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CN214232844U - Extraction device for extracting grape resveratrol by ultrasonic microbubble - Google Patents

Extraction device for extracting grape resveratrol by ultrasonic microbubble Download PDF

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Publication number
CN214232844U
CN214232844U CN202021206553.XU CN202021206553U CN214232844U CN 214232844 U CN214232844 U CN 214232844U CN 202021206553 U CN202021206553 U CN 202021206553U CN 214232844 U CN214232844 U CN 214232844U
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extraction
extraction tank
tank
extracting
ultrasonic
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CN202021206553.XU
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段斌
豆孝明
胡奇林
杨强
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Ningxia Grape And Wine Development Research Institute Co ltd
Ningxia Huida Yangguang Ecological Chateau Co ltd
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Ningxia Grape And Wine Development Research Institute Co ltd
Ningxia Huida Yangguang Ecological Chateau Co ltd
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Abstract

The utility model discloses an extraction device for extracting grape resveratrol by ultrasonic microbubbles, which comprises an extraction tank, wherein the lower end of the extraction tank is connected with a plurality of support legs, the lower ends of the support legs are fixedly connected with a support, the upper end of the extraction tank is provided with a skin residue inlet, the extraction tank is connected with an extractant input mechanism, a convex ultrasonic vibration plate is arranged in the extraction tank, the extraction tank is connected with a microbubble mechanism, the lower end of the extraction tank is provided with a slurry outlet, a blowoff valve is arranged on the slurry outlet, the lower end of the extraction tank is connected with an extract outlet valve, the extract outlet valve is connected with a high-shear homogeneous emulsifying machine, the high-shear homogeneous emulsifying machine is connected with the extraction tank through a return pipe, the high-shear homogeneous emulsifying machine is also connected with an extract outlet, and during the working process of the adopted ultrasonic microbubble equipment, the extraction solution system has continuous disturbance effect and is compared with the traditional motor-driven stirring blade, the material exchange efficiency is higher, and secondary pollution and damage to effective components can not be caused.

