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JPS5775992A - Purification of stevioside - Google Patents

Purification of stevioside

Info

Publication number
JPS5775992A
JPS5775992A JP15281980A JP15281980A JPS5775992A JP S5775992 A JPS5775992 A JP S5775992A JP 15281980 A JP15281980 A JP 15281980A JP 15281980 A JP15281980 A JP 15281980A JP S5775992 A JPS5775992 A JP S5775992A
Authority
JP
Japan
Prior art keywords
stevioside
activated charcoal
decoloring
activated
purification
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP15281980A
Other languages
Japanese (ja)
Other versions
JPH0245637B2 (en
Inventor
Masashi Osada
Tadashi Yamamoto
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tama Biochemical Co Ltd
Original Assignee
Tama Biochemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tama Biochemical Co Ltd filed Critical Tama Biochemical Co Ltd
Priority to JP15281980A priority Critical patent/JPS5775992A/en
Publication of JPS5775992A publication Critical patent/JPS5775992A/en
Publication of JPH0245637B2 publication Critical patent/JPH0245637B2/ja
Granted legal-status Critical Current

Links

Landscapes

  • Compounds Of Unknown Constitution (AREA)
  • Saccharide Compounds (AREA)

Abstract

PURPOSE: To carry out the decoloring and purification of stevioside, easily, in an industrial scale, by treating the extract liquid of the leaves of Stevia with activated charcoal and activated clay in combination, thereby effectively removing the impurities such as pigments from the liquid.
CONSTITUTION: The extract liquid obtained by the extraction of the sweetening substances (general name: stevioside) from the leaves of Stevia rebaudiana Bertoni, is mixed with a flocculant (e.g. common alum or polyaluminum chloride) to flocculate and remove the collidal impurities, and then treated with a non-polar resin (e.g. "Duolite " ES-861) to adsorb the sweetening substance to said non-polar resin. The adsorbed substance is eluted with an organic solvent (e.g. methanol, acetone, etc.), and the eluate is decolored and purified with activated charcoal and activated clay. Although activated charcoal can absorb the stevioside firmly in an aqueous solution, it hardly adsorbs in an organic solvent and nevertheless keeps the decoloring effect. The decoloring and purification effects of activated charcoal can be promoted by the combined use with activated clay.
COPYRIGHT: (C)1982,JPO&Japio
JP15281980A 1980-10-30 1980-10-30 Purification of stevioside Granted JPS5775992A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP15281980A JPS5775992A (en) 1980-10-30 1980-10-30 Purification of stevioside

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP15281980A JPS5775992A (en) 1980-10-30 1980-10-30 Purification of stevioside

Publications (2)

Publication Number Publication Date
JPS5775992A true JPS5775992A (en) 1982-05-12
JPH0245637B2 JPH0245637B2 (en) 1990-10-11

Family

ID=15548843

Family Applications (1)

Application Number Title Priority Date Filing Date
JP15281980A Granted JPS5775992A (en) 1980-10-30 1980-10-30 Purification of stevioside

Country Status (1)

Country Link
JP (1) JPS5775992A (en)

