The calendula grows well in the mountains and fields of Korea, and the calendula (calendula) includes marigolds, marigolds, and marigolds. It is also called a tree and has the property of growing well in sunny, sandy soil.
상기 부틸렌글라이콜다이카프릴레이트/다이카프레이트(Butylene Glycol Dicaprylate/Dicaprate)는 카프릴릭 및 카프릭애씨드의 부틸렌글라이콜다이에스터의 혼합물이다. 상기 부틸렌글라이콜다이카프릴레이트/다이카프레이트는 주로 피부컨디셔닝제(수분차단제), 용제로 사용되는 원료다. The Butylene Glycol Dicaprylate/Dicaprate is a mixture of butylene glycol diester of caprylic and capric acid. The butylene glycol dicaprylate/dicaprate is a raw material mainly used as a skin conditioning agent (moisture blocker) and solvent.
상기 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트는 0.01 : 99.99 ~ 99.99 : 0.01의 중량비로 혼합된 것일 수 있다. The calendula oil and butylene glycol dicaprylate/dicaprate may be mixed at a weight ratio of 0.01:99.99 to 99.99:0.01.
다만, 상기 유상부의 성분이 이에 한정되는 것은 아니며, 상기 유상부의 성분으로는, 극성 오일이라면 다 포함될 수 있을 것이다. 이에 상기 유상부에는 메도우폼씨오일, 해바라기씨오일, 카프릴릭/카프릭트라이글리세라이드, 포도씨오일, 아보카도오일로 구성된 군에서 어느 하나 이상을 선택하여 더 포함될 수 있다. However, the components of the oil phase are not limited to this, and the components of the oil phase may include any polar oil. Accordingly, the oily part may further include one or more selected from the group consisting of meadowfoam seed oil, sunflower seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil.
상기 메도우폼씨오일(Limnanthes Alba (Meadowfoam) Seed Oil)은 메도우폼 (Limnanthes alba)의 씨에서 추출한 오일을 칭한다.Limnanthes Alba (Meadowfoam) Seed Oil refers to oil extracted from the seeds of Limnanthes alba.
상기 해바라기씨오일(Helianthus Annuus (Sunflower) Seed Oil)은 해바라기 (Helianthus annuus)의 씨를 압착하여 얻은 오일을 칭한다.The sunflower seed oil (Helianthus Annuus (Sunflower) Seed Oil) refers to oil obtained by pressing the seeds of sunflower (Helianthus annuus).
상기 카프릴릭/카프릭트라이글리세라이드(Caprylic/Capric Triglyceride)는 카프릴릭과 카프릭애씨드 및 글리세린의 혼합 트라이에스터를 칭한다.The caprylic/capric triglyceride refers to a mixed triester of caprylic, capric acid, and glycerin.
상기 포도씨오일(Vitis Vinifera (Grape) Seed Oil)은 포도 (Vitis vinifera)의 씨를 압착하여 얻은 불휘발성 오일을 칭한다. The grape seed oil (Vitis Vinifera (Grape) Seed Oil) refers to a non-volatile oil obtained by pressing the seeds of grapes (Vitis vinifera).
상기 아보카도오일(Persea Gratissima (Avocado) Oil)은 아보카도 (Persea gratissima)에서 얻은 오일을 칭한다. The avocado oil (Persea Gratissima (Avocado) Oil) refers to the oil obtained from avocado (Persea gratissima).
한편, 유상부는 전체 화장료 조성물 100 중량부에 대해 1.0 ~ 30.0 중량부로 포함될 수 있다.Meanwhile, the oil phase may be included in an amount of 1.0 to 30.0 parts by weight based on 100 parts by weight of the total cosmetic composition.
또한, 상기 유상부에는 비극성오일이나 실리콘오일은 포함되지 않는 것이 적절하며, 극성오일만을 포함하는 것이 바람직하다. In addition, it is appropriate that the oil phase does not contain non-polar oil or silicone oil, and preferably contains only polar oil.
상기 유상부에는 보존제 등이 추가로 포함될 수 있다. The oily part may additionally contain a preservative or the like.
상기 유화부는 폴리글리세릴-10라우레이트 및 폴리글리세릴-10미리스테이트 의 혼합물을 주 유효성분으로 포함한다. The emulsification part contains a mixture of polyglyceryl-10 laurate and polyglyceryl-10 myristate as the main active ingredient.
상기 폴리글리세릴-10라우레이트(Polyglyceryl-10 Laurate)는 라우릭애씨드와 폴리글리세린-10의 에스터이다. 상기 폴리글리세릴-10라우레이트는 주로 피부컨디셔닝제, 계면활성제-유화제로 사용되는 원료다. The polyglyceryl-10 laurate is an ester of lauric acid and polyglycerin-10. The polyglyceryl-10 laurate is a raw material mainly used as a skin conditioning agent and surfactant-emulsifier.
상기 폴리글리세릴-10미리스테이트(Polyglyceryl-10 Myristate)는 미리스틱애씨드와 폴리글리세린-10의 에스터이다. 상기 폴리글리세릴-10미리스테이트는 주로 피부컨디셔닝제, 계면활성제-유화제로 사용되는 원료다.The polyglyceryl-10 myristate is an ester of myristic acid and polyglycerin-10. The polyglyceryl-10 myristate is a raw material mainly used as a skin conditioning agent and surfactant-emulsifier.
다만, 유화부의 성분이 이에 한정되는 것은 아니며, 상기 유화부에는 레시틴, 폴리글리세릴-10스테아레이트, 피이지-40하이드로제네이티드캐스터오일, 피이지-60하이드로제네이티드캐스터오일, 폴리소르베이트 20, 폴리소르베이트 60, 폴리소르베이트 80으로 구성되는 군에서 어느 하나 이상을 선택하여 더 포함될 수 있다. However, the ingredients of the emulsified part are not limited to this, and the emulsified part includes lecithin, polyglyceryl-10 stearate, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, and polysorbate 20. , polysorbate 60, and polysorbate 80 may be further included by selecting any one or more from the group consisting of.
상기 레시틴(Lecithin)은 스테아릭애씨드, 팔미틱애씨드 및 올레익애씨드의 천연에 존재하는 다이글리세라이드 혼합물로 포스포릭애씨드의 콜린에스터에 결합되어 있으며 살아있는 동식물에서 발견된다.The lecithin is a naturally occurring diglyceride mixture of stearic acid, palmitic acid, and oleic acid, and is bound to the choline ester of phosphoric acid and is found in living animals and plants.
상기 폴리글리세릴-10스테아레이트(Polyglyceryl-10 Stearate)는 스테아릭애씨드와 폴리글리세린-10의 에스터다. The polyglyceryl-10 stearate is an ester of stearic acid and polyglycerin-10.
상기 피이지-40하이드로제네이티드캐스터오일(PEG-40 Hydrogenated Castor Oil)은 평균 40몰의 에칠렌옥사이드를 함유한 하이드로제네이티드캐스터오일의 폴리에칠렌글라이콜 유도체이다.The PEG-40 Hydrogenated Castor Oil is a polyethylene glycol derivative of hydrogenated castor oil containing an average of 40 moles of ethylene oxide.
상기 피이지-60하이드로제네이티드캐스터오일(PEG-60 Hydrogenated Castor Oil)은 평균 60몰의 에칠렌옥사이드를 함유한 하이드로제네이티드캐스터오일의 폴리에칠렌글라이콜 유도체이다.The PEG-60 Hydrogenated Castor Oil is a polyethylene glycol derivative of hydrogenated castor oil containing an average of 60 moles of ethylene oxide.
상기 폴리소르베이트 20(Polysorbate 20)은 주로 모노에스터로 구성되며 에틸렌옥사이드 약 20몰로 축합된 솔비톨안하이드라이드와 솔비톨의 라우레이트에스터의 혼합물이다. Polysorbate 20 is mainly composed of monoesters and is a mixture of sorbitol anhydride and sorbitol laurate ester condensed with about 20 moles of ethylene oxide.
상기 폴리소르베이트 60(Polysorbate 60)은 주로 모노에스터로 구성되며 에틸렌옥사이드 약 60몰로 축합된 솔비톨안하이드라이드와 솔비톨의 스테아레이트에스터의 혼합물이다. Polysorbate 60 is mainly composed of monoesters and is a mixture of sorbitol anhydride and sorbitol stearate ester condensed with about 60 moles of ethylene oxide.
상기 폴리소르베이트 80(Polysorbate 80)은 주로 모노에스터로 구성되며 에틸렌옥사이드 약 80몰로 축합된 솔비톨안하이드라이드와 솔비톨의 올리에이트에스터의 혼합물로서 주로 다음의 구조를 갖는다.Polysorbate 80 is mainly composed of monoesters and is a mixture of sorbitol anhydride and sorbitol oleate ester condensed with about 80 moles of ethylene oxide, and has the following structure.
상기 유화부는 전체 화장료 조성물 100 중량부에 대해 1.0 ~ 30.0 중량부로 포함될 수 있다.The emulsifying part may be included in an amount of 1.0 to 30.0 parts by weight based on 100 parts by weight of the total cosmetic composition.
상기 수상부는 정제수 및 폴리올을 주 유효성분으로 포함한다. The aqueous phase contains purified water and polyol as main active ingredients.
상기 수상부의 보습제는 글리세린, 부틸렌글라이콜, 프로판다이올, 2,3-부탄다이올, 펜틸렌글라이콜, 소듐하이알루로네이트, 1,2-헥산다이올로 구성되는 군에서 어느 하나 이상일 수 있다. The moisturizing agent for the aqueous phase may be any one or more from the group consisting of glycerin, butylene glycol, propanediol, 2,3-butanediol, pentylene glycol, sodium hyaluronate, and 1,2-hexanediol. You can.
상기 글리세린(Glycerin)은 폴리하이드릭알코올로써, 변성제, 착향제, 헤어컨디셔닝제, 보습제, 피부보호제, 피부컨디셔닝제(보습제), 점도감소제로 사용되는 성분이다. Glycerin is polyhydric alcohol and is an ingredient used as a denaturant, flavoring agent, hair conditioning agent, moisturizing agent, skin protection agent, skin conditioning agent (moisturizer), and viscosity reducer.
상기 부틸렌글라이콜(Butylene Glycol)은 지방족 디올로써, 착향제, 피부컨디셔닝제, 용제, 점도감소제로 사용되는 성분이다. Butylene Glycol is an aliphatic diol and is an ingredient used as a flavoring agent, skin conditioning agent, solvent, and viscosity reducer.
