CN103274791B - Compound fertilizer for radix angelicae and radix bupleuri - Google Patents
Compound fertilizer for radix angelicae and radix bupleuri Download PDFInfo
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- CN103274791B CN103274791B CN201310214161.6A CN201310214161A CN103274791B CN 103274791 B CN103274791 B CN 103274791B CN 201310214161 A CN201310214161 A CN 201310214161A CN 103274791 B CN103274791 B CN 103274791B
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Abstract
The invention provides a compound fertilizer for radix angelicae and radix bupleuri. The compound fertilizer is prepared by comprising the following steps of: selecting multiple organic fertilizers of plant ash, pig manure, saw dust, straw, corn flour, soybean cakes and the like; fermenting so as to kill pathogenic bacteria and promote partial organisms to decompose to improve the fertilizer effects; combining and utilizing various substances of sea algae extracts and formulas so as to lower the premature seeding rate of radix angelicae and improve the content of imperatorin in radix angelicae and saponin a, d in radix bupleuri; regulating the carbon nitrogen ratio by a certain amount of nitrogenous fertilizers, phosphatic fertilizers and potash fertilizers, thereby obtaining a special nutritious compound fertilizer for culturing radix angelicae and radix bupleuri three-dimensionally. The compound fertilizer designed by the invention can meet the differences of different nutrition requirements and different growth seasons of radix angelicae and radix bupleuri purposefully, improves the medicinal material quality, and has obvious economical benefit. The compound fertilizer for radix angelicae and radix bupleuri provided by the invention is the special nutritious compound fertilizer for culturing radix angelicae and radix bupleuri three-dimensionally, and can be used for lowering the premature seeding rate of radix angelicae, improving the content of imperatorin in radix angelicae and saponin a, d in radix bupleuri, and improving the medicinal material quality of radix angelicae and radix bupleuri.
Description
Technical field
The present invention relates to a kind of composite fertilizer, particularly relate to a kind of composite fertilizer being applicable to the root of Dahurain angelica and radix bupleuri.
Background technology
The root of Dahurain angelica is umbelliferae per nnial herb, is used as medicine with root, containing more than 10 kinds of coumarin kind compounds.The root of Dahurain angelica is warm in nature, taste is pungent, has the function of dispersing wind and cold, eliminating dampness, apocenosis, pain relieving.For diseases such as common cold caused by wind-cold, headache, rhinitis, toothache.Root of Dahurain angelica absorption ability of nutrient is strong, is the fertile crop of happiness.Execute different types of fertilizer, root of Dahurain angelica seed output and quality is had a significant impact.Current people, when the cultivating and growing root of Dahurain angelica, generally adopt composite fertilizer, urea are main fertilizer, substantially can meet the nutritional needs of the root of Dahurain angelica, makes its normal growth, but do not make significant difference to its quality of medicinal material (as active constituent content in the root of Dahurain angelica).
Radix bupleuri is umbelliferae per nnial herb, is used as medicine with root, in having and inducing sweat, soothing the liver, effect of rising sun, for the disease such as cold, fever, alternate attacks of chills and fever.The supply of radix bupleuri depends on wild resource for a long time, but excessive to excavate, the shortage of sfgd., cause radix bupleuri wild resource seriously deficient, plantation radix bupleuri compensate for the deficiency of resource, but in implementation process, there is many urgent problems.If the quality (as active constituent content in radix bupleuri) being improved radix bupleuri by fertilising is the difficult problem requiring study at present and solve.
Summary of the invention
The invention reside in and a kind of composite fertilizer being applicable to the root of Dahurain angelica and radix bupleuri is provided, have employed the organic matters such as stalk, Semen Maydis powder, soybean cake, fertilizer efficiency can be improved; The premature bolting rate of the root of Dahurain angelica can be reduced simultaneously, improve the content of saponin(e a, d in root of Dahurain angelica Imperatorin and radix bupleuri, improve the quality of the root of Dahurain angelica and Radix Bupleuri.
