KR102688001B1 - 녹색 감광성 수지 조성물, 이를 포함하는 컬러필터 및 화상표시장치 - Google Patents
녹색 감광성 수지 조성물, 이를 포함하는 컬러필터 및 화상표시장치 Download PDFInfo
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- KR102688001B1 KR102688001B1 KR1020230017848A KR20230017848A KR102688001B1 KR 102688001 B1 KR102688001 B1 KR 102688001B1 KR 1020230017848 A KR1020230017848 A KR 1020230017848A KR 20230017848 A KR20230017848 A KR 20230017848A KR 102688001 B1 KR102688001 B1 KR 102688001B1
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- resin composition
- photosensitive resin
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- green photosensitive
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- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims abstract description 9
- 125000004169 (C1-C6) alkyl group Chemical group 0.000 claims abstract description 6
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- 125000005843 halogen group Chemical group 0.000 description 5
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- FVQMJJQUGGVLEP-UHFFFAOYSA-N (2-methylpropan-2-yl)oxy 2-ethylhexaneperoxoate Chemical compound CCCCC(CC)C(=O)OOOC(C)(C)C FVQMJJQUGGVLEP-UHFFFAOYSA-N 0.000 description 3
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
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- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical group [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 3
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- MKYBYDHXWVHEJW-UHFFFAOYSA-N N-[1-oxo-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propan-2-yl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(C(C)NC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 MKYBYDHXWVHEJW-UHFFFAOYSA-N 0.000 description 3
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- MPIAGWXWVAHQBB-UHFFFAOYSA-N [3-prop-2-enoyloxy-2-[[3-prop-2-enoyloxy-2,2-bis(prop-2-enoyloxymethyl)propoxy]methyl]-2-(prop-2-enoyloxymethyl)propyl] prop-2-enoate Chemical compound C=CC(=O)OCC(COC(=O)C=C)(COC(=O)C=C)COCC(COC(=O)C=C)(COC(=O)C=C)COC(=O)C=C MPIAGWXWVAHQBB-UHFFFAOYSA-N 0.000 description 2
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- 125000001511 cyclopentyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C1([H])[H] 0.000 description 2
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- SJMYWORNLPSJQO-UHFFFAOYSA-N tert-butyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OC(C)(C)C SJMYWORNLPSJQO-UHFFFAOYSA-N 0.000 description 1
- ISXSCDLOGDJUNJ-UHFFFAOYSA-N tert-butyl prop-2-enoate Chemical compound CC(C)(C)OC(=O)C=C ISXSCDLOGDJUNJ-UHFFFAOYSA-N 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 125000001712 tetrahydronaphthyl group Chemical group C1(CCCC2=CC=CC=C12)* 0.000 description 1
- 229920005992 thermoplastic resin Polymers 0.000 description 1
- 125000000335 thiazolyl group Chemical group 0.000 description 1
- 125000001544 thienyl group Chemical group 0.000 description 1
- 125000003396 thiol group Chemical group [H]S* 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
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- 238000004448 titration Methods 0.000 description 1
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- 125000004784 trichloromethoxy group Chemical group ClC(O*)(Cl)Cl 0.000 description 1
- 125000003866 trichloromethyl group Chemical group ClC(Cl)(Cl)* 0.000 description 1
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- DQZNLOXENNXVAD-UHFFFAOYSA-N trimethoxy-[2-(7-oxabicyclo[4.1.0]heptan-4-yl)ethyl]silane Chemical compound C1C(CC[Si](OC)(OC)OC)CCC2OC21 DQZNLOXENNXVAD-UHFFFAOYSA-N 0.000 description 1
- BPSIOYPQMFLKFR-UHFFFAOYSA-N trimethoxy-[3-(oxiran-2-ylmethoxy)propyl]silane Chemical compound CO[Si](OC)(OC)CCCOCC1CO1 BPSIOYPQMFLKFR-UHFFFAOYSA-N 0.000 description 1
- YUYCVXFAYWRXLS-UHFFFAOYSA-N trimethoxysilane Chemical compound CO[SiH](OC)OC YUYCVXFAYWRXLS-UHFFFAOYSA-N 0.000 description 1
- UJMBCXLDXJUMFB-UHFFFAOYSA-K trisodium;5-oxo-1-(4-sulfonatophenyl)-4-[(4-sulfonatophenyl)diazenyl]-4h-pyrazole-3-carboxylate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(=O)C1N=NC1=CC=C(S([O-])(=O)=O)C=C1 UJMBCXLDXJUMFB-UHFFFAOYSA-K 0.000 description 1
- 239000006097 ultraviolet radiation absorber Substances 0.000 description 1
- KOZCZZVUFDCZGG-UHFFFAOYSA-N vinyl benzoate Chemical compound C=COC(=O)C1=CC=CC=C1 KOZCZZVUFDCZGG-UHFFFAOYSA-N 0.000 description 1
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- 229920002554 vinyl polymer Polymers 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000001052 yellow pigment Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
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- C08F222/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a carboxyl radical and containing at least one other carboxyl radical in the molecule; Salts, anhydrides, esters, amides, imides, or nitriles thereof
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- C09B47/085—Preparation from other phthalocyanine compounds, e.g. cobaltphthalocyanineamine complex substituting the central metal atom
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Abstract
[화학식 1]
(상기 화학식 1에서,
A1은 수소 또는 메틸기이고,
A2는 C1 내지 C6의 알킬렌기 또는 C2 내지 C6의 알케닐렌기이며,
B는 C6 내지 C20의 아릴기, C3 내지 C10의 사이클로알킬기, C1 내지 C6의 알킬기 또는 C2 내지 C6의 알케닐기이다).