상기 프로판다이올(Propanediol)은 유기화합물의 일종으로, 용제, 점도감소제로 사용되는 성분이다. The propanediol is a type of organic compound and is used as a solvent and viscosity reducer.
상기 2,3-부탄다이올(2,3-Butanediol)은 유기화합물의 일종으로, 착향제, 보습제, 피부컨디셔닝제(보습제), 용제로 사용되는 성분이다. The 2,3-butanediol is a type of organic compound and is used as a flavoring agent, moisturizer, skin conditioning agent (moisturizer), and solvent.
상기 펜틸렌글라이콜(Pentylene Glycol)은 유기화합물의 일종으로, 피부컨디셔닝제, 용제로 사용되는 성분이다. Pentylene Glycol is a type of organic compound and is used as a skin conditioning agent and solvent.
상기 소듐하이알루로네이트(Sodium Hyaluronate)는 하이알루로닉애씨드의 소듐염으로, 피부컨디셔닝제로 사용되는 성분이다. Sodium Hyaluronate is the sodium salt of hyaluronic acid and is an ingredient used as a skin conditioning agent.
상기 1,2-헥산다이올(1,2-Hexanediol)은 유기화합물의 일종으로, 용제 등으로 사용되는 성분이다. The 1,2-hexanediol is a type of organic compound and is used as a solvent.
상기 수상부의 폴리올은 전체 화장료 조성물 100 중량부에 대해 5.0 ~ 30.0 중량부, 상기 수상부의 정제수는 잔량으로 포함될 수 있다.The polyol in the aqueous phase may be included in an amount of 5.0 to 30.0 parts by weight based on 100 parts by weight of the total cosmetic composition, and the purified water in the aqueous phase may be included in the remaining amount.
한편, 상기 수상부에는 상기 열거한 성분들 외에 기타 피부에 유용한 컨디셔닝제들이 더 포함될 수 있다. 다만, 상기 수상부에 카보머는 포함하지 않는 것이 적절할 것이다. Meanwhile, the water phase may further include other conditioning agents useful for the skin in addition to the ingredients listed above. However, it would be appropriate not to include carbomer in the aqueous phase.
이하, 본 발명에 따른 다층상 화장료 조성물의 제조방법에 대하여 간단히 설명한다. Hereinafter, the manufacturing method of the multilayer cosmetic composition according to the present invention will be briefly described.
본 발명에 따른 다층상 화장료 조성물의 제조방법은, 정제수와 폴리올을 혼합하여 제1혼합물을 형성하고, 50 ~ 80℃까지 가온하는 제1혼합물 제조 단계(S10); 유화부의 각 성분과와, 유상부의 각 성분을 혼합하여 제2혼합물을 형성하고, 50 ~ 80℃까지 가온하는 제2혼합물 제조 단계(S20); 상기 제1혼합물 제조 단계(S10)에서 가온 중인 제1혼합물과, 상기 제2혼합물 제조 단계(S20)에서 가온 중인 제2혼합물을 서로 혼합하여, 다층상 화장료 조성물을 제조하는 다층상 화장료 조성물 제조 단계(S30);를 포함한다. The method for producing a multilayer cosmetic composition according to the present invention includes a first mixture preparation step (S10) of mixing purified water and polyol to form a first mixture and heating to 50 to 80°C; A second mixture preparation step (S20) of mixing each component of the emulsified portion and each component of the oil phase to form a second mixture and heating to 50 to 80°C; A multi-layer cosmetic composition manufacturing step of mixing the first mixture being heated in the first mixture preparation step (S10) and the second mixture being heated in the second mixture preparation step (S20) to produce a multi-layer cosmetic composition. (S30); includes.
우선, 제1혼합물 제조 단계(S10)를 수행한다. First, the first mixture preparation step (S10) is performed.
상기 제1혼합물 제조 단계(S10)에서의 제1혼합물은 정제수와 폴리올을 혼합하여 형성되며, 50 ~ 80℃까지 가온하는 것이 바람직하다. The first mixture in the first mixture preparation step (S10) is formed by mixing purified water and polyol, and is preferably heated to 50 to 80°C.
이때, 상기 제1혼합물 제조 단계(S10)에서의 폴리올은 글리세린, 부틸렌글라이콜, 프로판다이올, 2,3-부탄다이올, 펜틸렌글라이콜, 소듐하이알루로네이트, 1,2-헥산다이올로 구성되는 군에서 선택된 어느 하나 이상일 수 있다. At this time, the polyol in the first mixture preparation step (S10) is glycerin, butylene glycol, propanediol, 2,3-butanediol, pentylene glycol, sodium hyaluronate, and 1,2-hexane. It may be any one or more selected from the group consisting of diol.
다음으로, 제2혼합물 제조 단계(S20)를 수행한다. Next, the second mixture preparation step (S20) is performed.
상기 제2혼합물 제조 단계(S20)에서의 제2혼합물은, 유화부의 각 성분과, 유상부의 각 성분을 혼합하여 형성되며, 50 ~ 80℃까지 가온하는 것이 바람직하다. The second mixture in the second mixture preparation step (S20) is formed by mixing each component of the emulsified portion and each component of the oil phase portion, and is preferably heated to 50 to 80°C.
이때, 상기 제2혼합물 제조 단계(S20)에서의 유화부는 폴리글리세릴-10라우레이트 및 폴리글리세릴-10미리스테이트인 것이 바람직하며, 그 외에 레시틴, 폴리글리세릴-10스테아레이트, 피이지-40하이드로제네이티드캐스터오일, 피이지-60하이드로제네이티드캐스터오일, 폴리소르베이트 20, 폴리소르베이트 60, 폴리소르베이트 80 등이 포함될 수 있다. At this time, the emulsifying part in the second mixture preparation step (S20) is preferably polyglyceryl-10 laurate and polyglyceryl-10 myristate, and in addition, lecithin, polyglyceryl-10 stearate, PEG- It may include 40 Hydrogenated Castor Oil, PEG-60 Hydrogenated Castor Oil, Polysorbate 20, Polysorbate 60, Polysorbate 80, etc.
이때, 상기 제2혼합물 제조 단계(S20)에서의 유상부는 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트인 것이 바람직하며, 그 외에 메도우폼씨오일, 해바라기씨오일, 카프릴릭/카프릭트라이글리세라이드, 포도씨오일, 아보카도오일 등이 포함될 수 있다. At this time, the oil phase in the second mixture preparation step (S20) is preferably calendula oil and butylene glycol dicaprylate/dicaprate, and in addition, meadowfoam seed oil, sunflower seed oil, and caprylic oil. /May include capric triglyceride, grape seed oil, avocado oil, etc.
다음으로, 다층상 화장료 조성물 제조 단계(S30)를 수행한다. Next, a multilayer cosmetic composition manufacturing step (S30) is performed.
상기 다층상 화장료 조성물 제조 단계(S30)에서의 다층상 화장료 조성물은, 상기 제1혼합물 제조 단계(S10)에서 50 ~ 80℃로 가온 중인 제1혼합물과, 상기 제2혼합물 제조 단계(S20)에서 50 ~ 80℃로 가온 중인 제2혼합물을 서로 혼합하여, 제조되는 것이 바람직하다. The multilayered cosmetic composition in the multilayered cosmetic composition manufacturing step (S30) is a first mixture being heated to 50 to 80° C. in the first mixture manufacturing step (S10), and a second mixture manufacturing step (S20). It is preferably prepared by mixing the second mixture, which is heated at 50 to 80°C.
상기 다층상 화장료 조성물 제조 단계(S30)를 수행하고 나면 본 발명에 따른 다층상 화장료가 제조된다. After performing the multi-layered cosmetic composition manufacturing step (S30), the multi-layered cosmetic according to the present invention is manufactured.
이하, 하기 실시예, 비교예 및 실험예를 통하여 본 발명에 따른 다층상 화장료 조성물이 갖는 효과에 대하여 자세히 살펴본다. Hereinafter, the effects of the multilayer cosmetic composition according to the present invention will be examined in detail through the following examples, comparative examples, and experimental examples.
실시예 1. 다층상 화장료 조성물의 제조Example 1. Preparation of multilayer cosmetic composition
하기 제조공정에 따라 실시예 1의 다층상 화장료 조성물을 제조하였다. 하기 제조공정에 있어서, 색소 및 보존제는 별도의 효과를 위해 적용되는 것일 뿐, 조성물의 기능에 영향을 미치는 성분은 아니다. The multilayer cosmetic composition of Example 1 was prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
제1혼합물 제조 단계(S10): 정제수와, 글리세린을 포함하는 폴리올을 혼합하고, 색소를 추가한 다음, 65℃까지 가온하여, 제1혼합물을 제조하였다. First mixture preparation step (S10): Purified water and polyol containing glycerin were mixed, colorant was added, and the mixture was heated to 65°C to prepare the first mixture.
제2혼합물 제조 단계(S20): 폴리글리세릴-10라우레이트, 폴리글리세릴-10미리스테이트를 포함하는 유화부 성분과, 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트를 포함하는 유상부 성분을 혼합하고, 색소 및 보존제를 추가한 다음, 65℃까지 가온하여 제2혼합물을 제조하였다. Second mixture preparation step (S20): Emulsifying component including polyglyceryl-10 laurate and polyglyceryl-10 myristate, calendula oil, and butylene glycol dicaprylate/dicaprate. The oil phase components were mixed, colorant and preservative were added, and then heated to 65°C to prepare a second mixture.
다층상 화장료 조성물 제조 단계(S30): 상기 제1혼합물 제조 단계(S10)에서 65℃로 가온 중인 제1혼합물과, 상기 제2혼합물 제조 단계(S20)에서 65℃로 가온 중인 제2혼합물을 서로 혼합하여, 다층상 화장료 조성물을 제조하였다. Multilayer cosmetic composition manufacturing step (S30): The first mixture being heated to 65°C in the first mixture manufacturing step (S10) and the second mixture being heated to 65°C in the second mixture manufacturing step (S20) are mixed with each other. By mixing, a multilayer cosmetic composition was prepared.
이때, 각 성분의 조성은 하기 표 1과 같다. At this time, the composition of each component is shown in Table 1 below.
