CN101164528B - Natural hair dyeing agent prepared by plant pigment catechu and hair dyeing method thereof - Google Patents
Natural hair dyeing agent prepared by plant pigment catechu and hair dyeing method thereof Download PDFInfo
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- CN101164528B CN101164528B CN200710133376XA CN200710133376A CN101164528B CN 101164528 B CN101164528 B CN 101164528B CN 200710133376X A CN200710133376X A CN 200710133376XA CN 200710133376 A CN200710133376 A CN 200710133376A CN 101164528 B CN101164528 B CN 101164528B
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Abstract
The present invention relates to a hair-dying agent, in particular, it relates to a natural hair-dying agent prepared by adopting plant colour matter catechu and its hair-dying method. Said hair-dying agent includes agent A and agent B. The agent A includes (by wt%) 3-10% of plant colour matter catechu, 10-50% of organic solvent and the rest is water; and the agent B includes (by wt%) 1-5% of ferrous salt mordant, 0.2-1.0% of reduced iron powder, 1-10% of surfactant, 1-5% of thickening agent, proper quantity of acidifying agent, 0.1-0.3% of natural essence and the rest is water. The catechu is a traditional Chinese medicinal material, and has the functions of clearing away heat, astringing dampness, resisting bacteria and inhibiting bacteria.
Description
Technical field
The present invention relates to a kind of hair dye, be meant a kind of natural hair dye and the hair colouring methods thereof that adopt the preparation of plant pigment catechu especially.
Background technology
The hair dye of producing both at home and abroad is many at present is that major ingredient is made with p-phenylenediamine (PPD) and derivant thereof, and its effect is that p-phenylenediamine (PPD) is through H
2O
2Generate dyestuff and with hair-dyeing, the disadvantage of this hair dye is possible make 0.4～6.3% user skin allergy Deng oxidant, and recent intoxicating, carcinogenesis at a specified future date are arranged.In this case, people have produced keen interest to the hair dyed agent with the natural pigment preparation.Germany patent No.3715326 has described a kind of hair dye that adopts the natural pigment exploitation, this hair dye is formed by two doses, wherein potion contains mantoquita in its medium, and another agent contains red or its hydroxy derivatives hematoxylin of Brazil wood in its medium, and these two doses of substeps impose on hair.The major defect of this hair dye is to have used certain toxic mantoquita as mordant, and simultaneously pH is that 9～10 alkaline medium hair dyeing can damage hair.Chinese patent 1045349A proposes two doses of hair dyes of a kind of novel Lignum Sappan, and wherein potion contains ferrous salt in medium, and another agent contains the natural dye haematein, and these two doses same substeps impose on hair.This hair dye does not use harmful reagent, and does not have noxious substance to generate in the reaction yet, but the hematoxylin price is more expensive.Chinese patent 1283449A has proposed a kind of hair dye of being made by pure plant melanin such as Semen Sesami Nigrum powder, Semen sojae atricolor powder, Ink sepiellae seu sepiae and water, and this hair dye is the impermanency hair dye, can be as required flush away at any time.
Summary of the invention
The object of the present invention is to provide and adopt the plant pigment catechu to prepare a kind of novel natural hair dye and hair colouring methods thereof.This hair dye is formed by two doses, and agent A contains the plant pigment catechu, and agent B contains the ferrous salt mordant.
According to technical scheme provided by the invention, adopt the plant pigment catechu to prepare a kind of novel natural hair dye and comprise agent A and agent B, it is characterized in that agent A comprises plant pigment catechu 3～10%, organic solvent 10～50%, Yu Weishui, its pH value are 5～6; Agent B comprises ferrous salt mordant 1～5%, reduced iron powder 0.2～1.0%, and surfactant 1～10%, thickening agent 1～5%, natural essence 0.1～0.3%, dripping acidulant to pH value is 4～7, Yu Weishui, unit is a percetage by weight.
Organic solvent among the agent A is a kind of in the monomethyl of ethanol, isopropyl alcohol, benzyl alcohol, phenethanol, ethylene glycol, 1,2 monoethylene glycol, single ethyl or single-butyl ether, the propylene glycol.