Description
조성 | 안료 분산액 | 알칼리 가용성 수지 | 광중합성 화합물 | 개시제 | 용매 | 첨가제 | |||||
A-1 | A-2 | A-3 | A-4 | B-1 | B-2 | B-3 | C-1 | D-1 | E-1 | F-1 | |
실시예 1 | 25.06 | - | - | 27.14 | 9.74 | - | - | 3.31 | 0.53 | 34.07 | 0.15 |
실시예 2 | 25.06 | - | - | 27.14 | - | 9.74 | - | 3.31 | 0.53 | 34.07 | 0.15 |
실시예 3 | - | 25.06 | - | 27.14 | 9.74 | - | - | 3.31 | 0.53 | 34.07 | 0.15 |
실시예 4 | - | 25.06 | - | 27.14 | 9.74 | - | 3.31 | 0.53 | 34.07 | 0.15 | |
비교예 1 | - | - | 41.58 | 12.42 | 9.38 | - | - | 3.19 | 0.51 | 32.77 | 0.15 |
비교예 2 | - | - | 41.58 | 12.42 | - | 9.38 | - | 3.19 | 0.51 | 32.77 | 0.15 |
비교예 3 | - | - | 41.58 | 12.42 | - | - | 9.38 | 3.19 | 0.51 | 32.77 | 0.15 |
비교예 4 | 25.06 | - | - | 27.14 | - | - | 9.74 | 3.31 | 0.53 | 34.07 | 0.15 |
비교예 5 | - | 25.06 | - | 27.14 | - | - | 9.74 | 3.31 | 0.53 | 34.07 | 0.15 |
A-1: 제조예 1-1의 안료 분산액 A-2: 제조예 1-2의 안료 분산액 A-3: 제조예 1-3의 안료 분산액 A-4: 제조예 1-4의 안료 분산액 B-1: 합성예 1의 알칼리 가용성 수지 B-2: 합성예 2의 알칼리 가용성 수지 B-3: 합성예 3의 알칼리 가용성 수지 C-1: KAYARAD DPHA(닛뽄가야꾸사 제) D-1: Irgacure OXE 03(BASF사 제) E-1: 프로필렌글리콜모노메틸에테르아세테이트 F-1: 실리콘계 레벨링지 SH-8400(Dow Corning Toray사 제) |
투과율(GY) | 투과율 | 현상속도 | 재용해성 | 밀착성 | 잔사 | 내화학성 | |
판정 | (sec) | ||||||
실시예 1 | 62.3 | OK | 13 | ○ | ○ | ○ | ○ |
실시예 2 | 62.2 | OK | 10 | ○ | △ | ○ | △ |
실시예 3 | 62 | OK | 12 | ○ | ○ | ○ | ○ |
실시예 4 | 61.9 | OK | 9 | ○ | △ | ○ | △ |
비교예 1 | 59.6 | NG | 33 | ○ | ○ | ○ | ○ |
비교예 2 | 59.4 | NG | 30 | ○ | △ | ○ | △ |
비교예 3 | 59.2 | NG | 42 | × | × | × | × |
비교예 4 | 61.2 | OK | 29 | × | △ | × | △ |
비교예 5 | 61.2 | OK | 30 | × | △ | × | △ |
Claims (12)
- N-벤질말레이미드 및 하기 화학식 1로 표시되는 화합물을 포함하여 공중합된 알칼리 가용성 수지; 및 알루미늄 프탈로시아닌 화합물을 함유하는 착색제;를 포함하고,
상기 알루미늄 프탈로시아닌 화합물은 C.I. 피그먼트 그린 62 또는 C.I. 피그먼트 그린 63을 포함하며,
상기 착색제는 안료로써 C.I. 피그먼트 옐로우 138 또는 C.I. 피그먼트 옐로우 231을 더 포함하고,