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 15.0중량%15.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 9.5중량%9.5% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 9.5중량%9.5% by weight
카렌둘라오일Calendula oil 10.0중량%10.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 10.0중량%10.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
비교예 1. 폴리올을 배제한 실험용 조성물의 제조Comparative Example 1. Preparation of experimental composition excluding polyol
하기 제조공정에 따라 비교예 1의 비교용 조성물을 제조하였다. 하기 제조공정에 있어서, 색소 및 보존제는 별도의 효과를 위해 적용되는 것일 뿐, 조성물의 기능에 영향을 미치는 성분은 아니다. The comparative composition of Comparative Example 1 was prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
제1혼합물 제조 단계(S10): 정제수에 색소를 추가한 다음, 65℃까지 가온하여, 제1혼합물을 제조하였다. First mixture preparation step (S10): Pigment was added to purified water and then heated to 65°C to prepare the first mixture.
제2혼합물 제조 단계(S20): 폴리글리세릴-10라우레이트, 폴리글리세릴-10미리스테이트를 포함하는 유화부 성분과, 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트를 포함하는 유상부 성분을 혼합하고, 색소 및 보존제를 추가한 다음, 65℃까지 가온하여 제2혼합물을 제조하였다. Second mixture preparation step (S20): Emulsifying component including polyglyceryl-10 laurate and polyglyceryl-10 myristate, calendula oil, and butylene glycol dicaprylate/dicaprate. The oil phase components were mixed, colorant and preservative were added, and then heated to 65°C to prepare a second mixture.
다층상 화장료 조성물 제조 단계(S30): 상기 제1혼합물 제조 단계(S10)에서 65℃로 가온 중인 제1혼합물과, 상기 제2혼합물 제조 단계(S20)에서 65℃로 가온 중인 제2혼합물을 서로 혼합하여, 다층상 화장료 조성물을 제조하였다. Multilayer cosmetic composition manufacturing step (S30): The first mixture being heated to 65°C in the first mixture manufacturing step (S10) and the second mixture being heated to 65°C in the second mixture manufacturing step (S20) are mixed with each other. By mixing, a multilayer cosmetic composition was prepared.
이때, 각 성분의 조성은 하기 표 2와 같다. At this time, the composition of each component is shown in Table 2 below.
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 9.5중량%9.5% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 9.5중량%9.5% by weight
카렌둘라오일Calendula oil 10.0중량%10.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 10.0중량%10.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
비교예 2. 폴리글리세릴-10라우레이트를 배제한 실험용 조성물의 제조Comparative Example 2. Preparation of experimental composition excluding polyglyceryl-10 laurate
하기 제조공정에 따라 비교예 2의 비교용 조성물을 제조하였다. 하기 제조공정에 있어서, 색소 및 보존제는 별도의 효과를 위해 적용되는 것일 뿐, 조성물의 기능에 영향을 미치는 성분은 아니다. The comparative composition of Comparative Example 2 was prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
제1혼합물 제조 단계(S10): 정제수와, 글리세린을 포함하는 폴리올을 혼합하고 색소를 추가한 다음, 65℃까지 가온하여, 제1혼합물을 제조하였다. First mixture preparation step (S10): Purified water and polyol containing glycerin were mixed, colorant was added, and the mixture was heated to 65°C to prepare the first mixture.
제2혼합물 제조 단계(S20): 폴리글리세릴-10미리스테이트를 포함하는 유화부 성분과, 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트를 포함하는 유상부 성분을 혼합하고, 색소 및 보존제를 추가한 다음, 65℃까지 가온하여 제2혼합물을 제조하였다. Second mixture preparation step (S20): Mixing the emulsified part component containing polyglyceryl-10 myristate and the oil phase component containing calendula oil and butylene glycol dicaprylate/dicaprate, and coloring. and a preservative were added and then heated to 65°C to prepare a second mixture.
다층상 화장료 조성물 제조 단계(S30): 상기 제1혼합물 제조 단계(S10)에서 65℃로 가온 중인 제1혼합물과, 상기 제2혼합물 제조 단계(S20)에서 65℃로 가온 중인 제2혼합물을 서로 혼합하여, 다층상 화장료 조성물을 제조하였다. Multilayer cosmetic composition manufacturing step (S30): The first mixture being heated to 65°C in the first mixture manufacturing step (S10) and the second mixture being heated to 65°C in the second mixture manufacturing step (S20) are mixed with each other. By mixing, a multilayer cosmetic composition was prepared.
이때, 각 성분의 조성은 하기 표 3와 같다. At this time, the composition of each component is shown in Table 3 below.
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 15.0중량%15.0% by weight
색소1Pigment 1 적량Appropriate amount
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 18.0중량%18.0% by weight
카렌둘라오일Calendula oil 10.0중량%10.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 10.0중량%10.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
비교예 3. 폴리글리세릴-10미리스테이트를 배제한 실험용 조성물의 제조Comparative Example 3. Preparation of experimental composition excluding polyglyceryl-10 myristate
하기 제조공정에 따라 비교예 3의 비교용 조성물을 제조하였다. 하기 제조공정에 있어서, 색소 및 보존제는 별도의 효과를 위해 적용되는 것일 뿐, 조성물의 기능에 영향을 미치는 성분은 아니다. The comparative composition of Comparative Example 3 was prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
제1혼합물 제조 단계(S10): 정제수와, 글리세린을 포함하는 폴리올을 혼합하고 색소를 추가한 다음, 65℃까지 가온하여, 제1혼합물을 제조하였다. First mixture preparation step (S10): Purified water and polyol containing glycerin were mixed, colorant was added, and the mixture was heated to 65°C to prepare the first mixture.
제2혼합물 제조 단계(S20): 폴리글리세릴-10라우레이트를 포함하는 유화부 성분과, 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트를 포함하는 유상부 성분을 혼합하고, 색소 및 보존제를 추가한 다음, 65℃까지 가온하여 제2혼합물을 제조하였다. Second mixture preparation step (S20): Mixing the emulsified part ingredients containing polyglyceryl-10 laurate and the oil part ingredients containing calendula oil and butylene glycol dicaprylate/dicaprate, and coloring. and a preservative were added and then heated to 65°C to prepare a second mixture.
다층상 화장료 조성물 제조 단계(S30): 상기 제1혼합물 제조 단계(S10)에서 65℃로 가온 중인 제1혼합물과, 상기 제2혼합물 제조 단계(S20)에서 65℃로 가온 중인 제2혼합물을 서로 혼합하여, 다층상 화장료 조성물을 제조하였다. Multilayer cosmetic composition manufacturing step (S30): The first mixture being heated to 65°C in the first mixture manufacturing step (S10) and the second mixture being heated to 65°C in the second mixture manufacturing step (S20) are mixed with each other. By mixing, a multilayer cosmetic composition was prepared.
이때, 각 성분의 조성은 하기 표 4와 같다. At this time, the composition of each component is shown in Table 4 below.
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 15.0중량%15.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 18.0중량%18.0% by weight
카렌둘라오일Calendula oil 10.0중량%10.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 10.0중량%10.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
비교예 4. 카렌둘라오일을 배제한 실험용 조성물의 제조Comparative Example 4. Preparation of experimental composition excluding calendula oil
하기 제조공정에 따라 비교예 4의 비교용 조성물을 제조하였다. 하기 제조공정에 있어서, 색소 및 보존제는 별도의 효과를 위해 적용되는 것일 뿐, 조성물의 기능에 영향을 미치는 성분은 아니다. The comparative composition of Comparative Example 4 was prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
제1혼합물 제조 단계(S10): 정제수와, 글리세린을 포함하는 폴리올을 혼합하고 색소를 추가한 다음, 65℃까지 가온하여, 제1혼합물을 제조하였다. First mixture preparation step (S10): Purified water and polyol containing glycerin were mixed, colorant was added, and the mixture was heated to 65°C to prepare the first mixture.
제2혼합물 제조 단계(S20): 폴리글리세릴-10라우레이트, 폴리글리세릴-10미리스테이트를 포함하는 유화부 성분과, 부틸렌글라이콜다이카프릴레이트/다이카프레이트를 포함하는 유상부 성분을 혼합하고, 색소 및 보존제를 추가한 다음, 65℃까지 가온하여 제2혼합물을 제조하였다. Second mixture preparation step (S20): Emulsifying component including polyglyceryl-10 laurate and polyglyceryl-10 myristate, and oil phase component including butylene glycol dicaprylate/dicaprate. It was mixed, colorant and preservative were added, and then heated to 65°C to prepare a second mixture.
다층상 화장료 조성물 제조 단계(S30): 상기 제1혼합물 제조 단계(S10)에서 65℃로 가온 중인 제1혼합물과, 상기 제2혼합물 제조 단계(S20)에서 65℃로 가온 중인 제2혼합물을 서로 혼합하여, 다층상 화장료 조성물을 제조하였다. Multilayer cosmetic composition manufacturing step (S30): The first mixture being heated to 65°C in the first mixture manufacturing step (S10) and the second mixture being heated to 65°C in the second mixture manufacturing step (S20) are mixed with each other. By mixing, a multilayer cosmetic composition was prepared.
이때, 각 성분의 조성은 하기 표 5와 같다. At this time, the composition of each component is shown in Table 5 below.
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 15.0중량%15.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 9.5중량%9.5% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 9.5중량%9.5% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 20.0중량%20.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
비교예 5. 부틸렌글라이콜다이카프릴레이트/다이카프레이트를 배제한 실험용 조성물의 제조Comparative Example 5. Preparation of experimental composition excluding butylene glycol dicaprylate/dicaprate
하기 제조공정에 따라 비교예 5의 비교용 조성물을 제조하였다. 하기 제조공정에 있어서, 색소 및 보존제는 별도의 효과를 위해 적용되는 것일 뿐, 조성물의 기능에 영향을 미치는 성분은 아니다. The comparative composition of Comparative Example 5 was prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
제1혼합물 제조 단계(S10): 정제수와, 글리세린을 포함하는 폴리올을 혼합하고 색소를 추가한 다음, 65℃까지 가온하여, 제1혼합물을 제조하였다. First mixture preparation step (S10): Purified water and polyol containing glycerin were mixed, colorant was added, and the mixture was heated to 65°C to prepare the first mixture.
제2혼합물 제조 단계(S20): 폴리글리세릴-10라우레이트, 폴리글리세릴-10미리스테이트를 포함하는 유화부 성분과, 카렌둘라오일을 포함하는 유상부 성분을 혼합하고, 색소 및 보존제를 추가한 다음, 65℃까지 가온하여 제2혼합물을 제조하였다. Second mixture preparation step (S20): Mixing the emulsified part ingredients including polyglyceryl-10 laurate and polyglyceryl-10 myristate and the oil part ingredients containing calendula oil, and adding coloring and preservative. Next, the second mixture was prepared by heating to 65°C.
