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CN102582095A - Dry process for forming arc-shaped continuous fiber composite board - Google Patents

Dry process for forming arc-shaped continuous fiber composite board Download PDF

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Publication number
CN102582095A
CN102582095A CN2012100047992A CN201210004799A CN102582095A CN 102582095 A CN102582095 A CN 102582095A CN 2012100047992 A CN2012100047992 A CN 2012100047992A CN 201210004799 A CN201210004799 A CN 201210004799A CN 102582095 A CN102582095 A CN 102582095A
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CN
China
Prior art keywords
fiber composite
dry
continuous fiber
arc
resin
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Pending
Application number
CN2012100047992A
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Chinese (zh)
Inventor
黄献中
高雄
张养会
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Jiangsu Aosheng Composite Materials Hi-tech Co Ltd
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Jiangsu Aosheng Composite Materials Hi-tech Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by Jiangsu Aosheng Composite Materials Hi-tech Co Ltd filed Critical Jiangsu Aosheng Composite Materials Hi-tech Co Ltd
Priority to CN2012100047992A priority Critical patent/CN102582095A/en
Publication of CN102582095A publication Critical patent/CN102582095A/en
Pending legal-status Critical Current

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Abstract

The invention relates to a dry process for forming an arc-shaped continuous fiber composite board. The process comprises the following steps of: preparing a required fiber yarn flock, and unfolding the fiber yarn flock, so that the fiber yarn flock are distributed uniformly to form silk bundles of which the widths are 90 to 120 millimeters; impregnating the silk bundles into resin; after the silk bundles are completely impregnated, baking the silk bundles to obtain fiber preimpregnated cloth; performing pultrusion on the fiber preimpregnated cloth to form an arc-shaped product; and curing the arc-shaped product to obtain a finished product. According to the process, the impregnation process and the pultrusion process are separated, namely the impregnation process is independent, so that the impregnation speed is improved greatly, the requirement on the manufacturability of the resin is reduced, and the resin with high mechanical properties and slightly low manufacturability can be selected; and during pultrusion, the impregnation process is eliminated, so the problem of low long-term applicability of the resin is solved, the quality stability of the product is improved, a process for replacing the resin by workers at regular time is also eliminated, and a production site is clean and tidy.

