CN103553772A - Compound preparation for nursing tapping panel dryness and strip ulcer of rubber trees, as well as preparation method and application thereof - Google Patents
Compound preparation for nursing tapping panel dryness and strip ulcer of rubber trees, as well as preparation method and application thereof Download PDFInfo
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Abstract
The invention relates to a compound preparation for nursing tapping panel dryness and strip ulcer of rubber trees. The preparation is prepared from the following components in percentage by weight: 1-50 percent of calcium peroxide, 10-70 percent of hydrogen peroxide, 1-10 percent of monopotassium phosphate, 4-10 percent of citric acid, 1-3 percent of diethyl aminoethyl hexanoate, 1-2 percent of glacial acetic acid, 1-3 percent of prochloraz, 2-4 percent of tween 80, 0.3-2 percent of copper sulfate, 0.3-2 percent of zinc sulfate, 0.3-2 percent of magnesium sulfate, 0.5-4 percent of ammonium molybdate, 0.1-2 percent of chitosan, 0.5-2 percent of polyvinyl alcohol, 0.5-2 percent of sodium lignin sulfonate, 0.5-4 percent of boric acid, 1-2 percent of moroxydine, and the balance of pharmaceutically acceptable carriers. The invention also relates to a preparation method and an application of the compound preparation. The compound preparation is easy to prepare, the tapping panel dryness and strip ulcer of rubber trees can be effectively treated.
Description
Technical field
The present invention relates to rubber tree cultivation and prevention and control of plant diseases, pest control field, specifically, the present invention relates to a kind of for taking good care of the dead skin disease of rubber tree and compound formulation of face Phytophthora spp and its preparation method and application.
Background technology
China's natural rubber place of production is mainly distributed in Hainan Province and Yunnan Province, due to factors such as weather, geographical conditions, rubber tapping technology, cause the 20%-30% of China's rubber tree total amount in dead skin state, normal binder removal, Rubber Yield declines year by year, has had a strong impact on the development of China's caoutchouc industry.
The same iron and steel of natural rubber, oil, coal together and be called four large industrial raw material, are basic industry and the strategic materials that involve the interests of the state and the people.As one of the world's four large industrial raw material, natural rubber is widely used in aspects such as industry, agricultural, national defence, communications and transportation, machinofacture, medical and health and daily lifes because having very strong elasticity, good insulativity, plasticity-, wear resistance, resistance to drawing property, water proof gas barrier properties etc., becomes one of indispensable material in national defence and industry.Rubber yielding plant in the world has kind more than 2000, but at present by establishing in large scale and become natural rubber unique commercial source, is Para rubber tree.But the harm that rubber tree " dead skin disease " is caused to ruber plantation is extremely serious, it is one of main limiting factor of natural rubber per unit area yield raising.According to latest survey, no matter Hainan Land Reclamation region, or reclamation area, Yunnan, rubber tree dead skin rate average out to 25% left and right.More seriously, in recent years dead skin tree also with 1% speed cumulative year after year.
Rubber tree " dead skin disease " (sometimes also referred to as face Phytophthora spp) is divided into two types of (Jacob JL, Prevot JC, Lacrotte is panel dryness in Hevea brasiliensis.Plantations R.1994.Tapping, Recherche, Development, 1 (3): 15-24.): gangrenosum acne " dead skin disease " and non-gangrenosum acne " dead skin disease ".Gangrenosum acne " dead skin disease " is called again " trunk phloem necorsis " (Trunk Phloem Necrosis, TPN), it is characterized in that latex dust and surrounding tissue thereof are old and feeble, brownization of endothelium, this symptom can rapid spread to whole face, when serious, extend to the non-face on opposite.Just just there will be gangrenosum acne " dead skin disease " in rubber tapping treelet soon, even in the treelet of not rubber tapping, also there is generation.This dead skin is irreversible, because the bark of regeneration is ill too.Someone thinks, gangrenosum acne " dead skin disease " is by pathogenic bacteria or cyanogen is poisoning causes that (tropical crops is studied, (4): 43-48) for Fan Siwei, the cause of disease of the few fine jade .1994. rubber tree dead skin of poplar and the hypothesis of relevant dead skin.The type " dead skin disease " occurs seldom, to producing, does not constitute a threat to.Non-gangrenosum acne " dead skin disease " is called again " face is dry sick " (Tapeing Panel Dryness, TPD), be now acknowledged as and a kind ofly by injury (rubber tapping) and ethene, stimulated (the generally well stimulation of employing on existing production) physiology syndromes that cause, complexity.The feature of non-gangrenosum acne TPD is that histology, the cytology variation of bark is less, but latex dust metabolism disorder is serious, during sick sending out, and rubber tree secant part or all latex dusts obstructions, binder removal amount greatly reduces not even binder removal.This TPD is reversible, as long as allow rubber tree rest and reorganize about 1 year, rubber tree just can rehabilitation.But the generation of this dead skin is very general, to producing, constitute a serious threat, the rubber tree dead skin carried in the industry just refers to this dead skin.Every the international rubber research and development council of 2-3Nian (IRRDB), just hold a dead skin symposium, that focus on is just non-gangrenosum acne TPD.
