CN101637303A - Lemon extract, preparation method thereof and application thereof in cigarette flavoring - Google Patents
Lemon extract, preparation method thereof and application thereof in cigarette flavoring Download PDFInfo
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- CN101637303A CN101637303A CN200810073704A CN200810073704A CN101637303A CN 101637303 A CN101637303 A CN 101637303A CN 200810073704 A CN200810073704 A CN 200810073704A CN 200810073704 A CN200810073704 A CN 200810073704A CN 101637303 A CN101637303 A CN 101637303A
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Abstract
The invention relates to a lemon extract, a preparation method thereof and application thereof in cigarette flavoring. The main raw material of the lemon extract is lemon. The preparation method comprises the steps of lemon, squeezing, solvent extraction, solid-liquid separation, clarification filtration, distilling and concentrating and lemon extract obtaining. The application of the lemon extract in cigarette flavoring is implemented by the following steps: dissolving 0.1 to 10 percent of lemon extract by weight of cigarette shreds, flakes or tobacco stalks into ethanol with certain concentration or solution of ethanol and propylene glycol solution, and evenly spraying the mixture to the cigarette shreds, the flakes or the tobacco stalks to be wrapped into cigarettes. The cigarette addedwith the lemon extract has the function of remarkably reducing stimulation produced by smoke on the throat, enables the cigarette smoke to be fine and soft, has comfortable after taste, reduces impurity gas, increases flavor, improves the mouth feel after taste, and relives the harm of smoking.
Description
Technical field
The present invention relates to the extraction and the application of natural essence spices, relate in particular to a kind of lemon extract and preparation method thereof and the application in perfuming cigarette is reinforced.
Background technology
China is first big country of World tobacco production and consumption.The annual leaf tobacco production amount of China accounts for 35% of world's total amount, and the cigarette volume of production and marketing accounts for 32% of world's total amount.Because factor affecting such as the defective of tobacco itself is big as assorted gas, bitter taste, fiber taste objectively need to improve or cover, so tobacco industry will be used a large amount of perfume additives in its product.With regard to the cigarette flavors additive, countries in the world all take much count of its research.Comparatively speaking, China is relatively weak in cigarette flavors additive industrial system, and the cigarette flavors additive product is of poor quality, the kind of Gong selecting for use is more limited, also these perfume additive major controls in supplier's hand, the overwhelming majority is a composite, product composition is indeterminate, the quality instability.For a long time, this is a bottleneck problem of restriction cigarette industry enterprise.
Lemon has another name called the lemon fruit, lemon, the female fruit of benefit.Originate in Malaysia, there is cultivation on ground such as China Taiwan, Fujian, Guangdong, Guangxi at present.Lemon is that one of fruit of medical value is arranged in the world most, and it is rich in vitamin C, citric acid, malic acid, plants essential oil etc., and is very useful to human body.Not only high-grade drink can be produced, also the lemonene essential oil can be produced.It is pure and fresh to have fresh powerful again brisk clean fragrance in fragrant and sweet, is best a kind of of the detoxifcation of citrus the inside, deodorizing effect, also is that a kind of good fragrance source of being used as fixastive is often brought in many perfume industry.Its smell delicate fragrance can improve spirit, help the state of mind clarification, eliminate taediumvitae, and tool is good for the stomach, helps digest, and is that excellent antibiotic antidote and beautifying skin are contained product.
Through the periodical literature retrieval, do not find the application study of lemon extract in perfuming cigarette is reinforced as yet.Through the Chinese patent literature retrieval, do not find the application patent of lemon extract in perfuming cigarette is reinforced equally.
Biochemical functions based on above lemon, research is effective component extracting from lemon, development Chinese style cigarette flavors additive green, pure natural, make the fragrant jealous improvement of cigarette, fragrance is coordinated, and pleasant impression is comfortable, flue gas exquisiteness, soft, and effectively reduce the pungent stimulation of flue gas to smoker's respiratory system, and alleviate harm of smoking, will have remarkable economical and social benefit.
Summary of the invention
The purpose of this invention is to provide a kind of lemon extract and preparation method thereof and the application in perfuming cigarette is reinforced.
For realizing the purpose of foregoing invention, be achieved through the following technical solutions:
The primary raw material of lemon extract is a lemon, and it is by following flow preparation:
Lemon → squeezing → solvent extraction → Separation of Solid and Liquid → clarification filtration → distillation concentrates → lemon extract.
The concrete preparation method of lemon extract is:
With the lemon raw material of 100 weight portions, after the squeezing fragmentation, with 10～100% ethanolic solution (wherein ethanolic solution is food-grade or pharmaceutical grade ethanol) of 500～2000 weight portions.Heating and refluxing extraction or soaking at room temperature are extracted 2～3 times, and each 1～24 hour, filter extract, under 40～80 ℃ condition, be evaporated to paste, obtain lemon extract.