Cited By (43)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8257948B1 (en) 2011-02-17 2012-09-04 Purecircle Usa Method of preparing alpha-glucosyl Stevia composition
US8299224B2 (en) 2009-10-15 2012-10-30 Purecircle Sdn Bhd High-purity Rebaudioside D
US8318459B2 (en) 2011-02-17 2012-11-27 Purecircle Usa Glucosyl stevia composition
US8334006B2 (en) 2005-10-11 2012-12-18 Purecircle Sdn Bhd Process for manufacturing a sweetener and use thereof
US8337927B2 (en) 2005-10-11 2012-12-25 Purecircle Sdn Bhd Process for manufacturing a sweetener and use thereof
US8414950B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie table top tablet containing the same
US8414952B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie diet cookies containing the same
US8414949B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie yogurt containing the same
US8414948B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie ice cream containing the same
US8414951B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity Rebaudioside D and low-calorie soy sauce containing the same
US8420147B2 (en) 2009-10-15 2013-04-16 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie cake containing the same
US8420146B2 (en) 2009-10-15 2013-04-16 Purecircle Sdn Bhd High-purity Rebaudioside D and low-calorie bread containing the same
US8507022B2 (en) 2009-10-15 2013-08-13 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie carbonated lemon-flavored beverage containing the same
US8512790B2 (en) 2009-10-15 2013-08-20 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie chocolate containing the same
US8568818B2 (en) 2009-10-15 2013-10-29 Pure Circle Sdn Bhd High-purity Rebaudioside D and low-calorie carbonated drink containing the same
US8574656B2 (en) 2009-10-15 2013-11-05 Purecircle Sdn Bhd High-purity Rebaudioside D and low-calorie fruit juice containing the same
EP2708548A2 (en) 2009-10-15 2014-03-19 Purecircle SDN BHD High-Purity Rebaudioside D and Applications
US8790730B2 (en) 2005-10-11 2014-07-29 Purecircle Usa Process for manufacturing a sweetener and use thereof
US8916138B2 (en) 2009-10-15 2014-12-23 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie tooth paste composition containing the same
CN105037459A (en) * 2015-07-23 2015-11-11 蚌埠市华东生物科技有限公司 Flocculant capable of improving refining efficiency of stevioside
US9752174B2 (en) 2013-05-28 2017-09-05 Purecircle Sdn Bhd High-purity steviol glycosides
US9771434B2 (en) 2011-06-23 2017-09-26 Purecircle Sdn Bhd Products from stevia rebaudiana
US9877501B2 (en) 2011-06-03 2018-01-30 Purecircle Sdn Bhd Stevia composition
US9894922B2 (en) 2011-05-18 2018-02-20 Purecircle Sdn Bhd Glucosyl rebaudioside C
US10004245B2 (en) 2009-11-12 2018-06-26 Purecircle Sdn Bhd Granulation of a stevia sweetener
US10021899B2 (en) 2011-05-31 2018-07-17 Purecircle Sdn Bhd Stevia composition
US10362797B2 (en) 2011-02-10 2019-07-30 Purecircle Sdn Bhd Stevia composition
US10480019B2 (en) 2011-08-10 2019-11-19 Purecircle Sdn Bhd Process for producing high-purity rubusoside
US10485257B2 (en) 2012-05-22 2019-11-26 Purecircle Sdn Bhd Method of making steviol glycosides
US10602762B2 (en) 2011-02-17 2020-03-31 Purecircle Sdn Bhd Glucosylated steviol glycoside as a flavor modifier
US10696706B2 (en) 2010-03-12 2020-06-30 Purecircle Usa Inc. Methods of preparing steviol glycosides and uses of the same
US10780170B2 (en) 2013-06-07 2020-09-22 Purecircle Sdn Bhd Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier
US10952458B2 (en) 2013-06-07 2021-03-23 Purecircle Usa Inc Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier
WO2021220948A1 (en) * 2020-04-27 2021-11-04 サントリーホールディングス株式会社 Production method of steviol glycoside composition
US11202461B2 (en) 2014-09-02 2021-12-21 Purecircle Sdn Bhd Stevia extracts
US11291232B2 (en) 2010-12-13 2022-04-05 Purecircle Sdn Bhd Highly soluble Rebaudioside D
US11464246B2 (en) 2011-09-07 2022-10-11 Purecircle Sdn Bhd Highly soluble Stevia sweetener
US11647771B2 (en) 2015-10-26 2023-05-16 Purecircle Usa Inc. Steviol glycoside compositions
US11653686B2 (en) 2015-12-15 2023-05-23 Purecircle Usa Inc. Steviol glycoside compositions
US11678685B2 (en) 2011-02-17 2023-06-20 Purecircle Sdn Bhd Glucosyl stevia composition
US11690391B2 (en) 2011-02-17 2023-07-04 Purecircle Sdn Bhd Glucosylated steviol glycoside as a flavor modifier
US11871771B2 (en) 2011-02-17 2024-01-16 Purecircle Sdn Bhd Glucosyl Stevia composition
US12016355B2 (en) 2011-02-10 2024-06-25 Purecircle Sdn Bhd Stevia composition

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5123300A (en) * 1974-08-19 1976-02-24 Toyo Sugar Refining Sutebiasaidono bunriseiseihoho
JPS5247961A (en) * 1975-10-16 1977-04-16 Chugai Pharmaceutical Co Ltd Isorating method of steviocide
JPS5430199A (en) * 1977-08-08 1979-03-06 Sanyo Kokusaku Pulp Co Ltd Purification of stevia sweetening agnet
JPS56137866A (en) * 1980-03-31 1981-10-28 Toyo Seito Kk Preparation of steviol glucoside having no bitter component, no puckery component, and no odor component

