CN111297759B - Oil-control astringent composition and preparation method thereof and cosmetic - Google Patents
Oil-control astringent composition and preparation method thereof and cosmetic Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/66—Enzymes
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9711—Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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Abstract
The invention relates to the technical field of cosmetics, in particular to an oil-control astringent composition, a preparation method thereof and a cosmetic. The oil-control astringent composition comprises, by weight, 1-10 parts of brown algae extract, 2-8 parts of aloe protease, 1-10 parts of sage extract, 3-20 parts of oriental cherry extract and 1-5 parts of tea polyphenol extract. The composition is compounded by the brown algae extract and the plant extract, so that sebaceous gland secretion is effectively controlled, oil production is reduced, pores are shrunk, the effect of long-term oil control and convergence is realized, the skin state is improved, and the composition has a synergistic effect.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to an oil-control astringent composition, a preparation method thereof and a cosmetic.
Background
Oily skin is a global problem, more common in men and adolescents, and particularly prominent among the 15-39 year old population, and is rooted in the exuberant secretion of sebum, which sebaceous glands can secrete sebum through ducts into hair follicles, where it drains through pores to the skin surface. Sebum is an oily semi-fluid mixture containing a variety of lipids. The main components are triglyceride, fatty acid, phospholipid, lipidated cholesterol, etc. Sebum forms a film, which is one of the components of the skin's chemical barrier and plays an important physiological role in moisturizing, etc. However, the excessive proliferation of the oil and fat also creates a good living environment for some bacteria, fungi, parasites and the like, and the excessive proliferation of the bacteria, fungi, parasites and the like can cause a series of skin problems, such as pore blockage, blackheads, large pores, unbalanced water and oil, dark yellow appearance, rough skin, easy ultraviolet absorption and other skin problems, and influence on the permeability of the skin. And the oil is too much for a long time, so that dust and dirt are easily adhered to the skin, skin infection is caused, and acne is formed. Therefore, excessive secretion of sebaceous glands is controlled, oil production is reduced, and development of a cosmetic with effects of controlling oil, astringing and relieving is needed.
At present, most of the oil control related cosmetics on the market aim at inhibiting sebum secretion, and although certain instant effect is achieved, the problem is not solved fundamentally, so that the long-acting and lasting effect cannot be achieved.
For example, patent publication No. CN110179703A discloses an oil-controlling and water-replenishing composition and its application, including an extract of pinus longifolia, an extract of ulmus pumila, an extract of oenothera biennis, an extract of pueraria mirifica, an extract of rubus idaeus, an extract of salix alba, an extract of hippophae rhamnoides, and an extract of commiphora mukul resin. The composition has the effects of controlling oil and replenishing water, mainly starts from the aspect of maintaining water-oil balance, does not solve the problem fundamentally, and does not achieve the long-acting and lasting effect.
Patent publication No. CN106361645A discloses a biological protease acne-removing essence milk. The invention comprises acrylic acid copolymer sodium, protease, butanediol, nicotinamide, lecithin, salicylic acid, silver oxide and a traditional Chinese medicine extract, achieves the purpose of reducing oil secretion by adding the salicylic acid, thereby avoiding excessive secretion of sebaceous glands due to abnormal inflammation, but the method adopts the active substance salicylic acid which belongs to a fruit acid type raw material and has certain skin irritation, so the method cannot be applied to people in a large area.
Therefore, the composition with the oil control and convergence effects has important significance and wide market prospect in the field of cosmetics.
Disclosure of Invention
In view of the above, the present invention provides an oil-controlling astringent composition, a preparation method thereof and a cosmetic. The oil-control astringent composition provided by the invention can inhibit oil secretion, control oil and astringe for a long time, and keep the skin fresh and not greasy.
In order to achieve the above object, the present invention provides the following technical solutions:
the invention provides an oil-control astringent composition which comprises, by weight, 1-10 parts of brown algae extract, 2-8 parts of aloe protease, 1-10 parts of salvia extract, 3-20 parts of cherry blossom extract and 1-5 parts of tea polyphenol extract.
Preferably, the oil-control astringent composition comprises 7-10 parts by weight of brown algae extract, 6-8 parts by weight of aloe protease, 7-10 parts by weight of sage extract, 14-20 parts by weight of oriental cherry extract and 3-5 parts by weight of tea polyphenol extract.
