CN102965981A - Thickening agent for printing and preparation method thereof - Google Patents
Thickening agent for printing and preparation method thereof Download PDFInfo
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- CN102965981A CN102965981A CN201210480781XA CN201210480781A CN102965981A CN 102965981 A CN102965981 A CN 102965981A CN 201210480781X A CN201210480781X A CN 201210480781XA CN 201210480781 A CN201210480781 A CN 201210480781A CN 102965981 A CN102965981 A CN 102965981A
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Abstract
The invention discloses a thickening agent for printing, which comprises the following components in parts by weight: 10-15 parts of etherified guar gum, 60-70 parts of sodium alginate, 30-50 parts of sodium carboxymethylcellulose, 20-30 parts of carboxymethyl starch, 12-20 parts of polyacrylic acid thickening agent blending stock, 10-20 parts of bentonites and 200-400 parts of water. The preparation method of the thickening agent comprises the following steps of: adding sodium alginate and sodium carboxymethylcellulose powder to water, and mechanically stirring till a solution is transparent and clear without a block; then adding the etherified guar gum, the carboxymethyl starch, the polyacrylic acid thickening agent blending stock and the bentonite, uniformly stirring, and standing to bulk the mixed solution so as to obtain the printing thickening agent. In the preparation process, with the bulking of the paste material, the sodium carboxymethylcellulose forms three-dimensional net structure among macromolecules of paste material or at the joints of molecular chain segments because of intermolecular attraction; moreover, besides a macromolecular chain hydration layer, a large amount of water is wrapped to form a gel state, so as to generate very high structural viscocity; therefore, a printing fabric has a clear outline.
Description
Technical field
The present invention relates to the thickener technical field, relate in particular to a kind of stamp thickener and preparation method thereof.
Background technology
Stamp requires the local place acquisition color that consists of pattern on fabric, therefore, in order to obtain clearly pattern, except the chemical agent of necessity, generally also will add suitable thickener prevents dyestuff along interfibrous capillary generation imbibition in the dye solution, and thickener is exactly to be added in to make it play the macromolecular compound of thickening power in the print paste.
At present, thickener commonly used is synthetic thickening agent, mainly by acrylic compounds, the maleic acid class is crosslinked forms, rheological characteristic is good, the fabric tinctorial yield is high behind the stamp, color development is bright-coloured, but viscoplasticity (draging a property) is poor, the PRINTED FABRIC profile is unintelligible.
Summary of the invention
Technical problem to be solved by this invention is: a kind of stamp thickener with high structural viscosity is provided.
For solving the problems of the technologies described above, the technical solution used in the present invention is: a kind of stamp thickener, and according to the mass fraction, it consists of:
Etherificate guar gum 10-15 part;
Sodium alginate 60-70 part;
Sodium carboxymethylcellulose 30-50 part;
Carboxymethyl starch 20-30 part;
Polyacrylate thickeners ready-mixed oil 12-20 part;
Bentonite 10-20 part;
Water 200-400 part.
Second technical problem to be solved by this invention is: the preparation method of a kind of stamp with thickener is provided.
For solving second technical problem, the technical solution used in the present invention is: a kind of stamp preparation method of thickener, and its preparation process is:
Sodium alginate and sodium carboxymethylcellulose powder are added to the water, with machine be stirred to transparent without piece, pure till, add again etherificate guar gum, carboxymethyl starch, Polyacrylate thickeners ready-mixed oil, bentonite stir (usually about 3-4h), leave standstill and make mixed liquor expanded, namely make printing thickening agent.
The temperature of described water is 0 ~ 5 ℃.
Described leaving standstill makes the expanded time of mixed liquor be: 10 ~ 12h.
Beneficial effect of the present invention is:
In preparation process, sodium carboxymethylcellulose is along with the swelling of thickener, between the thickener macromolecule or molecule segment junction, because intermolecular attraction forms tridimensional network, except the hydrated sheath of macromolecular chain, also net is being wrapped up in large water gaging and is being formed gel, produces very high structural viscosity, so that the PRINTED FABRIC clear-cut.
