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CN110721101A - Self-prepared two-component essence cream and preparation method thereof - Google Patents

Self-prepared two-component essence cream and preparation method thereof Download PDF

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Publication number
CN110721101A
CN110721101A CN201910988692.8A CN201910988692A CN110721101A CN 110721101 A CN110721101 A CN 110721101A CN 201910988692 A CN201910988692 A CN 201910988692A CN 110721101 A CN110721101 A CN 110721101A
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component
phase
oil
percent
cream
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Inventor
杨延辉
郑开明
焦娟娟
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Guangzhou Porcelain Cosmetics Co Ltd
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Guangzhou Porcelain Cosmetics Co Ltd
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Priority to CN201910988692.8A priority Critical patent/CN110721101A/en
Publication of CN110721101A publication Critical patent/CN110721101A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31Hydrocarbons
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • A61K8/9711Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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Abstract

The invention discloses a self-prepared two-component essence cream and a preparation method thereof, the self-prepared two-component essence cream comprises a basic moistening gel component and an enhanced maintenance essential oil cream component, the enhanced maintenance essential oil cream component and the basic moistening gel component are mutually isolated, a user can self-prepare the basic moistening gel component and the enhanced maintenance essential oil cream component to an optimal state according to the skin type, the current skin state and the climatic environment, the use flexibility is high, the application range is wide, the self-prepared two-component essence cream effectively cooperates with active substances of various natural plants, and the addition of plant essential oil enables the essence cream to have the effects of skin care, the volatilization of the essential oil fragrance, pressure relief and refreshing.

Description

Self-prepared two-component essence cream and preparation method thereof
Technical Field
The invention relates to a skin care product, in particular to a self-prepared two-component essence cream and a preparation method thereof.
Background
The skin of a person has five major categories of dryness, oiliness, mixability, neutrality and sensitivity, the existing skin care product has a single formula and fixed component proportion, and can only be suitable for one skin type, and the audience range is limited; on the other hand, facial skin of people is in different states due to different regional climates, different temperatures and humidities and different indoor environments, in addition, China is large in land and wide in width, the climate difference between the south and the north is very large, the climate in the north is dry, the climate in the south is wet, the existing skin care product cannot be flexibly prepared according to the climate of the current region where a consumer is located, the use flexibility is poor, and the applicable region is limited.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention provides the self-prepared two-component essence cream and the preparation method thereof, and solves the problem that the existing skin care product cannot be adjusted according to the skin state of a user.
The technical scheme adopted by the invention for solving the technical problems is as follows:
a self-prepared two-component essence cream comprises a basic moistening gel component and an enhanced maintenance essential oil cream component, wherein the enhanced maintenance essential oil cream component is represented by I, the basic moistening gel component is represented by II, and the enhanced maintenance essential oil cream component and the basic moistening gel component are isolated from each other.
The component (I) of the essential oil cream for enhancing and maintaining is composed of the following raw materials in percentage by weight:
A0.5-1.5% of macadamia nut seed oil, 1.5-2.5% of jojoba seed oil, and 0.5-1.5% of polyDimethyl siloxane, 1.5 to 2.5 percent of isononyl isononanoate, 1 to 2 percent of squalane, 0.05 to 0.15 percent of antioxidant, 1.5 to 2.5 percent of emulsifier and 1 to 2 percent of thickening agent,
the macadimia nut seed oil is rich in minerals, proteins and various unsaturated fatty acids, can be used for conditioning aged or dry skin, and has the greatest advantages of mild oiliness, no stimulation to the skin, good ductility and capability of softening and activating the skin; on the other hand, the macadamia nut seed oil also has the function of base oil as the component of the enhanced maintenance essential oil cream, because the component of the enhanced maintenance essential oil cream comprises various essential oils, and the macadamia nut seed oil has good permeability and high solubility to various essential oils, is good base oil, and can bring certain greasy skin feeling.
The jojoba seed oil is composed of single unsaturated fatty acid and single unsaturated fatty alcohol, the hydrophile/lipophile balance value of the jojoba seed oil is about 6, and the jojoba seed oil can be completely mixed with the surface sebum of the skin, so that the jojoba seed oil can easily enter the oil phase of the skin and be combined with the oil phase to form a layer of oil-free film on the skin, but pores and hair follicles are still in an open state, and the jojoba seed oil has the function of lubricating and caring the skin.
The polydimethylsiloxane has the function of resisting ultraviolet radiation, but has obvious physiological inertia and is easy to separate out, so the inventor chooses to add the isononyl isononanoate to solve the problem that the polydimethylsiloxane is easy to separate out. The isononyl isononanoate has excellent compatibility with the polydimethylsiloxane, can be used as a stabilizing agent and a coupling agent of the polydimethylsiloxane, has a polymethyl branched chain structure, is low in viscosity, has fresh skin feel, is an excellent emollient, and has an effect as an emollient in the invention.
The squalane can inhibit peroxidation of skin lipid, can effectively permeate into skin, can promote proliferation of skin basal cells, and has obvious physiological effects of delaying skin aging, and improving and eliminating chloasma.