Preferably, the oil-control astringent composition consists of 8 parts by weight of brown algae extract, 6 parts by weight of aloe protease, 7 parts by weight of salvia extract, 15 parts by weight of cherry blossom extract and 3 parts by weight of tea polyphenol extract.
In one embodiment of the present invention, the oil-controlling astringent composition comprises, by weight, 1 part of brown algae extract, 2 parts of aloe protease, 1 part of sage extract, 3 parts of oriental cherry extract, and 1 part of tea polyphenol extract.
In another embodiment provided by the present invention, the oil-controlling astringent composition is composed of 10 parts by weight of brown algae extract, 8 parts by weight of aloe protease, 10 parts by weight of sage extract, 20 parts by weight of cherry blossom extract, and 5 parts by weight of tea polyphenol extract.
In another embodiment provided by the present invention, the oil-controlling astringent composition is composed of 7 parts by weight of brown algae extract, 7 parts by weight of aloe protease, 7 parts by weight of sage extract, 14 parts by weight of cherry blossom extract, and 4 parts by weight of tea polyphenol extract.
In another embodiment provided by the present invention, the oil-controlling astringent composition is composed of, by weight, 4 parts of brown algae extract, 5 parts of aloe vera protease, 5 parts of sage extract, 10 parts of cherry extract, and 3 parts of tea polyphenol extract.
The invention also provides an oil-control convergence composition, which comprises the following components in percentage by mass: brown algae extract 1-10%, aloe protease 2-8%, sage extract 1-10%, cherry blossom extract 3-20%, tea polyphenol extract 1-5%, and the balance of water.
Preferably, the oil control astringent composition consists of the following components in percentage by mass: 7-10% of brown algae extract, 6-8% of aloe protease, 7-10% of sage extract, 14-20% of cherry blossom extract, 3-5% of tea polyphenol extract and the balance of water.
Preferably, the oil-control astringent composition consists of the following components in percentage by mass: 8% of brown algae extract, 6% of aloe protease, 7% of salvia extract, 15% of cherry blossom extract, 3% of tea polyphenol extract and the balance of water.
In one embodiment provided by the invention, the oil control convergence composition comprises the following components in percentage by mass: brown algae extract 1%, aloe protease 2%, sage extract 1%, cherry blossom extract 3%, tea polyphenol extract 1%, and the balance of water.
In another embodiment provided by the present invention, the oil control astringent composition consists of the following components in percentage by mass: 10% of brown algae extract, 8% of aloe protease, 10% of sage extract, 20% of cherry blossom extract, 5% of tea polyphenol extract and the balance of water.
In another embodiment provided by the present invention, the oil control astringent composition consists of the following components in percentage by mass: brown algae extract 7%, aloe protease 7%, sage extract 7%, cherry blossom extract 14%, tea polyphenol extract 4%, and the balance of water.
In another embodiment provided by the present invention, the oil control astringent composition consists of the following components in percentage by mass: brown algae extract 4%, aloe protease 5%, sage extract 5%, cherry blossom extract 10%, tea polyphenol extract 3%, and the balance of water.
The invention also provides a preparation method of the oil-control convergence composition, which comprises the following steps: mixing brown algae extract, aloe protease, herba Salvia officinalis extract, cherry blossom extract, tea polyphenols extract, and water uniformly to obtain the composition.
The invention also provides a cosmetic which comprises the oil-control astringent composition and cosmetically acceptable auxiliary materials.
Preferably, the oil control astringent composition is added in an amount of 0.1-8% of the total mass of the cosmetic.
Preferably, the oil control astringent composition is added in an amount of 1-5% of the total mass of the cosmetic.
Preferably, the cosmetic is in the form of lotion, essence, skin care emulsion, skin cream, skin care gel, facial mask or base makeup.
The invention provides an oil-control astringent composition, a preparation method thereof and a cosmetic. The oil-control astringent composition comprises, by weight, 1-10 parts of brown algae extract, 2-8 parts of aloe protease, 1-10 parts of sage extract, 3-20 parts of oriental cherry extract and 1-5 parts of tea polyphenol extract. The invention has the technical effects that:
the composition is compounded by the brown algae extract and the plant extract, so that sebaceous gland secretion is effectively controlled, oil is reduced, pores are shrunk, the effect of long-term oil control and convergence is realized, the skin state is improved, and the synergistic effect is achieved.
