JP6821487B2 - 2層式毛髪化粧料 - Google Patents
2層式毛髪化粧料 Download PDFInfo
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- JP6821487B2 JP6821487B2 JP2017059617A JP2017059617A JP6821487B2 JP 6821487 B2 JP6821487 B2 JP 6821487B2 JP 2017059617 A JP2017059617 A JP 2017059617A JP 2017059617 A JP2017059617 A JP 2017059617A JP 6821487 B2 JP6821487 B2 JP 6821487B2
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- CXQXSVUQTKDNFP-UHFFFAOYSA-N octamethyltrisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C CXQXSVUQTKDNFP-UHFFFAOYSA-N 0.000 description 1
- AEIJTFQOBWATKX-UHFFFAOYSA-N octane-1,2-diol Chemical compound CCCCCCC(O)CO AEIJTFQOBWATKX-UHFFFAOYSA-N 0.000 description 1
- YPMOZWCBANATQH-UHFFFAOYSA-N octyl 7-methyloctanoate Chemical compound CCCCCCCCOC(=O)CCCCCC(C)C YPMOZWCBANATQH-UHFFFAOYSA-N 0.000 description 1
- 229940073665 octyldodecyl myristate Drugs 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- BARWIPMJPCRCTP-UHFFFAOYSA-N oleic acid oleyl ester Natural products CCCCCCCCC=CCCCCCCCCOC(=O)CCCCCCCC=CCCCCCCCC BARWIPMJPCRCTP-UHFFFAOYSA-N 0.000 description 1
- BARWIPMJPCRCTP-CLFAGFIQSA-N oleyl oleate Chemical compound CCCCCCCC\C=C/CCCCCCCCOC(=O)CCCCCCC\C=C/CCCCCCCC BARWIPMJPCRCTP-CLFAGFIQSA-N 0.000 description 1
- 239000004006 olive oil Substances 0.000 description 1
- 235000008390 olive oil Nutrition 0.000 description 1
- UWJJYHHHVWZFEP-UHFFFAOYSA-N pentane-1,1-diol Chemical compound CCCCC(O)O UWJJYHHHVWZFEP-UHFFFAOYSA-N 0.000 description 1
- 239000013500 performance material Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- NEOZOXKVMDBOSG-UHFFFAOYSA-N propan-2-yl 16-methylheptadecanoate Chemical compound CC(C)CCCCCCCCCCCCCCC(=O)OC(C)C NEOZOXKVMDBOSG-UHFFFAOYSA-N 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000008165 rice bran oil Substances 0.000 description 1
- 239000003352 sequestering agent Substances 0.000 description 1
- 229940057910 shea butter Drugs 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 229940008424 tetradecamethylhexasiloxane Drugs 0.000 description 1
- 229930003799 tocopherol Natural products 0.000 description 1
