CN101461561B - Conversion agent of fire-cured tobacco odor type as well as preparation method and use method thereof - Google Patents
Conversion agent of fire-cured tobacco odor type as well as preparation method and use method thereof Download PDFInfo
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- CN101461561B CN101461561B CN2008100491703A CN200810049170A CN101461561B CN 101461561 B CN101461561 B CN 101461561B CN 2008100491703 A CN2008100491703 A CN 2008100491703A CN 200810049170 A CN200810049170 A CN 200810049170A CN 101461561 B CN101461561 B CN 101461561B
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Abstract
The invention discloses a cured tobacco leaf scent type modifier, preparation and use method thereof. The cured tobacco leaf scent type modifier comprises 1-3 by weight parts of fragrance adding impurity removing agent, 1.5-2.0 by weight parts of plant extract, 5-10 by weight parts of moisture keeping agent. The cured tobacco leaf scent type modifier comprises a plurality of natural fragrant, impurity removing and harm reducing ingredients, which is capable of fragrance adding, scent type modifying. Through industrial application, fume and impurity gas is reduced, harmful ingredients are reduced, and function of promoting scent of cigarette is obvious. The modifier has long storage period, and valid using period under low temperature storage condition can reach 1 year. The material is easy to be obtained. No waste water, gas and residue is generated in the whole preparation. The modifier can be produced into mixed fertilizer by mixing with other fertilizer, or be used as fuel. The preparation is simple, beneficial to industrial production.
Description
Technical field
The present invention relates to a kind of cured tobacco leaf additive, be specifically related to a kind of cigarette additive and preparation and using method that reduces the assorted gas of cigarette smoke and change the tobacco leaf odor type.
Background technology
Cigarette product can give out the strong fragrant tempting cigarette perfume (or spice) of fragrance when opening cigarette case, can produce strong fragrance and inhale flavor when smoking, and the fragrance of cigarette tends to become consumer's smoking habit, and wish stablizing of maintenance style.But tobacco leaf is the organism of a complexity, and its chemical composition and physical behavior depend on all multifactor.Because the tobacco leaf planting scope is wide, the difference of objective factors such as the soil between the different regions, weather, kind all can influence tobacco leaf suction quality, more or less can produce bad suction flavor and breath, such as middle odor type cured tobacco leaf, fragrance is thin, assorted gas is heavier, and industrial applicability is relatively poor.
At present, cigarette industry is used for increasing tabacco fragrance, the countermeasure that alleviates the assorted gas of flue gas mostly is to add to shelter the mix essence and flavoring agent of gas of flue gas in tobacco product.Yet add existing essence and flavoring agent, reduce assorted gas, the effect of improving fragrance is not clearly.
Summary of the invention
The purpose of this invention is to provide a kind of tobacco leaf flavouring, odor type of making and change, reduce the assorted gas of flue gas, reduce harmful components, cured tobacco leaf odor type agent transition of outstanding cigarette smoke style.
Another object of the present invention provides that a kind of extraction efficiency height, speed are fast, pollution-free, the preparation method of simple cured tobacco leaf odor type agent transition of technology.
The present invention also aims to provide a kind of using method of cured tobacco leaf odor type agent transition of the present invention.
To achieve these goals, the technical solution used in the present invention is:
Cured tobacco leaf odor type agent transition of the present invention, it comprises flavouring cleaner 1～3 weight portion, plant extracts 1.5～2 weight portions, humectant 5～10 weight portions.
Flavouring cleaner in agent transition of cured tobacco leaf odor type is mainly made by the fruit of Chinese magnoliavine 1.5～2.0 weight portions, blueberry seed shell 2.0～2.5 weight portions.Plant extracts is mainly by tobacco leaf fragment 2.0～3.0 weight portions, and wild perillaseed 1.5～2.0 weight portions, orrisroot 1.5～2.0 weight portions are made.Humectant is made up of propane diols 1～2 weight portion, glycerine 1～2 weight portion, corn syrup 2～4 weight portions.