Detailed Description
The invention discloses an oil-control astringent composition, a preparation method thereof and cosmetics, and a person skilled in the art can use the content to realize the oil-control astringent composition by properly improving process parameters. It is expressly intended that all such similar substitutes and modifications which would be obvious to one skilled in the art are deemed to be included in the invention. While the methods and applications of this invention have been described in terms of preferred embodiments, it will be apparent to those of ordinary skill in the art that variations and modifications in the methods and applications described herein, as well as other suitable variations and combinations, may be made to implement and use the techniques of this invention without departing from the spirit and scope of the invention.
The technical scheme adopted by the invention is as follows:
in a first aspect, the present invention provides an oil-controlling astringent composition, which consists of brown algae extract, aloe vera protease, sage extract, cherry blossom extract, tea polyphenol extract, and water.
Preferably, the oil-controlling astringent composition comprises, by mass, 1% -10% of brown algae extract, 2% -8% of aloe protease, 1% -10% of sage extract, 3% -20% of cherry blossom extract, 1% -5% of tea polyphenol extract, and the balance of water.
In the present invention, the content of the brown algae extract is 1% to 10%, and may be, for example, 1%, 2%, 5%, 8%, 10%.
In the present invention, the content of aloe protease is 2% to 8%, for example, 2%, 3%, 5%, 6%, 7%, 8%.
In the present invention, the content of the sage extract is 1% to 10%, and may be, for example, 1%, 2%, 4%, 5%, 7%, 9%, 10%.
In the present invention, the content of the cherry blossom extract is 3% to 20%, and may be, for example, 3%, 4%, 6%, 8%, 10%, 12%, 14%, 16%, 18%, 20%.
In the present invention, the content of the tea polyphenol extract is 1% to 5%, and may be, for example, 1%, 2%, 3%, 4%, 5%.
The preparation method comprises the following steps: adding brown algae extract, aloe protease, herba Salvia officinalis extract, oriental cherry extract, and tea polyphenols extract into water, and mixing to obtain the composition.
In a second aspect, the invention provides an application of the oil-control astringent composition in preparing cosmetics and a preparation method thereof.
Preferably, the oil control astringent composition is added in an amount of 0.1% to 8% by weight of the total cosmetic mass, e.g. 0.1%, 0.2%, 0.3%, 0.4%, 0.5%, 0.6%, 0.7%, 0.8%, 0.9%, 1%, 2%, 3%, 4%, 5%, 6%, 7%, 8%, preferably 1% to 5%;
preferably, the cosmetic comprises any one of lotion, essence, skin-care emulsion, skin-moistening cream, skin-care gel, mask or base.
The oil-control astringent composition, the preparation method thereof and raw materials or auxiliary materials used in cosmetics can be purchased from the market. Wherein the brown algae extract and the Salvia officinalis extract are obtained from Orxue chemical of Guangzhou, the aloe protease is obtained from Baihabo, the cherry blossom extract is obtained from Louis Biotech, Inc., and the tea polyphenol extract is obtained from Velcro.
The invention is further illustrated by the following examples:
example 1
The embodiment provides an oil control convergence composition, which comprises the following components in percentage by mass: brown algae extract 1%, aloe protease 2%, sage extract 1%, cherry blossom extract 3%, tea polyphenol extract 1% and water 92%.
The preparation method comprises the following steps: adding brown algae extract, aloe protease, herba Salvia officinalis extract, oriental cherry extract, and tea polyphenols extract into water, and mixing to obtain the composition.
Example 2
The embodiment provides an oil control convergence composition, which comprises the following components in percentage by mass: 10% of brown algae extract, 8% of aloe protease, 10% of sage extract, 20% of cherry blossom extract, 5% of tea polyphenol extract and 47% of water.
The preparation method comprises the following steps: adding brown algae extract, aloe protease, herba Salvia officinalis extract, oriental cherry extract, and tea polyphenols extract into water, and mixing to obtain the composition.
