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CN103865649A - Flavoring agent for dry flower and preparation method thereof - Google Patents

Flavoring agent for dry flower and preparation method thereof Download PDF

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Publication number
CN103865649A
CN103865649A CN201410076159.1A CN201410076159A CN103865649A CN 103865649 A CN103865649 A CN 103865649A CN 201410076159 A CN201410076159 A CN 201410076159A CN 103865649 A CN103865649 A CN 103865649A
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Prior art keywords
perfuming agent
ester compound
acrylic ester
essence
dried flower
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CN201410076159.1A
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CN103865649B (en
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陈佩英
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BEIJING YINGMAO PHARMACEUTICAL Co Ltd
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BEIJING YINGMAO PHARMACEUTICAL Co Ltd
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Abstract

The invention discloses a flavoring agent for a dry flower. The flavoring agent comprises the following components in percentage by weight: 20-50% of acrylic compounds and 2-10% of essence. The invention further discloses a preparation method which comprises the following steps: (1) grinding raw materials, and (2) uniformly mixing the powder prepared in the step (1) with the essence to obtain the finished product. The invention has the advantages that a dry flower flavoring agent is developed to make up for the blank of the special flavoring agent for the dry flower on the market, the choke point that the dry flower is flavored by only using perfume is broken through, the fragrance can be maintained and prolonged to half a year to one year; meanwhile, the dry flower is prevented from color fading, corroding, moisturizing and dust. The method for preparing the flavoring agent is simple, the complex operation flow is saved, the energy consumption is maximally reduced, and the cost is saved.

