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FR2578532B1 - Procede et installation de production d'azote - Google Patents

Procede et installation de production d'azote

Info

Publication number
FR2578532B1
FR2578532B1 FR8503515A FR8503515A FR2578532B1 FR 2578532 B1 FR2578532 B1 FR 2578532B1 FR 8503515 A FR8503515 A FR 8503515A FR 8503515 A FR8503515 A FR 8503515A FR 2578532 B1 FR2578532 B1 FR 2578532B1
Authority
FR
France
Prior art keywords
plant
nitrogen
production
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
FR8503515A
Other languages
English (en)
Other versions
FR2578532A1 (fr
Inventor
Maurice Grenier
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Air Liquide SA
Original Assignee
Air Liquide SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=9317050&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=FR2578532(B1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Air Liquide SA filed Critical Air Liquide SA
Priority to FR8503515A priority Critical patent/FR2578532B1/fr
Priority to IT19622/86A priority patent/IT1191980B/it
Priority to DE3606967A priority patent/DE3606967C2/de
Priority to NL8600582A priority patent/NL8600582A/nl
Priority to US06/837,049 priority patent/US4717410A/en
Priority to AU54406/86A priority patent/AU584174B2/en
Priority to BE0/216376A priority patent/BE904366A/fr
Priority to ES552844A priority patent/ES8800112A1/es
Priority to NO860874A priority patent/NO167167C/no
Priority to JP61050711A priority patent/JPH0731003B2/ja
Priority to CA000503741A priority patent/CA1298777C/fr
Publication of FR2578532A1 publication Critical patent/FR2578532A1/fr
Publication of FR2578532B1 publication Critical patent/FR2578532B1/fr
Application granted granted Critical
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04254—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using the cold stored in external cryogenic fluids
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/04321—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of oxygen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04406—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system
    • F25J3/04412—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system in a classical double column flowsheet, i.e. with thermal coupling by a main reboiler-condenser in the bottom of low pressure respectively top of high pressure column
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/20—Processes or apparatus using separation by rectification in an elevated pressure multiple column system wherein the lowest pressure column is at a pressure well above the minimum pressure needed to overcome pressure drop to reject the products to atmosphere
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/50—Processes or apparatus using separation by rectification using multiple (re-)boiler-condensers at different heights of the column
    • F25J2200/54—Processes or apparatus using separation by rectification using multiple (re-)boiler-condensers at different heights of the column in the low pressure column of a double pressure main column system
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2210/00—Processes characterised by the type or other details of the feed stream
    • F25J2210/42—Nitrogen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2235/00—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams
    • F25J2235/42—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams the fluid being nitrogen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2245/00—Processes or apparatus involving steps for recycling of process streams
    • F25J2245/42—Processes or apparatus involving steps for recycling of process streams the recycled stream being nitrogen
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S62/00—Refrigeration
    • Y10S62/912—External refrigeration system
    • Y10S62/913—Liquified gas

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Catalysts (AREA)
FR8503515A 1985-03-11 1985-03-11 Procede et installation de production d'azote Expired - Lifetime FR2578532B1 (fr)

Priority Applications (11)

Application Number Priority Date Filing Date Title
FR8503515A FR2578532B1 (fr) 1985-03-11 1985-03-11 Procede et installation de production d'azote
IT19622/86A IT1191980B (it) 1985-03-11 1986-03-04 Procedimento e impianto di produzione di azoto sotto pressione
DE3606967A DE3606967C2 (de) 1985-03-11 1986-03-04 Verfahren zur Herstellung von Stickstoff unter Druck und Anlage zur Durchführung des Verfahrens
NL8600582A NL8600582A (nl) 1985-03-11 1986-03-06 Werkwijze en inrichting voor de vorming van stikstof onder druk.
US06/837,049 US4717410A (en) 1985-03-11 1986-03-06 Process and installation for producing nitrogen under pressure
BE0/216376A BE904366A (fr) 1985-03-11 1986-03-07 Procede et installation de production d'azote sous pression.
AU54406/86A AU584174B2 (en) 1985-03-11 1986-03-07 Process and installation for producing nitrogen under pressure
ES552844A ES8800112A1 (es) 1985-03-11 1986-03-10 Procedimiento de produccion de nitrogeno a una presion llamada alta presion
NO860874A NO167167C (no) 1985-03-11 1986-03-10 Fremgangsmaate og anlegg til fremstilling av nitrogen ved et hoeyt trykk.
JP61050711A JPH0731003B2 (ja) 1985-03-11 1986-03-10 高圧下で窒素を製造する方法および装置
CA000503741A CA1298777C (fr) 1985-03-11 1986-03-11 Procede et installation de production d'azote sous pression