The preparation method of the flavouring cleaner in agent transition of cured tobacco leaf odor type step as follows carries out:
(1) fruit of Chinese magnoliavine was pulverized 20 mesh sieves and make meal, the blueberry press residue that brewing blueberry wine obtains is removed impurity, gets blueberry seed shell and dries.With above-mentioned fruit of Chinese magnoliavine meal 1.5～2.0 weight portions that obtain, blueberry seed shell 2.0～2.5 weight portions are inserted in the infuser, add 60% ethanol of 2.5～3.0 times of amounts of raw material weight, the sealing infuser flooded 3～5 days under 30 ℃ of temperature, the middle stirring 3～5 times, its composition is leached, filter, the filtrate of collection was left standstill 24 hours, discard precipitation, the supernatant decompression distillation that obtains is condensed into paste;
(2) paste that step (1) the is obtained ethanol that adds 2.0～2.5 times of amounts of its weight fully dissolves it, obtains the pure agent of the fruit of Chinese magnoliavine and blueberry seed shell;
(3) pure agent 3.0～3.5 weight portions that step (2) is obtained, penta flavor ketone, 1.0～1.5 weight portions, β-damascone 0.5～1.0 weight portion, Megastigmatrienone 0.5～1.0 weight portion are put into fully mixed dissolution of reactor, obtain the flavouring cleaner.
The preparation method of the plant extracts in agent transition of cured tobacco leaf odor type is: cured tobacco leaf is made fragment, and the orrisroot section is dried through natural slaking, pulverizes 20 mesh sieves after the fermentation and makes meal, and wild perillaseed is fried and made meal to there being cracker to pulverize 20 mesh sieves.With the above-mentioned tobacco leaf fragment that obtains 2.0～3.0 weight portions, wild perillaseed meal 1.5～2.0 weight portions, 1.5～2.0 weight portion orrisroot meal are put into supercritical CO
2In the fluid extraction device, add ethanol for guiding and supporting agent, amount of alcohol added is 7～9% of a raw material gross weight, at pressure 20～50Mpa, 30～60 ℃ of extraction temperature, the cycling extraction through 1～3 hour, the plant extraction liquid that obtains left standstill 24 hours, discard precipitation, the supernatant of acquisition is plant extracts.
Humectant in agent transition of cured tobacco leaf odor type is by the propane diols of 1～2 weight portion, the glycerine of 1～2 weight portion and mixed the getting of corn syrup of 2～4 weight portions.
The preparation method of cured tobacco leaf odor type agent transition is: flavouring cleaner 1～3 weight portion, plant extracts 1.5～2.0 weight portions and humectant 5～10 weight portions mix and obtain agent transition of cured tobacco leaf odor type.
The using method of cured tobacco leaf odor type agent transition is: cured tobacco leaf odor type agent transition of per 1 weight portion is dissolved the water dilution of back with 3～5 weight portions with the ethanol of 2～3 weight portions; Middle odor type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and cured tobacco leaf odor type dilution agent liquid transition is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 15～30 days; Cured tobacco leaf odor type agent transition addition is that the sheet cigarette of per 1000 weight portions adds cured tobacco leaf odor type agent transition 7～15 weight portions.
Cured tobacco leaf odor type agent transition of the present invention is become to be grouped into the removal of impurities harm reduction by multiple natural flavor, and these compositions can make the tobacco leaf flavouring, and odor type changes, and uses through cigarette industry, reduces the assorted gas of flue gas, reduces harmful components, and outstanding cigarette flavor style effect is obvious.Long shelf-life, low temperature preservation condition following effective life, can reach 1 year.The preparation raw material is easy to get, and does not produce waste water in the whole preparation process flow process, waste gas, and waste residue can be mixed to macerate and make mixed fertilizer or act as a fuel with other fertilizer.Preparation technology is simple, helps suitability for industrialized production.
Description of drawings
Accompanying drawing is a cured tobacco leaf odor type agent transition preparation method's of the present invention process chart.
The specific embodiment
Below by embodiment the present invention is elaborated.
