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JPS565429A - Preparation of acetal - Google Patents

Preparation of acetal

Info

Publication number
JPS565429A
JPS565429A JP7968979A JP7968979A JPS565429A JP S565429 A JPS565429 A JP S565429A JP 7968979 A JP7968979 A JP 7968979A JP 7968979 A JP7968979 A JP 7968979A JP S565429 A JPS565429 A JP S565429A
Authority
JP
Japan
Prior art keywords
catalyst
raw material
acid ester
alcohol
nitrous acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP7968979A
Other languages
Japanese (ja)
Other versions
JPS6136733B2 (en
Inventor
Shinichiro Uchiumi
Kiyoshi Iwayama
Takaaki Abe
Hirobumi Matsunaga
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ube Corp
Original Assignee
Ube Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ube Industries Ltd filed Critical Ube Industries Ltd
Priority to JP7968979A priority Critical patent/JPS565429A/en
Publication of JPS565429A publication Critical patent/JPS565429A/en
Publication of JPS6136733B2 publication Critical patent/JPS6136733B2/ja
Granted legal-status Critical Current

Links

Classifications

    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PURPOSE: To obtain the titled compound useful as a raw material of agricultural chemicals, in high yield without using a special apparatus and complicated operations, by using a nitrous acid ester as a cocatalyst in the reaction of an α-olefin, an alcohol and oxygen in the presence of a palladium metal catalyst.
CONSTITUTION: The titled compound is obtained by the catalytic reaction of an α- olefin, an alcohol and oxygen, usually at 20W150°C under atmospheric or positive pressure, using palladium metal or its salts as a catalyst and a nitrous acid ester as a cocatalyst. Said catalyst is favorably used in the range of 0.001W5g, reduced to palladium metal, to 100ml of the raw material alcohols, and the co-catalyst is favorably used in the range of at least 0.05 times, preferably 0.1W5 times the volume of the raw material alcohol. Methyl nitrite, butyl nitrite, decyl nitrite, etc. are useful as the nitrous acid ester.
COPYRIGHT: (C)1981,JPO&Japio
JP7968979A 1979-06-26 1979-06-26 Preparation of acetal Granted JPS565429A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP7968979A JPS565429A (en) 1979-06-26 1979-06-26 Preparation of acetal

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP7968979A JPS565429A (en) 1979-06-26 1979-06-26 Preparation of acetal

Publications (2)

Publication Number Publication Date
JPS565429A true JPS565429A (en) 1981-01-20
JPS6136733B2 JPS6136733B2 (en) 1986-08-20

Family

ID=13697163

Family Applications (1)

Application Number Title Priority Date Filing Date
JP7968979A Granted JPS565429A (en) 1979-06-26 1979-06-26 Preparation of acetal

Country Status (1)

Country Link
JP (1) JPS565429A (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5821636A (en) * 1981-07-30 1983-02-08 Ube Ind Ltd Preparation of acetal
JPS58225035A (en) * 1982-06-25 1983-12-27 Ube Ind Ltd Production of 1-phenyl-2,2-dialkoxypropane
JPS59128343A (en) * 1983-01-11 1984-07-24 Ube Ind Ltd Preparation of 1-phenyl-2,2-dialkoxypropanes
JPS59128344A (en) * 1983-01-13 1984-07-24 Ube Ind Ltd Preparation of 1-phenyl-2,2-dialkoxypropanes
JPS6064941A (en) * 1983-09-20 1985-04-13 Ube Ind Ltd Production of 1-phenoxy-2,2-dialkoxypropane
CN103936570A (en) * 2014-05-08 2014-07-23 山西大学 Method for preparing acetal by dehydrogenation coupling of first-stage fatty alcohol

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5821636A (en) * 1981-07-30 1983-02-08 Ube Ind Ltd Preparation of acetal
JPS6140213B2 (en) * 1981-07-30 1986-09-08 Ube Industries
JPS58225035A (en) * 1982-06-25 1983-12-27 Ube Ind Ltd Production of 1-phenyl-2,2-dialkoxypropane
JPH0229058B2 (en) * 1982-06-25 1990-06-27 Ube Industries
JPS59128343A (en) * 1983-01-11 1984-07-24 Ube Ind Ltd Preparation of 1-phenyl-2,2-dialkoxypropanes
JPH03371B2 (en) * 1983-01-11 1991-01-07 Ube Industries
JPS59128344A (en) * 1983-01-13 1984-07-24 Ube Ind Ltd Preparation of 1-phenyl-2,2-dialkoxypropanes
JPH034048B2 (en) * 1983-01-13 1991-01-22 Ube Industries
JPS6064941A (en) * 1983-09-20 1985-04-13 Ube Ind Ltd Production of 1-phenoxy-2,2-dialkoxypropane
CN103936570A (en) * 2014-05-08 2014-07-23 山西大学 Method for preparing acetal by dehydrogenation coupling of first-stage fatty alcohol
CN103936570B (en) * 2014-05-08 2016-05-11 山西大学 The method of acetal is prepared in one-level fatty alcohol dehydrogenation coupling

Also Published As

Publication number Publication date
JPS6136733B2 (en) 1986-08-20

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