Example 3
The embodiment provides an oil-control astringent composition, which comprises the following components in percentage by mass: 8% of brown algae extract, 6% of aloe protease, 7% of salvia extract, 15% of cherry blossom extract, 3% of tea polyphenol extract and 61% of water.
The preparation method comprises the following steps: adding brown algae extract, aloe protease, herba Salvia officinalis extract, oriental cherry extract, and tea polyphenols extract into water, and mixing to obtain the composition.
Example 4
The embodiment provides an oil control convergence composition, which comprises the following components in percentage by mass: 7% of brown algae extract, 7% of aloe protease, 7% of sage extract, 14% of cherry blossom extract, 4% of tea polyphenol extract and 61% of water.
The preparation method comprises the following steps: adding brown algae extract, aloe protease, herba Salvia officinalis extract, oriental cherry extract, and tea polyphenols extract into water, and mixing to obtain the composition.
Example 5
The embodiment provides an oil control convergence composition, which comprises the following components in percentage by mass: brown algae extract 4%, aloe protease 5%, sage extract 5%, cherry blossom extract 10%, tea polyphenol extract 3%, and water 73%.
The preparation method comprises the following steps: adding brown algae extract, aloe protease, herba Salvia officinalis extract, oriental cherry extract, and tea polyphenols extract into water, and mixing to obtain the composition.
Comparative example 1
The only difference from example 3 is that the oil control astringent composition comprises 39% brown algae extract and 61% deionized water by weight.
Comparative example 2
The only difference from example 3 is that the oil control astringent composition comprises 39% by weight of aloe vera protease and 61% by weight of deionized water.
Comparative example 3
The only difference from example 3 is that the oil control astringent composition comprises 39% by weight of sage extract and 61% by weight of deionized water.
Comparative example 4
The only difference from example 3 is that the oil control astringent composition comprises 39% by weight of oriental cherry extract and 61% by weight of deionized water.
Comparative example 5
The difference from example 3 is only that the oil control astringent composition comprises 39% by weight of tea polyphenol extract and 61% by weight of deionized water.
Comparative example 6
The only difference from example 3 is that no tea polyphenol extract was added. The oil control convergence composition comprises the following components in percentage by mass: 8% of brown algae extract, 6% of aloe protease, 7% of sage extract, 15% of cherry blossom extract and 64% of water.
Comparative example 7
The only difference from example 3 is that cherry blossom extract was not added. The oil-control convergence composition comprises the following components in percentage by mass: 8% of brown algae extract, 6% of aloe protease, 7% of sage extract, 3% of tea polyphenol extract and 76% of water.
Comparative example 8
The only difference from example 3 is that sage extract was not added. The oil-control convergence composition comprises the following components in percentage by mass: 8% of brown algae extract, 6% of aloe protease, 15% of oriental cherry extract, 3% of tea polyphenol extract and 68% of water.
Comparative example 9
The only difference from example 3 is that no aloe protease was added. The oil-control convergence composition comprises the following components in percentage by mass: 8% of brown algae extract, 7% of salvia officinalis extract, 15% of cherry blossom extract, 3% of tea polyphenol extract and 67% of water.
Comparative example 10
The only difference from example 3 is that no brown algae extract was added. The oil control convergence composition comprises the following components in percentage by mass: 6% of aloe protease, 7% of sage extract, 15% of cherry blossom extract, 3% of tea polyphenol extract and 69% of water.
Experimental example 1 chick embryo Hair follicle stimulation test
By utilizing the characteristics of complete, clear and transparent chorioallantoic membrane vascular system in the middle stage of hatched chick embryo, a certain quantity of test substance is directly contacted with chick embryo allantoic membrane, after a period of action, the change of chorioallantoic membrane toxicity effect indexes (such as hemorrhage, blood coagulation and blood vessel melting) is observed, these indexes can reflect the change of morphological structure, colour and permeability of blood vessel and blood vessel network, and can reflect the phenomena of chorioallantoic membrane protein denaturation and its damage degree, then they are combined to obtain a score for evaluating the ocular irritation of test substance.
The experimental method refers to the method in SNT2329-2009 for testing, adopts a reaction time method for testing, and adopts a stimulation score method for stimulation score calculation.