Embodiment 1
One, the preparation of cured tobacco leaf odor type agent transition
1. the preparation of flavouring cleaner
(1) fruit of Chinese magnoliavine was pulverized 20 mesh sieves and make meal, the blueberry press residue that brewing blueberry wine obtains is removed impurity, gets blueberry seed shell and dries.With above-mentioned fruit of Chinese magnoliavine meal 1.5 weight portions that obtain, blueberry seed shell 2.2 weight portions are inserted in the infuser, add 60% ethanol of 3.0 times of amounts (11.1 weight portion) of raw material weight, the sealing infuser flooded 3 days under 30 ℃ of left and right sides temperature, the middle stirring 3 times, its composition is leached, filter, the filtrate of collection was left standstill 24 hours, discard precipitation, the supernatant decompression distillation that obtains is condensed into paste;
(2) paste that step (1) the is obtained ethanol that adds 2.0 times of amounts of its weight fully dissolves it, obtains the pure agent of the fruit of Chinese magnoliavine and blueberry seed shell;
(3) pure agent 3.0 weight portions that step (2) is obtained, penta flavor ketone, 1.5 weight portions, β-damascone 0.6 weight portion, Megastigmatrienone 0.8 weight portion are put into fully mixed dissolution of reactor, obtain the flavouring cleaner.
2. the preparation of plant extracts
Cured tobacco leaf is made fragment, and the orrisroot section is dried through natural slaking, pulverizes 20 mesh sieves after the fermentation and makes meal, and wild perillaseed is fried and made meal to there being cracker to pulverize 20 mesh sieves.With the above-mentioned tobacco leaf fragment that obtains 2.0 weight portions, wild perillaseed meal 1.8 weight portions, 2.0 weight portion orrisroot meal are put into supercritical CO
2In the fluid extraction device, add ethanol for guiding and supporting agent, amount of alcohol added is 7% (0.41 weight portion) of raw material gross weight, at pressure 20Mpa, 40 ℃ of extraction temperature, the cycling extraction through 3 hours, the plant extraction liquid that obtains left standstill 24 hours, discard precipitation, the supernatant of acquisition is plant extracts.
3. the preparation of humectant
With the propane diols of 1.5 weight portions, the glycerine of 1.8 weight portions and mixed the getting of corn syrup of 2.0 weight portions.
4. the preparation of cured tobacco leaf odor type agent transition
Flavouring cleaner 2 weight portions, plant extracts 1.5 weight portions and humectant 5 weight portions are mixed obtain agent cured tobacco leaf odor type transition.
Two, the using method of cured tobacco leaf odor type agent transition
Cured tobacco leaf odor type agent transition of per 1 weight portion is dissolved the water dilution of back with 4 weight portions with the ethanol of 3 weight portions; Middle odor type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and cured tobacco leaf odor type dilution agent liquid transition is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 15 days; Cured tobacco leaf odor type agent transition addition is that the sheet cigarette of per 1000 weight portions adds cured tobacco leaf odor type agent transition 10 weight portions.
Embodiment 2
One, the preparation of cured tobacco leaf odor type agent transition
1. the preparation of flavouring cleaner
(1) fruit of Chinese magnoliavine was pulverized 20 mesh sieves and make meal, the blueberry press residue that brewing blueberry wine obtains is removed impurity, gets blueberry seed shell and dries.With above-mentioned fruit of Chinese magnoliavine meal 1.6 weight portions that obtain, blueberry seed shell 2.5 weight portions are inserted in the infuser, add 60% ethanol of 2.5 times of amounts (10.25 weight portion) of raw material weight, the sealing infuser flooded 4 days under 30 ℃ of left and right sides temperature, the middle stirring 4 times, its composition is leached, filter, the filtrate of collection was left standstill 24 hours, discard precipitation, the supernatant decompression distillation that obtains is condensed into paste;
(2) paste that step (1) the is obtained ethanol that adds 2.5 times of amounts of its weight fully dissolves it, obtains the pure agent of the fruit of Chinese magnoliavine and blueberry seed shell;
(3) pure agent 3.5 weight portions that step (2) is obtained, penta flavor ketone, 1.2 weight portions, β-damascone 0.5 weight portion, Megastigmatrienone 0.6 weight portion are put into fully mixed dissolution of reactor, obtain the flavouring cleaner.
2. the preparation of plant extracts
Cured tobacco leaf is made fragment, and the orrisroot section is dried through natural slaking, pulverizes 20 mesh sieves after the fermentation and makes meal, and wild perillaseed is fried and made meal to there being cracker to pulverize 20 mesh sieves.With the above-mentioned tobacco leaf fragment that obtains 2.2 weight portions, wild perillaseed meal 2.0 weight portions, 1.8 weight portion orrisroot meal are put into supercritical CO
2In the fluid extraction device, add ethanol for guiding and supporting agent, amount of alcohol added is 9% (0.54 weight portion) of raw material gross weight, at pressure 30Mpa, 30 ℃ of extraction temperature, the cycling extraction through 2 hours, the plant extraction liquid that obtains left standstill 24 hours, discard precipitation, the supernatant of acquisition is plant extracts.