다층상 화장료 조성물 제조 단계(S30): 상기 제1혼합물 제조 단계(S10)에서 65℃로 가온 중인 제1혼합물과, 상기 제2혼합물 제조 단계(S20)에서 65℃로 가온 중인 제2혼합물을 서로 혼합하여, 다층상 화장료 조성물을 제조하였다. Multilayer cosmetic composition manufacturing step (S30): The first mixture being heated to 65°C in the first mixture manufacturing step (S10) and the second mixture being heated to 65°C in the second mixture manufacturing step (S20) are mixed with each other. By mixing, a multilayer cosmetic composition was prepared.
이때, 각 성분의 조성은 하기 표 6과 같다. At this time, the composition of each component is shown in Table 6 below.
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 15.0중량%15.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 9.5중량%9.5% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 9.5중량%9.5% by weight
카렌둘라오일Calendula oil 20.0중량%20.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실시예 2 내지 4. 폴리올 성분을 다양하게 적용한 다층상 화장료 조성물의 제조Examples 2 to 4. Preparation of multilayer cosmetic compositions using various polyol components
하기 제조공정에 따라 실시예 2 내지 4의 다층상 화장료 조성물을 제조하였다. 하기 제조공정에 있어서, 색소 및 보존제는 별도의 효과를 위해 적용되는 것일 뿐, 조성물의 기능에 영향을 미치는 성분은 아니다. The multilayered cosmetic compositions of Examples 2 to 4 were prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
제1혼합물 제조 단계(S10): 정제수와, 글리세린 및 하기 표 7 내지 9의 조성과 같이 글리세린, 부틸렌글라이콜, 프로판다이올, 2,3-부탄다이올, 펜틸렌글라이콜, 소듐하이알루로네이트, 1,2-헥산다이올 중 어느 하나 이상의 폴리올을 혼합하고, 색소를 추가한 다음, 65℃까지 가온하여, 제1혼합물을 제조하였다. First mixture preparation step (S10): purified water, glycerin, and glycerin, butylene glycol, propanediol, 2,3-butanediol, pentylene glycol, and sodium hyaluron as shown in Tables 7 to 9 below. A first mixture was prepared by mixing at least one polyol of ronate and 1,2-hexanediol, adding pigment, and heating to 65°C.
제2혼합물 제조 단계(S20): 폴리글리세릴-10라우레이트, 폴리글리세릴-10미리스테이트를 포함하는 유화부 성분과, 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트를 포함하는 유상부 성분을 혼합하고, 색소 및 보존제를 추가한 다음, 65℃까지 가온하여 제2혼합물을 제조하였다. Second mixture preparation step (S20): Emulsifying component including polyglyceryl-10 laurate and polyglyceryl-10 myristate, calendula oil, and butylene glycol dicaprylate/dicaprate. The oil phase components were mixed, colorant and preservative were added, and then heated to 65°C to prepare a second mixture.
다층상 화장료 조성물 제조 단계(S30): 상기 제1혼합물 제조 단계(S10)에서 65℃로 가온 중인 제1혼합물과, 상기 제2혼합물 제조 단계(S20)에서 65℃로 가온 중인 제2혼합물을 서로 혼합하여, 다층상 화장료 조성물을 제조하였다. Multilayer cosmetic composition manufacturing step (S30): The first mixture being heated to 65°C in the first mixture manufacturing step (S10) and the second mixture being heated to 65°C in the second mixture manufacturing step (S20) are mixed with each other. By mixing, a multilayer cosmetic composition was prepared.
이때, 각 성분의 조성은 하기 표 7 내지 9과 같이, 실시예 2는 폴리올로 글리세린 및 부틸렌글라이콜 적용하였고, 실시예 3은 폴리올로 프로판다이올 및 2,3-부탄다이올 적용하였으며, 실시예 4는 폴리올로 펜틸렌글라이콜, 소듐하이알루로네이트 및 1,2-헥산다이올 적용하였다. At this time, the composition of each component is shown in Tables 7 to 9 below. In Example 2, glycerin and butylene glycol were used as polyols, and in Example 3, propanediol and 2,3-butanediol were used as polyols. In Example 4, pentylene glycol, sodium hyaluronate, and 1,2-hexanediol were applied as polyols.
실시예 2Example 2
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 5.0중량%5.0% by weight
부틸렌글라이콜Butylene glycol 10.0중량%10.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 9.5중량%9.5% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 9.5중량%9.5% by weight
카렌둘라오일Calendula oil 10.0중량%10.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 10.0중량%10.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실시예 3Example 3
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
프로판다이올Propanediol 5.0중량%5.0% by weight
2,3-부탄다이올2,3-Butanediol 10.0중량%10.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 9.5중량%9.5% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 9.5중량%9.5% by weight
카렌둘라오일Calendula oil 10.0중량%10.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 10.0중량%10.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실시예 4Example 4
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
펜틸렌글라이콜Pentylene glycol 5.0중량%5.0% by weight
소듐하이알루로네이트Sodium Hyaluronate 5.0중량%5.0% by weight
1,2-헥산다이올1,2-hexanediol 5.0중량%5.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 9.5중량%9.5% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 9.5중량%9.5% by weight
카렌둘라오일Calendula oil 10.0중량%10.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 10.0중량%10.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실시예 5 내지 11. 유화부 성분을 추가한 다층상 화장료 조성물의 제조Examples 5 to 11. Preparation of multilayer cosmetic composition with added emulsifying component
하기 제조공정에 따라 실시예 5 내지 11의 다층상 화장료 조성물을 제조하였다. 하기 제조공정에 있어서, 색소 및 보존제는 별도의 효과를 위해 적용되는 것일 뿐, 조성물의 기능에 영향을 미치는 성분은 아니다. The multilayered cosmetic compositions of Examples 5 to 11 were prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
제1혼합물 제조 단계(S10): 정제수와, 글리세린 및 부틸렌글라이콜을 포함하는 폴리올을 혼합하고, 색소를 추가한 다음, 65℃까지 가온하여, 제1혼합물을 제조하였다. First mixture preparation step (S10): Purified water and polyol containing glycerin and butylene glycol were mixed, colorant was added, and the mixture was heated to 65°C to prepare the first mixture.
제2혼합물 제조 단계(S20): 폴리글리세릴-10라우레이트, 폴리글리세릴-10미리스테이트를 포함하되, 하기 표 10 내지 16의 조성과 같이, 레시틴, 폴리글리세릴-10스테아레이트, 피이지-40하이드로제네이티드캐스터오일, 피이지-60하이드로제네이티드캐스터오일, 폴리소르베이트 20, 폴리소르베이트 60, 폴리소르베이트 80 중 어느 하나 이상을 더 포함하는 유화부 성분과, 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트를 포함하는 유상부 성분을 혼합하고, 색소 및 보존제를 추가한 다음, 65℃까지 가온하여 제2혼합물을 제조하였다. Second mixture preparation step (S20): It contains polyglyceryl-10 laurate and polyglyceryl-10 myristate, and as shown in Tables 10 to 16 below, lecithin, polyglyceryl-10 stearate, and PEG. -Emulsifying component further comprising one or more of 40 Hydrogenated Castor Oil, PEG-60 Hydrogenated Castor Oil, Polysorbate 20, Polysorbate 60, and Polysorbate 80, calendula oil, and butyl The oil phase components including len glycol dicaprylate/dicaprate were mixed, colorant and preservative were added, and then heated to 65°C to prepare a second mixture.
다층상 화장료 조성물 제조 단계(S30): 상기 제1혼합물 제조 단계(S10)에서 65℃로 가온 중인 제1혼합물과, 상기 제2혼합물 제조 단계(S20)에서 65℃로 가온 중인 제2혼합물을 서로 혼합하여, 다층상 화장료 조성물을 제조하였다. Multilayer cosmetic composition manufacturing step (S30): The first mixture being heated to 65°C in the first mixture manufacturing step (S10) and the second mixture being heated to 65°C in the second mixture manufacturing step (S20) are mixed with each other. By mixing, a multilayer cosmetic composition was prepared.
이때, 각 성분의 조성은 하기 표 10 내지 16과 같이, 실시예 5은 레시틴, 실시예 6은 폴리글리세릴-10스테아레이트, 실시예 7은 피이지-40하이드로제네이티드캐스터오일, 실시예 8은 피이지-60하이드로제네이티드캐스터오일, 실시예 9는 폴리소르베이트 20, 실시예 10은 폴리소르베이트 60, 실시예 11은 폴리소르베이트 80를 유화부 성분으로 더 포함하였다. At this time, the composition of each component is as shown in Tables 10 to 16 below, Example 5 is lecithin, Example 6 is polyglyceryl-10 stearate, Example 7 is PEG-40 hydrogenated castor oil, and Example 8. PEG-60 hydrogenated castor oil, Example 9 further included polysorbate 20, Example 10 contained polysorbate 60, and Example 11 further included polysorbate 80 as an emulsifying component.