TABLE 1 evaluation of stimulation scoring results
| Stimulation scoring | Irritation grading |
| IS＜1 | Has no irritation |
| 1≤IS＜5 | Light irritation |
| 5≤IS＜9 | Moderate irritation |
| IS≥10 | Strong irritation/corrosion |
The experimental results are as follows: by performing chick embryo hair follicle experiments on the oil control convergence compositions prepared in examples 1-5 and comparative examples 1-10 of the invention, the results show that the irritation grading of examples 1-5 is no irritation, which indicates that the oil control convergence compositions of the invention are mild and have no irritation.
Experimental example 2 sebum level (CSL) test
Selecting 75 volunteers with the age of 16-50 years, male and female, and the screening conditions are as follows: the sebum level is more than or equal to 150 mu g/cm after three hours of face cleaning in the morning2. After the face was cleansed, the oil-controlling astringent composition prepared in example 1-5 and the composition prepared in comparative example 1-10, which were soybean-sized samples, were applied to the forehead and absorbed by patting, and the composition was used once a day, morning and evening. And testing the sebum level (CSL) of the 4 th week by using a sebum test analyzer, and taking the average value of the test results of the user and taking the sebum level 30min after the test area is cleaned as an initial value. The test results are shown in table 2:
TABLE 2 sebum level test results
| Sample (I) | Degree of reduction in sebum levels |
| Example 1 | -22.67％ |
| Example 2 | -31.33％ |
| Example 3 | -31.54％ |
| Example 4 | -30.89％ |
| Example 5 | -26.57％ |
| Comparative example 1 | -3.59％ |
| Comparative example 2 | -2.67％ |
| Comparative example 3 | -6.84％ |
| Comparative example 4 | -9.66％ |
| Comparative example 5 | -8.21％ |
| Comparative example 6 | -13.68％ |
| Comparative example 7 | -15.39％ |
| Comparative example 8 | -14.52％ |
| Comparative example 9 | -12.67％ |
| Comparative example 10 | -16.38％ |
As can be seen from Table 2, the oil-controlling astringent compositions prepared in examples 1 to 5 and the compositions prepared in comparative examples 1 to 10 both have a reduction effect on the sebum level, but the oil-controlling astringent compositions prepared in examples 1 to 5 have a reduction degree on the sebum level, the reduction degree on the sebum level is between-20% and-32%, and the oil secretion inhibition degree is higher than that of the composition prepared in the ratio of 1 to 10, which is a single component or lacks any active ingredient, so that the oil-controlling astringent compositions of the invention have scientific and reasonable component ratios, play a role in synergy and can inhibit effective oil secretion.
Experimental example 3 Number of Active Pores (NAP) and percentage of skin Surface Sebum (SSP) test
Selecting 75 volunteers, the age of which is 16-50 years old, male and female are unlimited, and the screening conditions are as follows: the sebum level is more than or equal to 150 mu g/cm after three hours of face cleaning in the morning2. After the face was cleansed, the oil-controlling astringent composition prepared in example 1-5 and the composition prepared in comparative example 1-10, which were soybean-sized samples, were applied to the forehead and absorbed by patting, and the composition was used once a day, morning and evening. The Number of Active Pores (NAP) and the percentage of skin Surface Sebum (SSP) at week 4 were measured using an active skin surface analysis system, and the user test results were averaged to take the Number of Active Pores (NAP) and the percentage of skin Surface Sebum (SSP) 30min after cleaning of the test area as initial values.
TABLE 3 Number of Active Pores (NAP) and percent skin Surface Sebum (SSP) test results
As can be seen from the test results in table 3, the oil control astringent compositions prepared in examples 1 to 5 have a better effect of reducing the number of active pores and the percentage of sebum on the skin surface than the oil control astringent compositions prepared in examples 1 to 5, which indicates that the oil control astringent compositions of the present invention have a better oil control effect than the compositions containing a single component or lacking any active component, and thus the oil control astringent compositions of the present invention have a better effect of controlling oil and shrinking pores after the synergistic effect of the active components of the oil control astringent compositions of the present invention.
Application examples 1 to 5 and comparative example 11
The essential water prepared from the oil-control astringent composition prepared in example 3 is prepared from the following components in percentage by mass.