3. the preparation of humectant
With the propane diols of 2 weight portions, the glycerine of 1 weight portion and mixed the getting of corn syrup of 4 weight portions.
4. the preparation of cured tobacco leaf odor type agent transition
Flavouring cleaner 1 weight portion, plant extracts 1.6 weight portions and humectant 6 weight portions are mixed obtain agent cured tobacco leaf odor type transition.
Two, the using method of cured tobacco leaf odor type agent transition
Cured tobacco leaf odor type agent transition of per 1 weight portion is dissolved the water dilution of back with 5 weight portions with the ethanol of 2.2 weight portions; Middle odor type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and cured tobacco leaf odor type dilution agent liquid transition is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 30 days; Cured tobacco leaf odor type agent transition addition is that the sheet cigarette of per 1000 weight portions adds cured tobacco leaf odor type agent transition 7 weight portions.
Embodiment 3
One, the preparation of cured tobacco leaf odor type agent transition
1. the preparation of flavouring cleaner
(1) fruit of Chinese magnoliavine was pulverized 20 mesh sieves and make meal, the blueberry press residue that brewing blueberry wine obtains is removed impurity, gets blueberry seed shell and dries.With above-mentioned fruit of Chinese magnoliavine meal 1.7 weight portions that obtain, blueberry seed shell 2.4 weight portions are inserted in the infuser, add 60% ethanol of 2.4 times of amounts (9.84 weight portion) of raw material weight, the sealing infuser flooded 5 days under 30 ℃ of left and right sides temperature, the middle stirring 5 times, its composition is leached, filter, the filtrate of collection was left standstill 24 hours, discard precipitation, the supernatant decompression distillation that obtains is condensed into paste;
(2) paste that step (1) the is obtained ethanol that adds 2.4 times of amounts of its weight fully dissolves it, obtains the pure agent of the fruit of Chinese magnoliavine and blueberry seed shell;
(3) pure agent 3.3 weight portions that step (2) is obtained, penta flavor ketone, 1.3 weight portions, β-damascone 0.8 weight portion, Megastigmatrienone 0.5 weight portion are put into fully mixed dissolution of reactor, obtain the flavouring cleaner.
2. the preparation of plant extracts
Cured tobacco leaf is made fragment, and the orrisroot section is dried through natural slaking, pulverizes 20 mesh sieves after the fermentation and makes meal, and wild perillaseed is fried and made meal to there being cracker to pulverize 20 mesh sieves.With the above-mentioned tobacco leaf fragment that obtains 2.3 weight portions, wild perillaseed meal 1.6 weight portions, 1.5 weight portion orrisroot meal are put into supercritical CO
2In the fluid extraction device, add ethanol for guiding and supporting agent, amount of alcohol added is 7.5% (0.41 weight portion) of raw material gross weight, at pressure 40Mpa, 50 ℃ of extraction temperature, the cycling extraction through 1 hour, the plant extraction liquid that obtains left standstill 24 hours, discard precipitation, the supernatant of acquisition is plant extracts.
3. the preparation of humectant
With the propane diols of 1 weight portion, the glycerine of 1.5 weight portions and mixed the getting of corn syrup of 3 weight portions.
4. the preparation of cured tobacco leaf odor type agent transition
Flavouring cleaner 3 weight portions, plant extracts 1.8 weight portions and humectant 9 weight portions are mixed obtain agent cured tobacco leaf odor type transition.
Two, the using method of cured tobacco leaf odor type agent transition
Cured tobacco leaf odor type agent transition of per 1 weight portion is dissolved the water dilution of back with 3 weight portions with the ethanol of 2.5 weight portions; Middle odor type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and cured tobacco leaf odor type dilution agent liquid transition is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 25 days; Cured tobacco leaf odor type agent transition addition is that the sheet cigarette of per 1000 weight portions adds cured tobacco leaf odor type agent transition 15 weight portions.