The present invention is by being achieved through the following technical solutions:
Being applicable to a composite fertilizer for the root of Dahurain angelica and radix bupleuri, is be made up of the raw material of following weight proportion: plant ash 220-260 part, cow dung 110-130 part, sawdust 150-200 part, stalk 200-260 part, Semen Maydis powder 80-110 part, soybean cake 280-330 part, attapulgite 40-70 part, wilkinite 35-60 part, zeolite 105-145 part, Sodium salts humic acids 50-90 part, chicken manure 70-100 part, composite trace element 10-30 part, Seaweed Extract 130-180 part, human excrement 250-400 part, urea 150-200 part, double superhosphate 110-140 part, Repone K 180-220 part.
In described composite trace element, the weight ratio of each component is borax: copper sulfate: manganous sulfate: Sodium orthomolybdate: zinc sulfate=1:(2.3-4.5): (0.6-1.1): (0.3-0.9): (1.9-2.8);
Described Seaweed Extract obtains by the following method:
Get dry marine alga to pulverize, add the water of 3-6 times of weight again, regulate pH to 9.3-9.9 with diluted sodium hydroxide solution, soak 5-8 hour, then regulate pH to 6.2-7.1 with dilute hydrochloric acid, then concentrate and obtain the concentrated solution that relative density is 1.4-1.5, the volume fraction adding 9-12 times of concentrated solution weight is the ethanol of 80%, then adds the diatomite of 1.3-2.1 times of concentrated solution quality, stirs 30-50 minute, obtain pulverulent solids after heat drying, be Seaweed Extract.
Preparation method of the present invention is as follows:
1) attapulgite, wilkinite are mixed with plant ash, cow dung, sawdust, Semen Maydis powder, Seaweed Extract after pulverizing, add the human excrement of formula ratio 65%, ferment after stirring, fermentation time is 10-15 days, obtains tunning A;
2) mix with stalk, soybean cake, Sodium salts humic acids, chicken manure after being pulverized by zeolite, add the human excrement of formula ratio 35%, ferment after stirring, fermentation time is 13-15 days, obtains tunning B;
3) the tunning A obtained and tunning B and composite trace element, urea, double superhosphate and Repone K are fully mixed, then by normal temperature granulator granulation, to obtain final product.
The application dosage of the composite fertilizer that the present invention obtains is as follows:
The root of Dahurain angelica: every mu of fertilising 70-100kg;
Radix bupleuri: every mu of fertilising 90-130kg.
The present invention selects the multiple organic fertilizer such as plant ash, pig manure, sawdust, stalk, Semen Maydis powder, soybean cake, and after blending, heap fermentation is to kill pathogenic bacteria, promotes that part organic substance decomposing is to improve fertilizer efficiency; Seaweed Extract and the various agents in combination in filling a prescription use the premature bolting rate that can reduce the root of Dahurain angelica, improve the content of saponin(e a, d in root of Dahurain angelica Imperatorin and radix bupleuri, improve the quality of the root of Dahurain angelica and Radix Bupleuri; Also have a certain amount of nitrogenous fertilizer, phosphate fertilizer, potash fertilizer to regulate carbon-nitrogen ratio, obtain the special nutritional compound manure being applicable to the root of Dahurain angelica and radix bupleuri three-dimensional planting.This kind of composite fertilizer repeatedly topdresses on a small quantity, can thicken arable layer, strengthens its preserve moisture and fertility ability.The compound manure that the present invention designs, can meet the Different Nutrition needs of the root of Dahurain angelica and radix bupleuri and the difference of various seasons targetedly, improve quality of medicinal material, have significant economic benefit.
The present invention is the special nutritional compound manure of the root of Dahurain angelica and radix bupleuri three-dimensional planting, can reduce the premature bolting rate of the root of Dahurain angelica, improves the content of saponin(e a, d in root of Dahurain angelica Imperatorin and radix bupleuri, improves the quality of the root of Dahurain angelica and Radix Bupleuri.