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5123300A (en) * 1974-08-19 1976-02-24 Toyo Sugar Refining Sutebiasaidono bunriseiseihoho
JPS5247961A (en) * 1975-10-16 1977-04-16 Chugai Pharmaceutical Co Ltd Isorating method of steviocide
JPS5430199A (en) * 1977-08-08 1979-03-06 Sanyo Kokusaku Pulp Co Ltd Purification of stevia sweetening agnet
JPS56137866A (en) * 1980-03-31 1981-10-28 Toyo Seito Kk Preparation of steviol glucoside having no bitter component, no puckery component, and no odor component

Cited By (64)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8337927B2 (en) 2005-10-11 2012-12-25 Purecircle Sdn Bhd Process for manufacturing a sweetener and use thereof
US8790730B2 (en) 2005-10-11 2014-07-29 Purecircle Usa Process for manufacturing a sweetener and use thereof
US10531683B2 (en) 2005-10-11 2020-01-14 Purecircle Sdn Bhd Process for manufacturing a sweetener and use thereof
US8334006B2 (en) 2005-10-11 2012-12-18 Purecircle Sdn Bhd Process for manufacturing a sweetener and use thereof
US8568818B2 (en) 2009-10-15 2013-10-29 Pure Circle Sdn Bhd High-purity Rebaudioside D and low-calorie carbonated drink containing the same
US8574656B2 (en) 2009-10-15 2013-11-05 Purecircle Sdn Bhd High-purity Rebaudioside D and low-calorie fruit juice containing the same
US8414952B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie diet cookies containing the same
US8414949B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie yogurt containing the same
US8414948B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie ice cream containing the same
US8414951B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity Rebaudioside D and low-calorie soy sauce containing the same
US8420147B2 (en) 2009-10-15 2013-04-16 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie cake containing the same
US8420146B2 (en) 2009-10-15 2013-04-16 Purecircle Sdn Bhd High-purity Rebaudioside D and low-calorie bread containing the same
US8507022B2 (en) 2009-10-15 2013-08-13 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie carbonated lemon-flavored beverage containing the same
US8512790B2 (en) 2009-10-15 2013-08-20 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie chocolate containing the same
US8916138B2 (en) 2009-10-15 2014-12-23 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie tooth paste composition containing the same
US8414950B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie table top tablet containing the same
EP2708548A2 (en) 2009-10-15 2014-03-19 Purecircle SDN BHD High-Purity Rebaudioside D and Applications
US8299224B2 (en) 2009-10-15 2012-10-30 Purecircle Sdn Bhd High-purity Rebaudioside D
US10004245B2 (en) 2009-11-12 2018-06-26 Purecircle Sdn Bhd Granulation of a stevia sweetener
US11773125B2 (en) 2010-03-12 2023-10-03 Purecircle Usa Inc. Methods of preparing steviol glycosides and uses of the same
US11155570B2 (en) 2010-03-12 2021-10-26 Purecircle Usa Inc. Methods of preparing steviol glycosides and uses of the same
US10696706B2 (en) 2010-03-12 2020-06-30 Purecircle Usa Inc. Methods of preparing steviol glycosides and uses of the same
US11950611B2 (en) 2010-12-13 2024-04-09 Purecircle Sdn Bhd Highly soluble Rebaudioside D
US11291232B2 (en) 2010-12-13 2022-04-05 Purecircle Sdn Bhd Highly soluble Rebaudioside D
US12016355B2 (en) 2011-02-10 2024-06-25 Purecircle Sdn Bhd Stevia composition
US11856974B2 (en) 2011-02-10 2024-01-02 Purecircle Sdn Bhd Highly soluble stevia sweetener
US11812771B2 (en) 2011-02-10 2023-11-14 Purecircle Sdn Bhd Stevia composition
US10362797B2 (en) 2011-02-10 2019-07-30 Purecircle Sdn Bhd Stevia composition