BPhase 4.5-5.5% glycerol, 1.5-2.5% glyceryl polyether-26, 0.5-1.5% betaine, 0.01-0.1%Sodium hyaluronate, 0.01-0.1% of chelating agent, 12-13% of thickening agent and 0.1-0.15% of preservative,
different moisturizing agents have different moisturizing mechanisms, such as moisture blocking, moisture absorption, moisturizing and the like, and in practical production application, only one moisturizing agent is used, so that an ideal moisturizing effect cannot be achieved, and therefore, the B componentThe phases are hydrophilic moisturizers that differ by combining different moisturizing mechanisms to achieve the desired moisturizing effect.
The molecule of the glycerin contains three-OH groups, and the glycerin can form hydrogen bonds with water molecules to restrain water, so that the glycerin plays a good role in absorbing moisture and preserving moisture, has an obvious moisturizing effect on human skin, and also has a function of increasing the solubility of other components.
The addition of the glycerin results in the invention bringing less pleasant greasy feeling to the skin in a semi-dry state, and the glyceryl polyether-26 is a glycerin polymer of 26 EO, and the moisturizing effect is stronger than that of the glycerin even in a low addition amount, so the invention improves the sticky skin feeling caused by the addition of the glycerin by adding the glyceryl polyether-26 in a proper amount.
The betaine is a natural amino acid humectant, and the moisturizing mechanism of the betaine is as follows: the betaine can obviously inhibit the process by absorbing the moisture in the deep layer of the skin to the surface layer with water shortage, so that the surface layer of the skin also contains sufficient moisture, the problem of drying of the skin care product after being smeared can be avoided, and the betaine also has an antiallergic effect.
The sodium hyaluronate realizes moisture preservation by enhancing the water absorption and water binding capacity of the skin stratum corneum, and has the outstanding characteristics of film forming property and lubricity, and a breathable hydrated elastic film can be formed after the sodium hyaluronate acts on the skin surface.
CPhase 1-5% cyclopentadimethylsiloxane. A is describedPolydimethyl silicon in phaseAlthough the problem of easy separation of siloxane is improved by the isononyl isononanoate, the polydimethylsiloxane actually has the problem of heavy and greasy skin feel when the polydimethylsiloxane is applied, and the cyclopentasiloxane belongs to water-thin (water-thin) organic silicon and is unstable in property, so that the polydimethylsiloxane is helped to volatilize after being pushed away, the skin can not feel burdens, and the problem of heavy and greasy skin feel when the polydimethylsiloxane is applied is solved.
DPhase 0.2-0.3% of PH regulator,
E0.2-0.4% of natural antioxidant antiallergic extract of plant, 0.5-1.5% of Chondrus crispus extract, 0.5-1.5% of Ginseng radix extract, 1-2% of palmitoyl tripeptide-1, 0.05-0.15% of ethylhexyl glycerol, 0.1-0.5% of phenoxyethanol and 0.05-0.15% of colorant,
the invention selects the Chondrus crispus extract and the ginseng extract as main active ingredients, and then adds the natural antioxidant and antiallergic extract of the plants as auxiliary ingredients. The Chondrus crispus extract has the effects of inhibiting human leukocyte elastase, promoting the generation of collagen, slowing down skin aging, fading wrinkles and removing aged cutin.
The ginseng extract contains various ginsenosides, amino acids, vitamins and mineral substances, has good permeability, can deeply moisten skin, quickly adjust skin moisture balance, prevent skin dehydration, bring soft and smooth skin, and has the functions of promoting blood circulation of subcutaneous capillaries, strengthening cell vitality and promoting collagen vitality, wherein the phloretin can also effectively improve the elasticity of soles, and has the functions of reducing deep wrinkles, improving flabby skin, and improving skin contour and firming feeling.
The palmitoyl tripeptide-1 is a signal peptide, and can act on the dermis to promote the synthesis of extracellular matrix, such as type I and type III collagen, elastin, structural glycoprotein, to make the skin firmer and thicker, to improve wrinkles, and to enhance the skin's ability to resist ultraviolet radiation.
The mixture of phenoxyethanol and ethylhexyl glycerin has good antiseptic effect and high safety, and the ethylhexyl glycerin has the function of auxiliary antiseptic and also has the function of improving the greasy skin feeling caused by the addition of the macadamia nut seed oil and glycerin.
The colorant is mainly used for beautifying and modifying the color tone of the invention.
FThe oil phase comprises 0.1-0.5% of rosemary leaf oil, 0.05-0.15% of chamomile oil, 0.05-0.15% of ylang-ylang oil, 0.1-0.3% of sweet orange peel oil, 0.2-0.4% of lemon peel oil, 0.3-0.5% of peppermint oil, 0.1-0.3% of basil oil and 1-2% of solubilizer. Said FThe phases are extracted from pure natural plants, and have protective effect on sensitive muscles.
The rosemary leaf oil has strong contraction effect, can tighten loose skin, and can relieve congestion and swelling, and the dispersed smell of the rosemary leaf oil is helpful for refreshing.