Chinese patent ZL93107276.X discloses a kind of manufacture method for the treatment of vegetable rubber tree dead skin revivifier, and multiple herbal medicine is processed, dried, grinding and part liquor, mix and blend, propagandizes the quantitative package of sieving after (burying) hotly.Brown type, outer brown type, stable form, Phytophthora spp, mycosis, lines parasitosis, virus disease (containing diseases such as class gram Ci Shi bodies) in medicinal powder treatment intractable rubber tree dead skin, 1-15 is prolonged stops cutting the diseases such as rubber tree dead skin of not producing glue special curative effect, coat medicinal powder of the present invention once, after 3-12 month, just can open to cut and bring back to life rubber tree production glue.
Application number is that 97121908.7 Chinese patent application discloses a kind of preventing and treating chemical for brown spot of rubber tree, and it is mainly comprised of tetracyclines (chloramphenicol), methylcellulose gum, xanthan gum etc.Applicable painting imposes on the disease tree face of brown spot of rubber tree, can effectively prevent and treat brown spot of rubber tree, and can make rubber trunk glue output volume increase 14.27%, and cost and benefit ratio are 1:4.53-6.23.
Summary of the invention
The object of the present invention is to provide a kind of for taking good care of the dead skin disease of rubber tree and the compound formulation of face Phytophthora spp.
The present invention also aims to provide preparation method's application of this compound formulation.
In order to realize object of the present invention, the invention provides a kind of for taking good care of the dead skin disease of rubber tree and the compound formulation of face Phytophthora spp, the calcium peroxide of the material that comprises following weight percentage: 1%-50%, the hydrogen peroxide of 10-70%, the potassium primary phosphate of 1-10%, the Citric Acid of 4-10%, the amine DA-6 of 1-3%, the Glacial acetic acid of 1-2%, the prochloraz of 1-3%, the tween 80 of 2-4%, the copper sulfate of 0.3%-2%, the zinc sulfate of 0.3%-2%, the sal epsom of 0.3%-2%, the ammonium molybdate of 0.5%-4%, the chitosan of 0.1%-2%, the polyvinyl alcohol of 0.5%-2%, the sodium lignosulfonate of 0.5%-2%, the boric acid of 0.5%-4%, the Moroxydine of 1%-2%, surplus is pharmaceutically acceptable carrier.
Preferably, the material that comprises following weight percentage for taking good care of the dead skin disease of rubber tree and the compound formulation of face Phytophthora spp of the present invention: the calcium peroxide of 1%-50%, the hydrogen peroxide of 10-80%, the potassium primary phosphate of 1-10%, the Citric Acid of 4-10%, the amine DA-6 of 1-3%, the Glacial acetic acid of 1-2%, the prochloraz of 1-3%, the tween 80 of 2-4%, the copper sulfate of 0.3%-2%, the zinc sulfate of 0.3%-2%, the sal epsom of 0.3%-2%, the ammonium molybdate of 0.5%-4%, the chitosan of 0.1%-2%, the polyvinyl alcohol of 0.5%-2%, the sodium lignosulfonate of 0.5%-2%, the boric acid of 0.5%-4%, the Moroxydine of 1%-2%, surplus is pharmaceutically acceptable carrier.
