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DE16882443T1 - System und verfahren für flexibles dichtmittel mit dichtemodifizierungsmittel - Google Patents

System und verfahren für flexibles dichtmittel mit dichtemodifizierungsmittel Download PDF

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Publication number
DE16882443T1
DE16882443T1 DE16882443.1T DE16882443T DE16882443T1 DE 16882443 T1 DE16882443 T1 DE 16882443T1 DE 16882443 T DE16882443 T DE 16882443T DE 16882443 T1 DE16882443 T1 DE 16882443T1
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Prior art keywords
sealant composition
volume
composition according
cured
additives
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Sandra KOCUREK
Devin KOCUREK
Jonathan PERRIELLO
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Polymer Adhesive Sealant Systems Inc
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Polymer Adhesive Sealant Systems Inc
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Publication of DE16882443T1 publication Critical patent/DE16882443T1/de
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/32—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof from compositions containing microballoons, e.g. syntactic foams
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/22—After-treatment of expandable particles; Forming foamed products
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/0066—Use of inorganic compounding ingredients
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/04—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent
    • C08J9/06—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent by a chemical blowing agent
    • C08J9/10—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent by a chemical blowing agent developing nitrogen, the blowing agent being a compound containing a nitrogen-to-nitrogen bond
    • C08J9/101—Agents modifying the decomposition temperature
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/16—Making expandable particles
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/28—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/30—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by mixing gases into liquid compositions or plastisols, e.g. frothing with air
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K7/00—Use of ingredients characterised by shape
    • C08K7/22—Expanded, porous or hollow particles
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00—Use of pretreated ingredients
    • C08K9/02—Ingredients treated with inorganic substances
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J113/00—Adhesives based on rubbers containing carboxyl groups
    • C09J113/02—Latex
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
    • C09J133/04—Homopolymers or copolymers of esters
    • C09J133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
    • C09J133/08—Homopolymers or copolymers of acrylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
    • C09J133/18—Homopolymers or copolymers of nitriles
    • C09J133/20—Homopolymers or copolymers of acrylonitrile
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J9/00—Adhesives characterised by their physical nature or the effects produced, e.g. glue sticks
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2203/00—Foams characterized by the expanding agent
    • C08J2203/04—N2 releasing, ex azodicarbonamide or nitroso compound
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2203/00—Foams characterized by the expanding agent
    • C08J2203/22—Expandable microspheres, e.g. Expancel®
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2205/00—Foams characterised by their properties
    • C08J2205/04—Foams characterised by their properties characterised by the foam pores
    • C08J2205/052—Closed cells, i.e. more than 50% of the pores are closed
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2207/00—Foams characterised by their intended use
    • C08J2207/02—Adhesive
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2313/00—Characterised by the use of rubbers containing carboxyl groups
    • C08J2313/02—Latex
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2333/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers
    • C08J2333/04—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers esters
    • C08J2333/06—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers esters of esters containing only carbon, hydrogen, and oxygen, the oxygen atom being present only as part of the carboxyl radical
    • C08J2333/08—Homopolymers or copolymers of acrylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2333/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers
    • C08J2333/18—Homopolymers or copolymers of nitriles
    • C08J2333/20—Homopolymers or copolymers of acrylonitrile
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/24—Acids; Salts thereof
    • C08K3/26—Carbonates; Bicarbonates
    • C08K2003/265—Calcium, strontium or barium carbonate
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00—Use of pretreated ingredients
    • C08K9/10—Encapsulated ingredients

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Sealing Material Composition (AREA)
  • Paints Or Removers (AREA)

Abstract

Eine Dichtmittel-Zusammensetzung umfassend:a. bis zu etwa 80 Vol.-% einer Polymerdispersion;b. etwa 20 Vol.-% bis etwa 65 Vol.-% eines Dichtemodifizierungsmittels; undc. etwa 0 Vol.-% bis etwa 10 Vol.-% eines oder mehrerer Additive.

Claims (18)