Description

The dry-press process technology of arc continuous fiber composite material plate
Technical field
the present invention relates to field of compound material, particularly relate to a kind of dry-press process technology of arc continuous fiber composite material plate.
Background technology
Along with constant development of economy, medical industry also improves the requirement of Medical Devices gradually , and medical device is required to multifunction, high reinforcement, miniaturization, lightweight, stable words development.It is too heavy that a lot of steel constructions seem under the situation of proof strength.And carbon fibre composite has advantages such as light weight, intensity is high, thermal coefficient of expansion is low, corrosion-resistant, can solve the problem of equipment lightweight, miniaturization, and the particularly development in pluralism of carbon fiber product gets more and more people's extensive concerning.But present pultrusion preparation technology produces to linear pattern, uiform section product, has limited the application of product.
Summary of the invention
the object of the invention provides a kind of dry-press process technology of arc continuous fiber composite material plate.
For achieving the above object, the technical scheme that the present invention adopts is:
A kind of dry-press process technology of arc continuous fiber composite material plate, it may further comprise the steps:
(1), impregnation:
Prepare required silvalin group, described silvalin is rolled into a ball launched, evenly be scattered in the wide tow of 90-120mm that is; Described tow is carried out the resin impregnation; , described tow toasts and makes fiber preimpregnation cloth after soaking into fully;
(2), pultrusion:
Pultrusion camber goods are carried out with described fiber preimpregnation cloth in ; Described arc goods are cured, and solidification temperature is 150-200 ℃, and makes finished product.
preferably, the humidity of described silvalin group is less than 50%.
preferably, make described fiber preimpregnation cloth after, its two faces are carried out the covering of diaphragm, and rolling.
preferably, in the pultrusion process, described fiber pre-preg cloth is respectively through 3 humidity province: 70-90 ℃, 120-140 ℃ and 120-140 ℃.
Described tow 110-130 ℃ of baking in back 2-4 minute preferably soaked into fully in ; Perhaps 70-90 ℃ was toasted 2-4 minute, was adjusted to 100-120 ℃ and toasted 2-4 minute again.
preferably, described diaphragm is the PET mould release membrance.
preferably, described silvalin group adopts carbon fiber.
preferably, described resin adopts epoxy resin.
Because the technique scheme utilization, the present invention compared with prior art has advantage and effect:
1, impregnation and pultrusion separate among the present invention, and impregnation is listed separately, and impregnation speed promotes greatly, have reduced the technological requirement of resin, can choose the mechanical property excellence and the poor slightly resin of manufacturability;
Removed gum dipping process when 2, pultrusion: need not consider the long-time applicability problem of resin on the one hand, the stability of product quality improves; Also saved the workman on the other hand and regularly changed the resin operation, the production scene is neat and tidy more also.
Description of drawings
Accompanying drawing 1 is the equipment sketch map of gum dipping process of the present invention;
Accompanying drawing 2 is the equipment sketch map of pultrude process of the present invention;
accompanying drawing 3 is mould--the schematic top plan view of pulling equipment in the pultrude process equipment of the present invention.
wherein: 1, creel; 2, exhibition yarn equipment; 3, impregnation equipment; 4, post processing baking oven; 5, equipment for coating film; 6, rolling equipment; 7, mould; 8, back curing oven; 9, pulling equipment.
The specific embodiment
Below in conjunction with accompanying drawing and embodiment the present invention is further described:
are existing to be example to produce the arc carbon fiber composite panel, its wide 100mm, thick 1.4mm.
The carbon filament of the eastern UTS50 of nation that fiber uses, resin system is epoxy-resin systems AS2-02, wherein:
The east UTS50-12K of nation:
Hot strength: 4900 MPa,
Stretch modulus: 240GPa,
Density: 1.8 g/cm3,
Filament diameter: 6.9 μ m;
Epoxy-resin systems AS2-02:
Hot strength: 60-80 MPa,
Heat distortion temperature: 200-220 ℃,
Bending strength: 100-130 MPa,
elongation at break: 3-5%.
Impregnation equipment comprises: creel 1, exhibition yarn equipment 2, impregnation equipment 3, post processing baking oven 4, equipment for coating film 5 and rolling equipment 6;
extruding equipment comprises: mould 7, back curing oven 8 and pulling equipment 9.
(1), impregnation: as shown in Figure 1:
A, on creel 1, place required carbon fiber yarn group, humidity>=50% needs to introduce dehumidification equipment, to guarantee the mass dryness fraction of carbon fiber yarn group;
B, carbon fiber yarn are through exhibition yarn equipment 2, and evenly distributing becomes the tow of wide 105mm;
C, configuration AS2-2 resin are poured impregnation equipment 3 into, and carbon fibre tow soaks into through impregnation fully;
D, soak into carbon fibre tow fully and get into post processing baking oven 4,120 ℃ of bakings 3 minutes; Perhaps 80 ℃ were toasted 3 minutes, were adjusted to 110 ℃ and toasted 3 minutes again, made carbon fibre initial rinse fabric;
E, back through 6 rollings of rolling equipment by the two sides covered with protective film (PET mould release membrance or other) of 5 pairs of carbon fibre initial rinse fabrics of equipment for coating film;
(2), pultrusion: like Fig. 2, shown in 3:
a, carbon fibre initial rinse fabric are that the mould 7 of 900mm carries out the pultrusion of arc through length; While is 80 ℃, 130 ℃, 130 ℃ 3 humidity provinces in the carbon fibre initial rinse fabric process mould 7 in the pultrusion process; Because temperature is bigger to the quality influence of product; It is to arrive each satisfied curing degree of setting in back, district in order to control product that a plurality of humidity provinces are set, and the temperature that is controlled to type die 7 each paragraph through strictness can be improved the quality of products and stability.The temperature in 2 districts and 3 districts is according to the actual process condition, and both differ about 5 degree, do not have also can merging of specific (special) requirements for some quality, finally make the arc goods;
b, arc finished product get in the curing oven 8 of back and are cured, and make finished product and under the traction of pulling equipment 9, put in order.
except that present embodiment, resin matrix can also be other high-performance thermosettings or thermoplastic resin.Outside the carbon fiber, also can use other fiber, the making shape is similar, the arc goods that purposes is different.
the foregoing description only is explanation technical conceive of the present invention and characteristics, and its purpose is to let the personage who is familiar with this technology can understand content of the present invention and enforcement according to this, can not limit protection scope of the present invention with this.All equivalences that spirit is done according to the present invention change or modify, and all should be encompassed within protection scope of the present invention.

Claims (8)