More preferably, the material that comprises following weight percentage for taking good care of the dead skin disease of rubber tree and the compound formulation of face Phytophthora spp of the present invention: 20% calcium peroxide, 40% hydrogen peroxide, 5% potassium primary phosphate, 5% Citric Acid, 2% amine DA-6, 1% Glacial acetic acid, 1% prochloraz, 3% tween 80, 1% copper sulfate, 1% zinc sulfate, 1% sal epsom, 2% ammonium molybdate, 1% chitosan, 1% polyvinyl alcohol, 1% sodium lignosulfonate, 2% boric acid, 1% Moroxydine, surplus is pharmaceutically acceptable carrier.
Most preferably, described compound formulation can be aqua, pulvis or sprays.
It is a kind of for taking good care of the preparation method of the dead skin disease of rubber tree and the compound formulation of face Phytophthora spp that the present invention also provides, the method comprises the following steps: the calcium peroxide of 1%-50%, the hydrogen peroxide of 10-70%, the potassium primary phosphate of 1-10%, the Citric Acid of 4-10%, the amine DA-6 of 1-3%, the Glacial acetic acid of 1-2%, the prochloraz of 1-3%, the tween 80 of 2-4%, the copper sulfate of 0.3%-2%, the zinc sulfate of 0.3%-2%, the sal epsom of 0.3%-2%, the ammonium molybdate of 0.5%-4%, the chitosan of 0.1%-2%, the polyvinyl alcohol of 0.5%-2%, the sodium lignosulfonate of 0.5%-2%, the boric acid of 0.5%-4%, the Moroxydine of 1%-2% and the water of surplus add in reactor, stir, staticly settle, filling, bottling, encapsulate and get final product.
The present invention also provides compound formulation in the application for the preparation of taking good care of in the dead skin disease of rubber tree and the preparation of face Phytophthora spp, the calcium peroxide of the material that described compound formulation comprises following weight percentage: 1%-50%, the hydrogen peroxide of 10-70%, the potassium primary phosphate of 1-10%, the Citric Acid of 4-10%, the amine DA-6 of 1-3%, the Glacial acetic acid of 1-2%, the prochloraz of 1-3%, the tween 80 of 2-4%, the copper sulfate of 0.3%-2%, the zinc sulfate of 0.3%-2%, the sal epsom of 0.3%-2%, the ammonium molybdate of 0.5%-4%, the chitosan of 0.1%-2%, the polyvinyl alcohol of 0.5%-2%, the sodium lignosulfonate of 0.5%-2%, the boric acid of 0.5%-4%, the Moroxydine of 1%-2%, surplus is pharmaceutically acceptable carrier.
Preferably, the calcium peroxide of the material that described compound formulation comprises following weight percentage: 1%-50%, the hydrogen peroxide of 10-80%, the potassium primary phosphate of 1-10%, the Citric Acid of 4-10%, the amine DA-6 of 1-3%, the Glacial acetic acid of 1-2%, the prochloraz of 1-3%, the tween 80 of 2-4%, the copper sulfate of 0.3%-2%, the zinc sulfate of 0.3%-2%, the sal epsom of 0.3%-2%, the ammonium molybdate of 0.5%-4%, the chitosan of 0.1%-2%, the polyvinyl alcohol of 0.5%-2%, the sodium lignosulfonate of 0.5%-2%, the boric acid of 0.5%-4%, the Moroxydine of 1%-2%, surplus is pharmaceutically acceptable carrier.
More preferably, the material that described compound formulation comprises following weight percentage: 20% calcium peroxide, 40% hydrogen peroxide, 5% potassium primary phosphate, 5% Citric Acid, 2% amine DA-6,1% Glacial acetic acid, 1% prochloraz, 3% tween 80,1% copper sulfate, 1% zinc sulfate, 1% sal epsom, 2% ammonium molybdate, 1% chitosan, 1% polyvinyl alcohol, 1% sodium lignosulfonate, 2% boric acid, 1% Moroxydine, surplus is pharmaceutically acceptable carrier.