The specific embodiment
Embodiment 1
65g sodium alginate and 32g sodium carboxymethylcellulose powder are added in the 260g cold water, with electric blender stir about 50-60min, until transparent without piece, pure till, 12g etherificate guar gum, 23g carboxymethyl starch, 15g Polyacrylate thickeners ready-mixed oil, 12g bentonite stir 4h again, hold over night liquid to be mixed is fully expanded, namely makes printing thickening agent.
Embodiment 2
70g sodium alginate and 40g sodium carboxymethylcellulose powder are added in the 380g cold water, with electric blender stir about 50-60min, until transparent without piece, pure till, 14g etherificate guar gum, 26g carboxymethyl starch, 18g Polyacrylate thickeners ready-mixed oil, 18g bentonite stir 4h again, hold over night liquid to be mixed is fully expanded, namely makes printing thickening agent.
Claims (4)
1. stamp thickener, according to the mass fraction, it consists of:
Etherificate guar gum 10-15 part;
Sodium alginate 60-70 part;
Sodium carboxymethylcellulose 30-50 part;
Carboxymethyl starch 20-30 part;
Polyacrylate thickeners ready-mixed oil 12-20 part;
Bentonite 10-20 part;
Water 200-400 part.
2. a kind of stamp claimed in claim 1 is with the preparation method of thickener, and its preparation process is:
Sodium alginate and sodium carboxymethylcellulose powder are added to the water, with machine be stirred to transparent without piece, pure till, add again etherificate guar gum, carboxymethyl starch, Polyacrylate thickeners ready-mixed oil, bentonite and stir, leave standstill and make mixed liquor expanded, namely make printing thickening agent.
3. a kind of stamp according to claim 2 is with the preparation method of thickener, and it is characterized in that: the temperature of described water is 0 ~ 5 ℃.
4. a kind of stamp according to claim 2 is with the preparation method of thickener, and it is characterized in that: described described leaving standstill makes the expanded time of mixed liquor be: 10 ~ 12h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210480781.XA CN102965981B (en) | 2012-11-23 | 2012-11-23 | Thickening agent for printing and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210480781.XA CN102965981B (en) | 2012-11-23 | 2012-11-23 | Thickening agent for printing and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102965981A true CN102965981A (en) | 2013-03-13 |
| CN102965981B CN102965981B (en) | 2014-08-06 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201210480781.XA Expired - Fee Related CN102965981B (en) | 2012-11-23 | 2012-11-23 | Thickening agent for printing and preparation method thereof |
Country Status (1)
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Cited By (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103911883A (en) * | 2014-04-17 | 2014-07-09 | 苏州润弘贸易有限公司 | Reactive printing paste |
| CN103911887A (en) * | 2014-04-17 | 2014-07-09 | 苏州润弘贸易有限公司 | Reactive printing paste for all-cotton fabrics |
| CN103911884A (en) * | 2014-04-17 | 2014-07-09 | 苏州润弘贸易有限公司 | Reactive printing and dyeing paste for flax fabrics |
| CN103911885A (en) * | 2014-04-17 | 2014-07-09 | 苏州润弘贸易有限公司 | Printing and dyeing paste |
| CN103911882A (en) * | 2014-04-17 | 2014-07-09 | 苏州润弘贸易有限公司 | Preparation method of reactive printing paste for all-cotton fabrics |
| CN103924457A (en) * | 2014-04-17 | 2014-07-16 | 苏州润弘贸易有限公司 | Production process of printing and dyeing paste |
| CN103924456A (en) * | 2014-04-17 | 2014-07-16 | 苏州润弘贸易有限公司 | Production process of reactive printing paste |