- 239000011732 tocopherol Substances 0.000 description 1
- 235000019149 tocopherols Nutrition 0.000 description 1
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 1
- 229940118594 trimethylolpropane triisostearate Drugs 0.000 description 1
- VLPFTAMPNXLGLX-UHFFFAOYSA-N trioctanoin Chemical compound CCCCCCCC(=O)OCC(OC(=O)CCCCCCC)COC(=O)CCCCCCC VLPFTAMPNXLGLX-UHFFFAOYSA-N 0.000 description 1
- 229940099259 vaseline Drugs 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 description 1
- QUEDXNHFTDJVIY-UHFFFAOYSA-N γ-tocopherol Chemical class OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/892—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a hydroxy group, e.g. dimethiconol
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Description
(1)下記成分Aを含有する油層、並びに、下記成分B、下記成分C、下記成分D及び下記成分Eを含有する水層の2層からなる2層式毛髪化粧料であり、
水層含有量に対する油層含有量(油層/水層、質量比)が20/80以上であり、
成分Bの水層中の含有量が20〜32質量%である2層式毛髪化粧料
成分A:25℃における動粘度が10万mm2/s以上であるジメチコン及び/又はジメチコノール
成分B:炭素数2〜5の低級アルコール
成分C:ラウリルトリモニウムクロリド及び/又はN−ヤシ油脂肪酸アシル−L−アルギニンエチル・DL−ピロリドンカルボン酸塩
成分D:水溶性高分子増粘剤
成分E:水
(2)前記成分Cの含有量が0.01〜0.30質量%である前記(1)記載の2層式毛髪化粧料
に関する。
前記油層は、特定の動粘度を有するジメチコン及び/又はジメチコノール(成分A)を含有する。
前記水層は、炭素数2〜5の低級アルコール(成分B)、ラウリルトリモニウムクロリド及び/又はN−ヤシ油脂肪酸アシル−L−アルギニンエチル・DL−ピロリドンカルボン酸塩(成分C)、水溶性高分子増粘剤(成分D)並びに水(成分E)を含有する。
前記2層式毛髪化粧料中の水層含有量に対する油層含有量(油層/水層、質量比)は、2層に分離するかどうかの観点から、20.0/80.0以上であり、好ましくは25.0/75.0以上であり、より好ましくは30.0/70.0以上である。また、水層含有量に対する油層含有量(油層/水層)は、2層に分離するかどうかの観点から、70.0/30.0以下が好ましく、より好ましくは65.0/35.0以下であり、さらに好ましくは60.0/40.0以下である。
成分A
高重合ジメチコン:25℃の動粘度1800万mm2/s
その他成分(油層)
不揮発性シリコーン油1:KF 96−350CS(信越化学工業(株)製)
不揮発性シリコーン油2:DOW CORNING TORAY SH200 C FLUID 60,000 CS(東レ・ダウコーニング(株)製)
流動パラフィン:Carnation(Sonneborn Inc社製)
水添ポリイソブテン:マルカゾールR(丸善石油化学(株)製)
成分B
エタノール:95°一般発酵アルコール
成分C
ラウリルトリモニウムクロリド:コータミン24P(花王(株)製、純分27%、イソプロパノール20%、水53%含有)
CAE:N−ヤシ油脂肪酸アシル−L−アルギニンエチル・DL−ピロリドンカルボン酸塩(味の素(株)製)
成分D
ヒドロキシプロピルメチルセルロース:メトローズ60SH−4000(信越化学工業(株)製)
その他成分(水層)
ステアリルトリモニウムクロリド:コータミン86W(花王(株)製、純分28%、水72%)
塩化ナトリウム:ナクルM(ナイカイ塩業(株)製)
グリセリン:化粧用濃グリセリン(阪本薬品工業(株))
PPG−2−デセス−7:EMALEX DAPE−0207(日本エマルジョン(株)製)
表1〜3に記した各組成に従って調製した2層式毛髪化粧料を透明の真円状PET容器に充填することで、実施例1〜10および比較例1〜9の評価試験用試料を調製した。得られた各試料を下記評価試験に供した。結果をそれぞれ表1〜3に併記する。