The white flower spring yellow chrysanthemum oil contains various flavones, heparin, a-bisabolol, caffeic acid, saccharides, various amino acids and other nutrient substances, has excellent effects of resisting inflammation, diminishing swelling, promoting cell regeneration, skin metabolism and the like, can eliminate free radicals, has oxidation resistance, has an aging delaying effect, and has a certain inhibition effect on melanocytes, so that the white flower spring yellow chrysanthemum oil has a certain whitening and freckle removing effect, and the emitted smell of the white flower spring yellow chrysanthemum oil can endow the white flower spring yellow chrysanthemum oil with mild, fresh and natural feeling.
The ylang oil has perfect balance and correction effect on skin, can correct sebum secretion disorder, reduce facial microvascular exposure, and can release fragrance to relieve anxiety and pressure.
The sweet orange peel oil contains a large amount of vitamin C, so that the sweet orange peel oil has a good moisturizing effect on skin, can balance the pH value of the skin, helps collagen formation, has a good effect on the growth and repair of skin tissues, and can help the blocked skin to discharge toxins.
The lemon peel oil can remove old and dead cells, increase skin luster, tighten micro-vessels, promote collagen production and lighten freckles.
The addition of the peppermint oil enables the skin to have special cool feeling, and meanwhile, the effects of cleaning the skin and astringing pores are achieved.
The basil oil has moistening effect on dry, water-deficient, aged and wrinkled skin, and can effectively control acne.
The balance of water;
wherein the basic moistening gel component (II) is prepared from the following raw materials in parts by weight:
Aphase 6-10% of glycerin, 0.3-0.6% of thickening agent,
Bphase 0.3-0.5% of PH regulator,
C0.05-0.15% of coloring agent, 0.3-0.6% of preservative,
Dphase 0.4-0.6% rose oil, 1-2% chamomile oil and 1.5-2.5% solubilizer,
the balance being water.
The basic moistening gel component mainly ensures that the basic moistening gel component has basic moistening and moisturizing effects on skin, and the effects of all the components are the same as those of the same components in the enhanced maintenance essential oil cream component.
The rose essential oil has excellent effects of shrinking and strengthening facial capillaries, and also can fade spots, promote melanin decomposition, improve dry skin and tighten skin.
The chamomile oil can well relieve the skin and resist skin sensitivity, has the effects of inflammation resistance, bacteria resistance and oxidation resistance, contains flavonoid compounds, amino acid and other components, can well play a moisturizing effect, regulates the water-oil balance of the skin to a certain degree, and can reduce the generation of acnes, resist oxidation and slow down skin aging due to the anti-inflammatory effect.
A is describedThe antioxidant in the phase is tocopherol acetate, which functions to counteract the generation of free radicals in skin cells, and is preferred in view of the fact that the maintenance-enhancing essential oil cream component contains various natural plant essential oils, which are soluble in plant oils.
A is describedThe emulsifier in the phase is cetostearyl alcohol or whaleEither or both of the wax stearyl glucosides, considering that the present invention is applied directly to the skin, whereas conventional surfactants generally have some irritation to the skin, the cetearyl alcohol and cetearyl glucoside are advantageous in that the natural polysaccharides replace the ethoxylated groups, which are one of the characteristics of conventional nonionic surfactants, and thus both are mild in nature, low in irritation, highly safe and excellent in biodegradability; on the other hand, another advantage of both is that there is no cloud point, and there is no turbidity with the temperature rise during the production process, which is essential for the present invention to give an idea of the appearance of the finished product.
A is describedThe thickener in the phase is hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, has high temperature stability and wide pH range in use, does not influence the thickening effect and the stability even if the use amount is low, and has certain emulsification effect on the other hand, so that the use amount of the emulsifier disclosed by the invention can be reduced.
B isThe chelating agent in the phase is disodium EDTA, water is used as the solvent with the largest using amount in the invention, so that partial metal ions can not be avoided, the disodium EDTA can complex some metal ions, the oxidation effect of the metal ions on the whole system is reduced, and the disodium EDTA has a stabilizing effect on the invention.
B isThe preservative in the phase is methyl hydroxybenzoate, is a common water phase preservative, and is mixed with the B heated under stirring at 80-85 deg.C in consideration of its property of dissolving in hot water and slightly dissolving in water at room temperaturePhase (see below for details of the preparation).
B isPhase sum AThe thickeners in the phase are all carbomers, taking into account said BPhase sum ABoth phases are water soluble components, so the aqueous phase thickener carbomer is used.
Said DPhase B andthe pH regulator in the phase is triethanolamine.
Said EThe natural antioxidant antiallergic extract of the plants in the phase is fructus PhyllanthiOne or more of radix Glycyrrhizae extract, folium Camelliae sinensis extract, herba Rosmarini officinalis extract, herba Centellae extract, flos Matricariae Chamomillae extract, radix Scutellariae extract, and rhizoma Polygoni Cuspidati extract.
Said C isThe preservatives in the phase are one or two of phenoxyethanol and ethylhexyl glycerin, preferably, the phenoxyethanol and the ethylhexyl glycerin are mixed, so that the preservative effect is better, and the safety is higher.