US10602762B2 (en) 2011-02-17 2020-03-31 Purecircle Sdn Bhd Glucosylated steviol glycoside as a flavor modifier
US11229228B2 (en) 2011-02-17 2022-01-25 Purecircle Sdn Bhd Glucosyl stevia composition
US11678685B2 (en) 2011-02-17 2023-06-20 Purecircle Sdn Bhd Glucosyl stevia composition
US8257948B1 (en) 2011-02-17 2012-09-04 Purecircle Usa Method of preparing alpha-glucosyl Stevia composition
US9615599B2 (en) 2011-02-17 2017-04-11 Purecircle Sdn Bhd Glucosyl stevia composition
US10743572B2 (en) 2011-02-17 2020-08-18 Purecircle Sdn Bhd Glucosylated steviol glycoside as a flavor modifier
US8318459B2 (en) 2011-02-17 2012-11-27 Purecircle Usa Glucosyl stevia composition
US11690391B2 (en) 2011-02-17 2023-07-04 Purecircle Sdn Bhd Glucosylated steviol glycoside as a flavor modifier
US11871771B2 (en) 2011-02-17 2024-01-16 Purecircle Sdn Bhd Glucosyl Stevia composition
US11957144B2 (en) 2011-02-17 2024-04-16 Purecircle Sdn Bhd Glucosylated steviol glycoside as a flavor modifier
US9894922B2 (en) 2011-05-18 2018-02-20 Purecircle Sdn Bhd Glucosyl rebaudioside C
US10021899B2 (en) 2011-05-31 2018-07-17 Purecircle Sdn Bhd Stevia composition
US11712055B2 (en) 2011-05-31 2023-08-01 Purecircle Sdn Bhd Stevia composition
US9877501B2 (en) 2011-06-03 2018-01-30 Purecircle Sdn Bhd Stevia composition
US11825867B2 (en) 2011-06-03 2023-11-28 Purecircle Sdn Bhd Stevia composition
US11279773B2 (en) 2011-06-23 2022-03-22 Purecircle Sdn Bhd Products from Stevia rabaudiana
US9771434B2 (en) 2011-06-23 2017-09-26 Purecircle Sdn Bhd Products from stevia rebaudiana
US10480019B2 (en) 2011-08-10 2019-11-19 Purecircle Sdn Bhd Process for producing high-purity rubusoside
US11957149B2 (en) 2011-09-07 2024-04-16 Purecircle Sdn Bhd Highly soluble stevia sweetener
US11464246B2 (en) 2011-09-07 2022-10-11 Purecircle Sdn Bhd Highly soluble Stevia sweetener
US11542537B2 (en) 2012-05-22 2023-01-03 Purecircle Sdn Bhd High-purity steviol glycosides
US10485257B2 (en) 2012-05-22 2019-11-26 Purecircle Sdn Bhd Method of making steviol glycosides
US9752174B2 (en) 2013-05-28 2017-09-05 Purecircle Sdn Bhd High-purity steviol glycosides
US11312984B2 (en) 2013-05-28 2022-04-26 Purecircle Sdn Bhd High-purity steviol glycosides
US11957756B2 (en) 2013-06-07 2024-04-16 Purecircle Sdn Bhd Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier
US10780170B2 (en) 2013-06-07 2020-09-22 Purecircle Sdn Bhd Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier
US12011017B2 (en) 2013-06-07 2024-06-18 Purecircle Usa Inc. Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier
US10952458B2 (en) 2013-06-07 2021-03-23 Purecircle Usa Inc Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier
US11202461B2 (en) 2014-09-02 2021-12-21 Purecircle Sdn Bhd Stevia extracts
US11230567B2 (en) 2014-09-02 2022-01-25 Purecircle Usa Inc. Stevia extracts enriched in rebaudioside D, E, N and/or O and process for the preparation thereof
US11856972B2 (en) 2014-09-02 2024-01-02 Purecircle Sdn Bhd Stevia extracts
CN105037459A (en) * 2015-07-23 2015-11-11 蚌埠市华东生物科技有限公司 Flocculant capable of improving refining efficiency of stevioside
US11647771B2 (en) 2015-10-26 2023-05-16 Purecircle Usa Inc. Steviol glycoside compositions
US11653686B2 (en) 2015-12-15 2023-05-23 Purecircle Usa Inc. Steviol glycoside compositions
WO2021220948A1 (en) * 2020-04-27 2021-11-04 サントリーホールディングス株式会社 Production method of steviol glycoside composition
CN115996642A (en) * 2020-04-27 2023-04-21 三得利控股株式会社 Method for producing steviol glycoside composition

Also Published As

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