실시예 5Example 5
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 5.0중량%5.0% by weight
부틸렌글라이콜Butylene glycol 10.0중량%10.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 7.0중량%7.0% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 7.0중량%7.0% by weight
레시틴lecithin 5.0중량%5.0% by weight
카렌둘라오일Calendula oil 10.0중량%10.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 10.0중량%10.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실시예 6Example 6
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 5.0중량%5.0% by weight
부틸렌글라이콜Butylene glycol 10.0중량%10.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 7.0중량%7.0% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 7.0중량%7.0% by weight
폴리글리세릴-10스테아레이트Polyglyceryl-10 Stearate 5.0중량%5.0% by weight
카렌둘라오일Calendula oil 10.0중량%10.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 10.0중량%10.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실시예 7Example 7
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 5.0중량%5.0% by weight
부틸렌글라이콜Butylene glycol 10.0중량%10.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 7.0중량%7.0% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 7.0중량%7.0% by weight
피이지-40하이드로제네이티드캐스터오일PEG-40 Hydrogenated Castor Oil 5.0중량%5.0% by weight
카렌둘라오일Calendula oil 10.0중량%10.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 10.0중량%10.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실시예 8Example 8
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 5.0중량%5.0% by weight
부틸렌글라이콜Butylene glycol 10.0중량%10.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 7.0중량%7.0% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 7.0중량%7.0% by weight
피이지-60하이드로제네이티드캐스터오일PEG-60 Hydrogenated Castor Oil 5.0중량%5.0% by weight
카렌둘라오일Calendula oil 10.0중량%10.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 10.0중량%10.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실시예 9Example 9
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 5.0중량%5.0% by weight
부틸렌글라이콜Butylene glycol 10.0중량%10.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 7.0중량%7.0% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 7.0중량%7.0% by weight
폴리소르베이트 20Polysorbate 20 5.0중량%5.0% by weight
카렌둘라오일Calendula oil 10.0중량%10.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 10.0중량%10.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실시예 10Example 10
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 5.0중량%5.0% by weight
부틸렌글라이콜Butylene glycol 10.0중량%10.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 7.0중량%7.0% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 7.0중량%7.0% by weight
폴리소르베이트 60Polysorbate 60 5.0중량%5.0% by weight
카렌둘라오일Calendula oil 10.0중량%10.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 10.0중량%10.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실시예 11Example 11
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 5.0중량%5.0% by weight
부틸렌글라이콜Butylene glycol 10.0중량%10.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 7.0중량%7.0% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 7.0중량%7.0% by weight
폴리소르베이트 80Polysorbate 80 5.0중량%5.0% by weight
카렌둘라오일Calendula oil 10.0중량%10.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 10.0중량%10.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실시예 12 내지 16. 유상부 성분을 추가한 다층상 화장료 조성물의 제조Examples 12 to 16. Preparation of multilayer cosmetic composition with added oil phase component
하기 제조공정에 따라 실시예 12 내지 16의 다층상 화장료 조성물을 제조하였다. 하기 제조공정에 있어서, 색소 및 보존제는 별도의 효과를 위해 적용되는 것일 뿐, 조성물의 기능에 영향을 미치는 성분은 아니다. The multilayered cosmetic compositions of Examples 12 to 16 were prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
제1혼합물 제조 단계(S10): 정제수와, 글리세린을 포함하는 폴리올을 혼합하고, 색소를 추가한 다음, 65℃까지 가온하여, 제1혼합물을 제조하였다. First mixture preparation step (S10): Purified water and polyol containing glycerin were mixed, colorant was added, and the mixture was heated to 65°C to prepare the first mixture.
제2혼합물 제조 단계(S20): 폴리글리세릴-10라우레이트, 폴리글리세릴-10미리스테이트를 포함하는 유화부 성분과, 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트를 포함하되, 하기 표 17 내지 21의 조성과 같이 메도우폼씨오일, 해바라기씨오일, 카프릴릭/카프릭트라이글리세라이드, 포도씨오일, 아보카도오일 중 어느 하나 이상을 더 포함하는 유상부 성분을 혼합하고, 색소 및 보존제를 추가한 다음, 65℃까지 가온하여 제2혼합물을 제조하였다. Second mixture preparation step (S20): Emulsifying component including polyglyceryl-10 laurate and polyglyceryl-10 myristate, calendula oil, and butylene glycol dicaprylate/dicaprate. However, as shown in Tables 17 to 21 below, oily components further containing one or more of meadowfoam seed oil, sunflower seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil are mixed, and coloring is added. and a preservative were added and then heated to 65°C to prepare a second mixture.
다층상 화장료 조성물 제조 단계(S30): 상기 제1혼합물 제조 단계(S10)에서 65℃로 가온 중인 제1혼합물과, 상기 제2혼합물 제조 단계(S20)에서 65℃로 가온 중인 제2혼합물을 서로 혼합하여, 다층상 화장료 조성물을 제조하였다. Multilayer cosmetic composition manufacturing step (S30): The first mixture being heated to 65°C in the first mixture manufacturing step (S10) and the second mixture being heated to 65°C in the second mixture manufacturing step (S20) are mixed with each other. By mixing, a multilayer cosmetic composition was prepared.
이때, 각 성분의 조성은 하기 표 17 내지 21과 같이 실시예 12는 메도우폼씨오일, 실시예 13은 해바라기씨오일, 실시예 14는 카프릴릭/카프릭트라이글리세라이드, 실시예 15는 포도씨오일, 실시예 16은 아보카도오일을 유상부 성분으로 포함하였다. At this time, the composition of each component is as shown in Tables 17 to 21 below. Example 12 is meadowfoam seed oil, Example 13 is sunflower seed oil, Example 14 is caprylic/capric triglyceride, and Example 15 is grape seed. Oil, Example 16 included avocado oil as an oil phase component.
실시예 12Example 12
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 5.0중량%5.0% by weight
부틸렌글라이콜Butylene glycol 10.0중량%10.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 9.5중량%9.5% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 9.5중량%9.5% by weight
카렌둘라오일Calendula oil 7.0중량%7.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 7.0중량%7.0% by weight
메도우폼씨오일Meadowfoam seed oil 6.0중량%6.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실시예 13Example 13
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 5.0중량%5.0% by weight
부틸렌글라이콜Butylene glycol 10.0중량%10.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 9.5중량%9.5% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 9.5중량%9.5% by weight
카렌둘라오일Calendula oil 7.0중량%7.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 7.0중량%7.0% by weight
해바라기씨오일sunflower seed oil 6.0중량%6.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실시예 14Example 14
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 5.0중량%5.0% by weight
부틸렌글라이콜Butylene glycol 10.0중량%10.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 9.5중량%9.5% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 9.5중량%9.5% by weight
카렌둘라오일Calendula oil 7.0중량%7.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 7.0중량%7.0% by weight
카프릴릭/카프릭트라이글리세라이드Caprylic/Capric Triglyceride 6.0중량%6.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실시예 15Example 15
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 5.0중량%5.0% by weight
부틸렌글라이콜Butylene glycol 10.0중량%10.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 9.5중량%9.5% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 9.5중량%9.5% by weight
카렌둘라오일Calendula oil 7.0중량%7.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 7.0중량%7.0% by weight
포도씨오일grape seed oil 6.0중량%6.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실시예 16Example 16
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 5.0중량%5.0% by weight
부틸렌글라이콜Butylene glycol 10.0중량%10.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 9.5중량%9.5% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 9.5중량%9.5% by weight
카렌둘라오일Calendula oil 7.0중량%7.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 7.0중량%7.0% by weight
아보카도오일Avocado oil 6.0중량%6.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
제조예 1. 다양한 성분을 포함하는 다층상 화장료 조성물의 제조Preparation Example 1. Preparation of a multilayer cosmetic composition containing various ingredients
하기 제조공정에 따라 제조예 1의 다층상 화장료 조성물을 제조하였다. 하기 제조공정에 있어서, 색소 및 보존제는 별도의 효과를 위해 적용되는 것일 뿐, 조성물의 기능에 영향을 미치는 성분은 아니다. The multilayered cosmetic composition of Preparation Example 1 was prepared according to the following manufacturing process. In the following manufacturing process, colorants and preservatives are applied for separate effects and are not ingredients that affect the function of the composition.
제1혼합물 제조 단계(S10): 정제수와, 글리세린, 부틸렌글라이콜, 프로판다이올, 2,3-부탄다이올, 펜틸렌글라이콜, 소듐하이알루로네이트 및 1,2-헥산다이올을 포함하는 폴리올을 혼합하고, 색소를 추가한 다음, 65℃까지 가온하여, 제1혼합물을 제조하였다. First mixture preparation step (S10): Purified water, glycerin, butylene glycol, propanediol, 2,3-butanediol, pentylene glycol, sodium hyaluronate, and 1,2-hexanediol. The first mixture was prepared by mixing the polyol containing the mixture, adding a pigment, and heating to 65°C.
제2혼합물 제조 단계(S20): 폴리글리세릴-10라우레이트, 폴리글리세릴-10미리스테이트, 레시틴, 폴리글리세릴-10스테아레이트, 피이지-40하이드로제네이티드캐스터오일, 피이지-60하이드로제네이티드캐스터오일, 폴리소르베이트 20, 폴리소르베이트 60 및 폴리소르베이트 80을 포함하는 유화부 성분과, 카렌둘라오일, 부틸렌글라이콜다이카프릴레이트/다이카프레이트, 메도우폼씨오일, 해바라기씨오일, 카프릴릭/카프릭트라이글리세라이드, 포도씨오일, 아보카도오일을 포함하는 유상부 성분을 혼합하고, 색소 및 보존제를 추가한 다음, 65℃까지 가온하여 제2혼합물을 제조하였다. Second mixture preparation step (S20): polyglyceryl-10 laurate, polyglyceryl-10 myristate, lecithin, polyglyceryl-10 stearate, PEG-40 hydrogenated castor oil, PEG-60 hydro. Emulsifying components including generated castor oil, polysorbate 20, polysorbate 60, and polysorbate 80, calendula oil, butylene glycol dicaprylate/dicaprate, meadowfoam seed oil, and sunflower The oil phase components including seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil were mixed, colorant and preservative were added, and then heated to 65°C to prepare a second mixture.
다층상 화장료 조성물 제조 단계(S30): 상기 제1혼합물 제조 단계(S10)에서 65℃로 가온 중인 제1혼합물과, 상기 제2혼합물 제조 단계(S20)에서 65℃로 가온 중인 제2혼합물을 서로 혼합하여, 다층상 화장료 조성물을 제조하였다. Multilayer cosmetic composition manufacturing step (S30): The first mixture being heated to 65°C in the first mixture manufacturing step (S10) and the second mixture being heated to 65°C in the second mixture manufacturing step (S20) are mixed with each other. By mixing, a multilayer cosmetic composition was prepared.
이때, 각 성분의 조성은 하기 표 22와 같다. At this time, the composition of each component is shown in Table 22 below.