Said DThe solubilizer in the phase is PEG-40 hydrogenated castor oil, is an excellent non-ionic solubilizer, has wider pH value stability and low foam, can form a clear mixture with fatty acid and fatty alcohol at high temperature, can uniformly disperse a plurality of essential oils into water by adding the solubilizer to form a stable and transparent solution, and is added into the basic moisturizing gel component to ensure that the strong moisturizing essential oil component can be smoothly mixed during use.
A method for preparing the self-prepared two-component essence cream comprises the following steps:
preparation of the essential oil cream for enhancing and caring component (I)
S1: cleaning and disinfecting machine equipment;
S2: according to the weight percentage, configuring AMixing and heating to 80-85 ℃ for later use;
S3: configuring B according to the weight percentageAdding the mixture into a main emulsifying pot, adding a proper amount of water for dissolving, stirring and heating to 80-85 ℃ to uniformly dissolve;
S4: the A is addedPhase addition of said BHomogenizing for 3-5min, emulsifying, maintaining the temperature for 3-5min, and adding CHomogenizing for 3-5 min;
S5: will S4, cooling the prepared material to 60-65 ℃, and adding the DHomogenizing properly to make it uniform;
S6: will S5 cooling the prepared material to 40 DEG CAt-45 ℃, sequentially adding the dispersed EPhase sum FMixing the mixture evenly;
S7: will S6, if the prepared material is qualified, the enhanced maintenance essential oil cream component is prepared;
preparing the basic moistening gel component (II)
S1: cleaning and disinfecting machine equipment;
S2: according to the weight percentage, configuring AAdding appropriate amount of water for dissolving, mixing, heating to 80-85 deg.C, maintaining the temperature for 10min, and stirring to dissolve uniformly;
S3: will S2, cooling the prepared material to 60 ℃, and then adding the BStirring uniformly;
S4: will S3 cooling the obtained material to 45 ℃, and adding the CStirring the mixture evenly, and then adding the dispersed DAnd uniformly stirring the phases, and pumping and soaking for 5min to ensure that the materials are defoamed to be transparent, thus obtaining the basic moisturizing gel component.
The invention has the beneficial effects that: the user can automatically mix the basic moistening gel component and the enhanced maintenance essential oil cream component to the optimal state according to the skin type, the current skin state and the climate environment, the use flexibility is high, and the application range is wide; the plant essential oil is added, so that the skin-care tea has the effects of protecting skin, relieving pressure and refreshing brain due to volatilization of the aroma of the essential oil.
Detailed Description
Example 1:
a self-prepared two-component essence cream comprises a basic moistening gel component and an enhanced maintenance essential oil cream component, wherein the enhanced maintenance essential oil cream component is represented by I, the basic moistening gel component is represented by II, and the enhanced maintenance essential oil cream component and the basic moistening gel component are isolated from each other.
The component (I) of the essential oil cream for enhancing and maintaining is composed of the following raw materials in percentage by weight:
A0.5% macadamia nut seed oil, 1.5% jojoba seed oil, 0.5% polydimethylsiloxane, 1.5% isononyl isononanoate, 1% squalane, 0.05% antioxidant, 1.5% emulsifier and 1% thickener,
B4.5 percent of glycerin, 1.5 percent of glyceryl polyether-26, 0.5 percent of betaine, 0.01 percent of sodium hyaluronate, 0.01 percent of chelating agent, 12 percent of thickening agent and 0.1 percent of preservative,
Cphase 1% of cyclopentadimethylsiloxane,
Dphase 0.2% of a pH regulator,
E0.2% of natural antioxidant and antiallergic extract of plant, 0.5% of Chondrus crispus extract, 0.5% of Ginseng radix extract, 0.1% of antiseptic, 1% of palmitoyl tripeptide-1, 0.05% of ethylhexyl glycerol and 0.05% of colorant (caramel color),
Fthe oil phase comprises 0.1% of rosemary leaf oil, 0.05% of chamomile oil, 0.05% of ylang-ylang oil, 0.1% of sweet orange peel oil, 0.2% of lemon peel oil, 0.3% of peppermint oil, 0.1% of basil oil and 1% of solubilizer,
the balance of water;
wherein the basic moistening gel component (II) is prepared from the following raw materials in parts by weight:
Aphase 6% glycerol, 0.3% thickener,
Bphase 0.3% of a pH regulator,
Cphase 0.05% colorant (caramel color), 0.3% preservative,
Dphase 0.4% rose oil, 1% chamomile oil and 1.5% solubilizer,
the balance being water.
A is describedThe antioxidant in phase is tocopherol acetate, said AThe emulsifier in phase is cetostearyl alcohol, said AThe thickener in phase is hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer.
B isThe chelating agent in the phase is disodium EDTA, BThe preservative in the phase is methylparaben.
B isPhase sum AThe thickening agents in the phase are all carbomers.
Said DPhase B andthe pH regulator in the phase is triethanolamine.