0.5-3% of 1, 3-propylene glycol, 0.2-1% of butanediol, 0.5-1% of betaine, 1-2% of trehalose, 0.15-0.35% of carbomer, 0.3-0.8% of sodium citrate, 1-5% of the oil-controlling astringent composition prepared in example 3 and the balance of water.
The preparation method comprises the following steps:
firstly, mixing water, 1.3-propylene glycol and butanediol, heating to 80-85 ℃, keeping the temperature for 20-30min, cooling to 40-45 ℃, then adding betaine, trehalose and carbomer, stirring for 20-30min, and uniformly mixing; finally, the temperature is reduced to 37 ℃, the oil control convergence composition prepared in the example 3 is added, and the mixture is stirred and dispersed; and finally, adding sodium citrate to adjust the pH value to obtain the essence water.
Specific embodiments are shown in table 4 below:
table 4 essence formula table
Comparative example 12
The same as in application example 3, except that the composition of example 3 was replaced with the composition prepared in comparative example 8, and the contents of other components and the preparation method were not changed.
Comparative example 13
The same as in application example 3, except that the composition of example 3 was replaced with the composition prepared in comparative example 10, and the contents of other components and the preparation method were not changed.
Experimental example 4 product safety test
Selecting 30 healthy subjects with no allergic history of the skin diseases between the ages of 25 and 50, and sticking the spots: selecting a qualified spot tester, dripping about 20mg of the essence of the application examples 1-5 of the invention into the spot tester in a closed spot test mode, externally applying a special adhesive tape to the back of a test subject, respectively sticking the essence of the application examples 1-5, removing the test subject after 24 hours, observing skin reactions after 0.5, 6, 12, 24 and 48 hours after removal, and recording the result according to the skin reaction grading standard in the cosmetic sanitation standard.
And (3) test results: the result of the skin patch test of the human body shows that all the testees pass the patch test, and the skin reaction is observed in 0.5, 6, 12, 24 and 48 hours, wherein 0 case has adverse reactions such as skin erythema, pimple, blister and the like, which indicates that the essence water of the invention is safe to use and has no stimulation.
Experimental example 5 detection of product stability
The essential oils prepared in the application examples 1 to 5 and the comparative examples 11 to 13 of the present invention were subjected to a stability test.
And (3) centrifugal test: weighing a proper amount of the product in a centrifuge tube, centrifuging for 30min at 4000rpm, and observing appearance change.
Cold resistance test: taking a proper amount of the product, placing the product in a weighing bottle, sealing the weighing bottle, placing the weighing bottle in a refrigerator at the temperature of-20 ℃, sampling every 7 days, continuously inspecting for 3 months, and observing appearance change.
And (3) heat resistance test: taking a proper amount of the product, placing the product in a weighing bottle, sealing the product, placing the product in a 60 ℃ oven, sampling every 7 days, observing the product, continuously inspecting the product for 3 months, and observing appearance change.
The detection results show that the products prepared in application examples 1-5 and comparative examples 11-13 are not layered and have no change in appearance after centrifugation, high temperature and low temperature tests, which shows that the base material of the cosmetic is reasonably selected and has no adverse effect on the stability of the product.
Experimental example 6 evaluation of trial products
In order to evaluate the actual use effect of the oil-controlling and astringent composition, 80 oily skin volunteers were selected as test samples from the essential water prepared in application example 3 and the essential water prepared in application comparative example 11, and divided into 8 groups of 10 persons each, and sensory evaluation tests were performed, wherein the test items were the oil-controlling effect, pore-astringing effect, mildness and overall evaluation of the product, the test period was four weeks, and the test values indicated the number of volunteer subjects who approved the corresponding product. The specific test results are shown in table 5:
TABLE 5 trial evaluation results of the products
| Sample (I) | Oil control effect | Pore astringency effect | Mildness property | Overall evaluation |
| Application example 1 | 7 | 8 | 10 | 8 |
| Application example 2 | 8 | 9 | 10 | 9 |
| Application example 3 | 9 | 10 | 10 | 10 |
| Application example 4 | 8 | 9 | 10 | 9 |
| Application example 5 | 9 | 9 | 10 | 9 |
| Comparative example 11 | 1 | 2 | 10 | 2 |
| Comparative example 12 | 5 | 6 | 10 | 6 |
| Comparative example 13 | 6 | 4 | 10 | 5 |
The consumer acceptance of the use example 3 was higher as shown by the test results of table 5 by blindly testing the use example 3 prepared serum with the use comparative examples 11 to 13 prepared serum. The active components of the oil-control convergence composition are mutually matched, so that the oil-control convergence composition has a synergistic effect, and can be used for inhibiting oil secretion, reducing the activity of pores, maintaining the water-oil balance of skin, improving the moisture retention of the skin, strengthening the skin barrier, regulating the oil and the fat of the skin and achieving the long-acting and lasting oil-control convergence effect.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various modifications and amendments can be made without departing from the principle of the present invention, and these modifications and amendments should also be considered as the protection scope of the present invention.