It should be noted that unless otherwise indicated, is the aqueous hydrogen peroxide solution of 42 % by weight otherwise hydrogen peroxide used herein all refers to concentration.
The present invention has solved the technical barrier of the current Tapping Panel Dryness Symptom in Hevea of China and face Phytophthora spp well.The technical program, since Hainan Province and Yunnan Province's enforcement, has reached promising result: the recovery rate of dead skin disease and Phytophthora spp tree reaches more than 90%, and by digital proof, the present invention is at present domestic and international more satisfactory practical new technology.Technique will bring huge economic benefit after popularizing in an all-round way for Rubber Industry.
Embodiment
Below the invention will be further described for the description by embodiment, but this is not limitation of the present invention, those skilled in the art are according to basic thought of the present invention, can make various modifications or improvement, but only otherwise depart from basic thought of the present invention, all within the scope of the present invention.
The preparation of embodiment 1 compound formulation of the present invention
The formula rate of the compound formulation in the present embodiment is as follows: 20% calcium peroxide, 40% hydrogen peroxide, 5% potassium primary phosphate, 5% Citric Acid, 2% amine DA-6 (purchased from Shaanxi Kang Ze Chemical Industry Science Co., Ltd), 1% Glacial acetic acid, 1% prochloraz, 3% tween 80,1% copper sulfate, 1% zinc sulfate, 1% sal epsom, 2% ammonium molybdate, 1% chitosan, 1% polyvinyl alcohol, 1% sodium lignosulfonate, 2% boric acid, 1% Moroxydine, surplus is water.
Take the calcium peroxide of 20 kilograms, and take other compositions according to aforementioned proportion, then add in reactor, stir, staticly settle, filling, bottling, encapsulates and get final product.
The preparation of embodiment 2 compound formulations of the present invention
According to the mode identical with embodiment 1, prepare compound formulation, difference is not use calcium peroxide.
The preparation of embodiment 3 compound formulations of the present invention
According to the mode identical with embodiment 1, prepare compound formulation, difference is not use hydrogen peroxide.
The preparation of embodiment 4 compound formulations of the present invention
According to the mode identical with embodiment 1, prepare compound formulation, difference is not use amine DA-6.
The preparation of embodiment 5 compound formulations of the present invention
According to the mode identical with embodiment 1, prepare compound formulation, difference is not use sodium lignosulfonate.
The preparation of embodiment 6 compound formulations of the present invention
According to the mode identical with embodiment 1, prepare compound formulation, difference is not use Moroxydine.
The preparation of embodiment 7 compound formulations of the present invention
According to the mode identical with embodiment 1, prepare compound formulation, difference is not use Citric Acid.
The preparation of embodiment 8 compound formulations of the present invention
According to the mode identical with embodiment 1, prepare compound formulation, difference is to replace calcium peroxide with the hydrogen peroxide of identical weight.
Experimental example 1
By following standard, judge dead skin disease: the local or whole binder removal not of rubber tree secant, when serious, bark produces the symptom of brown spot, speckle, bark explosion and face deformation.And typical case is attended by the appearance of brown spot and speckle.And using the standard that above-mentioned transference cure cures as dead skin disease.
Get the ill rubber tree of 180 strain, be divided into 9 groups, every group of 20 strains.Control group is used brush to smear ethrel paste (2g/ strain) at gum face.Seven days once, smears continuously 49 days.
Before using the sample of embodiment 1-8, remove the Lao Pi of rubber tree, the trunk of ill rubber tree is sprayed.For every strain rubber tree, get 150 milliliters, corresponding sample, add 350 ml waters and dilute, then spray.Sample 1-8 sprays respectively the ill rubber tree of 20 strain.Seven days once, smears continuously 49 days.It should be noted that, for convenience's sake, above-mentioned sample 1-8 is directly preparation before use.
Above-mentioned all ill rubber trees all grow in same rubber plantation.Result is as follows.