Said EThe plant natural antioxidant antiallergic extract in the phase is a mixture of Glycyrrhiza glabra root extract, tea leaf extract, rosemary leaf extract, centella asiatica extract, chamomile flower extract, Scutellaria baicalensis root extract and Polygonum cuspidatum root extract.
Said EPhase sum CThe preservative in the phase is phenoxyethanol.
Said DThe solubilizer in the phase is PEG-40 hydrogenated castor oil.
A method for preparing the self-prepared two-component essence cream comprises the following steps:
preparation of the essential oil cream for enhancing and caring component (I)
S1: cleaning and disinfecting machine equipment;
S2: according to the weight percentage, configuring AMixing and heating to 80-85 ℃ for later use;
S3: configuring B according to the weight percentageAdding the mixture into a main emulsifying pot, adding a proper amount of water for dissolving, stirring and heating to 80-85 ℃ to uniformly dissolve;
S4: the A is addedPhase addition of said BHomogenizing for 3-5min, emulsifying, maintaining the temperature for 3-5min, and adding CHomogenizing for 3-5 min;
S5: will S4, cooling the prepared material to 60-65 ℃, and adding the DHomogenizing properly to make it uniform;
S6: will S5 the temperature of the prepared material is reduced to 40-45 ℃, and the dispersed E is added in sequencePhase sum FMixing the mixture evenly;
S7: will S6, if the prepared material is qualified, the enhanced maintenance essential oil cream component is prepared;
preparing the basic moistening gel component (II)
S1: cleaning and disinfecting machine equipment;
S2: according to the weight percentage, configuring AAdding appropriate amount of water for dissolving, mixing, heating to 80-85 deg.C, maintaining the temperature for 10min, and stirring to dissolve uniformly;
S3: will S2, cooling the prepared material to 60 ℃, and then adding the BStirring uniformly;
S4: will S3 cooling the obtained material to 45 ℃, and adding the CStirring the mixture evenly, and then adding the dispersed DAnd uniformly stirring the phases, and pumping and soaking for 5min to ensure that the materials are defoamed to be transparent, thus obtaining the basic moisturizing gel component.
Example 2:
a self-prepared two-component essence cream comprises a basic moistening gel component and an enhanced maintenance essential oil cream component, wherein the enhanced maintenance essential oil cream component is represented by I, the basic moistening gel component is represented by II, and the enhanced maintenance essential oil cream component and the basic moistening gel component are isolated from each other.
The component (I) of the essential oil cream for enhancing and maintaining is composed of the following raw materials in percentage by weight:
A1.5% macadamia nut seed oil, 2.5% jojoba seed oil, 1.5% polydimethylsiloxane, 2.5% isononyl isononanoate, 2% squalane, 0.15% antioxidant, 2.5% emulsifier and 2% thickener,
B5.5 percent of glycerin, 2.5 percent of glyceryl polyether-26, 1.5 percent of betaine, 0.01 to 0.1 percent of sodium hyaluronate, 0.1 percent of chelating agent, 13 percent of thickening agent and 0.15 percent of preservative,
Cphase 5% of cyclopenta dimethyl siloxane,
Dphase 0.3% of a pH regulator,
E0.4% of natural antioxidant antiallergic extract of plant, 1.5% of Chondrus crispus extract, 1.5% of Ginseng radix extract, 0.5% of antiseptic, 2% of palmitoyl tripeptide-1, 0.15% of ethylhexyl glycerol and 0.15% of colorant (caramel color),
Fthe oil phase comprises 0.5% of rosemary leaf oil, 0.15% of chamomile oil, 0.15% of ylang-ylang oil, 0.3% of sweet orange peel oil, 0.4% of lemon peel oil, 0.5% of peppermint oil, 0.3% of basil oil and 2% of solubilizer,
the balance of water;
wherein the basic moistening gel component (II) is prepared from the following raw materials in parts by weight:
Aphase 10% glycerol, 0.6% thickener,
Bphase 0.5% of a pH regulator,
Cphase 0.15% colorant (caramel color), 0.6% preservative, 6
DPhase 0.6% rose oil, 2% chamomile oil and 2.5% solubilizer,
the balance being water.
A is describedThe antioxidant in phase is tocopherol acetate, said AThe emulsifier in phase is cetearyl glucoside, said AThe thickener in phase is hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer.
B isThe chelating agent in the phase is disodium EDTA, BThe preservative in the phase is methylparaben.
B isPhase sum AThe thickening agents in the phase are all carbomers.
Said DPhase B andthe pH regulator in the phase is triethanolamine.
Said EThe plant natural antioxidant antiallergic extract in the phase is a mixture of Glycyrrhiza glabra root extract, tea leaf extract, rosemary leaf extract, centella asiatica extract, chamomile flower extract, Scutellaria baicalensis root extract and Polygonum cuspidatum root extract.
Said EPhase sum CThe preservatives in the phase are both a mixture of phenoxyethanol and ethylhexylglycerin.
Said DThe solubilizer in the phase is PEG-40 hydrogenated castor oil.
The preparation method of this example is the same as example 1.