| CN103938469A (en) * | 2014-04-17 | 2014-07-23 | 苏州润弘贸易有限公司 | Method for preparing reactive dyeing and printing paste of linen fabric |
| CN104278563A (en) * | 2014-09-27 | 2015-01-14 | 无锡市东北塘宏良染色厂 | Special printing paste for terylene |
| CN104278562A (en) * | 2014-09-27 | 2015-01-14 | 无锡市东北塘宏良染色厂 | Printing paste |
| CN104389202A (en) * | 2014-12-11 | 2015-03-04 | 上海雅运纺织助剂有限公司 | Composite printing paste and preparation method thereof |
| CN104452345A (en) * | 2014-12-23 | 2015-03-25 | 青岛明月海藻集团有限公司 | Printing gum for imitating batik |
| CN104695249A (en) * | 2015-03-06 | 2015-06-10 | 徐饶春 | Printing thickening agent |
| CN105369653A (en) * | 2014-08-13 | 2016-03-02 | 青岛海之林生物科技开发有限公司 | Composite active printing gum and preparing method thereof |
| CN105484067A (en) * | 2016-01-08 | 2016-04-13 | 湖州市千金丝织厂 | Novel disperse print thickening agent and preparation method thereof |
| CN105484069A (en) * | 2016-01-08 | 2016-04-13 | 湖州市千金丝织厂 | Multi-function printing thickener and preparation method thereof |
| CN105625051A (en) * | 2016-03-29 | 2016-06-01 | 湖南工程学院 | Environment-friendly and safe printing paste and printing color paste as well as application of printing paste and printing color paste |
| CN106012605A (en) * | 2016-05-31 | 2016-10-12 | 山东洁晶集团股份有限公司 | Thickener used for all-cotton and artificial cotton printing, and preparation method thereof |
| CN106638022A (en) * | 2016-10-14 | 2017-05-10 | 袁春华 | Preparation method of printing thickener |
| CN106758321A (en) * | 2016-10-28 | 2017-05-31 | 浙江嘉欣兴昌印染有限公司 | A kind of disperse dyes alkalescence stamp composite paste material mill base and preparation method thereof and textile printing process |
| CN106978738A (en) * | 2017-04-28 | 2017-07-25 | 山东轻工职业学院 | A kind of Dyeing with Disperse/Reactive Graft versus host disease composite paste material and its printing technology |
| WO2018201430A1 (en) * | 2017-05-05 | 2018-11-08 | 海安润德服装有限公司 | Natural printing thickening agent |
| CN108797162A (en) * | 2018-07-05 | 2018-11-13 | 吉向阳 | The printing technology of hydrophobic fabric |
| CN112127181A (en) * | 2020-08-24 | 2020-12-25 | 清远瑞华助剂有限公司 | Disperse printing paste and using method thereof |
| CN114921980A (en) * | 2022-06-08 | 2022-08-19 | 大连工业大学 | Supercritical CO 2 Method for printing with auxiliary cationic dye |
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| JPS5782586A (en) * | 1980-11-04 | 1982-05-24 | Chiyoda Kagaku Kenkyusho | Size composition for printing |
| JPS5940952B2 (en) * | 1979-09-20 | 1984-10-03 | 三晶株式会社 | printing paste |
| JPS62238888A (en) * | 1986-04-09 | 1987-10-19 | ユニチカ株式会社 | Printing of cellulosic fiber cloth |
| US5463036A (en) * | 1992-11-25 | 1995-10-31 | Wolff Walsrode Aktiengesellschaft | Carboxymethylcellulose and its use in textile printing |
| CN100519926C (en) * | 2006-12-12 | 2009-07-29 | 天津工业大学 | Ice printing adhesive cement and ice printing fabric production method |
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Patent Citations (5)
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| JPS5940952B2 (en) * | 1979-09-20 | 1984-10-03 | 三晶株式会社 | printing paste |
| JPS5782586A (en) * | 1980-11-04 | 1982-05-24 | Chiyoda Kagaku Kenkyusho | Size composition for printing |
| JPS62238888A (en) * | 1986-04-09 | 1987-10-19 | ユニチカ株式会社 | Printing of cellulosic fiber cloth |
| US5463036A (en) * | 1992-11-25 | 1995-10-31 | Wolff Walsrode Aktiengesellschaft | Carboxymethylcellulose and its use in textile printing |
| CN100519926C (en) * | 2006-12-12 | 2009-07-29 | 天津工业大学 | Ice printing adhesive cement and ice printing fabric production method |
Cited By (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103924457B (en) * | 2014-04-17 | 2016-04-06 | 苏州润弘贸易有限公司 | A kind of production technology of dyeing paste |