Claims (5)
1. The oil-control astringent composition is characterized by comprising the following components in percentage by mass: 1-10% of brown algae extract, 2-8% of aloe protease, 1-10% of sage extract, 3-20% of cherry blossom extract, 1-5% of tea polyphenol extract and the balance of water;
wherein the brown algae extract and the Salvia officinalis extract are obtained from Oxue chemical engineering of Guangzhou, the cherry blossom extract is obtained from Luojie Biotech, Inc., and the tea polyphenols extract is obtained from Veco.
2. The oil control convergence composition of claim 1, wherein the oil control convergence composition comprises, in mass percent: 7% -10% of brown algae extract, 6% -8% of aloe protease, 7% -10% of sage extract, 14% -20% of cherry blossom extract, 3% -5% of tea polyphenol extract and the balance of water.
3. The oil control convergence composition according to claim 1 or 2, wherein the oil control convergence composition consists of, in mass percent: 8% of brown algae extract, 6% of aloe protease, 7% of sage extract, 15% of cherry blossom extract, 3% of tea polyphenol extract and the balance of water.
4. A method of preparing an oil-controlling astringent composition as claimed in any one of claims 1 to 3, wherein the oil-controlling astringent composition is prepared by mixing brown algae extract, aloe vera protease, sage extract, cherry blossom extract, tea polyphenol extract and water uniformly.
5. A cosmetic is characterized by comprising 0.5 to 3 percent of 1, 3-propanediol;
0.2 to 1 percent of butanediol;
0.5-1% of betaine;
1-2% of trehalose;
carbomer 0.15-0.35%;
0.3 to 0.8 percent of sodium citrate;
1-5% of the oil control astringent composition of any one of claims 1 to 3;
the balance being water.
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Citations (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009221121A (en) * | 2008-03-14 | 2009-10-01 | Kao Corp | Skin detergent |
| CN101564360A (en) * | 2008-04-23 | 2009-10-28 | 东和酵素株式会社 | Micro-bubble washing composition, micro-bubble washing method and micro-bubble washing equipment |
| CN102475664A (en) * | 2010-11-30 | 2012-05-30 | 株式会社爱茉莉太平洋 | Cosmetic composition containing seaweed fiber for regulating sebum or shrinking pore |
| CN103655393A (en) * | 2013-10-22 | 2014-03-26 | 李本明 | Facial mask for whitening and moisturizing |
| CN104629965A (en) * | 2015-03-16 | 2015-05-20 | 理想科技集团有限公司 | Natural oil-controlled fruit tea soap and preparation method thereof |
| CN105362169A (en) * | 2015-12-27 | 2016-03-02 | 青岛克立克信息技术有限公司 | Oil-control and moisturizing facial cleanser |
| CN105963198A (en) * | 2016-06-26 | 2016-09-28 | 青岛艾派克生物科技有限公司 | Facial cleanser capable of shrinking pores and balancing grease |
| CN108056980A (en) * | 2016-11-09 | 2018-05-22 | 宋德强 | A kind of facial cleanser of pore refining equilibrium grease |
| CN108261348A (en) * | 2018-04-20 | 2018-07-10 | 佛山市三水区嘉华化学研究院（普通合伙） | A kind of anti-aging Face-protecting mask |
| CN108338960A (en) * | 2018-04-02 | 2018-07-31 | 四川力智久创知识产权运营有限公司 | A kind of tender skin face mask of traditional Chinese medicine |
| CN108635321A (en) * | 2018-07-04 | 2018-10-12 | 界首市众鑫科技服务有限公司 | A kind of beautifying liquid of oil-control contracting pore |