Example 3:
a self-prepared two-component essence cream comprises a basic moistening gel component and an enhanced maintenance essential oil cream component, wherein the enhanced maintenance essential oil cream component is represented by I, the basic moistening gel component is represented by II, and the enhanced maintenance essential oil cream component and the basic moistening gel component are isolated from each other.
The component (I) of the essential oil cream for enhancing and maintaining is composed of the following raw materials in percentage by weight:
A1% of macadamia nut seed oil, 2% of jojoba seed oil, 1% of polydimethylsiloxane, 2% of isononyl isononanoate, 1.5% of squalane, 0.1% of antioxidant, 2% of emulsifier and 1.5% of thickener,
B5 percent of glycerin, 2 percent of glyceryl polyether-26, 1 percent of betaine, 0.05 percent of sodium hyaluronate, 0.05 percent of chelating agent, 12.5 percent of thickening agent and 0.125 percent of preservative,
Cphase 3% of cyclopentadimethylsiloxane,
Dphase 0.25% of a pH regulator,
E0.3% of natural antioxidant antiallergic extract of plant, 1% of Chondrus crispus extract, 1% of Ginseng radix extract, 0.3% of antiseptic, 1.5% of palmitoyl tripeptide-1, 0.1% of ethylhexyl glycerol and 0.1% of colorant (caramel color),
Fthe oil phase comprises 0.3% of rosemary leaf oil, 0.1% of chamomile oil, 0.1% of ylang-ylang oil, 0.2% of sweet orange peel oil, 0.3% of lemon peel oil, 0.4% of peppermint oil, 0.2% of basil oil and 1.5% of solubilizer,
the balance of water;
wherein the basic moistening gel component (II) is prepared from the following raw materials in parts by weight:
A8% of looks sweetOil, 0.45% of a thickening agent,
Bphase 0.4% of a pH regulator,
Cphase 0.1% coloring agent (caramel color), 0.45% preservative,
Dphase 0.5% rose oil, 1.5% chamomile oil and 2% solubilizer,
the balance being water.
A is describedThe antioxidant in phase is tocopherol acetate, said AThe emulsifier in phase is cetearyl alcohol or cetearyl glucoside, and the component A is cetearyl alcohol or cetearyl glucosideThe thickener in phase is hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer.
B isThe chelating agent in the phase is disodium EDTA, BThe preservative in the phase is methylparaben.
B isPhase sum AThe thickening agents in the phase are all carbomers.
Said DPhase B andthe pH regulator in the phase is triethanolamine.
Said EThe plant natural antioxidant antiallergic extract in the phase is a mixture of Glycyrrhiza glabra root extract, tea leaf extract, rosemary leaf extract, centella asiatica extract, chamomile flower extract, Scutellaria baicalensis root extract and Polygonum cuspidatum root extract.
Said EPhase sum CThe preservatives in the phase are both phenoxyethanol and ethylhexyl glycerol.
Said DThe solubilizer in the phase is PEG-40 hydrogenated castor oil.
The preparation method of this example is the same as example 1.
Comparative example 1:
the composition, proportion and preparation method of the raw materials of the comparison example are the same as those of the example 1, the only difference is that the example 1 is placed for at least three months, and the time of the finished product prepared by the comparison example is not more than three days before the finished product is sent to volunteers.
Comparative example 2:
the composition, proportion and preparation method of the raw materials of the comparison example are the same as those of the example 2, the only difference is that the example 2 is placed for at least three months, and the time of the finished product prepared by the comparison example is not more than three days from the time of sending the finished product to volunteers.
Comparative example 3:
the composition, proportion and preparation method of the raw materials of the comparison example are the same as those of the example 3, the only difference is that the example 3 is placed for at least three months, and the time of the finished product prepared by the comparison example is not more than three days from the time of sending the finished product to volunteers.
Effect testing
1. The characteristics are as follows: the enhanced nourishing essential oil cream component and the basic nourishing gel component prepared in examples 1-3 are both suitable in viscosity, good in ductility, fine and smooth in texture.
2. Acidity and pH test: the enhanced maintenance essential cream component, the basic moisturizing gel component and the mixture of the two prepared in examples 1-3 were tested separately using a wetted pH paper, all tested samples falling within a suitable pH of 6-7.
3. Cold and hot test: the enhanced nourishing essential oil cream component and the basic nourishing gel component prepared in the examples 1-3 are respectively filled in a transparent storage container and refrigerated in a refrigerator at 4 ℃ for about one week, and no layering phenomenon exists in the examples 1-3; the samples of examples 1 to 3 were kept in a thermostat at 55 ℃ for 24 hours without delamination and deterioration.
4. And (3) centrifugal experiment: the enhanced nourishing essential oil cream component and the basic nourishing gel component prepared in the examples 1-3 are respectively filled in a centrifugal test tube and are centrifuged at the speed of 2500r/min for 20 minutes, and no layering phenomenon exists in the examples 1-3.