Specific embodiment
Embodiment 1: a kind of composite fertilizer being applicable to the root of Dahurain angelica and radix bupleuri is made up of the raw material of following weight proportion: plant ash 240 parts, cow dung 120 parts, 180 parts, sawdust, stalk 230 parts, Semen Maydis powder 95 parts, soybean cake 305 parts, attapulgite 55 parts, wilkinite 50 parts, 125 parts, zeolite, Sodium salts humic acids 65 parts, chicken manure 80 parts, composite trace element 20 parts, Seaweed Extract 160 parts, human excrement 320 parts, 170 parts, urea, double superhosphate 120 parts, 200 parts, Repone K.
In described composite trace element, the weight ratio of each component is borax: copper sulfate: manganous sulfate: Sodium orthomolybdate: zinc sulfate=1:3.2:0.8:0.6:2.3;
Described Seaweed Extract obtains by the following method:
Get dry marine alga to pulverize, add the water of 4 times of weight again, regulate pH to 9.6 with diluted sodium hydroxide solution, soak 6 hours, then regulate pH to 6.7 with dilute hydrochloric acid, then concentrate and obtain the concentrated solution that relative density is 1.45, the volume fraction adding 10 times of concentrated solution weight is the ethanol of 80%, then adds the diatomite of 1.7 times of concentrated solution quality, stirs 40 minutes, obtain pulverulent solids after heat drying, be Seaweed Extract.
Preparation method of the present invention is as follows:
1) attapulgite, wilkinite are mixed with plant ash, cow dung, sawdust, Semen Maydis powder, Seaweed Extract after pulverizing, add the human excrement of formula ratio 65%, ferment after stirring, fermentation time is 12 days, obtains tunning A;
2) mix with stalk, soybean cake, Sodium salts humic acids, chicken manure after being pulverized by zeolite, add the human excrement of formula ratio 35%, ferment after stirring, fermentation time is 14 days, obtains tunning B;
3) the tunning A obtained and tunning B and composite trace element, urea, double superhosphate and Repone K are fully mixed, then by normal temperature granulator granulation, to obtain final product.
The application dosage of the composite fertilizer that the present invention obtains is as follows:
The root of Dahurain angelica: every mu of fertilising 80kg;
Radix bupleuri: every mu of fertilising 110kg.
Embodiment 2: a kind of composite fertilizer being applicable to the root of Dahurain angelica and radix bupleuri is made up of the raw material of following weight proportion: plant ash 220 parts, cow dung 110 parts, 150 parts, sawdust, stalk 200 parts, Semen Maydis powder 80 parts, soybean cake 280 parts, attapulgite 40 parts, wilkinite 35 parts, 105 parts, zeolite, Sodium salts humic acids 50 parts, chicken manure 70 parts, composite trace element 10 parts, Seaweed Extract 130 parts, human excrement 250 parts, 150 parts, urea, double superhosphate 110 parts, 180 parts, Repone K.
In described composite trace element, the weight ratio of each component is borax: copper sulfate: manganous sulfate: Sodium orthomolybdate: zinc sulfate=1:2.3:0.6:0.3:1.9;
Described Seaweed Extract obtains by the following method:
Get dry marine alga to pulverize, add the water of 3 times of weight again, regulate pH to 9.3 with diluted sodium hydroxide solution, soak 5 hours, then regulate pH to 6.2 with dilute hydrochloric acid, then concentrate and obtain the concentrated solution that relative density is 1.4, the volume fraction adding 9 times of concentrated solution weight is the ethanol of 80%, then adds the diatomite of 1.3 times of concentrated solution quality, stirs 30 minutes, obtain pulverulent solids after heat drying, be Seaweed Extract.