  1. Eine Dichtmittel-Zusammensetzung umfassend: a. bis zu etwa 80 Vol.-% einer Polymerdispersion; b. etwa 20 Vol.-% bis etwa 65 Vol.-% eines Dichtemodifizierungsmittels; und c. etwa 0 Vol.-% bis etwa 10 Vol.-% eines oder mehrerer Additive.
  2. Die Dichtmittel-Zusammensetzung nach Anspruch 1, wobei das Dichtemodifizierungsmittel Mikrosphären enthält, umfassend eine Außenschale, die ein Gas einschließt.
  3. Die Dichtmittel-Zusammensetzung nach Anspruch 2, wobei die Außenschale ein thermoplastisches Polymer ist, ausgewählt aus der Gruppe, bestehend aus Acrylonitril, Acrylonitril-Copolymere mit anderen Acrylverbindungen, Methylmethacrylat, Vinylidenchlorid und Kombinationen davon.
  4. Die Dichtmittel-Zusammensetzung nach Anspruch 2, wobei die Außenschale mit Calciumcarbonat beschichtet ist.
  5. Die Dichtmittel-Zusammensetzung nach Anspruch 2, wobei das Gas aus der Gruppe ausgewählt ist, bestehend aus Isopentan, Isobuten, und anderen Gasen mit einem Siedepunkt unter einem Erweichungspunkt der Außenschale.
  6. Die Dichtmittel-Zusammensetzung nach Anspruch 2, wobei die Mikrosphären eine Partikelgröße von etwa 15 µm bis etwa 200 µm besitzen.
  7. Die Dichtmittel-Zusammensetzung nach Anspruch 2, wobei die Mikrosphären eine Dichte von etwa 6,5 kg/m3 bis etwa 100 kg/m3 besitzen.
  8. Die Dichtmittel-Zusammensetzung nach Anspruch 1, wobei ein ausgehärteter Zustand der Dichtmittel-Zusammensetzung ein erstes ausgehärtetes Volumen besitzt und in der Lage ist, von dem ersten ausgehärteten Volumen zu einem zweiten ausgehärteten Volumen, ohne überzustehen, komprimiert zu werden, wenn ein Druck auf den ausgehärteten Zustand der Dichtmittel-Zusammensetzung ausgeübt wird.
  9. Die Dichtmittel-Zusammensetzung nach Anspruch 8, wobei das zweite ausgehärtete Volumen von etwa 50% bis etwa 95% des ersten ausgehärteten Volumens reicht.
  10. Die Dichtmittel-Zusammensetzung nach Anspruch 8, wobei der ausgehärtete Zustand der Dichtmittel-Zusammensetzung konfiguriert wird, um das erste ausgehärtete Volumen wieder einzunehmen, wenn der Druck entfernt wird.
  11. Die Dichtmittel-Zusammensetzung nach Anspruch 1, wobei ein flüssiger Zustand der Dichtmittel-Zusammensetzung ein erstes flüssiges Volumen besitzt und in der Lage ist, von dem ersten flüssigen Volumen zu einem zweiten flüssigen Volumen komprimiert zu werden.
  12. Die Dichtmittel-Zusammensetzung nach Anspruch 11, wobei das zweite flüssige Volumen von etwa 15% bis etwa 45% des ersten flüssigen Volumens reicht.
  13. Die Dichtmittel-Zusammensetzung nach Anspruch 1, wobei ein oder mehrere Additive aus der Gruppe ausgewählt sind, bestehend aus Glimmer, Aluminiumtrihydrat (ATH), Magnesiumhydroxid, expandierbarem Graphit, Ammoniumpolyphosphat, Ammoniumphosphat, Harnstoff, Natriumsilikat und Kombinationen davon.
  14. Ein Verfahren zur Herstellung einer Dichtmittel-Zusammensetzung, wobei das Verfahren umfasst: Mischen einer Flüssigkeit und Additive, wobei die Additive etwa 0 Vol.-% bis etwa 10 Vol.-% der Dichtmittel-Zusammensetzung umfassen; Dosieren einer Polymerdispersion in die Mischung aus Flüssigkeit und Additiven, wobei die Polymerdispersion bis zu 80 Vol.-% der Dichtmittel-Zusammensetzung umfasst; und Dosieren eines Dichtemodifizierungsmittels, wobei das Dichtemodifizierungsmittel etwa 20 Vol.-% bis etwa 65 Vol.-% der Dichtmittel-Zusammensetzung umfasst.
  15. Das Verfahren nach Anspruch 14, außerdem umfassend: Zugabe trockener Materialien; Benetzen der trockenen Materialien während des Mischens der Dichtmittel-Zusammensetzung; Zugabe eines Verdickungsmittels und pH-Modifikators zu der Dichtmittel-Zusammensetzung; und Entgasen der Dichtmittel-Zusammensetzung.
  16. Das Verfahren nach Anspruch 14, außerdem umfassend Filtration der Dichtmittel-Zusammensetzung zur Verwendung in einer Sprühanwendung, wobei die Filtration der Dichtmittel-Zusammensetzung eines von: (a) Ziehen der Dichtmittel-Zusammensetzung durch ein Sieb mit einer Vakuumpumpe und (b) kontinuierlicher Durchlauf der Dichtmittel-Zusammensetzung durch ein Sieb umfasst.
  17. Das Verfahren nach Anspruch 14, wobei das Dichtemodifizierungsmittel Mikrosphären enthält, umfassend eine Außenschale, die ein Gas einschließt.
  18. Das Verfahren nach Anspruch 14, wobei ein oder mehrere Additive aus der Gruppe ausgewählt sind, bestehend aus Glimmer, Aluminiumtrihydrat (ATH), Magnesiumhydroxid, expandierbarem Graphit, Ammoniumpolyphosphat, Ammoniumphosphat, Harnstoff, Natriumsilikat und Kombinationen davon.
DE16882443.1T 2015-12-31 2016-12-22 System und verfahren für flexibles dichtmittel mit dichtemodifizierungsmittel Pending DE16882443T1 (de)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US201562273970P 2015-12-31 2015-12-31
US201562273970P 2015-12-31
EP16882443.1A EP3397677A4 (de) 2015-12-31 2016-12-22 System und verfahren für flexibles dichtmittel mit dichtemodifizierungsmittel
PCT/US2016/068388 WO2017117013A1 (en) 2015-12-31 2016-12-22 System and method for flexible sealant with density modifier

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DE16882443T1 true DE16882443T1 (de) 2019-05-02

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US (4) US11098174B2 (de)
EP (1) EP3397677A4 (de)
CN (3) CN118406280A (de)
CA (1) CA3010012A1 (de)
DE (1) DE16882443T1 (de)
WO (1) WO2017117013A1 (de)

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CN118406280A (zh) 2024-07-30
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CA3010012A1 (en) 2017-07-06
CN108770358A (zh) 2018-11-06
US20170190864A1 (en) 2017-07-06
EP3397677A1 (de) 2018-11-07
US20200255617A1 (en) 2020-08-13
CN118515904A (zh) 2024-08-20
US20230082565A1 (en) 2023-03-16
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WO2017117013A1 (en) 2017-07-06
US20200255616A1 (en) 2020-08-13

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