Embodiment 4
One, the preparation of cured tobacco leaf odor type agent transition
1. the preparation of flavouring cleaner
(1) fruit of Chinese magnoliavine was pulverized 20 mesh sieves and make meal, the blueberry press residue that brewing blueberry wine obtains is removed impurity, gets blueberry seed shell and dries.With above-mentioned fruit of Chinese magnoliavine meal 1.8 weight portions that obtain, blueberry seed shell 2.3 weight portions are inserted in the infuser, add 60% ethanol of 2.8 times of amounts (11.48 weight portion) of raw material weight, the sealing infuser flooded 3.5 days under 30 ℃ of left and right sides temperature, the middle stirring 3 times, its composition is leached, filter, the filtrate of collection was left standstill 24 hours, discard precipitation, the supernatant decompression distillation that obtains is condensed into paste;
(2) paste that step (1) the is obtained ethanol that adds 2.1 times of amounts of its weight fully dissolves it, obtains the pure agent of the fruit of Chinese magnoliavine and blueberry seed shell;
(3) pure agent 3.4 weight portions that step (2) is obtained, penta flavor ketone, 1.4 weight portions, β-damascone 0.9 weight portion, Megastigmatrienone 1.0 weight portions are put into fully mixed dissolution of reactor, obtain the flavouring cleaner.
2. the preparation of plant extracts
Cured tobacco leaf is made fragment, and the orrisroot section is dried through natural slaking, pulverizes 20 mesh sieves after the fermentation and makes meal, and wild perillaseed is fried and made meal to there being cracker to pulverize 20 mesh sieves.With the above-mentioned tobacco leaf fragment that obtains 2.4 weight portions, wild perillaseed meal 1.5 weight portions, 1.6 weight portion orrisroot meal are put into supercritical CO
2In the fluid extraction device, add ethanol for guiding and supporting agent, amount of alcohol added is 8% (0.44 weight portion) of raw material gross weight, at pressure 50Mpa, 60 ℃ of extraction temperature, the cycling extraction through 2.5 hours, the plant extraction liquid that obtains left standstill 24 hours, discard precipitation, the supernatant of acquisition is plant extracts.
3. the preparation of humectant
With the propane diols of 1.2 weight portions, the glycerine of 2.0 weight portions and mixed the getting of corn syrup of 2.5 weight portions.
4. the preparation of cured tobacco leaf odor type agent transition
Flavouring cleaner 1.5 weight portions, plant extracts 1.9 weight portions and humectant 8 weight portions are mixed obtain agent cured tobacco leaf odor type transition.
Two, the using method of cured tobacco leaf odor type agent transition
Cured tobacco leaf odor type agent transition of per 1 weight portion is dissolved the water dilution of back with 3.5 weight portions with the ethanol of 2.8 weight portions; Middle odor type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and cured tobacco leaf odor type dilution agent liquid transition is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 20 days; Cured tobacco leaf odor type agent transition addition is that the sheet cigarette of per 1000 weight portions adds cured tobacco leaf odor type agent transition 12 weight portions.
Embodiment 5
One, the preparation of cured tobacco leaf odor type agent transition
1. the preparation of flavouring cleaner
(1) fruit of Chinese magnoliavine was pulverized 20 mesh sieves and make meal, the blueberry press residue that brewing blueberry wine obtains is removed impurity, gets blueberry seed shell and dries.With above-mentioned fruit of Chinese magnoliavine meal 2.0 weight portions that obtain, blueberry seed shell 2.0 weight portions are inserted in the infuser, add 60% ethanol of 2.9 times of amounts (11.6 weight portion) of raw material weight, the sealing infuser flooded 4.5 days under 30 ℃ of left and right sides temperature, the middle stirring 4 times, its composition is leached, filter, the filtrate of collection was left standstill 24 hours, discard precipitation, the supernatant decompression distillation that obtains is condensed into paste;
(2) paste that step (1) the is obtained ethanol that adds 2.2 times of amounts of its weight fully dissolves it, obtains the pure agent of the fruit of Chinese magnoliavine and blueberry seed shell;
(3) pure agent 3.2 weight portions that step (2) is obtained, penta flavor ketone, 1.0 weight portions, β-damascone 1.0 weight portions, Megastigmatrienone 0.9 weight portion are put into fully mixed dissolution of reactor, obtain the flavouring cleaner.