For the ill rubber tree of smearing ethrel paste, curative ratio only reaches 20%, and for the situation of using sample 1, ill rubber tree is all cured, and this shows using the situation of the superoxide of low levels also can treat ill rubber tree.Therefore superoxide often has certain corrodibility, can damage operator, and this is significant in actual applications.
For the sample of embodiment 2 and 3, curative ratio reaches respectively 71% and 74%.For the sample of embodiment 4-6, curative ratio reaches respectively 84%, 88%, 91%, and ironically, for the sample of embodiment 7, ill rubber tree is also all cured unexpectedly.For the sample of embodiment 8, curative ratio is 90%.
Claims (8)
1. one kind for taking good care of the dead skin disease of rubber tree and the compound formulation of face Phytophthora spp, it is characterized in that, the calcium peroxide of the material that comprises following weight percentage: 1%-50%, the hydrogen peroxide of 10-70%, the potassium primary phosphate of 1-10%, the Citric Acid of 4-10%, the amine DA-6 of 1-3%, the Glacial acetic acid of 1-2%, the prochloraz of 1-3%, the tween 80 of 2-4%, the copper sulfate of 0.3%-2%, the zinc sulfate of 0.3%-2%, the sal epsom of 0.3%-2%, the ammonium molybdate of 0.5%-4%, the chitosan of 0.1%-2%, the polyvinyl alcohol of 0.5%-2%, the sodium lignosulfonate of 0.5%-2%, the boric acid of 0.5%-4%, the Moroxydine of 1%-2%, surplus is pharmaceutically acceptable carrier.
2. according to claim 1 for taking good care of the dead skin disease of rubber tree and the compound formulation of face Phytophthora spp, it is characterized in that, the calcium peroxide of the material that comprises following weight percentage: 1%-50%, the hydrogen peroxide of 10-80%, the potassium primary phosphate of 1-10%, the Citric Acid of 4-10%, the amine DA-6 of 1-3%, the Glacial acetic acid of 1-2%, the prochloraz of 1-3%, the tween 80 of 2-4%, the copper sulfate of 0.3%-2%, the zinc sulfate of 0.3%-2%, the sal epsom of 0.3%-2%, the ammonium molybdate of 0.5%-4%, the chitosan of 0.1%-2%, the polyvinyl alcohol of 0.5%-2%, the sodium lignosulfonate of 0.5%-2%, the boric acid of 0.5%-4%, the Moroxydine of 1%-2%, surplus is pharmaceutically acceptable carrier.
3. according to claim 2 for taking good care of the dead skin disease of rubber tree and the compound formulation of face Phytophthora spp, it is characterized in that, the material that comprises following weight percentage: 20% calcium peroxide, 40% hydrogen peroxide, 5% potassium primary phosphate, 5% Citric Acid, 2% amine DA-6, 1% Glacial acetic acid, 1% prochloraz, 3% tween 80, 1% copper sulfate, 1% zinc sulfate, 1% sal epsom, 2% ammonium molybdate, 1% chitosan, 1% polyvinyl alcohol, 1% sodium lignosulfonate, 2% boric acid, 1% Moroxydine, surplus is pharmaceutically acceptable carrier.
According to described in any one in claims 1 to 3 for taking good care of the dead skin disease of rubber tree and the compound formulation of face Phytophthora spp, it is characterized in that described compound formulation
canfor aqua, pulvis or sprays.
5. one kind for taking good care of the preparation method of the dead skin disease of rubber tree and the compound formulation of face Phytophthora spp, the method comprises the following steps: the calcium peroxide of 1%-50%, the hydrogen peroxide of 10-70%, the potassium primary phosphate of 1-10%, the structure rafter acid of 4-10%, the amine DA-6 of 1-3%, the Glacial acetic acid of 1-2%, the prochloraz of 1-3%, the tween 80 of 2-4%, the copper sulfate of 0.3%-2%, the zinc sulfate of 0.3%-2%, the sal epsom of 0.3%-2%, the ammonium molybdate of 0.5%-4%, the chitosan of 0.1%-2%, the polyvinyl alcohol of 0.5%-2%, the sodium lignosulfonate of 0.5%-2%, the boric acid of 0.5%-4%, the Moroxydine of 1%-2% and the water of surplus add in reactor, stir, staticly settle, filling, bottling, encapsulate and get final product.