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR8503515A FR2578532B1 (fr) 1985-03-11 1985-03-11 Procede et installation de production d'azote

Publications (2)

Publication Number Publication Date
FR2578532A1 FR2578532A1 (fr) 1986-09-12
FR2578532B1 true FR2578532B1 (fr) 1990-05-04

Family

ID=9317050

Family Applications (1)

Application Number Title Priority Date Filing Date
FR8503515A Expired - Lifetime FR2578532B1 (fr) 1985-03-11 1985-03-11 Procede et installation de production d'azote

Country Status (11)

Country Link
US (1) US4717410A (fr)
JP (1) JPH0731003B2 (fr)
AU (1) AU584174B2 (fr)
BE (1) BE904366A (fr)
CA (1) CA1298777C (fr)
DE (1) DE3606967C2 (fr)
ES (1) ES8800112A1 (fr)
FR (1) FR2578532B1 (fr)
IT (1) IT1191980B (fr)
NL (1) NL8600582A (fr)
NO (1) NO167167C (fr)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4957524A (en) * 1989-05-15 1990-09-18 Union Carbide Corporation Air separation process with improved reboiler liquid cleaning circuit
US5058387A (en) * 1989-07-05 1991-10-22 The Boc Group, Inc. Process to ultrapurify liquid nitrogen imported as back-up for nitrogen generating plants
FR2665755B1 (fr) * 1990-08-07 1993-06-18 Air Liquide Appareil de production d'azote.
US5098457A (en) * 1991-01-22 1992-03-24 Union Carbide Industrial Gases Technology Corporation Method and apparatus for producing elevated pressure nitrogen
US5197296A (en) * 1992-01-21 1993-03-30 Praxair Technology, Inc. Cryogenic rectification system for producing elevated pressure product
FR2699992B1 (fr) * 1992-12-30 1995-02-10 Air Liquide Procédé et installation de production d'oxygène gazeux sous pression.
US5303556A (en) * 1993-01-21 1994-04-19 Praxair Technology, Inc. Single column cryogenic rectification system for producing nitrogen gas at elevated pressure and high purity
US5355682A (en) * 1993-09-15 1994-10-18 Air Products And Chemicals, Inc. Cryogenic air separation process producing elevated pressure nitrogen by pumped liquid nitrogen
US5355681A (en) * 1993-09-23 1994-10-18 Air Products And Chemicals, Inc. Air separation schemes for oxygen and nitrogen coproduction as gas and/or liquid products
US5402647A (en) * 1994-03-25 1995-04-04 Praxair Technology, Inc. Cryogenic rectification system for producing elevated pressure nitrogen
US5678425A (en) * 1996-06-07 1997-10-21 Air Products And Chemicals, Inc. Method and apparatus for producing liquid products from air in various proportions
US5682762A (en) * 1996-10-01 1997-11-04 Air Products And Chemicals, Inc. Process to produce high pressure nitrogen using a high pressure column and one or more lower pressure columns
DE19735154A1 (de) * 1996-10-30 1998-05-07 Linde Ag Verfahren und Vorrichtung zur Gewinnung von Druckstickstoff
US5740683A (en) * 1997-03-27 1998-04-21 Praxair Technology, Inc. Cryogenic rectification regenerator system
US5934104A (en) * 1998-06-02 1999-08-10 Air Products And Chemicals, Inc. Multiple column nitrogen generators with oxygen coproduction
DE19902255A1 (de) * 1999-01-21 2000-07-27 Linde Tech Gase Gmbh Verfahren und Vorrichtung zur Gewinnung von Druckstickstoff
US6330812B2 (en) 2000-03-02 2001-12-18 Robert Anthony Mostello Method and apparatus for producing nitrogen from air by cryogenic distillation
GB0119500D0 (en) * 2001-08-09 2001-10-03 Boc Group Inc Nitrogen generation
EP1300640A1 (fr) * 2001-10-04 2003-04-09 Linde Aktiengesellschaft Procédé et dispositif de production d'azote ultra-pur par séparation cryogénique d'air
US6499312B1 (en) 2001-12-04 2002-12-31 Praxair Technology, Inc. Cryogenic rectification system for producing high purity nitrogen
US6494060B1 (en) 2001-12-04 2002-12-17 Praxair Technology, Inc. Cryogenic rectification system for producing high purity nitrogen using high pressure turboexpansion
US6568208B1 (en) * 2002-05-03 2003-05-27 Air Products And Chemicals, Inc. System and method for introducing low pressure reflux to a high pressure column without a pump
US8991209B2 (en) 2010-12-13 2015-03-31 L'air Liquide Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Process and installation for producing high-pressure nitrogen
US9097459B2 (en) 2011-08-17 2015-08-04 Air Liquide Process & Construction, Inc. Production of high-pressure gaseous nitrogen
WO2018213507A1 (fr) 2017-05-16 2018-11-22 Ebert Terrence J Appareil et procédé de liquéfaction de gaz