제조예 1Manufacturing Example 1
구분division 성분ingredient 함량content
AA 정제수Purified water 잔량remaining amount
글리세린glycerin 2.0중량%2.0% by weight
부틸렌글라이콜Butylene glycol 3.0중량%3.0% by weight
프로판다이올Propanediol 2.0중량%2.0% by weight
2,3-부탄다이올2,3-Butanediol 2.0중량%2.0% by weight
펜틸렌글라이콜Pentylene glycol 2.0중량%2.0% by weight
소듐하이알루로네이트Sodium Hyaluronate 2.0중량%2.0% by weight
1,2-헥산다이올1,2-hexanediol 2.0중량%2.0% by weight
색소1Pigment 1 적량Appropriate amount
BB 폴리글리세릴-10라우레이트Polyglyceryl-10 Laurate 2.0중량%2.0% by weight
폴리글리세릴-10미리스테이트Polyglyceryl-10 myristate 2.0중량%2.0% by weight
레시틴lecithin 2.0중량%2.0% by weight
폴리글리세릴-10스테아레이트Polyglyceryl-10stearate 2.0중량%2.0% by weight
피이지-40하이드로제네이티드캐스터오일PEG-40 Hydrogenated Castor Oil 2.0중량%2.0% by weight
피이지-60하이드로제네이티드캐스터오일PEG-60 Hydrogenated Castor Oil 2.0중량%2.0% by weight
폴리소르베이트 20Polysorbate 20 2.0중량%2.0% by weight
폴리소르베이트 60Polysorbate 60 2.0중량%2.0% by weight
폴리소르베이트 80Polysorbate 80 2.0중량%2.0% by weight
카렌둘라오일Calendula oil 3.0중량%3.0% by weight
부틸렌글라이콜다이카프릴레이트/다이카프레이트Butylene Glycol Dicaprylate/Dicaprate 3.0중량%3.0% by weight
메도우폼씨오일Meadowfoam seed oil 3.0중량%3.0% by weight
해바라기씨오일sunflower seed oil 3.0중량%3.0% by weight
카프릴릭/카프릭트라이글리세라이드Caprylic/Capric Triglyceride 3.0중량%3.0% by weight
포도씨오일grape seed oil 3.0중량%3.0% by weight
아보카도오일Avocado oil 2.0중량%2.0% by weight
색소2Pigment 2 적량Appropriate amount
보존제preservative 적량Appropriate amount
실험예 1. 층상 분리 정도 확인Experimental Example 1. Confirmation of degree of layer separation
상기 실시예 1 내지 16, 비교예 1 내지 5, 제조예 1에서 제조한 내용물을 용기에 담아 소비자가 사용 시와 동일하게 손으로 흔들어 상온에서 3시간 방치하고, 이들이 유상부, 유화부 및 수상부의 각층으로 분리되는지에 대해 평가하였다. The contents prepared in Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 were placed in a container, shaken by hand in the same way as when used by consumers, and left at room temperature for 3 hours, and each layer of the oil phase, emulsified phase, and water phase was separated. It was evaluated whether it could be separated.
시험은 상온에서 3시간 방치된 실시예 1 내지 16, 비교예 1 내지 5, 제조예 1에 대해 20인의 화장료 성분 전문가가 육안으로 확인하여 5점척도법(분리가 일어나지 않은 경우 1점, 희미하게 성상 구분만 가능하고 확실한 분리가 일어나지 않은 경우 2점, 각 층의 경계선이 뿌연 색상을 띄며 층 구분이 애매한 경우 3점, 층 분리는 일어났으나 각 층의 경계선에 방울이 많고 지저분한 경우 4점, 각 층이 구분되고 경계선이 깔끔한 경우 5점)으로 평가하고, 이를 평균으로 계산하였다. The test was performed on Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1, which were left at room temperature for 3 hours, and were visually inspected by 20 cosmetic ingredient experts, using a 5-point scale (1 point if separation did not occur, faint appearance). 2 points if only distinction is possible but no clear separation has occurred; 3 points if the boundaries of each layer are in a hazy color and the layer distinction is unclear; 4 points if layer separation has occurred but the boundaries of each layer are dirty and have many drops; 4 points for each layer If the boundaries are distinct and the boundaries are clear, it was evaluated as 5 points, and this was calculated as the average.
층상 분리 정도(평가점수)Degree of layer separation (evaluation score)
실시예1Example 1 4.44.4
비교예1Comparative Example 1 1.51.5
비교예2Comparative example 2 3.33.3
비교예3Comparative Example 3 3.53.5
비교예4Comparative example 4 3.43.4
비교예5Comparative Example 5 3.43.4
실시예2Example 2 4.44.4
실시예3Example 3 4.44.4
실시예4Example 4 4.44.4
실시예5Example 5 4.64.6
실시예6Example 6 4.54.5
실시예7Example 7 4.74.7
실시예8Example 8 4.64.6
실시예9Example 9 4.74.7
실시예10Example 10 4.64.6
실시예11Example 11 4.54.5
실시예12Example 12 4.64.6
실시예13Example 13 4.74.7
실시예14Example 14 4.64.6
실시예15Example 15 4.54.5
실시예16Example 16 4.64.6
제조예1Manufacturing Example 1 4.84.8
그 결과, 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트의 혼합물을 주 성분으로 포함하는 유상부, 폴리글리세릴-10라우레이트 및 폴리글리세릴-10미리스테이트의 혼합물을 주성분으로 포함하는 유화부; 및, 정제수 및 폴리올을 포함하는 수상부를 모두 포함하는 실시예 1의 경우, 층 분리가 잘 일어난 것을 확인할 수 있었다. 이에 반해, 일부 성분이 결여된 비교예 1 내지 5의 경우 층 분리 정도가 현저히 떨어지는 것을 확인할 수 있었다. As a result, the oil phase contains a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main ingredients, and the oil phase contains a mixture of polyglyceryl-10 laurate and polyglyceryl-10 myristate as main ingredients. oil painting department; And, in the case of Example 1, which included both purified water and an aqueous phase containing polyol, it was confirmed that layer separation occurred well. On the other hand, in the case of Comparative Examples 1 to 5 lacking some components, it was confirmed that the degree of layer separation was significantly reduced.
한편, 실시예 1에서 폴리올의 종류만 바꾼 실시예 2, 실시예 3, 실시예 4의 경우, 실시예 1과 비슷한 수치가 나타나 폴리올의 종류는 본 발명에 기재된 종류 내에서 임의로 바꾸어도 무방함을 나타낸다. Meanwhile, in the case of Example 2, Example 3, and Example 4 in which only the type of polyol was changed from Example 1, similar values to Example 1 appeared, indicating that the type of polyol may be arbitrarily changed within the types described in the present invention. .
또한, 유상부와, 유화부에 있어, 유상부에 메도우폼씨오일, 해바라기씨오일, 카프릴릭/카프릭트라이글리세라이드, 포도씨오일, 아보카도오일로 구성된 군에서 어느 하나 이상을 더 포함하고, 유화부에 레시틴, 폴리글리세릴-10스테아레이트, 피이지-40하이드로제네이티드캐스터오일, 피이지-60하이드로제네이티드캐스터오일, 폴리소르베이트 20, 폴리소르베이트 60, 폴리소르베이트 80으로 구성되는 군에서 어느 하나 이상을 더 포함하는 경우, 층상 분리정도에 관한 평가 점수가 다소 높게 나타났음을 확인할 수 있었다. 가장 우수한 것은 제조예 1이였다. In addition, in the oily part and the emulsified part, the oily part further includes any one or more from the group consisting of meadowfoam seed oil, sunflower seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil, and the emulsified part In the group consisting of lecithin, polyglyceryl-10 stearate, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, polysorbate 20, polysorbate 60, and polysorbate 80. When more than one was included, it was confirmed that the evaluation score regarding the degree of layer separation was somewhat high. The most excellent one was Preparation Example 1.
실험예 2. 혼합 속도 확인Experimental Example 2. Check mixing speed
상기 실시예 1 내지 16, 비교예 1 내지 5, 제조예 1에서 제조한 내용물을 용기에 담아 소비자가 사용 시와 동일하게 손으로 흔들어 유상부, 유화부 및 수상부가 혼합되는 시간을 측정하였다. The contents prepared in Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 were placed in a container and shaken by hand in the same manner as when used by consumers, and the time for mixing the oil phase, emulsified phase, and water phase was measured.
시험은 각 시료에 대해 5회 반복 진행되었으며, 이를 평균으로 계산하였다. The test was repeated 5 times for each sample, and the average was calculated.
혼합되는데 걸린 속도(초)Speed of mixing (seconds)
실시예1Example 1 6.76.7
비교예1Comparative Example 1 27.327.3
비교예2Comparative example 2 14.714.7
비교예3Comparative Example 3 16.416.4
비교예4Comparative Example 4 15.615.6
비교예5Comparative Example 5 17.317.3
실시예2Example 2 6.76.7
실시예3Example 3 6.66.6
실시예4Example 4 6.76.7
실시예5Example 5 5.55.5
실시예6Example 6 5.35.3
실시예7Example 7 5.55.5
실시예8Example 8 5.45.4
실시예9Example 9 5.65.6
실시예10Example 10 5.55.5
실시예11Example 11 5.35.3
실시예12Example 12 5.45.4
실시예13Example 13 5.55.5
실시예14Example 14 5.75.7
실시예15Example 15 5.55.5
실시예16Example 16 5.45.4
제조예1Manufacturing Example 1 3.23.2
그 결과, 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트의 혼합물을 주 성분으로 포함하는 유상부, 폴리글리세릴-10라우레이트 및 폴리글리세릴-10미리스테이트의 혼합물을 주성분으로 포함하는 유화부; 및, 정제수 및 폴리올을 포함하는 수상부를 모두 포함하는 실시예 1의 경우, 혼합 속도가 빨라 단 시간 내에 혼합이 용이하게 잘 이루어짐을 확인할 수 있었다. 이에 반해, 일부 성분이 결여된 비교예 1 내지 5의 경우 현저히 느리게 혼합되는 것을 확인할 수 있었다. As a result, the oil phase contains a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main components, and the oil phase contains a mixture of polyglyceryl-10 laurate and polyglyceryl-10 myristate as main components. oil painting department; And, in the case of Example 1, which includes both purified water and an aqueous phase containing polyol, it was confirmed that the mixing speed was fast and mixing was easily accomplished within a short time. On the other hand, in the case of Comparative Examples 1 to 5 lacking some components, it was confirmed that mixing was significantly slow.
한편, 실시예 1에서 폴리올의 종류만 바꾼 실시예 2, 실시예 3, 실시예 4의 경우, 실시예 1과 비슷한 시간이 소모되었으며, 폴리올의 종류는 본 발명에 기재된 종류 내에서 임의로 바꾸어도 무방함을 나타낸다. Meanwhile, in the case of Examples 2, 3, and 4 in which only the type of polyol was changed from Example 1, a similar time was consumed as Example 1, and the type of polyol may be arbitrarily changed within the types described in the present invention. represents.
또한, 유상부와, 유화부에 있어, 유상부에 메도우폼씨오일, 해바라기씨오일, 카프릴릭/카프릭트라이글리세라이드, 포도씨오일, 아보카도오일로 구성된 군에서 어느 하나 이상을 더 포함하고, 유화부에 레시틴, 폴리글리세릴-10스테아레이트, 피이지-40하이드로제네이티드캐스터오일, 피이지-60하이드로제네이티드캐스터오일, 폴리소르베이트 20, 폴리소르베이트 60, 폴리소르베이트 80으로 구성되는 군에서 어느 하나 이상을 더 포함하는 경우, 혼합속도가 다소 빠르게 나타났음을 확인할 수 있었다. 가장 빠른 것은 제조예 1이였다. In addition, in the oily part and the emulsified part, the oily part further includes any one or more from the group consisting of meadowfoam seed oil, sunflower seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil, and the emulsified part In the group consisting of lecithin, polyglyceryl-10 stearate, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, polysorbate 20, polysorbate 60, and polysorbate 80. It was confirmed that when more than one was included, the mixing speed appeared somewhat faster. The fastest one was Preparation Example 1.