6. compound formulation is in the application for the preparation of taking good care of in the dead skin disease of rubber tree and the preparation of face Phytophthora spp, it is characterized in that, the calcium peroxide of the material that described compound formulation comprises following weight percentage: 1%-50%, the hydrogen peroxide of 10-70%, the potassium primary phosphate of 1-10%, the Citric Acid of 4-10%, the amine DA-6 of 1-3%, the Glacial acetic acid of 1-2%, the prochloraz of 1-3%, the tween 80 of 2-4%, the copper sulfate of 0.3%-2%, the zinc sulfate of 0.3%-2%, the sal epsom of 0.3%-2%, the ammonium molybdate of 0.5%-4%, the chitosan of 0.1%-2%, the polyvinyl alcohol of 0.5%-2%, the sodium lignosulfonate of 0.5%-2%, the boric acid of 0.5%-4%, the Moroxydine of 1%-2%, surplus is pharmaceutically acceptable carrier.
7. application according to claim 6, it is characterized in that, the calcium peroxide of the material that comprises following weight percentage: 1%-50%, the hydrogen peroxide of 10-80%, the potassium primary phosphate of 1-10%, the Citric Acid of 4-10%, the amine DA-6 of 1-3%, the Glacial acetic acid of 1-2%, the prochloraz of 1-3%, the tween 80 of 2-4%, the copper sulfate of 0.3%-2%, the zinc sulfate of 0.3%-2%, the sal epsom of 0.3%-2%, the ammonium molybdate of 0.5%-4%, the chitosan of 0.1%-2%, the polyvinyl alcohol of 0.5%-2%, the sodium lignosulfonate of 0.5%-2%, the boric acid of 0.5%-4%, the Moroxydine of 1%-2%, surplus is pharmaceutically acceptable carrier.
8. application according to claim 7, it is characterized in that, the material that comprises following weight percentage: 20% calcium peroxide, 40% hydrogen peroxide, 5% potassium primary phosphate, 5% Citric Acid, 2% amine DA-6,1% Glacial acetic acid, 1% prochloraz, 3% tween 80,1% copper sulfate, 1% zinc sulfate, 1% sal epsom, 2% ammonium molybdate, 1% chitosan, 1% polyvinyl alcohol, 1% sodium lignosulfonate, 2% boric acid, 1% Moroxydine, surplus is pharmaceutically acceptable carrier.
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| CN104003810A (en) * | 2014-03-28 | 2014-08-27 | 中国热带农业科学院橡胶研究所 | Rubber tree dead skin prevention and cure smearing agent and preparing method for rubber tree dead skin prevention and cure smearing agent |
| CN104430546A (en) * | 2014-12-09 | 2015-03-25 | 陈干忠 | High-yield disease-resistant and mothproof composite preparation for rubber trees as well as preparation method and application thereof |
| WO2022098227A1 (en) * | 2020-11-09 | 2022-05-12 | Palaniappan Kavitha | Compositions for treatment or rehabilitation of rubber trees |
| CN115281186A (en) * | 2022-08-06 | 2022-11-04 | 贵州大学 | Smearing preparation for preventing and treating kiwifruit canker and preparation method thereof |
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| CN104430546B (en) * | 2014-12-09 | 2017-04-19 | 陈干忠 | High-yield disease-resistant and mothproof composite preparation for rubber trees as well as preparation method and application thereof |
| WO2022098227A1 (en) * | 2020-11-09 | 2022-05-12 | Palaniappan Kavitha | Compositions for treatment or rehabilitation of rubber trees |
| CN115281186A (en) * | 2022-08-06 | 2022-11-04 | 贵州大学 | Smearing preparation for preventing and treating kiwifruit canker and preparation method thereof |
| CN115281186B (en) * | 2022-08-06 | 2023-06-27 | 贵州大学 | Smearing preparation for preventing and treating kiwi fruit canker and preparation method thereof |
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