CN106236663A - A kind of preparation method of high colouring natural botanical hair dye - Google Patents
A kind of preparation method of high colouring natural botanical hair dye Download PDFInfo
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- CN106236663A CN106236663A CN201610776541.2A CN201610776541A CN106236663A CN 106236663 A CN106236663 A CN 106236663A CN 201610776541 A CN201610776541 A CN 201610776541A CN 106236663 A CN106236663 A CN 106236663A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/463—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/10—Preparations for permanently dyeing the hair
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Abstract
The invention discloses the preparation method of a kind of high colouring natural botanical hair dye, belong to hair dye preparing technical field.nullFirst water-soluble cell plant pigment and glacial acetic acid solution are prepared acidifying plant pigment solution by the present invention，Ultrasonic disperse after subsequently it being stirred with deionized water，Carry out freezing processing again，The charge-modified pigment granule that obtains is polished makes powder，Mix with deionized water after again green tea being made powder，Regulate pH subsequently and heat centrifugal treating，Collect the supernatant and i.e. obtain tea polyphenol extract liquid，Finally by above-mentioned charge-modified pigment powder and tea polyphenol extract liquid、The stirring such as sodium carboxymethyl cellulose still aging process，A kind of high colouring natural botanical hair dye，The natural botanical hair dye colorability that the present invention prepares is strong，Hair colouring is fast，And upper chromatic effect is lasting，Color is good，Human body will not be caused damage，Skin sensitivity person is not also resulted in allergic phenomena，It it is a kind of preferably safety hair dye.
Description
Technical field
The invention discloses the preparation method of a kind of high colouring natural botanical hair dye, belong to hair dye technology of preparing neck
Territory.
Background technology
Along with the raising of living standards of the people, hair dye changes the daily cosmetics of color development the most progressively as a kind of
Come into common people, become modern self-expression and pursue the declaration of individual character.On the one hand, hair dye can make color development return certainly
So, some congenital defects or posteriori sorry are made up；On the other hand, as individual character and fashionable interspersing, many people require to change
The hair color that oneself is single, to pursue colorful color development.In recent years, hair dyeing had become the wind direction mark of fashion.
Hair dye refers to dyestuff penetration to hair deep inside quality or sticks to the coloring of hair top layer, to reach beautiful
Send out the cosmetics of purpose.Hair dye, with the chemical of its product, mainly can be divided into oxidative hair dyes and Direct-type hair dye
Two big classes.Hair dye product is various informative, has paste, liquid, powder, foam-like, pomade type, aerosol type etc..In recent years,
The whole world hair dye market demand is powerful, it has also become develop product the most active in cosmetic field.
At present, tradition hair dye is relatively big to skin irritation, and skin sensitivity person can cause allergic phenomena, and traditional hair dyeing
Agent contains poisonous carcinogen, can cause damage human body, and natural hair dye then colorability is not strong, and after dyeing, color comes off relatively
Hurry up, do not possess permanence dyeing condition.
Summary of the invention
The technical problem that present invention mainly solves: relatively big to skin irritation for tradition hair dye at present, and containing poisonous
Carcinogen, can cause damage to human body, and natural hair dye then colorability is not strong, and after dyeing, color comes off and asks faster
Topic, it is provided that the preparation method of a kind of high colouring natural botanical hair dye, the method first by water-soluble cell plant pigment with
Glacial acetic acid solution prepares acidifying plant pigment solution, ultrasonic disperse after it being stirred subsequently with deionized water, then carries out at freezing
Reason, the polished powder of making of charge-modified pigment granule obtained, then mix with deionized water after green tea is made powder
Close, regulate pH subsequently and heat centrifugal treating, collect the supernatant and i.e. obtain tea polyphenol extract liquid, finally by above-mentioned charge-modified color
Stirring the still aging process such as element powder and tea polyphenol extract liquid, sodium carboxymethyl cellulose, a kind of high colouring sky
So botanical hair dye, the natural botanical hair dye colorability that the present invention prepares is strong, and hair colouring is fast, and upper chromatic effect is lasting,
Color is good, will not cause damage human body, and skin sensitivity person is not also resulted in allergic phenomena, is a kind of preferably safety
Type hair dye.