実施例および比較例の各試料をよく振った後、手のひらに適量取り出し、手のひらでよく伸ばしてから、人口毛の毛束(30cm)に塗布してなじませ、べたつき及び塗布性を、以下の基準に従って評価した。
<べたつきの評価基準>
◎(非常に良好):10名中9名以上が、べたつきがないと回答
○(良好):10名中7〜8名が、べたつきがないと回答
△(やや不良):10名中4〜6名が、べたつきがないと回答
×(不良):10名中3名以下が、べたつきがないと回答
<塗布性の評価基準>
◎(非常に良好):10名中9名以上が、掌からの垂れ落ちが無く毛髪への伸び馴染みがよく、良好な塗布性であると回答
○(良好):10名中7〜8名が、掌からの垂れ落ちが無く毛髪への伸び馴染みがよく、良好な塗布性であると回答
△(やや不良):10名中4〜6名が、掌からの垂れ落ちが無く毛髪への伸び馴染みがよく、良好な塗布性であると回答
×(不良):10名中3名以下が、掌からの垂れ落ちが無く毛髪への伸び馴染みがよく、良好な塗布性であると回答
実施例および比較例の各試料を油層及び水層が乳化して均一になるまで振盪し、乳化しやすさを以下の基準に従って評価した。
<乳化しやすさの評価基準>
◎(非常に良好):10名中9名以上が、容易に乳化できると回答
○(良好):10名中7〜8名が、容易に乳化できると回答
△(やや不良):10名中4〜6名が、容易に乳化できると回答
×(不良):10名中3名以下が、容易に乳化できると回答
実施例および比較例の各試料を油層及び水層が乳化して均一になるまで振盪した後、恒温環境下で静置し、5分後の乳化状態、並びに1時間後、3時間後及び5時間後の分離状態を目視にて確認し、以下の基準に従って評価した。
<乳化状態の評価基準>
◎(非常に良好):均一に白濁し、乳化状態が確認でき、分離は認められない。
○(良好):白濁し、乳化状態が確認できるが、上層に分離した油層が僅かに認められる。
△(やや不良):白濁し、乳化状態が確認できるが、上層に分離した油層が認められ、下層にも分離した水層が認められる。
×(不良):乳化状態が確認できず、油層と水層に分離している。
<分離状態の評価基準>
○(良好):乳化状態が確認できず、界面が明瞭な状態で2層に分離している。
△(やや不良):分離不良により界面付近に全体積の1/3以下の乳化層が認められる。
×(不良):分離不良により界面付近に全体積の1/3以上の乳化層が認められる。
処方例1
高重合ジメチコン 3.0質量%
水添ポリイソブテン 25.0質量%
デカメチルシクロペンタシロキサン 5.0質量%
イソノナン酸イソノニル 5.0質量%
オクタン酸セチル 4.0質量%
t−ブチルメトキシジベンゾイルメタン 0.02質量%
メトキシケイヒ酸エチルヘキシル 0.5質量%
エタノール 17.0質量%
ジグリセリン 6.0質量%
ヒドロキシプロピルグアガム 0.3質量%
N−ヤシ油脂肪酸アシル−L−アルギニンエチル・
DL−ピロリドンカルボン酸塩 0.2質量%
塩化ナトリウム 0.2質量%
クエン酸 0.01質量%
クエン酸ナトリウム 0.05質量%
エデト酸二ナトリウム 0.05質量%
精製水 33.67質量%
合計 100.00質量%
高重合ジメチコン 3.5質量%
水添ポリイソブテン 30.0質量%
トリ(カプリル酸/カプリン酸)グリセリル 7.0質量%
αオレフィンオリゴマー 3.0質量%
t−ブチルメトキシジベンゾイルメタン 0.02質量%
メトキシケイヒ酸エチルヘキシル 0.5質量%
香料 0.8質量%
エタノール 15.0質量%
ポリグリセリン 4.0質量%
ヒドロキシエチルセルロース 0.25質量%
ラウリルトリモニウムクロリド 0.11質量%
イソプロパノール 0.08質量%
PPG−2−デセス−7 0.2質量%
クエン酸 0.01質量%
クエン酸ナトリウム 0.05質量%
エデト酸二ナトリウム 0.05質量%
精製水 35.43質量%
合計 100.00質量%
Claims (2)
- 下記成分Aを含有する油層、並びに、下記成分B、下記成分C、下記成分D及び下記成分Eを含有する水層の2層からなる2層式毛髪化粧料であり、
水層含有量に対する油層含有量(油層/水層、質量比)が20.0/80.0以上であり、
成分Bの水層中の含有量が20〜32質量%である2層式毛髪化粧料。
成分A:25℃の動粘度が10万mm2/s以上であるジメチコン及び/又はジメチコノール
成分B:炭素数2〜5の低級アルコール
成分C:ラウリルトリモニウムクロリド及び/又はN−ヤシ油脂肪酸アシル−L−アルギニンエチル・DL−ピロリドンカルボン酸塩
成分D:水溶性高分子増粘剤
成分E:水 - 前記成分Cの2層式毛髪化粧料中の含有量が0.01〜0.30質量%である請求項1記載の2層式毛髪化粧料。
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