Description

Extraction device for extracting grape resveratrol by ultrasonic microbubble
Technical Field
The utility model relates to a resveratrol makes relevant field, specifically is an extraction device that grape resveratrol was drawed to supersound microbubble.
Background
The conventional resveratrol extraction mainly comprises a solvent extraction method, a microwave extraction method, supercritical CO extraction, enzymatic extraction, ultrasonic-assisted extraction and the like, wherein the solvent extraction method has the advantages of high efficiency, solvent recovery and the like and is widely applied, but the conventional immersion solvent extraction method has the advantages of low extraction efficiency, small extraction amount, solvent residue problem and long period, and is the main problem faced by the conventional solvent extraction method.
In order to further improve the ultrasonic extraction efficiency, grape skin residues, a solvent and the like need to be stirred, mechanical stirring is adopted, and the change of the ultrasonic extraction efficiency is not obvious after verification, because the ultrasonic effect is inhibited by the liquid turbulence state caused by the mechanical stirring, if an air bubbling technology can be applied to the ultrasonic extraction device, the skin residues and the solvent are disturbed by air, secondary pollution is avoided, and the effective components are not damaged, so that an extraction device for extracting the resveratrol from the grape by using ultrasonic microbubbles is urgently needed.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide an extraction device of grape resveratrol is drawed to supersound microbubble to solve the problem that provides in the above-mentioned background art.
In order to achieve the above object, the utility model provides a following technical scheme:
the utility model provides an extraction device that grape resveratrol was drawed to supersound microbubble, is including drawing the jar, the lower extreme that draws the jar is connected with a plurality of landing legs, and is a plurality of the lower extreme of landing leg all with support fixed connection, it is provided with the skin sediment import to draw jar upper end, it is connected with extractant input mechanism to draw jar, it shakes the board to be provided with protruding type ultrasonic wave in the jar to draw, it shakes with microbubble mechanism and is connected to draw the jar, the lower extreme that draws the jar is provided with the thick liquid export, be provided with the blowoff valve in the thick liquid export, it is connected with the extract outlet valve to draw jar lower extreme, the extract outlet valve is connected with high shear homogenizing emulsifying machine, high shear homogenizing emulsifying machine passes through the back flow and is connected with the extraction jar, high shear homogenizing emulsifying machine still is connected with the extract liquid outlet.
As a further aspect of the present invention: the extraction agent input mechanism comprises an extraction agent storage tank, the extraction agent storage tank is connected with an extraction agent liquid inlet pump, and an extraction agent inlet is formed in the extraction tank.
As a further aspect of the present invention: the microbubble mechanism includes the air compressor machine, the air compressor machine is connected with the admission valve, the admission valve is connected with the manometer, the manometer with draw the jar and be connected, still include a plurality of from rotating spray head, it is a plurality of from rotating spray head sets up in drawing the jar, and is a plurality of from rotating spray head all is connected with the manometer through the connecting pipe, it is provided with the grid board in the jar to draw.
As a further aspect of the present invention: the number of the self-rotating type spray heads is five.
As a further aspect of the present invention: the extraction tank is connected with the extraction agent recovery mechanism, the extraction agent recovery mechanism comprises a gas-liquid separator, an evacuation port is arranged at the upper end of the gas-liquid separator, and the lower end of the gas-liquid separator is connected with the extraction agent recovery tank.
Compared with the prior art, the beneficial effects of the utility model are that: the extraction tank is connected with an extractant input mechanism, the extraction tank is connected with a micro-bubble mechanism, the extractant input mechanism comprises an extractant storage tank, the extractant storage tank is connected with an extractant liquid inlet pump, the extractant liquid inlet pump provides power for the extractant to enter the extraction tank, an extractant inlet is arranged on the extraction tank, a liquid inlet valve controls the entering of the extractant, a filter filters impurities in the extractant, a flow meter controls the amount of the extractant in the extraction tank, the micro-bubble mechanism comprises an air compressor, the air compressor is connected with an air inlet valve, the air inlet valve is connected with a pressure gauge, the micro-bubble mechanism further comprises a plurality of self-rotating nozzles, the plurality of self-rotating nozzles are all connected with the pressure gauge through connecting pipes, a grating plate is arranged in the extraction tank and separates skin slag raw materials above the plurality of self-rotating nozzles to facilitate micro-bubble operation of the self-rotating nozzles, the air compressor extracts air from the outside and is sprayed out by the plurality of self-rotating nozzles through the connecting pipes, carry out the microbubble operation to the skin sediment raw materials, make the efficiency of extraction promote, it retrieves the mechanism with the extractant to extract the jar and is connected, the tail gas that obtains after the extraction gets into vapour and liquid separator, gas is discharged by the evacuation mouth, liquid gets into extractant recovery tank, the extractant that obtains can recycle, resources are saved, the extraction device that grape resveratrol was drawed to the supersound microbubble in this application, in the supersound microbubble equipment course of operation of adoption, have continuous disturbance effect to drawing the solution system, compare traditional motor drive's stirring vane, material exchange efficiency is higher, can not bring secondary pollution, and to the destruction of active ingredient.
Drawings
Fig. 1 is a schematic structural diagram of an extraction device for extracting resveratrol from grape by using ultrasonic microbubbles.
In the figure: 1-extraction tank, 2-convex ultrasonic vibration plate, 3-skin residue inlet, 4-support leg, 5-slurry outlet, 6-blowdown valve, 7-extract outlet valve, 8-high-shear homogenizing emulsifying machine, 9-extract outlet, 10-support, 11-gas-liquid separator, 12-evacuation port, 13-extractant recovery tank, 14-grating plate, 15-self-rotating spray head, 16-extractant inlet, 17-extractant storage tank, 18-extractant liquid inlet pump, 19-liquid inlet valve, 20-filter, 21-flowmeter, 22-air compressor, 23-air inlet valve, 24-pressure gauge and 25-return pipe.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Example 1