| CN109692135A (en) * | 2019-02-28 | 2019-04-30 | 广东芭薇生物科技股份有限公司 | A kind of composition and its application with pore refining and moisture-keeping efficacy |
| KR101993363B1 (en) * | 2018-09-12 | 2019-06-26 | 고윤우 | Functional cosmetic composition containing manuka honey and zeolite component and manufacturing method thereof |
| CN110538133A (en) * | 2019-09-27 | 2019-12-06 | 广州环亚化妆品科技有限公司 | Oil control convergence composition and preparation method and application thereof |
-
2020
- 2020-03-26 CN CN202010224213.8A patent/CN111297759B/en active Active
Patent Citations (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009221121A (en) * | 2008-03-14 | 2009-10-01 | Kao Corp | Skin detergent |
| CN101564360A (en) * | 2008-04-23 | 2009-10-28 | 东和酵素株式会社 | Micro-bubble washing composition, micro-bubble washing method and micro-bubble washing equipment |
| CN102475664A (en) * | 2010-11-30 | 2012-05-30 | 株式会社爱茉莉太平洋 | Cosmetic composition containing seaweed fiber for regulating sebum or shrinking pore |
| CN103655393A (en) * | 2013-10-22 | 2014-03-26 | 李本明 | Facial mask for whitening and moisturizing |
| CN104629965A (en) * | 2015-03-16 | 2015-05-20 | 理想科技集团有限公司 | Natural oil-controlled fruit tea soap and preparation method thereof |
| CN105362169A (en) * | 2015-12-27 | 2016-03-02 | 青岛克立克信息技术有限公司 | Oil-control and moisturizing facial cleanser |
| CN105963198A (en) * | 2016-06-26 | 2016-09-28 | 青岛艾派克生物科技有限公司 | Facial cleanser capable of shrinking pores and balancing grease |
| CN108056980A (en) * | 2016-11-09 | 2018-05-22 | 宋德强 | A kind of facial cleanser of pore refining equilibrium grease |
| CN108338960A (en) * | 2018-04-02 | 2018-07-31 | 四川力智久创知识产权运营有限公司 | A kind of tender skin face mask of traditional Chinese medicine |
| CN108261348A (en) * | 2018-04-20 | 2018-07-10 | 佛山市三水区嘉华化学研究院（普通合伙） | A kind of anti-aging Face-protecting mask |
| CN108635321A (en) * | 2018-07-04 | 2018-10-12 | 界首市众鑫科技服务有限公司 | A kind of beautifying liquid of oil-control contracting pore |
| KR101993363B1 (en) * | 2018-09-12 | 2019-06-26 | 고윤우 | Functional cosmetic composition containing manuka honey and zeolite component and manufacturing method thereof |
| CN109692135A (en) * | 2019-02-28 | 2019-04-30 | 广东芭薇生物科技股份有限公司 | A kind of composition and its application with pore refining and moisture-keeping efficacy |
| CN110538133A (en) * | 2019-09-27 | 2019-12-06 | 广州环亚化妆品科技有限公司 | Oil control convergence composition and preparation method and application thereof |
Non-Patent Citations (6)
| Title |
|---|
| Antioxidant, free radical scavenging activities of Salvia brachyantha and its protective effect against oxidative cardiac cell injury;Mohammad Ali Esmaeili et al.;《Food and Chemical Toxicology》;20100331;第846-853页 * |
| Cosmetic attributes of algae - A review;Maíra BuenoAriede et al.;《Algal Reserach》;20170731;第483-487页 * |
| 海藻在功能性化妆品中的应用;李传茂 等;《广东化工》;20171231;第44卷(第16期);第157-159页 * |
| 茶多酚在化妆品中的研究进展;田丽丽 等;《广东茶业》;20071231;第15-17页 * |
| 茶提取物在化妆品领域中的应用;王普兵 等;《广东化工》;20191231;第46卷(第7期);第142-143页 * |
| 褐藻多酚在化妆品中的应用及研究进展;陈红红 等;《渔业研究》;20200225;第90-96页 * |
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