2. the preparation of plant extracts
Cured tobacco leaf is made fragment, and the orrisroot section is dried through natural slaking, pulverizes 20 mesh sieves after the fermentation and makes meal, and wild perillaseed is fried and made meal to there being cracker to pulverize 20 mesh sieves.With the above-mentioned tobacco leaf fragment that obtains 2.5 weight portions, wild perillaseed meal 1.7 weight portions, 1.4 weight portion orrisroot meal are put into supercritical CO
2In the fluid extraction device, add ethanol for guiding and supporting agent, amount of alcohol added is 8.5% (0.45 weight portion) of raw material gross weight, at pressure 35Mpa, 45 ℃ of extraction temperature, the cycling extraction through 1.5 hours, the plant extraction liquid that obtains left standstill 24 hours, discard precipitation, the supernatant of acquisition is plant extracts.
3. the preparation of humectant
With the propane diols of 1.8 weight portions, the glycerine of 1.3 weight portions and mixed the getting of corn syrup of 3.5 weight portions.
4. the preparation of cured tobacco leaf odor type agent transition
Flavouring cleaner 2.5 weight portions, plant extracts 2.0 weight portions and humectant 10 weight portions are mixed obtain agent cured tobacco leaf odor type transition.
Two, the using method of cured tobacco leaf odor type agent transition
Cured tobacco leaf odor type agent transition of per 1 weight portion is dissolved the water dilution of back with 4.5 weight portions with the ethanol of 2 weight portions; Middle odor type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and cured tobacco leaf odor type dilution agent liquid transition is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 22 days; Cured tobacco leaf odor type agent transition addition is that the sheet cigarette of per 1000 weight portions adds cured tobacco leaf odor type agent transition 9 weight portions.
Embodiment 6
One, the cured tobacco leaf preparation of table material
1. the preparation of flavouring cleaner
The method that repeats embodiment 1 obtains the flavouring cleaner.
2. the preparation of plant extracts
The method that repeats embodiment 1 obtains plant extracts.
3. the preparation of humectant
The method that repeats embodiment 1 obtains humectant.
4. the preparation of cured tobacco leaf odor type agent transition
The method that repeats embodiment 1 obtains agent transition of cured tobacco leaf odor type.
Two, the using method of cured tobacco leaf odor type agent transition
Cured tobacco leaf odor type agent transition of per 1 weight portion is diluted with the back water with 4.2 weight portions of the ethanol dissolving of 2.4 times of weight portions.Middle odor type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and cured tobacco leaf odor type dilution agent liquid transition is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 18 days; Cured tobacco leaf odor type agent transition addition is that the sheet cigarette of per 1000 weight portions adds cured tobacco leaf odor type agent transition 11 weight portions.
Weight portion in the embodiment of the invention can be gram, kilogram or other unit of weight.
Claims (2)
1. cured tobacco leaf odor type agent transition, it is characterized in that: it comprises flavouring cleaner 1～3 weight portion, plant extracts 1.5～2.0 weight portions, humectant 5～10 weight portions;
Described flavouring cleaner is mainly by the fruit of Chinese magnoliavine 1.5～2.0 weight portions, blueberry seed shell 2.0～2.5 weight portions are made by following method: (1) was pulverized 20 mesh sieves with the fruit of Chinese magnoliavine and was made meal, the blueberry press residue that brewing blueberry wine obtains, remove impurity, getting blueberry seed shell dries, with above-mentioned fruit of Chinese magnoliavine meal 1.5～2.0 weight portions that obtain, blueberry seed shell 2.0～2.5 weight portions are inserted in the infuser, 60% the ethanol that adds 2.5～3.0 times of amounts of raw material weight, the sealing infuser, under 30 ℃ of temperature, flooded 3～5 days, the middle stirring 3～5 times leached its composition, filters, the filtrate of collecting was left standstill 24 hours, discard precipitation, the supernatant that obtains is at 35～40 ℃, and decompression distillation is condensed into paste under the 80Kpa;