Referring to fig. 1, in an embodiment of the present invention, an extraction apparatus for extracting resveratrol from grape by using ultrasonic microbubbles includes an extraction tank 1, the extraction tank 1 is used for carrying out the whole reaction, the lower end of the extraction tank 1 is connected to a plurality of support legs 4, the lower ends of the plurality of support legs 4 are all fixedly connected to a support 10, the extraction tank 1 is supported by the cooperation of the support legs 4 and the support 10, the upper end of the extraction tank 1 is provided with a skin residue inlet 3, raw materials are input through the skin residue inlet 3, the extraction tank 1 is connected to an extractant input mechanism, the extractant input mechanism inputs extractant into the extraction tank 1, a convex ultrasonic vibration plate 2 is disposed in the extraction tank 1, the convex ultrasonic vibration plate 2 sends out ultrasonic waves into the extraction tank 1 for extraction, the extraction tank 1 is connected to a microbubble mechanism, the microbubble mechanism sends out bubbles into the extraction tank 1 to cooperate with the convex ultrasonic vibration plate 2, so that the extraction efficiency is improved, the lower end of the extraction tank 1 is provided with a slurry outlet 5, the slurry outlet 5 is provided with a blowoff valve 6, extracted residues are discharged through the blowoff valve 6, the lower end of the extraction tank 1 is connected with an extract outlet valve 7, the inlet and outlet of an obtained extraction product are controlled through the extract outlet valve 7, the extract outlet valve 7 is connected with a high-shear homogenizing emulsifying machine 8, the high-shear homogenizing emulsifying machine 8 is connected with the extraction tank 1 through a return pipe 25, the high-shear homogenizing emulsifying machine 8 is also connected with an extract outlet 9, the finally obtained extraction product is output through the extract outlet 9, the extract is processed by the extract outlet valve 7 through the high-shear homogenizing emulsifying machine 8, the initially homogenized and emulsified slurry is conveyed into the extraction tank 1 through the return pipe 25, and the slurry enters a next process through the extract outlet 9 after being fully extracted.
The specific form of the extracting agent input mechanism is not limited, in this embodiment, preferably, the extracting agent input mechanism includes an extracting agent storage tank 17, the extracting agent storage tank 17 is connected with an extracting agent liquid inlet pump 18, the extracting agent liquid inlet pump 18 provides power for the extracting agent to enter the extracting tank 1, the extracting agent liquid inlet pump 18 is sequentially connected with a liquid inlet valve 19, a filter 20 and a flow meter 21, the extracting tank 1 is provided with an extracting agent inlet 16, the liquid inlet valve 19 controls the entering of the extracting agent, the filter 20 filters impurities in the extracting agent, and the flow meter 21 controls the amount of the extracting agent in the extracting tank 1.
The concrete form of microbubble mechanism does not restrict, in this embodiment, it is preferred that the microbubble mechanism includes air compressor 22, air compressor 22 is connected with admission valve 23, admission valve 23 is connected with manometer 24, manometer 24 is connected with extraction jar 1, air compressor 22 draws the air input to extraction jar 1 from the external world, rethread manometer 24 monitors the pressure in the extraction jar 1 to the extraction jar 1 size of pressure, so that extraction jar 1 is in suitable operating pressure, still include a plurality of from rotating spray head 15, a plurality of from rotating spray head 15 sets up in extraction jar 1, a plurality of from rotating spray head 15 all is connected with manometer 24 through the connecting pipe, in this embodiment, it is preferred that the quantity of from rotating spray head 15 is five, be provided with grid plate 14 in the extraction jar 1, grid plate 14 separates the skin sediment raw materials in the top of a plurality of from rotating spray head 15, be convenient for carry out the microbubble operation to it, air compressor machine 22 is from external extraction air, is sprayed by a plurality of from rotating spray head 15 again through the connecting pipe, carries out the microbubble operation to the skin sediment raw materials for the efficiency of extraction can promote.
Each component adopted in this embodiment all adopts the stainless steel after the processing, has guaranteed the required cleanliness factor such as follow-up vacuum drying that carries on.
The working principle of the embodiment is as follows: the extraction tank 1 is connected with an extractant input mechanism, the extraction tank 1 is connected with a micro-bubble mechanism, the extractant input mechanism comprises an extractant storage tank 17, the extractant storage tank 17 is connected with an extractant liquid inlet pump 18, the extractant liquid inlet pump 18 provides power for the extractant to enter the extraction tank 1, an extractant inlet 16 is arranged on the extraction tank 1, a liquid inlet valve 19 controls the entering of the extractant, a filter 20 filters impurities in the extractant, a flowmeter 21 controls the amount of the extractant in the extraction tank 1, the micro-bubble mechanism comprises an air compressor 22, the air compressor 22 is connected with an air inlet valve 23, the air inlet valve 23 is connected with a pressure gauge 24, the extraction tank further comprises a plurality of self-rotating nozzles 15, the plurality of self-rotating nozzles 15 are all connected with the pressure gauge 24 through connecting pipes, a grating plate 14 is arranged in the extraction tank 1, the grating plate 14 blocks the skin residue raw material above the plurality of self-rotating nozzles 15, be convenient for carry out the microbubble operation to it, air compressor machine 22 is from external extraction air, is sprayed by a plurality of from rotating spray head 15 again through the connecting pipe, carries out the microbubble operation to the skin sediment raw materials for the efficiency of extraction can promote.
Example 2
In order to save resources and respond to the green call, the present embodiment makes the following improvements on the basis of embodiment 1, and the improvements are: the extraction tank 1 is connected with an extractant recovery mechanism, the concrete form of the extractant recovery mechanism is not limited, in this embodiment, preferably, the extractant recovery mechanism includes a gas-liquid separator 11, an evacuation port 12 is arranged at the upper end of the gas-liquid separator 11, the lower end of the gas-liquid separator 11 is connected with an extractant recovery tank 13, tail gas obtained after extraction enters the gas-liquid separator 11, gas is discharged from the evacuation port 12, liquid enters the extractant recovery tank 13, and the obtained extractant can be recycled, so that resources are saved.
The working principle of the embodiment is as follows: the extraction tank 1 is connected with an extractant recovery mechanism, tail gas obtained after extraction enters a gas-liquid separator 11, gas is discharged from a vent 12, liquid enters an extractant recovery tank 13, and the obtained extractant can be recycled, so that resources are saved.
It is obvious to a person skilled in the art that the invention is not restricted to details of the above-described exemplary embodiments, but that it can be implemented in other specific forms without departing from the spirit or essential characteristics of the invention. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.