실험예 3. 혼합 후 분산 정도 확인Experimental Example 3. Checking the degree of dispersion after mixing
상기 실시예 1 내지 16, 비교예 1 내지 5, 제조예 1에서 제조한 내용물을 용기에 담아 소비자가 사용 시와 동일하게 손으로 흔들어 유상부, 유화부 및 수상부가 균일하게 혼합되는지 여부를 확인하였다. The contents prepared in Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 were placed in a container and shaken by hand in the same manner as when used by consumers to check whether the oil phase, emulsified phase, and water phase were uniformly mixed.
시험은 동일시간 동안 흔들어 20인의 화장료 성분 전문가가 육안으로 확인하여 5점척도법(균일하게 섞이지 않고 오일 방울이 크게 형성되는 경우 1점, 균일하게 섞이지 않고 오일방울이 보통으로 형성되는 경우 2점, 보통 정도로 섞이며 오일방울이 작게 형성되는 경우 3점, 균일하게 섞이되 각 성분의 성상이 희미하게 구분되는 경우 4점, 균일하게 분산되어 단일 성분처럼 섞이는 경우 5점)으로 평가하고, 이를 평균으로 계산하였다. The test is shaken for the same amount of time and visually checked by 20 cosmetic ingredient experts using a 5-point scale (1 point if it is not mixed uniformly and large oil droplets are formed; 2 points if it is not mixed uniformly and oil droplets are formed normally; 2 points if it is mixed to an average degree) It was evaluated as 3 points if oil droplets were formed in small sizes, 4 points if they were uniformly mixed but the properties of each component were vaguely distinguished, and 5 points if they were uniformly dispersed and mixed like a single component), and this was calculated as the average.
혼합 후 분산 정도(평가점수)Degree of dispersion after mixing (evaluation score)
실시예1Example 1 4.64.6
비교예1Comparative Example 1 1.81.8
비교예2Comparative example 2 3.53.5
비교예3Comparative example 3 3.33.3
비교예4Comparative example 4 3.63.6
비교예5Comparative Example 5 3.43.4
실시예2Example 2 4.64.6
실시예3Example 3 4.64.6
실시예4Example 4 4.64.6
실시예5Example 5 4.74.7
실시예6Example 6 4.84.8
실시예7Example 7 4.74.7
실시예8Example 8 4.74.7
실시예9Example 9 4.84.8
실시예10Example 10 4.84.8
실시예11Example 11 4.74.7
실시예12Example 12 4.74.7
실시예13Example 13 4.84.8
실시예14Example 14 4.84.8
실시예15Example 15 4.74.7
실시예16Example 16 4.84.8
제조예1Manufacturing example 1 4.94.9
그 결과, 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트의 혼합물을 주 성분으로 포함하는 유상부, 폴리글리세릴-10라우레이트 및 폴리글리세릴-10미리스테이트의 혼합물을 주성분으로 포함하는 유화부; 및, 정제수 및 폴리올을 포함하는 수상부를 모두 포함하는 실시예 1의 경우, 혼합 후 분산 정도에 대한 평가 점수가 높게 나타남을 확인할 수 있었다. 이에 반해, 일부 성분이 결여된 비교예 1 내지 5의 경우 현저히 떨어지는 수치를 나타내었다. As a result, the oil phase contains a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main ingredients, and the oil phase contains a mixture of polyglyceryl-10 laurate and polyglyceryl-10 myristate as main ingredients. oil painting department; And, in the case of Example 1, which includes both purified water and an aqueous phase containing polyol, it was confirmed that the evaluation score for the degree of dispersion after mixing was high. On the other hand, Comparative Examples 1 to 5 lacking some components showed significantly lower values.
한편, 실시예 1에서 폴리올의 종류만 바꾼 실시예 2, 실시예 3, 실시예 4의 경우, 실시예 1과 비슷한 평가점수가 나타났으며, 폴리올의 종류는 본 발명에 기재된 종류 내에서 임의로 바꾸어도 무방함을 나타낸다. Meanwhile, in the case of Example 2, Example 3, and Example 4 in which only the type of polyol was changed from Example 1, evaluation scores similar to Example 1 were shown, and the type of polyol could be arbitrarily changed within the types described in the present invention. It indicates freedom.
또한, 유상부와, 유화부에 있어, 유상부에 메도우폼씨오일, 해바라기씨오일, 카프릴릭/카프릭트라이글리세라이드, 포도씨오일, 아보카도오일로 구성된 군에서 어느 하나 이상을 더 포함하고, 유화부에 레시틴, 폴리글리세릴-10스테아레이트, 피이지-40하이드로제네이티드캐스터오일, 피이지-60하이드로제네이티드캐스터오일, 폴리소르베이트 20, 폴리소르베이트 60, 폴리소르베이트 80으로 구성되는 군에서 어느 하나 이상을 더 포함하는 경우, 혼합 후 분산 정도에 대한 평가 점수가 다소 높음을 확인할 수 있었다. 가장 우수한 것은 제조예 1이였다. In addition, in the oily part and the emulsified part, the oily part further includes any one or more from the group consisting of meadowfoam seed oil, sunflower seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil, and the emulsified part In the group consisting of lecithin, polyglyceryl-10 stearate, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, polysorbate 20, polysorbate 60, and polysorbate 80. When more than one was included, it was confirmed that the evaluation score for the degree of dispersion after mixing was somewhat high. The most excellent one was Preparation Example 1.
실험예 4. 보습효과 확인Experimental Example 4. Confirmation of moisturizing effect
상기 실시예 1 내지 16, 비교예 1 내지 5, 제조예 1에서 제조한 내용물에 대한 피부 보습효과를 확인하였다. 실험은 공지된 방법을 통해 수행되었다. The skin moisturizing effect of the contents prepared in Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 was confirmed. The experiment was performed using known methods.
상기 실시예 1 내지 16, 비교예 1 내지 5, 제조예 1에서 제조한 조성물을 피시험자(20세-45세의 남성 및 여성) 30명을 대상으로 1일 2회씩 4주간 안면 양쪽의 얼굴 및 전반부에 실시예 1 내지 16, 비교예 1 내지 5, 제조예 1에서 제조한 조성물을 각각 도포하여 도포하기 전, 30분 경과 후, 그리고 1시간 경과 후의 피부보습개선상태를 피부수분측정기 Corneometer CM 820 (Courage + Khazaka, Germany)를 이용하여 측정하였으며, 단위는 기기에서 부여하는 임의의 단위(Arbitrary Unit, AU)로 표현되며, 측정값이 높을수록 피부표면에 수분량이 높음을 의미한다.The compositions prepared in Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 were applied to 30 test subjects (men and women aged 20 to 45 years) on both sides of the face twice a day for 4 weeks. The compositions prepared in Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1 were applied to the first half, respectively, and the improvement in skin moisture was measured before application, after 30 minutes, and after 1 hour, using a skin moisture meter Corneometer CM 820. It was measured using (Courage + Khazaka, Germany), and the unit is expressed in an arbitrary unit (AU) given by the device. The higher the measured value, the higher the moisture content on the skin surface.
피부보습 효과(Au)Skin moisturizing effect (Au)
도포 전Before application 30분 후30 minutes later 1시간 후1 hour later
실시예1Example 1 57.457.4 60.260.2 64.464.4
비교예1Comparative Example 1 57.557.5 57.557.5 57.857.8
비교예2Comparative example 2 57.457.4 58.858.8 59.559.5
비교예3Comparative Example 3 57.457.4 58.558.5 59.959.9
비교예4Comparative example 4 57.557.5 57.857.8 59.859.8
비교예5Comparative Example 5 57.357.3 57.757.7 59.359.3
실시예2Example 2 57.557.5 60.460.4 64.564.5
실시예3Example 3 57.457.4 60.560.5 64.664.6
실시예4Example 4 57.557.5 60.660.6 64.664.6
실시예5Example 5 57.457.4 63.763.7 66.366.3
실시예6Example 6 57.357.3 62.862.8 66.766.7
실시예7Example 7 57.357.3 63.263.2 66.166.1
실시예8Example 8 57.557.5 63.463.4 66.366.3
실시예9Example 9 57.457.4 63.563.5 66.266.2
실시예10Example 10 57.557.5 63.763.7 66.566.5
실시예11Example 11 57.457.4 63.563.5 66.666.6
실시예12Example 12 57.557.5 63.363.3 66.366.3
실시예13Example 13 57.457.4 63.263.2 66.466.4
실시예14Example 14 57.557.5 63.863.8 66.566.5
실시예15Example 15 57.457.4 63.163.1 66.266.2
실시예16Example 16 57.457.4 63.363.3 66.366.3
제조예1Manufacturing example 1 57.457.4 65.365.3 69.369.3
그 결과, 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트의 혼합물을 주 성분으로 포함하는 유상부, 폴리글리세릴-10라우레이트 및 폴리글리세릴-10미리스테이트의 혼합물을 주성분으로 포함하는 유화부; 및, 정제수 및 폴리올을 포함하는 수상부를 모두 포함하는 실시예 1의 경우, 보습효과가 우수함을 확인할 수 있었다. 이에 반해, 일부 성분이 결여된 비교예 1 내지 5의 경우 현저히 떨어지는 수치를 나타내었다. As a result, the oil phase contains a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main components, and the oil phase contains a mixture of polyglyceryl-10 laurate and polyglyceryl-10 myristate as main components. oil painting department; And, in the case of Example 1, which included both purified water and an aqueous phase containing polyol, it was confirmed that the moisturizing effect was excellent. On the other hand, Comparative Examples 1 to 5 lacking some components showed significantly lower values.
한편, 실시예 1에서 폴리올의 종류만 바꾼 실시예 2, 실시예 3, 실시예 4의 경우, 실시예 1과 비슷한 보습효과가 나타났으며, 폴리올의 종류는 본 발명에 기재된 종류 내에서 임의로 바꾸어도 무방함을 나타낸다. On the other hand, in the case of Examples 2, 3, and 4 in which only the type of polyol was changed from Example 1, a moisturizing effect similar to Example 1 was observed, and the type of polyol could be arbitrarily changed within the types described in the present invention. It indicates freedom.