The application of lemon extract in cigarette:
Lemon extract is dissolved in the solution of certain density ethanol or certain density ethanol and propane diols in 0.1～10% ratio of cigarette shreds, thin slice or offal weight, is sprayed at equably on cigarette shreds, thin slice or the offal, and rolls into cigarette and prop up.
The invention has the beneficial effects as follows: the smell delicate fragrance of lemon can improve spirit, help the state of mind clarification, eliminate taediumvitae, and function such as tool is good for the stomach, helps digest, and is the excellent antibiotic antidote, and its deodorizing effect is good.Fragrance that increases cigarette and the lemon extract that improves the cigarette mouthfeel are added in the cigarette, can make the fragrant jealous improvement of cigarette, fragrance is coordinated, pleasant impression is comfortable, flue gas exquisiteness, soft effectively reduces the pungent stimulation of flue gas to smoker's respiratory system, alleviates harm of smoking, and this cigarette additive preparation technology is simple, cost is low, has good market prospects and using value.
The specific embodiment
In order to understand the present invention better, be described in further detail with following preferred embodiment, but the scope of the invention is not limited to these embodiment.
Embodiment 1
Broken lemon raw material 100 grams are pressed in pressure, place the 2000ml distilling flask, add 50% ethanolic solution 1000ml, and soaking at room temperature is extracted 2 times, and each 24 hours, leach lemon dregs with emery cloth, filter extract, under 60 ℃ condition, be evaporated to paste.With the ratio of prepared lemon extract in cigarette shreds weight 2%, be dissolved in 30% ethanol and the propylene glycol solution, according to the reinforced process of conventional perfuming cigarette, be sprayed on the finished cut tobacco, sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 2
Broken lemon raw material 100 grams are pressed in pressure, place the 2000ml distilling flask, add 50% ethanolic solution 1500ml, heating and refluxing extraction 2 times, and each 3 hours, leach lemon dregs with emery cloth, filter extract, under 60 ℃ condition, be evaporated to paste.With the ratio of prepared lemon extract in cigarette shreds weight 1.5%, be dissolved in 40% ethanol and the propylene glycol solution, according to the reinforced process of conventional perfuming cigarette, be sprayed on the finished product tobacco leaf formulation (wherein pipe tobacco account for 70%, thin slice 20% and offal 10%), sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 3
Broken lemon raw material 100 grams are pressed in pressure, place the 2000ml distilling flask, add 60% ethanolic solution 1000ml, and soaking at room temperature is extracted 3 times, and each 5 hours, leach lemon dregs with emery cloth, filter extract, under 60 ℃ condition, be evaporated to paste.With the ratio of prepared lemon extract in cigarette shreds weight 2%, be dissolved in 70% ethanolic solution, according to the reinforced process of conventional perfuming cigarette, be sprayed on the finished cut tobacco, sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 4
Broken lemon raw material 100 grams are pressed in pressure, place the 2000ml distilling flask, add 70% ethanolic solution 1000ml, heating and refluxing extraction 2 times, and each 3 hours, leach lemon dregs with emery cloth, filter extract, under 60 ℃ condition, be evaporated to paste.With the ratio of prepared lemon extract in cigarette shreds weight 1.5%, be dissolved in 70% ethanol and the propylene glycol solution, according to the reinforced process of conventional perfuming cigarette, be sprayed on the finished product tobacco leaf formulation (wherein pipe tobacco account for 70%, thin slice 20% and offal 10%), sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 5
Broken lemon raw material 100 grams are pressed in pressure, place the 2000ml distilling flask, add 80% ethanolic solution 1000ml, soaking at room temperature is extracted 3 times, each 10 hours, leaches lemon dregs with emery cloth, filter extract, filter, under 60 ℃ condition, be evaporated to paste.With the ratio of prepared lemon extract in cigarette shreds weight 2%, be dissolved in 70% ethanolic solution, according to the reinforced process of conventional perfuming cigarette, be sprayed on the finished cut tobacco, sealing was preserved 24 hours, made cigarette and propped up.
Embodiment 6
Broken lemon raw material 100 grams are pressed in pressure, place the 2000ml distilling flask, add 90% ethanolic solution 1000ml, heating and refluxing extraction 2 times, and each 5 hours, leach lemon dregs with emery cloth, filter extract, under 60 ℃ condition, be evaporated to paste.With the ratio of prepared lemon extract in cigarette shreds weight 1%, be dissolved in 50% ethanol and propylene glycol solution of equivalent, according to the reinforced process of conventional perfuming cigarette, be sprayed on the finished product tobacco leaf formulation (wherein pipe tobacco account for 70%, thin slice 20% and offal 10%), sealing was preserved 24 hours, made cigarette and propped up.