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL72599C (fr) * 1949-04-23
DE1117616B (de) * 1960-10-14 1961-11-23 Linde Eismasch Ag Verfahren und Einrichtung zum Gewinnen besonders reiner Zerlegungsprodukte in Tieftemperaturgaszerlegungsanlagen
DE1136355B (de) * 1961-01-26 1962-09-13 Linde S Eismaschinen Ag Zweign Verfahren und Einrichtung zur Tieftemperaturrektifikation von Gasgemischen
GB1052146A (fr) * 1965-02-26 1966-12-21
DE1501722A1 (de) * 1966-01-13 1969-06-26 Linde Ag Verfahren zur Tieftemperatur-Luftzerlegung zur Erzeugung von hochverdichtetem gasfoermigem und/oder fluessigem Sauerstoff
US3760596A (en) * 1968-10-23 1973-09-25 M Lemberg Method of liberation of pure nitrogen and oxygen from air
DE2402246A1 (de) * 1974-01-18 1975-07-31 Linde Ag Verfahren zur gewinnung von sauerstoff mittlerer reinheit
DE3016317A1 (de) * 1980-04-28 1981-10-29 Messer Griesheim Gmbh, 6000 Frankfurt Verfahren zur gewinnung von fluessigen stickstoff
US4420317A (en) * 1981-10-29 1983-12-13 Nelson Stewart Process for recovering vaporized solvent which eliminates heat exchangers
US4453957A (en) * 1982-12-02 1984-06-12 Union Carbide Corporation Double column multiple condenser-reboiler high pressure nitrogen process
US4464188A (en) * 1983-09-27 1984-08-07 Air Products And Chemicals, Inc. Process and apparatus for the separation of air
US4543115A (en) * 1984-02-21 1985-09-24 Air Products And Chemicals, Inc. Dual feed air pressure nitrogen generator cycle
US4556404A (en) * 1984-09-19 1985-12-03 Air Products And Chemicals, Inc. Split-column extractive distillation

Also Published As

Publication number Publication date
JPH0731003B2 (ja) 1995-04-10
NO860874L (no) 1986-09-12
NO167167C (no) 1991-10-09
BE904366A (fr) 1986-09-08
DE3606967C2 (de) 2000-08-10
ES552844A0 (es) 1987-11-01
FR2578532A1 (fr) 1986-09-12
IT8619622A0 (it) 1986-03-04
IT1191980B (it) 1988-03-31
DE3606967A1 (de) 1986-09-11
JPS61252474A (ja) 1986-11-10
NO167167B (no) 1991-07-01
CA1298777C (fr) 1992-04-14
AU5440686A (en) 1986-09-18
ES8800112A1 (es) 1987-11-01
NL8600582A (nl) 1986-10-01
AU584174B2 (en) 1989-05-18
IT8619622A1 (it) 1987-09-04
US4717410A (en) 1988-01-05

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