Preparation method of the present invention is as follows:
1) attapulgite, wilkinite are mixed with plant ash, cow dung, sawdust, Semen Maydis powder, Seaweed Extract after pulverizing, add the human excrement of formula ratio 65%, ferment after stirring, fermentation time is 10 days, obtains tunning A;
2) mix with stalk, soybean cake, Sodium salts humic acids, chicken manure after being pulverized by zeolite, add the human excrement of formula ratio 35%, ferment after stirring, fermentation time is 13 days, obtains tunning B;
3) the tunning A obtained and tunning B and composite trace element, urea, double superhosphate and Repone K are fully mixed, then by normal temperature granulator granulation, to obtain final product.
The application dosage of the composite fertilizer that the present invention obtains is as follows:
The root of Dahurain angelica: every mu of fertilising 70kg;
Radix bupleuri: every mu of fertilising 90kg.
Embodiment 3: a kind of composite fertilizer being applicable to the root of Dahurain angelica and radix bupleuri is made up of the raw material of following weight proportion: plant ash 260 parts, cow dung 130 parts, 200 parts, sawdust, stalk 260 parts, Semen Maydis powder 110 parts, soybean cake 330 parts, attapulgite 70 parts, wilkinite 60 parts, 145 parts, zeolite, Sodium salts humic acids 90 parts, chicken manure 100 parts, composite trace element 30 parts, Seaweed Extract 180 parts, human excrement 400 parts, 200 parts, urea, double superhosphate 140 parts, 220 parts, Repone K.
In described composite trace element, the weight ratio of each component is borax: copper sulfate: manganous sulfate: Sodium orthomolybdate: zinc sulfate=1:4.5:1.1:0.9:2.8;
Described Seaweed Extract obtains by the following method:
Get dry marine alga to pulverize, add the water of 6 times of weight again, regulate pH to 9.9 with diluted sodium hydroxide solution, soak 8 hours, then regulate pH to 7.1 with dilute hydrochloric acid, then concentrate and obtain the concentrated solution that relative density is 1.5, the volume fraction adding 12 times of concentrated solution weight is the ethanol of 80%, then adds the diatomite of 2.1 times of concentrated solution quality, stirs 50 minutes, obtain pulverulent solids after heat drying, be Seaweed Extract.
Preparation method of the present invention is as follows:
1) attapulgite, wilkinite are mixed with plant ash, cow dung, sawdust, Semen Maydis powder, Seaweed Extract after pulverizing, add the human excrement of formula ratio 75%, ferment after stirring, fermentation time is 15 days, obtains tunning A;
2) mix with stalk, soybean cake, Sodium salts humic acids, chicken manure after being pulverized by zeolite, add the human excrement of formula ratio 25%, ferment after stirring, fermentation time is 115 days, obtains tunning B;
3) the tunning A obtained and tunning B and composite trace element, urea, double superhosphate and Repone K are fully mixed, then by normal temperature granulator granulation, to obtain final product.
The application dosage of the composite fertilizer that the present invention obtains is as follows:
The root of Dahurain angelica: every mu of fertilising 100kg;
Radix bupleuri: every mu of fertilising 130kg.
Embodiment 4: a kind of composite fertilizer being applicable to the root of Dahurain angelica and radix bupleuri is made up of the raw material of following weight proportion: plant ash 210 parts, cow dung 140 parts, 130 parts, sawdust, stalk 280 parts, Semen Maydis powder 70 parts, soybean cake 260 parts, attapulgite 80 parts, wilkinite 70 parts, 100 parts, zeolite, Sodium salts humic acids 30 parts, chicken manure 60 parts, composite trace element 8 parts, Seaweed Extract 110 parts, human excrement 220 parts, 140 parts, urea, double superhosphate 150 parts, 230 parts, Repone K.
In described composite trace element, the weight ratio of each component is borax: copper sulfate: manganous sulfate: Sodium orthomolybdate: zinc sulfate=1:2.1:1.3:0.2:2.9;
Described Seaweed Extract obtains by the following method:
Get dry marine alga to pulverize, add the water of 2 times of weight again, regulate pH to 9.1 with diluted sodium hydroxide solution, soak 9 hours, then regulate pH to 6.0 with dilute hydrochloric acid, then concentrate and obtain the concentrated solution that relative density is 1.6, the volume fraction adding 8 times of concentrated solution weight is the ethanol of 80%, then adds the diatomite of 1.2 times of concentrated solution quality, stirs 60 minutes, obtain pulverulent solids after heat drying, be Seaweed Extract.
