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DK1188779T3 - Process for the preparation of a storage stable, rheologically active solution of urea urethane with broad compatibility - Google Patents

Process for the preparation of a storage stable, rheologically active solution of urea urethane with broad compatibility

Info

Publication number
DK1188779T3
DK1188779T3 DK01116384T DK01116384T DK1188779T3 DK 1188779 T3 DK1188779 T3 DK 1188779T3 DK 01116384 T DK01116384 T DK 01116384T DK 01116384 T DK01116384 T DK 01116384T DK 1188779 T3 DK1188779 T3 DK 1188779T3
Authority
DK
Denmark
Prior art keywords
preparation
storage stable
active solution
urea urethane
broad compatibility
Prior art date
Application number
DK01116384T
Other languages
Danish (da)
Inventor
Karlheinz Haubennestel
Ulrich Dr Orth
Axel Woocker
Heribert Holtkamp
Christoph Buchmann
Original Assignee
Byk Chemie Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Byk Chemie Gmbh filed Critical Byk Chemie Gmbh
Application granted granted Critical
Publication of DK1188779T3 publication Critical patent/DK1188779T3/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C08G18/3225—Polyamines
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G71/00—Macromolecular compounds obtained by reactions forming a ureide or urethane link, otherwise, than from isocyanate radicals in the main chain of the macromolecule
    • C08G71/04—Polyurethanes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/22—Catalysts containing metal compounds
    • C08G18/225—Catalysts containing metal compounds of alkali or alkaline earth metals
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/2805—Compounds having only one group containing active hydrogen
    • C08G18/2815—Monohydroxy compounds
    • C08G18/282—Alkanols, cycloalkanols or arylalkanols including terpenealcohols
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/2805—Compounds having only one group containing active hydrogen
    • C08G18/2815—Monohydroxy compounds
    • C08G18/282—Alkanols, cycloalkanols or arylalkanols including terpenealcohols
    • C08G18/2825—Alkanols, cycloalkanols or arylalkanols including terpenealcohols having at least 6 carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/2805—Compounds having only one group containing active hydrogen
    • C08G18/2815—Monohydroxy compounds
    • C08G18/283—Compounds containing ether groups, e.g. oxyalkylated monohydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/2805—Compounds having only one group containing active hydrogen
    • C08G18/2815—Monohydroxy compounds
    • C08G18/284—Compounds containing ester groups, e.g. oxyalkylated monocarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C08G18/3225—Polyamines
    • C08G18/3237—Polyamines aromatic
    • C08G18/324—Polyamines aromatic containing only one aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/04—Thixotropic paints

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Paints Or Removers (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicinal Preparation (AREA)

Abstract

The invention relates to a process for preparing a solution which comprises urea urethanes and is effective as a thixotropic agent, which involves reacting at least two structurally different monohydroxy compounds with an excess of toluylene diisocyanate to form monoisocyanate adducts, removing the unreacted portion of the toluylene diisocyanate, and reacting the resultant monoisocyanate adducts with diamines in an aprotic solvent in the presence of a lithium salt to form urea urethanes. The invention also relates to the use of the solution to receive thixotropic coating compositions.
DK01116384T 2000-08-16 2001-07-06 Process for the preparation of a storage stable, rheologically active solution of urea urethane with broad compatibility DK1188779T3 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE10039837A DE10039837C2 (en) 2000-08-16 2000-08-16 Process for the preparation of a storage-stable, rheologically effective urea urethane solution with broad compatibility

Publications (1)

Publication Number Publication Date
DK1188779T3 true DK1188779T3 (en) 2004-08-30

Family

ID=7652494

Family Applications (1)

Application Number Title Priority Date Filing Date
DK01116384T DK1188779T3 (en) 2000-08-16 2001-07-06 Process for the preparation of a storage stable, rheologically active solution of urea urethane with broad compatibility

Country Status (10)

Country Link
EP (1) EP1188779B1 (en)
JP (1) JP4942262B2 (en)
KR (1) KR100796040B1 (en)
CN (1) CN1204117C (en)
AT (1) ATE268790T1 (en)
CA (1) CA2352660C (en)
DE (2) DE10039837C2 (en)
DK (1) DK1188779T3 (en)
ES (1) ES2220631T3 (en)
TW (1) TWI226892B (en)