1. the dry-press process technology of an arc continuous fiber composite material plate, it is characterized in that: it may further comprise the steps:
(1), impregnation:
Prepare required silvalin group, described silvalin is rolled into a ball launched, evenly be scattered in the wide tow of 90-120mm that is; Described tow is carried out the resin impregnation; , described tow toasts and makes fiber preimpregnation cloth after soaking into fully;
(2), pultrusion:
Described fiber preimpregnation cloth is carried out pultrusion camber goods; Described arc goods are cured, and solidification temperature is 150-200 ℃, and makes finished product.
2. the dry-press process technology of arc continuous fiber composite material plate according to claim 1 is characterized in that: the humidity that described silvalin is rolled into a ball is less than 50%.
3. the dry-press process technology of arc continuous fiber composite material plate according to claim 1 is characterized in that: after making described fiber preimpregnation cloth, its two faces are carried out the covering of diaphragm, and rolling.
4. the dry-press process technology of arc continuous fiber composite material plate according to claim 1 is characterized in that: in the pultrusion process, described fiber pre-preg cloth is respectively through 3 humidity province: 70-90 ℃, 120-140 ℃ and 120-140 ℃.
5. the dry-press process technology of arc continuous fiber composite material plate according to claim 1 is characterized in that: soak into described tow 110-130 ℃ of baking in back 2-4 minute fully; Perhaps 70-90 ℃ was toasted 2-4 minute, was adjusted to 100-120 ℃ and toasted 2-4 minute again.
6. the dry-press process technology of arc continuous fiber composite material plate according to claim 1 is characterized in that: described diaphragm is the PET mould release membrance.
7. the dry-press process technology of arc continuous fiber composite material plate according to claim 1 is characterized in that: described silvalin is rolled into a ball and is adopted carbon fiber.
8. the dry-press process technology of arc continuous fiber composite material plate according to claim 1 is characterized in that: described resin adopts epoxy resin.
CN2012100047992A 2012-01-10 2012-01-10 Dry process for forming arc-shaped continuous fiber composite board Pending CN102582095A (en)

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Application Number Priority Date Filing Date Title
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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104802426A (en) * 2015-04-03 2015-07-29 上海华渔新材料科技有限公司 Carbon fiber thermoplastic prepreg with complex structure and preparation method of carbon fiber thermoplastic prepreg
CN104802423A (en) * 2015-04-03 2015-07-29 上海华渔新材料科技有限公司 Preparation method of fiber reinforced thermoplastic resin based composite automobile hub
CN106488836A (en) * 2014-05-12 2017-03-08 德侯特科技公司 For impregnating the cotton rope of natural fiber especially Caulis et Folium Lini or the continuous apparatus of band in a single step
CN109867908A (en) * 2017-12-05 2019-06-11 广州金发碳纤维新材料发展有限公司 A kind of manufacturing method of the fibre reinforced sheet moulding material of high fluidity
CN110831746A (en) * 2017-05-04 2020-02-21 泽菲罗斯有限公司 Pultruded impregnated fibers and uses thereof
CN112824574A (en) * 2019-11-20 2021-05-21 南京启复新材料科技有限公司 Production process of impregnation twisted chopped fiber bundles
CN114043750A (en) * 2021-09-30 2022-02-15 安徽智达电气科技有限公司 Preparation process of epoxy board for electrical insulation

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1603363A (en) * 2004-08-10 2005-04-06 大连理工大学 Preparation for continuous fibre reinforced poly(phthalazinone ehter sulfone ketone) composite materials
CN101870171A (en) * 2010-07-08 2010-10-27 廖济柙 Pultrusion method and special equipment for producing bent section

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1603363A (en) * 2004-08-10 2005-04-06 大连理工大学 Preparation for continuous fibre reinforced poly(phthalazinone ehter sulfone ketone) composite materials
CN101870171A (en) * 2010-07-08 2010-10-27 廖济柙 Pultrusion method and special equipment for producing bent section

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106488836A (en) * 2014-05-12 2017-03-08 德侯特科技公司 For impregnating the cotton rope of natural fiber especially Caulis et Folium Lini or the continuous apparatus of band in a single step
CN104802426A (en) * 2015-04-03 2015-07-29 上海华渔新材料科技有限公司 Carbon fiber thermoplastic prepreg with complex structure and preparation method of carbon fiber thermoplastic prepreg
CN104802423A (en) * 2015-04-03 2015-07-29 上海华渔新材料科技有限公司 Preparation method of fiber reinforced thermoplastic resin based composite automobile hub
CN104802423B (en) * 2015-04-03 2020-10-30 上海华渔新材料科技有限公司 Preparation method of fiber-reinforced thermoplastic resin-based composite material automobile hub
CN110831746A (en) * 2017-05-04 2020-02-21 泽菲罗斯有限公司 Pultruded impregnated fibers and uses thereof
CN109867908A (en) * 2017-12-05 2019-06-11 广州金发碳纤维新材料发展有限公司 A kind of manufacturing method of the fibre reinforced sheet moulding material of high fluidity
CN109867908B (en) * 2017-12-05 2021-09-03 广州金发碳纤维新材料发展有限公司 Manufacturing method of high-fluidity carbon fiber reinforced sheet die-pressing material
CN112824574A (en) * 2019-11-20 2021-05-21 南京启复新材料科技有限公司 Production process of impregnation twisted chopped fiber bundles
CN114043750A (en) * 2021-09-30 2022-02-15 安徽智达电气科技有限公司 Preparation process of epoxy board for electrical insulation

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Application publication date: 20120718