Preparation method of the present invention is as follows:
1) mix with Sodium salts humic acids, chicken manure, Semen Maydis powder, Seaweed Extract after being pulverized by attapulgite, add the human excrement of formula ratio 65%, ferment after stirring, fermentation time is 9 days, obtains tunning A;
2) zeolite, wilkinite are mixed with stalk, plant ash, cow dung, sawdust, soybean cake after pulverizing, add the human excrement of formula ratio 35%, ferment after stirring, fermentation time is 16 days, obtains tunning B;
3) the tunning A obtained and tunning B and composite trace element, urea, double superhosphate and Repone K are fully mixed, then by normal temperature granulator granulation, to obtain final product.
The application dosage of the composite fertilizer that the present invention obtains is as follows:
The root of Dahurain angelica: every mu of fertilising 110kg;
Radix bupleuri: every mu of fertilising 80kg.
Embodiment 5: a kind of composite fertilizer being applicable to the root of Dahurain angelica and radix bupleuri is made up of the raw material of following weight proportion: plant ash 270 parts, cow dung 100 parts, 210 parts, sawdust, stalk 190 parts, Semen Maydis powder 120 parts, soybean cake 260 parts, attapulgite 30 parts, wilkinite 30 parts, 155 parts, zeolite, Sodium salts humic acids 100 parts, chicken manure 120 parts, composite trace element 40 parts, Seaweed Extract 190 parts, human excrement 240 parts, 220 parts, urea, double superhosphate 150 parts, 230 parts, Repone K.
In described composite trace element, the weight ratio of each component is borax: copper sulfate: manganous sulfate: Sodium orthomolybdate: zinc sulfate=1:4.6:0.5:0.2:1.7;
Described Seaweed Extract obtains by the following method:
Get dry marine alga to pulverize, add the water of 7 times of weight again, regulate pH to 10.1 with diluted sodium hydroxide solution, soak 4 hours, then regulate pH to 7.2 with dilute hydrochloric acid, then concentrate and obtain the concentrated solution that relative density is 1.3, the volume fraction adding 13 times of concentrated solution weight is the ethanol of 80%, then adds the diatomite of 1.2 times of concentrated solution quality, stirs 20 minutes, obtain pulverulent solids after heat drying, be Seaweed Extract.
All the other are with embodiment 1.
Embodiment 6: a kind of composite fertilizer being applicable to the root of Dahurain angelica and radix bupleuri, its preparation method is as follows:
1) zeolite, wilkinite are mixed with plant ash, cow dung, sawdust, soybean cake, Sodium salts humic acids after pulverizing, add the human excrement of formula ratio 55%, ferment after stirring, fermentation time is 16 days, obtains tunning A;
2) mix with stalk, Semen Maydis powder, Seaweed Extract, chicken manure after being pulverized by attapulgite, add the human excrement of formula ratio 45%, ferment after stirring, fermentation time is 11 days, obtains tunning B;
3) the tunning A obtained and tunning B and composite trace element, urea, double superhosphate and Repone K are fully mixed, then by normal temperature granulator granulation, to obtain final product.
The application dosage of the composite fertilizer that the present invention obtains is as follows:
The root of Dahurain angelica: every mu of fertilising 60kg;
Radix bupleuri: every mu of fertilising 140kg.