Claims (4)
1. lemon extract, it is characterized in that: primary raw material is a lemon, and lemon is concentrated by squeezing → solvent extraction → Separation of Solid and Liquid → clarification filtration → distillation, obtains lemon extract.
2. according to the preparation method of the described lemon extract of claim 1, it is characterized in that: with the lemon raw material of 100 weight portions, after the squeezing fragmentation, 10～100% ethanolic solution with 500～2000 weight portions, heating and refluxing extraction or soaking at room temperature are extracted 2～3 times, each 1～24 hour, filter extract, under 40～80 ℃ condition, be evaporated to paste, obtain lemon extract.
3. according to the described lemon extract of claim 2, it is characterized in that: described ethanolic solution is food-grade or pharmaceutical grade ethanolic solution.
4. according to the application of claim 1 or 2 described lemon extracts, lemon extract solution is sprayed on cigarette shreds, thin slice or the offal equably, and roll into cigarette and prop up, it is characterized in that: described lemon extract solution is with 0.1～10% the ratio of lemon extract in cigarette shreds, thin slice or offal weight, is dissolved in the solution of certain density ethanol or certain density ethanol and propane diols.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200810073704A CN101637303A (en) | 2008-07-28 | 2008-07-28 | Lemon extract, preparation method thereof and application thereof in cigarette flavoring |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200810073704A CN101637303A (en) | 2008-07-28 | 2008-07-28 | Lemon extract, preparation method thereof and application thereof in cigarette flavoring |
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| Publication Number | Publication Date |
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| CN101637303A true CN101637303A (en) | 2010-02-03 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN200810073704A Pending CN101637303A (en) | 2008-07-28 | 2008-07-28 | Lemon extract, preparation method thereof and application thereof in cigarette flavoring |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103266014A (en) * | 2013-05-29 | 2013-08-28 | 江苏中烟工业有限责任公司徐州卷烟厂 | Spicy sweet flue-cured tobacco essence and application thereof |
| CN103627523A (en) * | 2012-08-29 | 2014-03-12 | 江西中烟工业有限责任公司 | Sun-cured red tobacco leaf extract, preparation method therefor and applications thereof in cigarettes |
| CN103627524A (en) * | 2012-08-29 | 2014-03-12 | 江西中烟工业有限责任公司 | Longan peel extract, preparation method therefor and applications thereof in cigarettes |
| CN105062688A (en) * | 2015-08-25 | 2015-11-18 | 云南中烟工业有限责任公司 | Manufacturing method of lemon hydrolat and application thereof |
| CN107495460A (en) * | 2017-08-17 | 2017-12-22 | 云南中烟工业有限责任公司 | A kind of preparation method of Chu Cheng tastes reconstituted tobacco |
| CN109852480A (en) * | 2019-04-09 | 2019-06-07 | 成都宏亿实业集团有限公司 | A kind of preparation method and its usage of lemon juice extract |
| CN109846076A (en) * | 2018-12-12 | 2019-06-07 | 云南中烟工业有限责任公司 | A method of promoting poorly rated property quality of tobacco |
-
2008
- 2008-07-28 CN CN200810073704A patent/CN101637303A/en active Pending
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103627523A (en) * | 2012-08-29 | 2014-03-12 | 江西中烟工业有限责任公司 | Sun-cured red tobacco leaf extract, preparation method therefor and applications thereof in cigarettes |
| CN103627524A (en) * | 2012-08-29 | 2014-03-12 | 江西中烟工业有限责任公司 | Longan peel extract, preparation method therefor and applications thereof in cigarettes |
| CN103266014A (en) * | 2013-05-29 | 2013-08-28 | 江苏中烟工业有限责任公司徐州卷烟厂 | Spicy sweet flue-cured tobacco essence and application thereof |
| CN105062688A (en) * | 2015-08-25 | 2015-11-18 | 云南中烟工业有限责任公司 | Manufacturing method of lemon hydrolat and application thereof |
| CN107495460A (en) * | 2017-08-17 | 2017-12-22 | 云南中烟工业有限责任公司 | A kind of preparation method of Chu Cheng tastes reconstituted tobacco |
| CN109846076A (en) * | 2018-12-12 | 2019-06-07 | 云南中烟工业有限责任公司 | A method of promoting poorly rated property quality of tobacco |
| CN109846076B (en) * | 2018-12-12 | 2022-09-13 | 云南中烟工业有限责任公司 | Method for improving quality of low-applicability tobacco leaves |
| CN109852480A (en) * | 2019-04-09 | 2019-06-07 | 成都宏亿实业集团有限公司 | A kind of preparation method and its usage of lemon juice extract |
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Application publication date: 20100203 |