| CN103924456B (en) * | 2014-04-17 | 2016-04-06 | 苏州润弘贸易有限公司 | A kind of production technology of reactive printing thickener |
| CN103911884A (en) * | 2014-04-17 | 2014-07-09 | 苏州润弘贸易有限公司 | Reactive printing and dyeing paste for flax fabrics |
| CN103911885A (en) * | 2014-04-17 | 2014-07-09 | 苏州润弘贸易有限公司 | Printing and dyeing paste |
| CN103911882A (en) * | 2014-04-17 | 2014-07-09 | 苏州润弘贸易有限公司 | Preparation method of reactive printing paste for all-cotton fabrics |
| CN103924457A (en) * | 2014-04-17 | 2014-07-16 | 苏州润弘贸易有限公司 | Production process of printing and dyeing paste |
| CN103924456A (en) * | 2014-04-17 | 2014-07-16 | 苏州润弘贸易有限公司 | Production process of reactive printing paste |
| CN103938469A (en) * | 2014-04-17 | 2014-07-23 | 苏州润弘贸易有限公司 | Method for preparing reactive dyeing and printing paste of linen fabric |
| CN103911887A (en) * | 2014-04-17 | 2014-07-09 | 苏州润弘贸易有限公司 | Reactive printing paste for all-cotton fabrics |
| CN103911883A (en) * | 2014-04-17 | 2014-07-09 | 苏州润弘贸易有限公司 | Reactive printing paste |
| CN105369653A (en) * | 2014-08-13 | 2016-03-02 | 青岛海之林生物科技开发有限公司 | Composite active printing gum and preparing method thereof |
| CN104278563A (en) * | 2014-09-27 | 2015-01-14 | 无锡市东北塘宏良染色厂 | Special printing paste for terylene |
| CN104278562A (en) * | 2014-09-27 | 2015-01-14 | 无锡市东北塘宏良染色厂 | Printing paste |
| CN104389202B (en) * | 2014-12-11 | 2016-08-24 | 上海雅运纺织助剂有限公司 | A kind of complex printing gum and preparation method thereof |
| CN104389202A (en) * | 2014-12-11 | 2015-03-04 | 上海雅运纺织助剂有限公司 | Composite printing paste and preparation method thereof |
| CN104452345A (en) * | 2014-12-23 | 2015-03-25 | 青岛明月海藻集团有限公司 | Printing gum for imitating batik |
| CN104695249A (en) * | 2015-03-06 | 2015-06-10 | 徐饶春 | Printing thickening agent |
| CN105484067A (en) * | 2016-01-08 | 2016-04-13 | 湖州市千金丝织厂 | Novel disperse print thickening agent and preparation method thereof |
| CN105484069A (en) * | 2016-01-08 | 2016-04-13 | 湖州市千金丝织厂 | Multi-function printing thickener and preparation method thereof |
| CN105625051A (en) * | 2016-03-29 | 2016-06-01 | 湖南工程学院 | Environment-friendly and safe printing paste and printing color paste as well as application of printing paste and printing color paste |
| CN106012605A (en) * | 2016-05-31 | 2016-10-12 | 山东洁晶集团股份有限公司 | Thickener used for all-cotton and artificial cotton printing, and preparation method thereof |
| CN106638022A (en) * | 2016-10-14 | 2017-05-10 | 袁春华 | Preparation method of printing thickener |
| CN106758321A (en) * | 2016-10-28 | 2017-05-31 | 浙江嘉欣兴昌印染有限公司 | A kind of disperse dyes alkalescence stamp composite paste material mill base and preparation method thereof and textile printing process |
| CN106978738A (en) * | 2017-04-28 | 2017-07-25 | 山东轻工职业学院 | A kind of Dyeing with Disperse/Reactive Graft versus host disease composite paste material and its printing technology |
| WO2018201430A1 (en) * | 2017-05-05 | 2018-11-08 | 海安润德服装有限公司 | Natural printing thickening agent |
| CN108797162A (en) * | 2018-07-05 | 2018-11-13 | 吉向阳 | The printing technology of hydrophobic fabric |
| CN112127181A (en) * | 2020-08-24 | 2020-12-25 | 清远瑞华助剂有限公司 | Disperse printing paste and using method thereof |
| CN114921980A (en) * | 2022-06-08 | 2022-08-19 | 大连工业大学 | Supercritical CO 2 Method for printing with auxiliary cationic dye |
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| CN102965981B (en) | 2014-08-06 |
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Granted publication date: 20140806 Termination date: 20181123 |