Embodiment 7: according to application number a kind of herbal medicine crop special active biological medicine fertilizer disclosed in the Chinese patent of 201210104700.6, disclosed in embodiment 1, embodiment is: a kind of herbal medicine crop special active biological medicine fertilizer, and during its preparation, the weight percent of each raw material composition is:
Photosynthetic microbial inoculum 10% effective active bacterium 8-10 hundred million/ml
Xanthohumic acid 9%
Urea 7%
Monoammonium phosphate 3%
Potassium sulfate 7%
Potassium silicate 0.2%
Ammonium molybdate 0.3
Magnesium sulfate 0.2%
Radix aconiti agrestis 0.6% is added using aqueous extract as raw material by radix aconiti agrestis
Surplus is water.Wherein increase by 1% Oleum Cinnamomi ethanolic soln, spray after high-speed stirring dispersion.
Using method: mu consumption 100ml, doubly dilutes by 1:400-600, foliar spray, moistening for degree with the page.
Embodiment 8: according to application number a kind of radix angelicae Chinese herbal medicine nutrient fertilizer disclosed in the Chinese patent of 201010182058.4, by embodiment disclosed in embodiment 1 be: fertile 30000 grams of dried poultrymanure 25000 grams, dried poultrymanure 30000 grams, 25000 grams, dry rabbit excrement, 25000 grams, dry human excrement, Semen Maydis powder 20000 grams, soybean cake 20000 grams, 20000 grams, cotton seed hull powder, grass meal 20000 grams, 20000 grams, potash fertilizer, chlorine, composite fertilizer 10000 grams, zinc fertilizer 10000 gram, gram are reach special 1000 grams, removed bacterium spirit 1000 grams, glucose powder 2000 grams, chlorinated rubber 10000 grams.
Get above-mentioned pulvis to be in proportion all grouped together, put into stirrer to stir 90 minutes, put into after taking-up pulverizer be ground into 60 orders about particle, and then put into stirrer stirring 140 minutes, all pour in fermentation vat after taking-up, add in proportion the human excrement of 1:1. 5 waterborne under to mix heap thoroughly in heaps, make real and to be tightly compacted fermentation 28 hours with plastic cloth, carry out first time turning, lower floor should be translated into from upper strata when turning over, internal layer translates into skin, the inside is to turning up, outside is to turning in, add again in proportion after turning the human excrement of 1:1. 5 waterborne under to mix heap thoroughly in heaps, make real, second time turning is carried out after 52 hours with the plastic cloth fermentation that is tightly compacted, the method of turning is consistent with above-mentioned, pile in heaps fermentation again 70 hours.The mould nutritious fertilizer fermented being put into one high 30 centimeters, wide 25 centimeters, long 40 centimeters close break into nutrition fertilizer block qualified nutrition fertilizer.
Fertilizing method: the root of Dahurain angelica just bloomed knot flower mushroom time be best Stage of Top Dressing, dig out the hole of dark 40 centimeters, wide 30 centimeters, long 50 centimeters from root of Dahurain angelica root 30 centimeters of place's spades, it is good that production promoting fertilizer is put into earth mulch, pours into 30 jin.
1. root of Dahurain angelica premature bolting rate and the test of pentosalen content
8 treatment group are established in test altogether, and give the composite fertilizer that embodiment 1-8 is obtained respectively, rate of fertilizer application and fertilizing method are undertaken by the explanation in each embodiment, and often group establishes 3 repetitions, and each community is 2m × 5m.Observe root of Dahurain angelica bolting phenomenon in planting process, record the premature bolting rate of each group.Results Shi Mei community takes 2m
2plant samples, clean earth dries surface-moisture, natural air drying.Root of Dahurain angelica block root Imperatorin measures by pentosalen content assaying method under " Chinese Pharmacopoeia " version in 2010 root of Dahurain angelica item.Test-results is in table 1.
Table 1 root of Dahurain angelica premature bolting rate and pentosalen comparision contents
Root of Dahurain angelica root lignifying after premature bolting, can not do medicinal, reduce the seed output and quality of the root of Dahurain angelica.Embodiment 1-3(technical parameter is all in the scope of technical solution of the present invention) the premature bolting rate of corresponding test group is all less than 1.5%, significantly lower than the test group that other embodiments are corresponding.And the pentosalen content of test group corresponding to embodiment 1-3 is also higher than other test group, especially the premature bolting rate of the test group of embodiment 1 correspondence is minimum, and pentosalen content is the highest.Therefore the present invention can significantly improve the quality of angelica root, it is a kind of root of Dahurain angelica composite fertilizer of excellent effect.
