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GB754862A - Process and apparatus for decomposing organic hydroperoxides - Google Patents

Process and apparatus for decomposing organic hydroperoxides

Info

Publication number
GB754862A
GB754862A GB9914/54A GB991454A GB754862A GB 754862 A GB754862 A GB 754862A GB 9914/54 A GB9914/54 A GB 9914/54A GB 991454 A GB991454 A GB 991454A GB 754862 A GB754862 A GB 754862A
Authority
GB
United Kingdom
Prior art keywords
organic hydroperoxides
hydroperoxides
decomposing organic
mineral acid
pump
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB9914/54A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bergwerksgesellschaft Hibernia AG
Original Assignee
Bergwerksgesellschaft Hibernia AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bergwerksgesellschaft Hibernia AG filed Critical Bergwerksgesellschaft Hibernia AG
Publication of GB754862A publication Critical patent/GB754862A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00—Preparation of peroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00—Preparation of peroxy compounds
    • C07C407/003—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C409/00—Peroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Organic hydroperoxides of the formula <FORM:0754862/IV(a)/1> in which R1 and R2 represent alkyl, preferably lower alkyl, and Ar is aryl or substituted aryl, are decomposed with a mineral acid, e.g. sulphuric, in a rotary pump which is not more than half full, the ratio of hydroperoxide to mineral acid being between 1 : 14 and 1 : 20. The excess acid keeps the temperature low, and the reaction mixture is cooled after leaving the pump. Supersonic waves may be used. Reference is made to the production of acetone and phenol or p-cresol or naphthol from cumol, cymol, and isopropylnaphthalene hydroperoxides respectively. A conventional form of apparatus is described.
GB9914/54A 1953-05-08 1954-04-05 Process and apparatus for decomposing organic hydroperoxides Expired GB754862A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE754862X 1953-05-08

Publications (1)

Publication Number Publication Date
GB754862A true GB754862A (en) 1956-08-15

Family

ID=6659458

Family Applications (1)

Application Number Title Priority Date Filing Date
GB9914/54A Expired GB754862A (en) 1953-05-08 1954-04-05 Process and apparatus for decomposing organic hydroperoxides

Country Status (1)

Country Link
GB (1) GB754862A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3833491A (en) * 1973-03-02 1974-09-03 C Kennedy Production of macrocyclic compounds
EP0796833A2 (en) * 1996-03-20 1997-09-24 Rütgers Kureha Solvents GmbH Process for the preparation of hydroxyaromatics

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3833491A (en) * 1973-03-02 1974-09-03 C Kennedy Production of macrocyclic compounds
EP0796833A2 (en) * 1996-03-20 1997-09-24 Rütgers Kureha Solvents GmbH Process for the preparation of hydroxyaromatics
EP0796833A3 (en) * 1996-03-20 1998-04-01 Rütgers Kureha Solvents GmbH Process for the preparation of hydroxyaromatics
US6107527A (en) * 1996-03-20 2000-08-22 Rutgers Kureha Solvents Gmbh Process for the production of hydroxy-aromatic substances

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