상기 알칼리 가용성 수지는 중량평균분자량이 18,000 내지 23,000인 것을 특징으로 하는 녹색 감광성 수지 조성물:
[화학식 1]
(상기 화학식 1에서,
A1은 수소 또는 메틸기이고,
A2는 C1 내지 C6의 알킬렌기 또는 C2 내지 C6의 알케닐렌기이며,
B는 C6 내지 C20의 아릴기, C3 내지 C10의 사이클로알킬기, C1 내지 C6의 알킬기 또는 C2 내지 C6의 알케닐기이다). - 청구항 1에 있어서,
상기 화학식 1로 표시되는 화합물은 하기 화학식 2로 표시되는 화합물을 포함하는 것을 특징으로 하는 녹색 감광성 수지 조성물:
[화학식 2]
(상기 화학식 2에서,
A3은 수소 또는 메틸기이고,
A4는 C1 내지 C6의 알킬렌기 또는 C2 내지 C6의 알케닐렌기이다). - 삭제
- 삭제
- 삭제
- 삭제
- 제1항에 있어서,
상기 알칼리 가용성 수지는 이를 포함하는 녹색 감광성 수지 조성물 중 고형분 전체 100중량%에 대하여 5 내지 80중량%로 포함되는 것을 특징으로 하는 녹색 감광성 수지 조성물. - 제1항에 있어서,
상기 착색제는 이를 포함하는 녹색 감광성 수지 조성물 중 고형분 전체 100중량%에 대하여 5 내지 60중량%로 포함되는 것을 특징으로 하는 녹색 감광성 수지 조성물. - 제1항에 있어서,
상기 알루미늄 프탈로시아닌 화합물은 이를 포함하는 착색제 전체 100중량%에 대하여 30 내지 100중량%로 포함되는 것을 특징으로 하는 녹색 감광성 수지 조성물. - 제1항에 있어서,
상기 녹색 감광성 수지 조성물은 광중합성 화합물, 광중합 개시제 및 용제를 더 포함하는 것을 특징으로 하는 녹색 감광성 수지 조성물. - 제1항, 제2항 및 제7항 내지 제10항 중 어느 한 항의 녹색 감광성 수지 조성물의 경화물을 포함하는 것을 특징으로 하는 컬러필터.
- 제11항의 컬러필터를 포함하는 것을 특징으로 하는 화상표시장치.
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JP5743588B2 (ja) * | 2011-02-17 | 2015-07-01 | 富士フイルム株式会社 | 着色感放射線性組成物、パターンの形成方法、カラーフィルタの製造方法、カラーフィルタ、および固体撮像素子 |
KR20160115347A (ko) * | 2015-03-26 | 2016-10-06 | 동우 화인켐 주식회사 | 착색 감광성 수지 조성물 |
KR102491715B1 (ko) * | 2015-03-27 | 2023-01-25 | 미쯔비시 케미컬 주식회사 | 착색 수지 조성물, 컬러 필터, 및 화상 표시 장치 |
KR102497605B1 (ko) * | 2015-12-23 | 2023-02-08 | 동우 화인켐 주식회사 | 착색 감광성 수지 조성물, 이를 이용하여 제조된 칼라필터, 화상표시장치, 및 칼라필터의 제조방법 |
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KR102364788B1 (ko) * | 2016-03-24 | 2022-02-18 | 동우 화인켐 주식회사 | 착색 감광성 수지 조성물, 이를 포함하는 컬러필터 및 표시장치 |
JP6862706B2 (ja) * | 2016-07-27 | 2021-04-21 | 東洋インキScホールディングス株式会社 | 固体撮像素子用緑色着色組成物および固体撮像素子用カラーフィルタ |
KR102398257B1 (ko) * | 2016-08-01 | 2022-05-13 | 토요잉크Sc홀딩스주식회사 | 감광성 착색 조성물 및 컬러 필터 |
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