2. saponin(e a, d content test in radix bupleuri
7 treatment group are established in test altogether, and give the composite fertilizer that embodiment 1-7 is obtained respectively, rate of fertilizer application and fertilizing method are undertaken by the explanation in each embodiment, and often group establishes 3 repetitions, and each community is 2m × 5m.Results Shi Mei community takes 2m
2plant samples, clean earth dries surface-moisture, natural air drying.Adopt saponin(e a, d content of high effective liquid chromatography for measuring radix bupleuri root, concrete grammar is as follows:
1) chromatographic condition
Chromatographic column: Agilent TC-C
18(4.6 mm × 250 mm, 5 μm); Column temperature: 20 DEG C; Drift tube temperature: 93 DEG C; Air velocity: 2. 5L/min; Flow velocity: 0.8mL/min; Moving phase: acetonitrile-water (50:50).
2) need testing solution preparation: the radix bupleuri root dry sample of the test group results that Example 1-7 is corresponding, pulverize, cross 40 mesh sieves, get each sample powder respectively and be about 1g, accurately weighed, precision adds 5% ammoniacal liquor methanol solution 30 mL, weighs, 1 h that refluxes (80 DEG C of water-baths), take out after extraction and be placed to room temperature, weighed and supply weight, mixing, precision gets subsequent filtrate 15 mL, evaporate to dryness (80 DEG C of water-baths), add methanol constant volume to 5 mL, cross millipore filtration (0. 45 lam), obtain need testing solution.
3) reference substance solution preparation: precision takes radix bupleuri soap general a 19. 01 mg, and the general d 19.03mg of radix bupleuri soap is placed in 25 mL measuring bottles respectively, adds dissolve with methanol and is settled to scale, shaking up, to obtain final product.
4) saponin(e a, d assay: accurate absorption need testing solution 6 μ L respectively, saikoside a 5,20 μ L, saikoside d 5,25 μ L sample introduction, external standard two-point method measures the content of saikoside a, d in each sample, the results are shown in Table 2.
Saponin(e a, d comparision contents in table 2 radix bupleuri
Passable from above-mentioned test, embodiment 1-3(technical parameter is all in the scope of technical solution of the present invention) saikoside a of corresponding test group, d content is all higher than other test group, especially the highest with the saikoside a of the test group of embodiment 1 correspondence, d content, reach 0.7973% and 1.408% respectively.Illustrate that complex fertilizer product that the present invention obtains can significantly improve the quality of Radix Bupleuri.
Claims (6)
1. one kind is applicable to the composite fertilizer of the root of Dahurain angelica and radix bupleuri, it is characterized in that: be made up of the raw material of following weight proportion: plant ash 220-260 part, cow dung 110-130 part, sawdust 150-200 part, stalk 200-260 part, Semen Maydis powder 80-110 part, soybean cake 280-330 part, attapulgite 40-70 part, wilkinite 35-60 part, zeolite 105-145 part, Sodium salts humic acids 50-90 part, chicken manure 70-100 part, composite trace element 10-30 part, Seaweed Extract 130-180 part, human excrement 250-400 part, urea 150-200 part, double superhosphate 110-140 part, Repone K 180-220 part,
Wherein in composite trace element, the weight ratio of each component is borax: copper sulfate: manganous sulfate: Sodium orthomolybdate: zinc sulfate=1:2.3-4.5:0.6-1.1:0.3-0.9:1.9-2.8;
Wherein the preparation method of Seaweed Extract is: get dry marine alga and pulverize, add the water of 3-6 times of weight again, pH to 9.3-9.9 is regulated with diluted sodium hydroxide solution, soak 5-8 hour, pH to 6.2-7.1 is regulated again with dilute hydrochloric acid, then concentrate and obtain the concentrated solution that relative density is 1.4-1.5, the volume fraction adding 9-12 times of concentrated solution weight is the ethanol of 80%, add the diatomite of 1.3-2.1 times of concentrated solution quality again, stir 30-50 minute, obtain pulverulent solids after heat drying, be Seaweed Extract.
