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JPS5740447A - Preparation of 3-nitro-4- lower alkoxy aniline - Google Patents

Preparation of 3-nitro-4- lower alkoxy aniline

Info

Publication number
JPS5740447A
JPS5740447A JP11568180A JP11568180A JPS5740447A JP S5740447 A JPS5740447 A JP S5740447A JP 11568180 A JP11568180 A JP 11568180A JP 11568180 A JP11568180 A JP 11568180A JP S5740447 A JPS5740447 A JP S5740447A
Authority
JP
Japan
Prior art keywords
lower alkoxy
paa
aniline
nitric acid
mixing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP11568180A
Other languages
Japanese (ja)
Other versions
JPS6318573B2 (en
Inventor
Yoshiyuki Takeda
Osamu Kawashima
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Kasei Corp
Original Assignee
Mitsubishi Kasei Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Kasei Corp filed Critical Mitsubishi Kasei Corp
Priority to JP11568180A priority Critical patent/JPS5740447A/en
Publication of JPS5740447A publication Critical patent/JPS5740447A/en
Publication of JPS6318573B2 publication Critical patent/JPS6318573B2/ja
Granted legal-status Critical Current

Links

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

PURPOSE: To prepare the titled compound useful as an intermediate for the preparation of dyes, in high yield, suppressing the hydrolysis, by mixing a p-(lower alkoxy) aniline with nitric acid at a specific molar ratio, and reacting at a specific temperature in the presence of sulfuric acid.
CONSTITUTION: p-(Lower alkoxy)aniline (PAA) is made to react with nitric acid in the presence of sulfuric acid to obtain 3-nitro-4-(lower alkoxy)aniline (NAA). The reaction is carried out by mixing 0.7W1.3mol, pref. 0.9W1.1mol of nitric acid to 1mol of PAA, and keeping the temperature of the reaction mixture at -10W +20°C, pref. -5W+10°C. The PAA is e.g. p-methoxyaniline. The mixing of PAA and nitric acid is carried out continuously or intermittently at the above molar ratio. The feeding rate of the raw material is selected within the range in which the reaction system can be kept at the desired temperature.
COPYRIGHT: (C)1982,JPO&Japio
JP11568180A 1980-08-22 1980-08-22 Preparation of 3-nitro-4- lower alkoxy aniline Granted JPS5740447A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP11568180A JPS5740447A (en) 1980-08-22 1980-08-22 Preparation of 3-nitro-4- lower alkoxy aniline

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP11568180A JPS5740447A (en) 1980-08-22 1980-08-22 Preparation of 3-nitro-4- lower alkoxy aniline

Publications (2)

Publication Number Publication Date
JPS5740447A true JPS5740447A (en) 1982-03-06
JPS6318573B2 JPS6318573B2 (en) 1988-04-19

Family

ID=14668633

Family Applications (1)

Application Number Title Priority Date Filing Date
JP11568180A Granted JPS5740447A (en) 1980-08-22 1980-08-22 Preparation of 3-nitro-4- lower alkoxy aniline

Country Status (1)

Country Link
JP (1) JPS5740447A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002048089A1 (en) * 2000-12-12 2002-06-20 Ube Industries, Ltd. Process for producing mononitrated aromatic ether compound

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01158746U (en) * 1988-04-25 1989-11-02

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002048089A1 (en) * 2000-12-12 2002-06-20 Ube Industries, Ltd. Process for producing mononitrated aromatic ether compound

Also Published As

Publication number Publication date
JPS6318573B2 (en) 1988-04-19

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