In order to solve above-mentioned technical problem, the technical solution adopted in the present invention is:
(1) choosing 5～6g water-soluble cell plant pigment to be placed in 100～120mL glacial acetic acid solutions, stirring is mixed is incorporated in 110
～heating in water bath 10～15min at 120 DEG C, it is warming up to 140～145 DEG C by 1 DEG C/min subsequently, after Heat preservation 3～5h, stands
It is cooled to room temperature, collects acidifying plant pigment solution；
(2) at 0～5 DEG C, 1:1 by volume, the acidifying plant pigment solution of above-mentioned preparation is mixed with deionized water stirring,
Ultrasonic disperse 10～15min under 200～300W, insulation standing subsequently 1～2h, then vacuum lyophilization are also collected charge-modified
Pigment granule, is placed in charge-modified pigment granule in mortar, grinds and collect and to obtain charge-modified pigment powder, standby；
(3) green tea is pulverized and is crossed 65～70 mesh sieves, collect tea-leaf power and be placed at 100～105 DEG C being dried 6～8h,
1:5 the most in mass ratio, mixes dry tea-leaf power with deionized water stirring, regulates pH to 5.5～6.0 with glacial acetic acid, then
Under 200～300W sonic oscillations, 55～60 DEG C of condition of water bath heating, react 45～50min, stop heating subsequently and 1800
～centrifugation 10～15min under 2000r/min, collect the supernatant, obtain tea polyphenol extract liquid；
(4) count by weight, weigh respectively charge-modified pigment powder prepared by 10～15 parts of steps (2), 45～50 parts go
Ionized water, the tea polyphenol extract liquid of 10～15 parts of above-mentioned preparations, 5～6 parts of sodium carboxymethyl cellulose, 1～2 part of lauryl sulphate acid
Sodium and 3～5 parts of polyvinyl alcohol are placed in beaker, stirring mixing still aging 6～8h, can be prepared into a kind of high colouring property sky
So botanical hair dye.
The application process of the present invention is: taking the natural botanical hair dye that the 80～150mL present invention prepare, uniform application is at head
On Faing, stand 15～20min afterwash subsequently.The natural botanical hair dye colorability that after testing, the present invention prepares is strong,
Hair colouring is fast, and dyeing time more originally shortened 20～30%, and hair dye performance is gentle, and on this hair dye, chromatic effect is lasting,
After 80～100 times are had one's hair wash, there is not significant change in hair color development and glossiness.
The invention has the beneficial effects as follows:
(1) the natural botanical hair dye colorability that the present invention prepares is strong, it is not necessary to adds baking the affected part after applying some drugs and sends out, and can quickly make head at normal temperatures
Send out colouring, possess permanence dyeing condition；
(2) natural botanical hair dye that the present invention prepares has the Color of excellence, and the long-time holding head luminance of energy is soft
Suitable, hair quality and scalp etc. will not cause after hair dyeing damage, skin sensitivity person also do not result in allergic phenomena.
Detailed description of the invention
First choosing 5～6g water-soluble cell plant pigment to be placed in 100～120mL glacial acetic acid solutions, stirring mixing is also
Heating in water bath 10～15min at 110～120 DEG C, are warming up to 140～145 DEG C by 1 DEG C/min subsequently, Heat preservation 3～5h
After, stand and be cooled to room temperature, collect acidifying plant pigment solution；Subsequently at 0～5 DEG C, 1:1 by volume, by above-mentioned preparation
The stirring of acidifying plant pigment solution and deionized water mix, under 200～300W, ultrasonic disperse 10～15min, are incubated subsequently
Stand 1～2h, then vacuum lyophilization collect charge-modified pigment granule, charge-modified pigment granule be placed in mortar,
Grind and collect and to obtain charge-modified pigment powder, standby；Green tea is pulverized and crossed 65～70 mesh sieves again, collects tea-leaf power
It is placed at 100～105 DEG C being dried 6～8h, 1:5 the most in mass ratio, dry tea-leaf power is mixed with deionized water stirring,
Regulate pH to 5.5～6.0 with glacial acetic acid, then under 200～300W sonic oscillations, 55～60 DEG C of condition of water bath heating, react 45
～50min, stop heating centrifugation 10～15min, the collection supernatant under 1800～2000r/min subsequently, obtain tea
Polyphenol extracting solution；Finally count by weight, weigh respectively charge-modified pigment powder prepared by 10～15 parts of above-mentioned steps, 45
～50 parts of deionized waters, the tea polyphenol extract liquid of 10～15 parts of above-mentioned preparations, 5～6 parts of sodium carboxymethyl cellulose, 1～2 part 12
Alkyl sodium sulfate and 3～5 parts of polyvinyl alcohol are placed in beaker, stirring mixing still aging 6～8h, can be prepared into a kind of high
Colouring property natural botanical hair dye.