Ferrous salt mordant among the agent B is any Fe of containing that allows use in the cosmetics
2+Salt, surfactant comprises anion, cation, both sexes or non-ionic surface active agent, thickening agent comprises the one or more combination in Radix Acaciae senegalis, methylcellulose, carboxymethyl cellulose, hydroxyethyl-cellulose, the hydroxypropyl cellulose, acidulant comprises hydrochloric acid, phosphoric acid, acetic acid, lactic acid, Tartaric acid or citric acid, and natural essence can adopt a kind of in lavandula angustifolia essence, jasmine flower essence, the Flos Rosae Rugosae essence.
Agent A and agent B are solution or any degree thickening or liquid or the Emulsion form that adds glue.
Described ferrous salt mordant comprises FeSO
4, surfactant comprises Polyethylene Glycol.
The hair colouring methods of a kind of natural hair dye of described employing plant pigment catechu preparation, it is characterized in that, during hair dyeing, earlier agent A evenly is applied on the clean hair, at room temperature to 50 ℃ following hair dyeing 20～40min, then agent B evenly is applied in hair, behind mordant dyeing 10～20min, hair cleaned dry up, dye the brownish black that the back hair is nature.
The inventor once applied for Chinese invention patent " method of refining powdered catechu dye by film separation technique and colouring method thereof ".Catechu is the Chinese medicine material, have heat clearing away, removing dampness, effect such as antibiotic, antibacterial, and resource is extensive, in Chinese yunnan province, Zhejiang Province, Fujian Province, Taiwan Province, Hainan Province, Guangdong Province, Guangxi autonomous region distribution is arranged all.Catechu pigment main component is catechutannic acid, catechin, epicatechin, catechu red etc.
The organic solvent that is added helps to make the surperficial scale of hair to open, and increases infiltration and the adsorptivity of catechu pigment to hair, and reduced iron powder helps to keep the stable of ferrous salt, prevents its oxidation; Surfactant can increase the uniformity of hair dyeing; Thickening agent can reduce the flowability of hair dye, improves the controllability to dyeing part; Acidulant mainly is to be used for the pH value of regulator B, makes it reach 4～7; Natural essence helps to improve the abnormal smells from the patient that reaches hair dyeing back hair in the hair dyeing process, makes the people joyful.
Hair dye of the present invention has following characteristics: (1) A, B are water formulation for two doses, and keep faintly acid or neutrality, help under the prerequisite of not damaging hair hair to be dyeed; (2) replace synthetic dyestuffs with the plant pigment catechu, do not had to use the reagent that human body is had potential hazard in the preparation, and also do not had noxious substance to generate in the reaction; (3) catechu low price is 1/tens of a haematein, and is with low cost with the hair dye of its exploitation.Therefore, this hair dye has no side effect, safe and reliable, hair dyeing effect good, and low price.
The specific embodiment
Embodiment 1:
Agent A: catechu pigment 20g, ethanol 100g adds water to 200g;
Agent B:FeSO
47H
2O 10g, reduced iron powder 2.0g, Polyethylene Glycol 10g, carboxymethyl cellulose 2g, acetic acid 0.3g, lavender fragrance 0.2g adds water to 200g.
Hair colouring methods: agent A evenly is applied in clean hair, at 40 ℃ of following hair dyeing 30min, then agent B evenly is applied to hair, behind the mordant dyeing 20min hair cleaned and dry up, hair is the dark brown black of nature.
Embodiment 2:
Agent A: catechu pigment 6g, ethanol 50g adds water to 200g;
Agent B:FeSO
47H
2O 2g, reduced iron powder 0.4g, Polyethylene Glycol 20g, carboxymethyl cellulose 10g, acetic acid 1g, lavender fragrance 0.6g adds water to 200g.
Hair colouring methods: agent A evenly is applied in clean hair, and the 40min that has hair dyed at normal temperatures evenly is applied to hair with agent B then, behind the mordant dyeing 10min hair is cleaned to dry up, and hair is the more shallow brownish black of nature.
Embodiment 3:
Agent A: catechu pigment 10g, ethanol 20g adds water to 200g;
Agent B:FeSO
47H
2O 4g, reduced iron powder 0.8g, Polyethylene Glycol 6g, carboxymethyl cellulose 4g, acetic acid 1g, lavender fragrance 0.2g adds water to 200g.
Hair colouring methods: agent A evenly is applied in clean hair, at 40 ℃ of following hair dyeing 20min, then agent B evenly is applied to hair, behind the mordant dyeing 10min hair cleaned and dry up, hair is the brownish black of nature.