Description

A kind of perfuming agent for dried flower and preparation method thereof
Technical field
The present invention relates to the technical field of flower drying, in particular to a kind of sweetener for dried flower and preparation method thereof.
Background technology
Along with improving constantly of people's living standard, uphold nature and more and more higher to the grade of beautiful pursuit.Nowadays, increasing people at home or office space all to lay out the flowers and plants of oneself liking.But because the fresh flower fresh keeping time picking is very short, be subject to certain limitation so fresh flower uses, even if at home can water or soil build the condition of flowers and plants growth, but fresh and alive flowers and plants still have certain life cycle.So people just make dried flower by fresh flower by ways such as dehydrations, then pass through design typification processing, make the appreciation flowers that can put for a long time in various places., although beautiful outward appearance when dried flower can keep original fresh and alive state, the really fragrance of few flower, thereby affected people's liking dried flower.In order to give dried flower perfuming, be mainly to make dried flower savory by the method for perfumes on dried flower at present.But this method cost is expensive, and the fragrant time of guarantor is short, often spray, and operates also inconvenient.
Summary of the invention
In order to solve, the perfume cost adopting to dried flower perfuming in prior art is high, the fragrant short defect of time of guarantor, the invention discloses a kind of perfuming agent for dried flower, cost is low, use after this perfuming agent, make the fragrant time lengthening of guarantor of dried flower and there is fade-proof, anticorrosion, moistureproof, dustproof effect simultaneously, and then extending the duration of service of dried flower.
For achieving the above object, the technical solution used in the present invention is, a kind of perfuming agent for dried flower that the present invention develops, comprise acrylic ester compound, essence, the mass percent of each composition in perfuming agent be, acrylic ester compound 20%~50%, essence 2%~10%.Adopt acrylic ester compound to replace to fall the consumption of essence, the very thin film of layer of transparent that adopts this composition and quality proportioning to form on dried flower surface, existing employing perfume is during to dried flower perfuming, general fragrance retains 15-30 days, adopt this formula perfuming agent to dried flower perfuming, fragrance can retain half a year~mono-year.In addition also can play anti-moisture absorption, fade-proof, anti-dust suction effect to dried flower.
This perfuming agent also comprises triethyl citrate, calcium carbonate, glycerine, three kinds of compositions mass percent in perfuming agent is triethyl citrate 1%~5%, calcium carbonate 3%~10%, glycerine 10%~25%, wherein, triethyl citrate is softening agent, assist acrylic ester compound to form pliable and tough protective membrane on dried flower surface, calcium carbonate is as filler, can strengthen the physical strength of protective membrane, prevent that protective membrane from coming off in dried flower skin breakage, glycerine is softening agent, jointly assist acrylic ester compound to form pliable and tough protective membrane on dried flower surface with triethyl citrate.Adopt the quality proportioning of above-mentioned three kinds of compositions, can further make mutually for keep lasting in cost accomplish minimum.
Described acrylic ester compound is mixed and is formed by ethyl propenoate, methyl methacrylate, methacrylic acid chlorination trimethylamine groups ethyl ester, and the mass ratio of three kinds of compositions is 1:2:0.1.
Apart from the above, the invention also discloses the method for this perfuming agent of preparation, comprise the steps (1) comminuted starting materials: it is 100 object powder that acrylic ester compound is crushed to granularity;
(2) acrylic ester compound (1) step being prepared evenly mixes with essence, and the mass percent of each composition in perfuming agent be, acrylic ester compound 20%~50%, and essence 2%~10%, had both obtained perfuming agent after mixing.Starting material are ground into the powder of 100 granularities, for after finished product is prepared in combination with essence, in use, after adding ethanol, dissolve to greatest extent, and can form a kind of film at dried flower surface spreading after ejection, dried flower fragrance is maintained lastingly, can accomplish again fade-proof effect, through test, finally obtained this preparation method and be the easiest, economize the method for operating process, cost-saving most, can also play and maintain fragrance, bleed off look, rot-resistant best effect simultaneously.
In the time that perfuming agent comprises triethyl citrate, calcium carbonate, glycerine, preparation method is, (1) comminuted starting materials: it is 100 object powder that acrylic ester compound, Paris white are broken to granularity;
(2) after the powder (1) step being prepared mixes with triethyl citrate, glycerine, mix with essence again, after evenly mixing, both obtained perfuming agent, each composition is acrylic ester compound 20%~50% in the mass percent of perfuming agent, essence 2%~10%, triethyl citrate 1%~5%, calcium carbonate 3%~10%, glycerine 10%~25%.In the time that perfuming agent adds triethyl citrate, calcium carbonate, glycerine, just can obtain perfuming agent according to its preparation method.
The using method of this perfuming agent, when use, get the perfuming agent of 8 grams of left and right and pour in 100ml95% ethanol, stir and make to be uniformly dispersed, be mixed with suspension, suspension is packed in spraying equipment, evenly be sprayed on when dried flower is surperficial can form certain film, dried flower is dry under 25 DEG C of-32 DEG C of conditions, can obtain keeping permanent fragrant dried flower, this dried flower can be placed on indoor naturally, play beautify the environment, the effect of fragrant room air.