Claims (5)

1. The extraction device for extracting the grape resveratrol by using the ultrasonic microbubbles is characterized by comprising an extraction tank (1), wherein the lower end of the extraction tank (1) is connected with a plurality of support legs (4), the lower ends of the support legs (4) are fixedly connected with a support (10), a skin residue inlet (3) is formed in the upper end of the extraction tank (1), the extraction tank (1) is connected with an extracting agent input mechanism, a convex ultrasonic vibration plate (2) is arranged in the extraction tank (1), the extraction tank (1) is connected with a microbubble mechanism, a slurry outlet (5) is formed in the lower end of the extraction tank (1), a blowoff valve (6) is arranged on the slurry outlet (5), the lower end of the extraction tank (1) is connected with an extraction liquid outlet valve (7), the extraction liquid outlet valve (7) is connected with a high-shear homogenizing emulsifying machine (8), the high-shear homogenizing emulsifying machine (8) is connected with the extraction tank (1) through a return pipe (25), the high-shear homogenizing and emulsifying machine (8) is also connected with an extract liquor outlet (9).
2. The device for extracting resveratrol from grapes through ultrasonic microbubble extraction according to claim 1, wherein the extracting agent input mechanism comprises an extracting agent storage tank (17), the extracting agent storage tank (17) is connected with an extracting agent liquid inlet pump (18), and an extracting agent inlet (16) is formed in the extracting tank (1).
3. The device for extracting resveratrol from grapes according to claim 1, wherein the microbubble mechanism comprises an air compressor (22), the air compressor (22) is connected with an air inlet valve (23), the air inlet valve (23) is connected with a pressure gauge (24), the pressure gauge (24) is connected with an extraction tank (1), the device further comprises a plurality of self-rotating nozzles (15), the plurality of self-rotating nozzles (15) are arranged in the extraction tank (1), the plurality of self-rotating nozzles (15) are connected with the pressure gauge (24) through connecting pipes, and a grating plate (14) is arranged in the extraction tank (1).
4. The extraction device for extracting resveratrol from grapes through ultrasonic microbubbles according to claim 3, wherein the number of the spin nozzles (15) is five.
5. The extraction device for extracting grape resveratrol through ultrasonic microvesicles according to claim 1, wherein the extraction tank (1) is connected with an extractant recovery mechanism, the extractant recovery mechanism comprises a gas-liquid separator (11), an evacuation port (12) is arranged at the upper end of the gas-liquid separator (11), and the lower end of the gas-liquid separator (11) is connected with an extractant recovery tank (13).
CN202021206553.XU 2020-06-28 2020-06-28 Extraction device for extracting grape resveratrol by ultrasonic microbubble Active CN214232844U (en)

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Application Number Priority Date Filing Date Title
CN202021206553.XU CN214232844U (en) 2020-06-28 2020-06-28 Extraction device for extracting grape resveratrol by ultrasonic microbubble

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202021206553.XU CN214232844U (en) 2020-06-28 2020-06-28 Extraction device for extracting grape resveratrol by ultrasonic microbubble

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CN214232844U true CN214232844U (en) 2021-09-21

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN118179085A (en) * 2024-05-14 2024-06-14 广州伽能生物科技有限公司 Medicinal material draws concentrator

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN118179085A (en) * 2024-05-14 2024-06-14 广州伽能生物科技有限公司 Medicinal material draws concentrator
CN118179085B (en) * 2024-05-14 2024-08-13 广州伽能生物科技有限公司 Medicinal material extraction and concentration method

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