2. a kind of composite fertilizer being applicable to the root of Dahurain angelica and radix bupleuri as claimed in claim 1, is characterized in that: be made up of the raw material of following weight proportion: plant ash 240 parts, cow dung 120 parts, 180 parts, sawdust, stalk 230 parts, Semen Maydis powder 95 parts, soybean cake 305 parts, attapulgite 55 parts, wilkinite 50 parts, 125 parts, zeolite, Sodium salts humic acids 65 parts, chicken manure 80 parts, composite trace element 20 parts, Seaweed Extract 160 parts, human excrement 320 parts, 170 parts, urea, double superhosphate 120 parts, 200 parts, Repone K;
Wherein in composite trace element, the weight ratio of each component is borax: copper sulfate: manganous sulfate: Sodium orthomolybdate: zinc sulfate=1:3.2:0.8:0.6:2.3;
Wherein the preparation method of Seaweed Extract is: get dry marine alga and pulverize, add the water of 4 times of weight again, regulate pH to 9.6 with diluted sodium hydroxide solution, soak 6 hours, then regulate pH to 6.7 with dilute hydrochloric acid, then concentrate and obtain the concentrated solution that relative density is 1.45, the volume fraction adding 10 times of concentrated solution weight is the ethanol of 80%, then adds the diatomite of 1.7 times of concentrated solution quality, stirs 40 minutes, obtain pulverulent solids after heat drying, be Seaweed Extract.
3. a kind of composite fertilizer being applicable to the root of Dahurain angelica and radix bupleuri as claimed in claim 1 or 2, is characterized in that: preparation method is:
1) attapulgite, wilkinite are mixed with plant ash, cow dung, sawdust, Semen Maydis powder, Seaweed Extract after pulverizing, add the human excrement of formula ratio 65%, ferment after stirring, fermentation time is 10-15 days, obtains tunning A;
2) mix with stalk, soybean cake, Sodium salts humic acids, chicken manure after being pulverized by zeolite, add the human excrement of formula ratio 35%, ferment after stirring, fermentation time is 13-15 days, obtains tunning B;
3) the tunning A obtained and tunning B and composite trace element, urea, double superhosphate and Repone K are fully mixed, then by normal temperature granulator granulation, to obtain final product.
4. a kind of composite fertilizer being applicable to the root of Dahurain angelica and radix bupleuri as claimed in claim 3, is characterized in that: preparation method is:
1) attapulgite, wilkinite are mixed with plant ash, cow dung, sawdust, Semen Maydis powder, Seaweed Extract after pulverizing, add the human excrement of formula ratio 65%, ferment after stirring, fermentation time is 12 days, obtains tunning A;
2) mix with stalk, soybean cake, Sodium salts humic acids, chicken manure after being pulverized by zeolite, add the human excrement of formula ratio 35%, ferment after stirring, fermentation time is 14 days, obtains tunning B;
3) the tunning A obtained and tunning B and composite trace element, urea, double superhosphate and Repone K are fully mixed, then by normal temperature granulator granulation, to obtain final product.
5. a kind of composite fertilizer being applicable to the root of Dahurain angelica and radix bupleuri as claimed in claim 1 or 2, is characterized in that: application dosage is:
The root of Dahurain angelica: every mu of fertilising 70-100kg;
Radix bupleuri: every mu of fertilising 90-130kg.
6. a kind of composite fertilizer being applicable to the root of Dahurain angelica and radix bupleuri as claimed in claim 5, is characterized in that: application dosage is:
The root of Dahurain angelica: every mu of fertilising 80kg;
Radix bupleuri: every mu of fertilising 110kg.
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