또한, 유상부와, 유화부에 있어, 유상부에 메도우폼씨오일, 해바라기씨오일, 카프릴릭/카프릭트라이글리세라이드, 포도씨오일, 아보카도오일로 구성된 군에서 어느 하나 이상을 더 포함하고, 유화부에 레시틴, 폴리글리세릴-10스테아레이트, 피이지-40하이드로제네이티드캐스터오일, 피이지-60하이드로제네이티드캐스터오일, 폴리소르베이트 20, 폴리소르베이트 60, 폴리소르베이트 80으로 구성되는 군에서 어느 하나 이상을 더 포함하는 경우, 보습효과가 다소 높음을 확인할 수 있었다. 가장 우수한 것은 제조예 1이였다. In addition, in the oily part and the emulsified part, the oily part further includes any one or more from the group consisting of meadowfoam seed oil, sunflower seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil, and the emulsified part In the group consisting of lecithin, polyglyceryl-10 stearate, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, polysorbate 20, polysorbate 60, and polysorbate 80. When more than one was included, it was confirmed that the moisturizing effect was somewhat high. The most excellent one was Preparation Example 1.
결론. conclusion.
상기 실시예 1 내지 16, 비교예 1 내지 5, 제조예 1을 통해 수행된 실험예 1 내지 4를 통하여, 본 발명에 따른 다층상 화장료 조성물은 다층상 분리 정도가 높고, 혼합까지 걸리는 시간이 빠르며, 혼합 후 분산 정도가 우수함은 물론, 피부 도포 후 보습효과가 우수한 것을 확인할 수 있었다. 즉, 본 발명에 따른 다층상 화장료 조성물은 층 분리 효과, 혼합의 용이성, 혼합 후 분산성, 그리고, 피부 보습 효과가 우수함을 확인할 수 있다. Through Experimental Examples 1 to 4 performed through Examples 1 to 16, Comparative Examples 1 to 5, and Preparation Example 1, the multilayer cosmetic composition according to the present invention has a high degree of multilayer separation, a quick mixing time, and , it was confirmed that not only was the degree of dispersion excellent after mixing, but also the moisturizing effect was excellent after application to the skin. That is, it can be confirmed that the multilayer cosmetic composition according to the present invention has excellent layer separation effect, ease of mixing, dispersibility after mixing, and skin moisturizing effect.
이와 같은 효과는 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트의 혼합물을 포함하는 유상부, 폴리글리세릴-10라우레이트 및 폴리글리세릴-10미리스테이트의 혼합물을 포함하는 유화부 및, 정제수 및 폴리올을 포함하는 수상부의 다층상으로 이루어지는 경우에만 확인할 수 있는 특성이며, 이들 중 어느 하나의 성분이 결여되면, 본 발명에 따른 층 분리 효과, 혼합의 용이성, 혼합 후 분산성, 피부 보습 효과가 용이하게 나타나기 어렵다는 것을, 일부 성분이 결여된 비교예를 통해 확인할 수 있었으며, 본 발명에 따른 다층상 화장료 조성물은 각 성분의 조합에 따라 예기치 못한 효과를 가져왔음을 확인할 수 있었다. This effect is achieved by an oily part containing a mixture of calendula oil and butylene glycol dicaprylate/dicaprate, an emulsified part containing a mixture of polyglyceryl-10 laurate and polyglyceryl-10 myristate, and , This is a characteristic that can be confirmed only when the aqueous phase consists of a multi-layered phase containing purified water and polyol, and if any one of these components is lacking, the layer separation effect according to the present invention, ease of mixing, dispersibility after mixing, and skin moisturization It was confirmed through a comparative example lacking some ingredients that the effect was difficult to appear, and it was confirmed that the multilayer cosmetic composition according to the present invention brought about unexpected effects depending on the combination of each ingredient.
이에 본 발명은, 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트의 혼합물을 주 성분으로 포함하는 유상부와, 폴리글리세릴-10라우레이트 및 폴리글리세릴-10미리스테이트의 혼합물을 주성분으로 포함하는 유화부, 정제수 및 폴리올을 포함하는 수상부로 이루어져, 층 분리 효과, 혼합의 용이성, 혼합 후 분산성 및 피부 보습 효과를 갖는 신규한 조성물로써, 다층상 화장료 조성물을 개발하였음을 명시한다. Accordingly, the present invention is a mixture of an oil phase containing a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as main ingredients, and a mixture of polyglyceryl-10 laurate and polyglyceryl-10 myristate. It is stated that a multi-layered cosmetic composition has been developed as a novel composition consisting of an emulsified part containing as the main ingredient and an aqueous part containing purified water and polyol, and has a layer separation effect, ease of mixing, dispersibility after mixing, and skin moisturizing effect. .
본 발명을 첨부된 도면과 함께 설명하였으나, 이는 본 발명의 요지를 포함하는 다양한 실시 형태 중의 하나의 실시 예에 불과하며, 당 업계에서 통상의 지식을 가진 자가 용이하게 실시할 수 있도록 하는 데에 그 목적이 있는 것으로, 본 발명은 상기 설명된 실시예에만 국한되는 것이 아님은 명확하다. 따라서, 본 발명의 보호범위는 하기의 청구범위에 의해 해석되어야 하며, 본 발명의 요지를 벗어나지 않는 범위 내에서 변경, 치환, 대체 등에 의해 그와 동등한 범위 내에 있는 모든 기술 사상은 본 발명의 권리에 포함될 것이다. 또한, 도면의 일부 구성은 구성을 보다 명확하게 설명하기 위한 것으로 실제보다 과장되거나 축소되어 제공되는 것임을 명확히 한다.Although the present invention has been described with the accompanying drawings, this is only one example among various embodiments including the gist of the present invention, and is intended to enable those skilled in the art to easily implement the present invention. For this purpose, it is clear that the present invention is not limited to the embodiments described above. Accordingly, the scope of protection of the present invention should be interpreted in accordance with the following claims, and all technical ideas within the equivalent scope by change, substitution, substitution, etc. without departing from the gist of the present invention are subject to the rights of the present invention. will be included In addition, it is clarified that some of the configurations in the drawings are provided in an exaggerated or reduced form compared to the actual figure for the purpose of explaining the configuration more clearly.

Claims (5)

  1. 카렌둘라오일 및 부틸렌글라이콜다이카프릴레이트/다이카프레이트의 혼합물을 유효성분으로 포함하는 유상부, An oily part containing a mixture of calendula oil and butylene glycol dicaprylate/dicaprate as active ingredients,
    폴리글리세릴-10라우레이트 및 폴리글리세릴-10미리스테이트의 혼합물을 유효성분으로 포함하는 유화부; 및, An emulsifying portion containing a mixture of polyglyceryl-10 laurate and polyglyceryl-10 myristate as active ingredients; and,
    정제수 및 폴리올을 포함하는 수상부;의 다층상으로 이루어지는 것을 특징으로 하는 다층상 화장료 조성물. A multi-layer cosmetic composition, characterized in that it consists of a multi-layer phase; an aqueous phase containing purified water and polyol.
  2. 제1항에 있어서, According to paragraph 1,
    상기 유상부는 메도우폼씨오일, 해바라기씨오일, 카프릴릭/카프릭트라이글리세라이드, 포도씨오일, 아보카도오일로 구성된 군에서 어느 하나 이상을 선택하여 더 포함하는 것을 특징으로 하는 다층상 화장료 조성물. A multi-layered cosmetic composition, characterized in that the oil phase further includes one or more selected from the group consisting of meadowfoam seed oil, sunflower seed oil, caprylic/capric triglyceride, grape seed oil, and avocado oil.
  3. 제1항에 있어서, According to paragraph 1,
    상기 유화부는 레시틴, 폴리글리세릴-10스테아레이트, 피이지-40하이드로제네이티드캐스터오일, 피이지-60하이드로제네이티드캐스터오일, 폴리소르베이트 20, 폴리소르베이트 60, 폴리소르베이트 80으로 구성되는 군에서 어느 하나 이상을 선택하여 더 포함하는 것을 특징으로 하는 화장료 조성물. The emulsifying part consists of lecithin, polyglyceryl-10 stearate, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, polysorbate 20, polysorbate 60, and polysorbate 80. A cosmetic composition further comprising one or more selected from the group.
  4. 제1항에 있어서, According to paragraph 1,
    상기 수상부의 폴리올은 글리세린, 부틸렌글라이콜, 프로판다이올, 2,3-부탄다이올, 펜틸렌글라이콜, 소듐하이알루로네이트, 1,2-헥산다이올로 구성되는 군에서 어느 하나 이상인 것을 특징으로 하는 다층상 화장료 조성물. The polyol of the aqueous phase is any one or more from the group consisting of glycerin, butylene glycol, propanediol, 2,3-butanediol, pentylene glycol, sodium hyaluronate, and 1,2-hexanediol. A multi-layered cosmetic composition characterized in that.
  5. 제1항에 있어서, According to paragraph 1,
    전체 화장료 조성물 100 중량부에 대해, For 100 parts by weight of the total cosmetic composition,
    상기 유상부는 1.0 ~ 30.0 중량부로 포함되며, 상기 유화부는 1.0 ~ 30.0 중량부로 포함되고, 상기 수상부의 폴리올은 5.0 ~ 30.0 중량부, 상기 수상부의 정제수는 잔량으로 포함되는 것을 특징으로 하는 다층상 화장료 조성물. The oil phase part is contained in an amount of 1.0 to 30.0 parts by weight, the emulsified part is contained in an amount of 1.0 to 30.0 parts by weight, the polyol in the aqueous phase part is contained in an amount of 5.0 to 30.0 parts by weight, and the purified water in the aqueous phase part is contained in the remaining amount. .
PCT/KR2023/014302 2022-09-23 2023-09-20 Multi-layer phase cosmetic composition WO2024063540A1 (en)

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KR20110097336A (en) * 2010-02-25 2011-08-31 차인수 Cosmetic composition containing pear and method of the same
KR101991248B1 (en) * 2019-01-10 2019-06-20 주식회사 솔레오코스메틱 Emulsion composition for cosmetics and cosmetics composition for sheet mask using the same
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KR102560840B1 (en) * 2022-09-23 2023-07-28 (주)에델프라우 Multi-Layered Cosmetic Composition

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KR102395902B1 (en) * 2017-11-17 2022-05-09 (주)아모레퍼시픽 Transparent cosmetic composition
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