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KR100482427B1 (en) * 2003-12-19 2005-04-14 박장원 Crosslinked foam which has inner-cavity structure, and process of forming thereof
US7220300B2 (en) * 2004-12-04 2007-05-22 Xerox Corporation Phase change inks containing bis(urea-urethane) compounds
US7144450B2 (en) * 2004-12-04 2006-12-05 Xerox Corporation Phase change inks containing trans-1,2-cyclohexane bis(urea-urethane) compounds
US7560587B2 (en) * 2004-12-04 2009-07-14 Xerox Corporation Bis[urea-urethane] compounds
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DE102008029858A1 (en) * 2008-04-23 2009-10-29 Byk-Chemie Gmbh Stable dispersions of inorganic nanoparticles
DE202008008419U1 (en) 2008-04-23 2009-06-04 Byk-Chemie Gmbh Stable dispersions of inorganic nanoparticles
DE102008038488A1 (en) 2008-08-20 2010-02-25 Henkel Ag & Co. Kgaa Moisture-curing waterproof coating
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DE102009021912A1 (en) 2009-05-19 2010-12-02 Byk-Chemie Gmbh From oxetane-based macromonomers available polymers, processes for their preparation and their use as additives in coating materials and plastics
DE102009021913A1 (en) 2009-05-19 2010-12-02 Byk-Chemie Gmbh Terminal unsaturated, oxetane-based macromonomers and process for their preparation
EP2292675A1 (en) 2009-09-08 2011-03-09 BYK-Chemie GmbH Polyureas as a rheology controlling agents.
JP5436698B2 (en) 2010-01-28 2014-03-05 ビイク−ヒエミー ゲゼルシャフト ミツト ベシユレンクテル ハフツング Coating preparations containing urea and amide components
WO2012113739A1 (en) * 2011-02-22 2012-08-30 Basf Se Rheological agent for radiation-curable coating materials
EP2644633A1 (en) * 2012-03-29 2013-10-02 Huntsman International Llc Isocyanate-based prepolymer
EP2644632A1 (en) * 2012-03-29 2013-10-02 Huntsman International Llc Isocyanate-based prepolymer
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CN106232698B (en) 2014-04-15 2018-09-18 比克化学股份有限公司 Composition for rheology control
US9796860B2 (en) 2014-04-15 2017-10-24 Byk-Chemie Gmbh Storage-stable urea preparations which are suitable as rheology control agents
JP6249195B2 (en) 2014-04-15 2017-12-20 ベーイプシロンカー−シェミー ゲーエムベーハーＢＹＫ−Ｃｈｅｍｉｅ ＧｍｂＨ Rheology control agent containing a combination of agents
KR102555666B1 (en) * 2015-07-27 2023-07-18 비와이케이-케미 게엠베하 Urea urethane for rheology control
KR101835720B1 (en) 2015-11-30 2018-03-08 케이에스케미칼 주식회사 Manufacturing method of thixotropic agent with shear thinning
JP6975792B2 (en) 2017-01-30 2021-12-01 ベーイプシロンカー ヘミー ゲゼルシャフト ミット ベシュレンクター ハフトゥング Urea group-and / or urethane group-containing amides as rheology control agents and in rheology control agents, their production and use thereof.
EP3459985B1 (en) * 2017-09-22 2020-06-17 Cliq Swisstech Gmbh Urea urethanes (ii)
EP3609941B1 (en) 2017-04-13 2021-06-30 BYK-Chemie GmbH Polymer suitable as thickener
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ES2904482T3 (en) 2017-12-21 2022-04-05 Byk Chemie Gmbh Urea group containing anti-buckling rheology control agents
US20200308106A1 (en) 2017-12-21 2020-10-01 Byk-Chemie Gmbh Urea and urethane group containing anti-settling rheology control additive
KR102071950B1 (en) 2017-12-28 2020-01-31 낙우산업(주) Nanoclay to improve thickening and thixotropic behavior in natural paints and the preparing process the same
CN108070066B (en) * 2017-12-29 2020-11-27 陈鹏 Paint and ink anti-settling agent and preparation method thereof
KR102645600B1 (en) * 2018-03-27 2024-03-08 어드밴식스 레진즈 앤드 케미컬즈 엘엘씨 Thixotropic rheology modifier composition
JP7332251B2 (en) * 2018-06-28 2023-08-23 ホヤ レンズ タイランド リミテッド Polymerizable composition for optical members
JP7196316B2 (en) 2019-01-04 2022-12-26 ベーイプシロンカー ヘミー ゲゼルシャフト ミット ベシュレンクター ハフトゥング Urea group-containing rheology control additive
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Also Published As

Publication number Publication date
DE10039837A1 (en) 2002-03-07
CA2352660A1 (en) 2002-02-16
JP2002105042A (en) 2002-04-10
ATE268790T1 (en) 2004-06-15
CA2352660C (en) 2008-10-21
EP1188779A1 (en) 2002-03-20
DE10039837C2 (en) 2003-03-20
DE50102521D1 (en) 2004-07-15
CN1338453A (en) 2002-03-06
KR100796040B1 (en) 2008-01-21
CN1204117C (en) 2005-06-01
EP1188779B1 (en) 2004-06-09
TWI226892B (en) 2005-01-21
KR20020014680A (en) 2002-02-25
JP4942262B2 (en) 2012-05-30
ES2220631T3 (en) 2004-12-16

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