Embodiment 4
Agent A: catechu pigment 15g, ethanol 50g adds water to 200g;
Agent B:FeSO
47H
2O 6g, reduced iron powder 1g, Polyethylene Glycol 2g, carboxymethyl cellulose 4g, lactic acid 0.5g, jasmine flower essence 0.6g adds water to 200g.
Hair colouring methods: agent A evenly is applied in clean hair, and the 40min that has hair dyed at normal temperatures evenly is applied to hair with agent B then, behind the mordant dyeing 20min hair is cleaned to dry up, and hair is the brownish black of nature.
Embodiment 5
Agent A: catechu pigment 18g, ethanol 30g adds water to 200g;
Agent B:FeSO
47H
2O 7g, reduced iron powder 1.5g, Polyethylene Glycol 20g, hydroxypropyl cellulose 3.0g, acetic acid 0.5g, rose essence 0.2g adds water to 200g.
Hair colouring methods: agent A evenly is applied in clean hair, at 50 ℃ of following hair dyeing 20min, then agent B evenly is applied in hair, behind the mordant dyeing 15min hair cleaned and dry up, hair is the brownish black of nature.
Claims (4)
1. adopt a kind of natural hair dye of plant pigment catechu preparation, comprise agent A and agent B, it is characterized in that agent A comprises plant pigment catechu 3～10%, organic solvent 10～50%, Yu Weishui, its pH value are 5～6; Agent B comprises ferrous salt mordant 1～5%, reduced iron powder 0.2～1.0%, and surfactant 1～10%, thickening agent 1～5%, natural essence 0.1～0.3%, dripping acidulant to pH value is 4～7, Yu Weishui; Unit is a percetage by weight;
Organic solvent among the agent A is a kind of in the monomethyl of ethanol, isopropyl alcohol, benzyl alcohol, phenethanol, ethylene glycol, 1,2 monoethylene glycol, single ethyl or single-butyl ether, the propylene glycol;
Ferrous salt mordant among the agent B is any Fe of containing that allows use in the cosmetics
2+Salt;
Surfactant among the agent B comprises anion, cation, both sexes or non-ionic surface active agent;
Thickening agent among the agent B comprises the one or more combination in Radix Acaciae senegalis, methylcellulose, carboxymethyl cellulose, hydroxyethyl-cellulose, the hydroxypropyl cellulose;
Acidulant among the agent B comprises hydrochloric acid, phosphoric acid, acetic acid, lactic acid, tartaric acid or citric acid;
Natural essence among the agent B comprises a kind of in lavandula angustifolia essence, jasmine flower essence, the Flos Rosae Rugosae essence.
2. adopt a kind of natural hair dye of plant pigment catechu preparation according to claim 1, it is characterized in that agent A and agent B are solution or any degree thickening or liquid or the Emulsion form that adds glue.
3. adopt a kind of natural hair dye of plant pigment catechu preparation according to claim 1, it is characterized in that the ferrous salt mordant comprises FeSO
4, surfactant comprises Polyethylene Glycol.
4. adopt the hair colouring methods of a kind of natural hair dye of plant pigment catechu preparation according to claim 1, it is characterized in that, during hair dyeing, earlier agent A evenly is applied on the clean hair, at room temperature to 50 ℃ following hair dyeing 20～40min, then agent B evenly is applied in hair, behind mordant dyeing 10～20min, hair cleaned dry up, dye the brownish black that the back hair is nature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200710133376XA CN101164528B (en) | 2007-10-19 | 2007-10-19 | Natural hair dyeing agent prepared by plant pigment catechu and hair dyeing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200710133376XA CN101164528B (en) | 2007-10-19 | 2007-10-19 | Natural hair dyeing agent prepared by plant pigment catechu and hair dyeing method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101164528A CN101164528A (en) | 2008-04-23 |
| CN101164528B true CN101164528B (en) | 2010-06-23 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN200710133376XA Expired - Fee Related CN101164528B (en) | 2007-10-19 | 2007-10-19 | Natural hair dyeing agent prepared by plant pigment catechu and hair dyeing method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2012065576A1 (en) | 2010-11-19 | 2012-05-24 | 浙江养生堂天然药物研究所有限公司 | Use of tea polyphenols and/or tea pigments as dyes and products thereof |