5. Irritation, allergy test: the back hair of the rabbits was removed, and the enhanced nourishing essential oil cream component, the basic nourishing gel component and the mixture of the two prepared in examples 1-3 were applied, respectively, and the test result showed that the rabbits did not show irritation and allergic reaction, compared with the parts not applied with the present invention.
6. Room temperature standing experiment: the enhanced maintenance essential oil cream component and the basic moisturizing gel component prepared in the examples 1-3 are respectively filled in cosmetic bottles, standing observation is carried out at room temperature for 6 months, no layering phenomenon exists in the examples 1-3, no change exists in smell, the batch of examples 1-3 which are kept standing for 6 months are used for experiments of volunteers below, and the result proves that the effects of the examples 1-3 which are kept standing for 6 months are not obviously attenuated, and the specific detection method is shown below.
7. Comprehensive effect investigation of the invention
Considering that the female flight attendants need to go to and go from a plurality of places, skin is often in different climatic environments, and the female flight attendants need to keep a better mental state due to occupational reasons are selected as volunteers because the female flight attendants are used for coping with different skin states and different climates and the plurality of essential oil components added in the invention have the function of relieving the mental state. 90 local female flight attendants (20-50 years old) are selected as volunteers and divided into six groups, each group comprises volunteers of all age layers and various skin types (namely neutral, oily, dry, mixed and sensitive), three groups of the volunteers respectively use the just-produced control examples 1-3 (the components and the preparation method are completely the same as those of the examples 1-3, and the only difference is that the finished product is not more than three days), and the other three groups of the control examples 1-3 which are kept still for 6 months in the room-temperature standing experiment are used, and each volunteer is required to be applied to the face in the morning and evening and continuously for one month.
Before the trial starts, the hand parts of the volunteers are respectively coated with the enhanced nourishing essential oil cream component and the basic nourishing gel component prepared in the examples 1-3 and the comparative examples 1-3 and the mixture of the enhanced nourishing essential oil cream component and the basic nourishing gel component, and compared with the part which is not coated, the test result shows that no allergic reaction occurs in the volunteers.
Before beginning to try on and after trying on and detect and record each volunteer's skin type and skin state, the test instrument is: the seventh generation VISA skin tester (VISA usa), skin melanin and heme tester MX18 (CK, germany), MPA580 skin elasticity tester (CK, germany), skin moisture tester CM825 (CK, germany).
Grading standard: 5 is the highest score which shows that the skin of the volunteer is improved by more than 50 percent compared with the skin before trial; score 4 indicates that the skin of the volunteer is improved by more than 40-50% compared with the skin before trial, and score 3 indicates that the skin of the volunteer is improved by more than 30-40% compared with the skin before trial; score 2 indicates that the skin of the volunteer is improved by more than 20-30% compared with the skin before trial; score 1 indicates that the skin of the volunteer is improved by more than 10-20% compared with the skin before trial; score 0 indicates no significant improvement in the skin of the volunteer compared to before trial. The following table is the average score for each property.
Examples 1 2 3 4 5 6
Fineness of skin 4.6 4.7 4.8 4.6 4.8 4.9
Skin elasticity 4.8 4.8 4.9 4.8 4.9 4.9
Reduction of fine lines in skin 4.4 4.5 4.6 4.5 4.7 4.7
Oil control effect 4.6 4.6 4.8 4.6 4.8 4.8
As can be seen from the above tests, the present invention has the advantages of more significantly improving the skin condition of the user, making the skin tender and soft, lightening facial spots, and improving skin roughness and wrinkles. The skin of each volunteer is obviously improved, the moisturizing and maintaining effects are ideal, and the wrinkle improving effect is good.
8. Evaluation of Functionality
Evaluation was performed by the above 90 volunteers using a method of poll scoring.
Grading standard: very poor (score 1), relatively poor (score 2), slightly poor (score 3), generally (score 4), slightly good (score 5), relatively good (score 6), very good (score 7). The following is the average score for each property,
examples 1 2 3 4 5 6
Moistening and caring 6 7 7 7 7 7
Moisturizing and oil controlling device 6 6 7 6 7 7
Wrinkle removing and speckle reducing 5 5 6 6 6 7
Soothing the mind 7 7 7 7 7 7
The above embodiments do not limit the scope of the present invention, and those skilled in the art can make equivalent modifications and variations without departing from the overall concept of the present invention.