(2) paste that step (1) the is obtained ethanol that adds 2.0～2.5 times of amounts of its weight fully dissolves it, obtains the pure agent of the fruit of Chinese magnoliavine and blueberry seed shell;
(3) pure agent 3.0～3.5 weight portions that step (2) is obtained, penta flavor ketone, 1.0～1.5 weight portions, β-damascone 0.5～1.0 weight portion, Megastigmatrienone 0.5～1.0 weight portion are put into fully mixed dissolution of reactor, obtain the flavouring cleaner;
Described plant extracts is mainly by tobacco leaf fragment 2.0～3.0 weight portions, wild perillaseed 1.5～2.0 weight portions, orrisroot 1.5～2.0 weight portions are made by following method: cured tobacco leaf is made fragment, the orrisroot section is dried through natural slaking, pulverized 20 mesh sieves after the fermentation and make meal, wild perillaseed is fried and is made meal to there being cracker to pulverize 20 mesh sieves; With the above-mentioned tobacco leaf fragment that obtains 2.0～3.0 weight portions, wild perillaseed meal 1.5～2.0 weight portions, 1.5～2.0 weight portion orrisroot meal are put into supercritical CO
2In the fluid extraction device, add ethanol for guiding and supporting agent, amount of alcohol added is 7～9% of a raw material gross weight, at pressure 20～50Mpa, 30～60 ℃ of extraction temperature, the cycling extraction through 1～3 hour, the plant extraction liquid that obtains left standstill 24 hours, discard precipitation, the supernatant of acquisition is plant extracts;
Described humectant is mixed by propane diols 1～2 weight portion, glycerine 1～2 weight portion, corn syrup 2～4 weight portions.
2. the using method of the described cured tobacco leaf odor type of claim 1 agent transition is characterized in that: cured tobacco leaf odor type agent transition of per 1 weight portion is diluted with the ethanol dissolving back of 2～3 weight portions water with 3～5 weight portions; Middle odor type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and cured tobacco leaf odor type dilution agent liquid transition is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 15～30 days; Cured tobacco leaf odor type agent transition addition is that the sheet cigarette of per 1000 weight portions adds cured tobacco leaf odor type agent transition 7～15 weight portions.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN2008100491703A CN101461561B (en) | 2008-01-29 | 2008-01-29 | Conversion agent of fire-cured tobacco odor type as well as preparation method and use method thereof |
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| CN2008100491703A CN101461561B (en) | 2008-01-29 | 2008-01-29 | Conversion agent of fire-cured tobacco odor type as well as preparation method and use method thereof |
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| CN101461561A CN101461561A (en) | 2009-06-24 |
| CN101461561B true CN101461561B (en) | 2011-05-18 |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102524932B (en) * | 2010-12-21 | 2013-11-13 | 湖北中烟工业有限责任公司 | Method for applying natural solid flavors and fragrances to papermaking-reconstructed tobacco sheets |
| CN105901772A (en) * | 2016-04-29 | 2016-08-31 | 郑志炫 | Odorizing block filler with blood circulation promoting and phlegm reducing functions and preparation method |
| CN105852214A (en) * | 2016-04-29 | 2016-08-17 | 郑志炫 | Odorizing filler with nerve soothing/sleep improving function and preparation method |
| CN109349678B (en) * | 2018-11-09 | 2021-04-16 | 湖北中烟工业有限责任公司 | Preparation method and application of composite tobacco leaf extract |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1064792A (en) * | 1991-03-18 | 1992-09-30 | 杨一兵 | The production method of tobacco extract |
| CN1494837A (en) * | 2002-04-30 | 2004-05-12 | 吴上辉 | Xinjian tobacco. health-care cigarette |
| CN1933744A (en) * | 2004-02-19 | 2007-03-21 | 三荣源有限公司 | Nicotine-reducing agent and nicotine reduction method |
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2008
- 2008-01-29 CN CN2008100491703A patent/CN101461561B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1064792A (en) * | 1991-03-18 | 1992-09-30 | 杨一兵 | The production method of tobacco extract |
| CN1494837A (en) * | 2002-04-30 | 2004-05-12 | 吴上辉 | Xinjian tobacco. health-care cigarette |
| CN1933744A (en) * | 2004-02-19 | 2007-03-21 | 三荣源有限公司 | Nicotine-reducing agent and nicotine reduction method |
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| CN101461561A (en) | 2009-06-24 |
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