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| CN101812246B (en) * | 2009-02-20 | 2014-10-01 | 浙江养生堂天然药物研究所有限公司 | Mordant and hair dyeing product containing same |
| CN102743306B (en) * | 2011-04-20 | 2015-04-01 | 浙江医药股份有限公司新昌制药厂 | Natural hair dye adopting water-soluble plant melanin, preparation method thereof and hair dyeing method thereof |
| CN103622844B (en) | 2012-08-24 | 2016-04-20 | 浙江养生堂天然药物研究所有限公司 | hair dyeing product |
| CN104083307B (en) * | 2014-07-28 | 2016-08-17 | 江南大学 | Use a kind of natural hair dye of preparing of plant pigment carthamin and hair colouring methods thereof |
| CN105168016B (en) * | 2015-08-19 | 2018-05-18 | 广州市康妆化妆品有限公司 | A kind of hair dye |
| CN106176453A (en) * | 2016-08-29 | 2016-12-07 | 河南染匠科技有限公司 | A kind of botanical hair dye |
| CN106236663A (en) * | 2016-08-31 | 2016-12-21 | 郭迎庆 | A kind of preparation method of high colouring natural botanical hair dye |
| CN106491431B (en) * | 2016-11-21 | 2019-07-02 | 福建泉州飞扬生物科技有限公司 | A kind of natural botanical hair dye |
| CN106420499A (en) * | 2016-11-28 | 2017-02-22 | 河南工程学院 | Natural hair dye prepared from fructus chebulae pigment and dyeing method thereof |
| CN108030704B (en) * | 2017-12-21 | 2021-04-13 | 北京工商大学 | Plant hair dye with graphene oxide as dyeing assistant and preparation method thereof |
| TWI713829B (en) * | 2018-03-23 | 2020-12-21 | 田錦衡 | Plant-based black hair dye and hair dyeing method |
| CN111374216B (en) * | 2018-12-28 | 2023-04-07 | 丰益(上海)生物技术研发中心有限公司 | A method for preparing plant-derived protein isolate and the protein obtained |
| CN110393686A (en) * | 2019-08-30 | 2019-11-01 | 忻州师范学院 | A kind of preparation method and application of bush tealeaves compound botanical hair dye |
| CN110840763A (en) * | 2019-12-14 | 2020-02-28 | 山东大学 | Cyclic hair dyeing method based on metal-polyphenol network structure |
| CN111840166A (en) * | 2020-08-14 | 2020-10-30 | 张曼曼 | Traditional Chinese medicine hair dyeing cream and preparation method thereof |
| CN115517989A (en) * | 2022-01-25 | 2022-12-27 | 西南医科大学 | Four-agent type ammonia-free non-toxic permanent hair dyeing composition and preparation method thereof |
| CN115517991B (en) * | 2022-01-25 | 2024-03-22 | 西南医科大学 | Three-agent type safe and nontoxic hair dye and preparation method thereof |
| CN115844785A (en) * | 2022-12-24 | 2023-03-28 | 广西大学 | Plant hair dye and preparation method thereof |
| CN116617101B (en) * | 2023-07-25 | 2023-10-13 | 北京立仁堂医药科技开发有限公司 | Pigment composition for dyeing hair, blackening hair and nourishing hair and application thereof |
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| CN1045349A (en) * | 1989-03-07 | 1990-09-19 | 天津师范专科学校 | The hair dyed agent of natural dye |
| CN1462184A (en) * | 2001-04-27 | 2003-12-17 | 株式会社科思美 | Hair dye composition for dressing hair |
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2007
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1045349A (en) * | 1989-03-07 | 1990-09-19 | 天津师范专科学校 | The hair dyed agent of natural dye |
| CN1462184A (en) * | 2001-04-27 | 2003-12-17 | 株式会社科思美 | Hair dye composition for dressing hair |
Non-Patent Citations (1)
| Title |
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| 王雨来.现代染发剂新进展.新技术 新工艺 新产品.2003,23-24. * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2012065576A1 (en) | 2010-11-19 | 2012-05-24 | 浙江养生堂天然药物研究所有限公司 | Use of tea polyphenols and/or tea pigments as dyes and products thereof |
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| Publication number | Publication date |
|---|---|
| CN101164528A (en) | 2008-04-23 |
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Assignee: Yixing Xinyu Chemicals Co., Ltd. Assignor: Jiangnan University Contract record no.: 2012320010149 Denomination of invention: Natural hair dyeing agent prepared by plant pigment catechu and hair dyeing method thereof Granted publication date: 20100623 License type: Exclusive License Open date: 20080423 Record date: 20120619 |
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Granted publication date: 20100623 Termination date: 20161019 |