Claims (10)

1. A self-prepared two-component essence cream is characterized by comprising a basic moistening gel component and an enhanced maintenance essential oil cream component, wherein the enhanced maintenance essential oil cream component is represented by I, the basic moistening gel component is represented by II, the enhanced maintenance essential oil cream component and the basic moistening gel component are isolated from each other,
the component (I) of the essential oil cream for enhancing and maintaining is composed of the following raw materials in percentage by weight:
A0.5 to 1.5 percent of macadamia nut seed oil, 1.5 to 2.5 percent of jojoba seed oil, 0.5 to 1.5 percent of polydimethylsiloxane, 1.5 to 2.5 percent of isononyl isononanoate, 1 to 2 percent of squalane, 0.05 to 0.15 percent of antioxidant, 1.5 to 2.5 percent of emulsifier and 1 to 2 percent of thickener,
B4.5 to 5.5 percent of glycerin, 1.5 to 2.5 percent of glyceryl polyether-26, 0.5 to 1.5 percent of betaine, 0.01 to 0.1 percent of sodium hyaluronate, 0.01 to 0.1 percent of chelating agent, 12 to 13 percent of thickening agent and 0.1 to 0.15 percent of preservative,
Cphase 1-5% cyclopentasiloxane,
Dphase 0.2-0.3% of PH regulator,
E0.2-0.4% of natural antioxidant antiallergic extract of plant, 0.5-1.5% of Chondrus crispus extract, 0.5-1.5% of Ginseng radix extract, 1-2% of palmitoyl tripeptide-1, 0.05-0.15% of ethylhexyl glycerol, 0.1-0.5% of phenoxyethanol and 0.05-0.15% of colorant,
Fthe phases are 0.1 to 0.5 percent of rosemary leaf oil, 0.05 to 0.15 percent of chamomile oil,0.05-0.15% of ylang-ylang flower oil, 0.1-0.3% of sweet orange peel oil, 0.2-0.4% of lemon peel oil, 0.3-0.5% of peppermint oil, 0.1-0.3% of basil oil and 1-2% of solubilizer,
the balance of water;
wherein the basic moistening gel component (II) is prepared from the following raw materials in parts by weight:
Aphase 6-10% of glycerin, 0.3-0.6% of thickening agent,
Bphase 0.3-0.5% of PH regulator,
C0.05-0.15% of coloring agent, 0.3-0.6% of preservative,
Dphase 0.4-0.6% rose oil, 1-2% chamomile oil and 1.5-2.5% solubilizer,
the balance being water.
2. The self-dispensable two-component essence cream according to claim 1, wherein the a isThe antioxidant in phase is tocopheryl acetate.
3. The self-dispensable two-component essence cream according to claim 1, wherein the a isThe emulsifier in phase is cetearyl alcohol or cetearyl glucoside, and the A is cetearyl alcohol or cetearyl glucosideThe thickener in phase is hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer.
4. The self-dispensable two-component essence cream according to claim 1, wherein the B isThe chelating agent in the phase is disodium EDTA, BThe preservative in the phase is methylparaben.
5. The self-dispensable two-component essence cream according to claim 1, wherein the B isPhase sum AThe thickening agents in the phase are all carbomers.
6. The self-dispensable two-pack of claim 1Essence cream characterized in that DPhase B andthe pH regulator in the phase is triethanolamine.
7. The self-dispensable two-component essence cream according to claim 1, wherein E isThe plant natural antioxidant antiallergic extract in the phase is one or more of Glycyrrhiza glabra root extract, tea leaf extract, rosemary leaf extract, centella asiatica extract, chamomile flower extract, Scutellaria baicalensis root extract and Polygonum cuspidatum root extract.
8. The self-dispensable two-component essence cream according to claim 1, wherein C isThe preservative in the phase is one or a mixture of phenoxyethanol and ethylhexyl glycerin.
9. The self-dispensable two-component essence cream according to claim 1, wherein D isThe solubilizer in the phase is PEG-40 hydrogenated castor oil.
10. A method of preparing the self-dispensable two-component essence cream of claim 1, comprising the steps of:
preparation of the essential oil cream for enhancing and caring component (I)
S1: cleaning and disinfecting machine equipment;
S2: the composition according to claim 1, wherein A is aMixing and heating to 80-85 ℃ for later use;
S3: the composition according to claim 1, wherein B is in the form of a powderAdding the mixture into a main emulsifying pot, adding a proper amount of water for dissolving, stirring and heating to 80-85 ℃ to uniformly dissolve;
S4: the A is addedPhase addition of said BHomogenizing for 3-5min, emulsifying, maintaining the temperature for 3-5min, and adding CHomogenizing for 3-5 min;
S5: will S4, cooling the prepared material to 60-65 ℃, and adding the DHomogenizing properly to make it uniform;
S6: will S5 the temperature of the prepared material is reduced to 40-45 ℃, and the dispersed E is added in sequencePhase sum FMixing the mixture evenly;
S7: will S6, if the prepared material is qualified, the enhanced maintenance essential oil cream component is prepared;
preparing the basic moistening gel component (II)
S1: cleaning and disinfecting machine equipment;
S2: the composition according to claim 1, wherein A is aAdding appropriate amount of water for dissolving, mixing, heating to 80-85 deg.C, maintaining the temperature for 10min, and stirring to dissolve uniformly;
S3: will S2, cooling the prepared material to 60 ℃, and then adding the BStirring uniformly;
S4: will S3 cooling the obtained material to 45 ℃, and adding the CStirring the mixture evenly, and then adding the dispersed DAnd uniformly stirring the phases, and pumping and soaking for 5min to ensure that the materials are defoamed to be transparent, thus obtaining the basic moisturizing gel component.
CN201910988692.8A 2019-10-17 2019-10-17 Self-prepared two-component essence cream and preparation method thereof Pending CN110721101A (en)

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Application publication date: 20200124