To sum up, the invention has the beneficial effects as follows, develop a kind of dried flower perfuming agent, make up the blank that is specifically designed to dried flower perfuming agent on market, broken through the bottleneck that adopts only perfume, fragrance held time extend to half a year~mono-year, can play dried flower simultaneously anticorrosion, anti-ly fade, moistureproof, dustproof effect, can make dried flower fresh and alive, lasting fragrance of color still in triennium, extend the duration of service of dried flower; The method of preparing this perfuming agent is simple, has saved complicated operating process, has reduced energy consumption to greatest extent, has saved cost.
Embodiment
Further illustrate content of the present invention below in conjunction with specific embodiment.
Embodiment mono-: a kind of perfuming agent for dried flower that the present invention develops, this perfuming agent comprises acrylic ester compound, essence, the mass percent of each composition in perfuming agent be, acrylic ester compound 20%, essence 10%.
Acrylic ester compound is mixed and is formed by ethyl propenoate, methyl methacrylate, methacrylic acid chlorination trimethylamine groups ethyl ester, and the mass ratio of three kinds of compositions is 1:2:0.1.
The acrylic compounds of above-mentioned three kinds of compositions composition also can bought finished product use on the market, and this name of product is EudragitRS100, and manufacturer is German Romo Co.,Ltd.
The method of preparing this perfuming agent, comprises the steps, (1) comminuted starting materials: it is 100 object powder that acrylic ester compound is crushed to granularity;
(2) acrylic ester compound (1) step being prepared evenly mixes with essence, and the mass percent of each composition in perfuming agent be, acrylic ester compound 20%, and essence 10%, had both obtained perfuming agent after mixing.Specified otherwise in addition not in preparation method below, condition is all to produce under room temperature condition, condition of normal pressure.
The using method of this perfuming agent, when use, get 8 grams of perfuming agents and pour in 95% ethanol of 100ml, stir and make to be uniformly dispersed, be mixed with suspension, suspension is packed in spraying equipment, evenly be sprayed on when dried flower is surperficial can form certain film, dried flower is dry under 25 DEG C of-32 DEG C of conditions, can obtain keeping permanent fragrant dried flower, this dried flower can be placed on indoor naturally, play beautify the environment, the effect of fragrant room air.
Below to adopt perfuming agent of the present invention to process and the contrast effect of existing perfume to dried flower processing dried flower:
Figure 615307DEST_PATH_IMAGE001
Embodiment bis-: a kind of perfuming agent for dried flower that the present invention develops, comprise acrylic ester compound, essence, the mass percent of each composition in perfuming agent be, acrylic ester compound 50%, essence 5%.
Perfuming agent also comprises triethyl citrate, calcium carbonate, glycerine, and three kinds of compositions mass percent in perfuming agent is triethyl citrate 1%, calcium carbonate 3%, glycerine 10%.
Acrylic ester compound is mixed and is formed by ethyl propenoate, methyl methacrylate, methacrylic acid chlorination trimethylamine groups ethyl ester, and the mass ratio of three kinds of compositions is 1:2:0.1.
The method of preparing perfuming agent of the present invention is, preparation method is, (1) comminuted starting materials: it is 100 object powder that acrylic ester compound, Paris white are broken to granularity;
(2) after the powder (1) step being prepared mixes with triethyl citrate, glycerine, mix with essence again, after evenly mixing, both obtained perfuming agent, each composition is acrylic ester compound 50% in the mass percent of perfuming agent, essence 5%, triethyl citrate 1%, calcium carbonate 3%, glycerine 10%.
Below to adopt perfuming agent of the present invention to process and the contrast effect of existing perfume to dried flower processing dried flower:
Figure 367362DEST_PATH_IMAGE002
Embodiment tri-: a kind of perfuming agent for dried flower that the present invention develops, comprise acrylic ester compound, essence, the mass percent of each composition in perfuming agent be, acrylic ester compound 25%, essence 2%.
Perfuming agent also comprises triethyl citrate, calcium carbonate, glycerine, and three kinds of compositions mass percent in perfuming agent is triethyl citrate 5%, calcium carbonate 10%, glycerine 25%.
Acrylic ester compound is mixed and is formed by ethyl propenoate, methyl methacrylate, methacrylic acid chlorination trimethylamine groups ethyl ester, and the mass ratio of three kinds of compositions is 1:2:0.1.
Preparation method is with embodiment bis-.
Below to adopt perfuming agent of the present invention to process and the contrast effect of existing perfume to dried flower processing dried flower:
Embodiment tetra-: a kind of perfuming agent for dried flower that the present invention develops, comprise acrylic ester compound, essence, the mass percent of each composition in perfuming agent be, acrylic ester compound 40%, essence 8%.
Perfuming agent also comprises triethyl citrate, calcium carbonate, glycerine, and three kinds of compositions mass percent in perfuming agent is triethyl citrate 3%, calcium carbonate 5%, glycerine 12%.
Acrylic ester compound is mixed and is formed by ethyl propenoate, methyl methacrylate, methacrylic acid chlorination trimethylamine groups ethyl ester, and the mass ratio of three kinds of compositions is 1:2:0.1.
Preparation method is with embodiment bis-.
Below to adopt perfuming agent of the present invention to process and the contrast effect of existing perfume to dried flower processing dried flower:
Figure 394541DEST_PATH_IMAGE002
Technique scheme has only embodied the optimal technical scheme of technical solution of the present invention, and those skilled in the art have all embodied principle of the present invention to some variations that wherein some part may be made, within belonging to protection scope of the present invention.

Claims (6)

1. for a perfuming agent for dried flower, it is characterized in that, this perfuming agent comprises acrylic ester compound, essence, and the mass percent of each composition in perfuming agent be, acrylic ester compound 20%~50%, essence 2%~10%.
2. according to claim 1 for the perfuming agent of dried flower, it is characterized in that, perfuming agent comprises triethyl citrate, calcium carbonate, glycerine, and three kinds of compositions mass percent in perfuming agent is triethyl citrate 1%~5%, calcium carbonate 3%~10%, glycerine 10%~25%.
3. according to claim 1 for the perfuming agent of dried flower, it is characterized in that, acrylic ester compound is mixed and is formed by ethyl propenoate, methyl methacrylate, methacrylic acid chlorination trimethylamine groups ethyl ester, and the mass ratio of three kinds of compositions is 1:2:0.1.
4. a method of preparing perfuming agent described in claim 1, is characterized in that, the method comprises the steps, (1) comminuted starting materials: it is 100 object powder that acrylic ester compound is crushed to granularity;
(2) acrylic ester compound (1) step being prepared evenly mixes with essence, and the mass percent of each composition in perfuming agent be, acrylic ester compound 20%~50%, and essence 2%~10%, obtains perfuming agent after mixing.
5. prepare according to claim 4 the method for perfuming agent, it is characterized in that, in the time that perfuming agent comprises triethyl citrate, calcium carbonate, glycerine, preparation method is, (1) comminuted starting materials: it is 100 object powder that acrylic ester compound, Paris white are broken to granularity;
(2) after the powder (1) step being prepared mixes with triethyl citrate, glycerine, mix with essence again, after evenly mixing, both obtained perfuming agent, each composition is acrylic ester compound 20%~50% in the mass percent of perfuming agent, essence 2%~10%, triethyl citrate 1%~5%, calcium carbonate 3%~10%, glycerine 10%~25%.
6. according to the method for preparing perfuming agent described in claim 4 or 5, it is characterized in that, acrylic ester compound is mixed and is formed by ethyl propenoate, methyl methacrylate, methacrylic acid chlorination trimethylamine groups ethyl ester, and the mass ratio of three kinds of compositions is 1:2:0.1.
CN201410076159.1A 2014-03-04 2014-03-04 A kind of perfuming agent for dried flower and preparation method thereof Active CN103865649B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107372474A (en) * 2017-08-16 2017-11-24 河南科技学院 A kind of dried flower color preserving agent, preparation method and color-retention method
CN112472859A (en) * 2020-12-08 2021-03-12 华东理工大学 Fragrance aromatherapy candle with twelve fragrances and lasting fragrance

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1784210A (en) * 2003-05-07 2006-06-07 弗门尼舍有限公司 Sprayable perfume with an improved tenacity
FR2902655A1 (en) * 2006-06-23 2007-12-28 Oreal Topical cosmetic composition with long-lasting skin cooling and refreshing effect, comprises cooling agent and film-forming polymer in aqueous alcohol
CN101679914A (en) * 2007-06-01 2010-03-24 可泰克斯有限合伙公司 Method for formulating odoriferous active ingredients in order to protect same and to increase the persistence thereof
CN102395423A (en) * 2009-04-17 2012-03-28 巴斯夫欧洲公司 Carrier system for fragrances

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1784210A (en) * 2003-05-07 2006-06-07 弗门尼舍有限公司 Sprayable perfume with an improved tenacity
FR2902655A1 (en) * 2006-06-23 2007-12-28 Oreal Topical cosmetic composition with long-lasting skin cooling and refreshing effect, comprises cooling agent and film-forming polymer in aqueous alcohol
CN101679914A (en) * 2007-06-01 2010-03-24 可泰克斯有限合伙公司 Method for formulating odoriferous active ingredients in order to protect same and to increase the persistence thereof
CN102395423A (en) * 2009-04-17 2012-03-28 巴斯夫欧洲公司 Carrier system for fragrances

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107372474A (en) * 2017-08-16 2017-11-24 河南科技学院 A kind of dried flower color preserving agent, preparation method and color-retention method
CN112472859A (en) * 2020-12-08 2021-03-12 华东理工大学 Fragrance aromatherapy candle with twelve fragrances and lasting fragrance

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