Example 1
First choosing 5g water-soluble cell plant pigment to be placed in 100mL glacial acetic acid solution, stirring is mixed is incorporated in water-bath at 110 DEG C
Heating 10min, is warming up to 140 DEG C by 1 DEG C/min subsequently, after Heat preservation 3h, stands and is cooled to room temperature, collects acidifying plant color
Cellulose solution；Subsequently at 0 DEG C, 1:1 by volume, by mixed with deionized water stirring for the acidifying plant pigment solution of above-mentioned preparation
Conjunction, ultrasonic disperse 10min under 200W, the 1h of insulation standing subsequently, then vacuum lyophilization also collect charge-modified pigment granule,
Charge-modified pigment granule is placed in mortar, grinds and collect and to obtain charge-modified pigment powder, standby；Again by green tea powder
Broken and cross 65 mesh sieves, collect tea-leaf power be placed at 100 DEG C be dried 6h, the most in mass ratio 1:5, by dry tea-leaf power with
Deionized water stirring mixing, regulates pH to 5.5 with glacial acetic acid, then under 200W sonic oscillation, 55 DEG C of condition of water bath heating, reaction
45min, stops heating centrifugation 10min, the collection supernatant under 1800r/min subsequently, obtains tea polyphenol extract liquid；?
After count by weight, weigh respectively charge-modified pigment powder prepared by 10 parts of above-mentioned steps, 45 parts of deionized waters, on 10 parts
State the tea polyphenol extract liquid of preparation, 5 parts of sodium carboxymethyl cellulose, 1 part of sodium lauryl sulphate and 3 parts of polyvinyl alcohol and be placed in beaker
In, stirring mixing still aging 6h, a kind of high colouring property natural botanical hair dye can be prepared into.
This example operation is easy, during use, takes the natural botanical hair dye that the 80mL present invention prepares, and uniform application is at hair
On, stand 15min afterwash subsequently.After testing, the natural botanical hair dye colorability that the present invention prepares is strong, on hair
Color is fast, and dyeing time more originally shortened 20%, and hair dye performance is gentle, and after skin sensitivity person uses, allergy rate is only 1%, and
On this hair dye, chromatic effect is lasting, and after 80 times are had one's hair wash, hair color development and glossiness do not occur significant change.
Example 2
First choosing 5.5g water-soluble cell plant pigment to be placed in 110mL glacial acetic acid solution, stirring is mixed is incorporated in water at 115 DEG C
Bath heating 13min, is warming up to 143 DEG C by 1 DEG C/min subsequently, after Heat preservation 4h, stands and is cooled to room temperature, collects acidifying plant
Pigment solution；Subsequently at 3 DEG C, 1:1 by volume, by mixed with deionized water stirring for the acidifying plant pigment solution of above-mentioned preparation
Conjunction, ultrasonic disperse 13min under 250W, the 1.5h of insulation standing subsequently, then vacuum lyophilization also collect charge-modified pigment
Grain, is placed in charge-modified pigment granule in mortar, grinds and collect and to obtain charge-modified pigment powder, standby；Again by green tea tea
68 mesh sieves are pulverized and crossed to leaf, collects tea-leaf power and is placed at 103 DEG C being dried 7h, the most in mass ratio 1:5, by dry Folium Camelliae sinensis powder
End mixes with deionized water stirring, regulates pH to 5.8 with glacial acetic acid, then under 250W sonic oscillation, 58 DEG C of condition of water bath heating,
Reaction 48min, stops heating centrifugation 13min, the collection supernatant under 1900r/min subsequently, obtains tea polyphenol extract
Liquid；Finally count by weight, weigh respectively charge-modified pigment powder prepared by 13 parts of above-mentioned steps, 48 parts of deionized waters,
The tea polyphenol extract liquid of 13 parts of above-mentioned preparations, 5.5 parts of sodium carboxymethyl cellulose, 1.5 parts of sodium lauryl sulphates and 4 parts of polyethylene
Alcohol is placed in beaker, stirring mixing still aging 7h, can be prepared into a kind of high colouring property natural botanical hair dye.
This example operation is easy, during use, takes the natural botanical hair dye that the 115mL present invention prepares, and uniform application is at head
On Faing, stand 18min afterwash subsequently.After testing, the natural botanical hair dye colorability that the present invention prepares is strong, hair
Colouring is fast, and dyeing time more originally shortened 25%, and hair dye performance is gentle, and after skin sensitivity person uses, allergy rate is only
On 1.5%, and this hair dye, chromatic effect is lasting, and after 90 times are had one's hair wash, hair color development and glossiness do not occur significant change.
Example 3
First choosing 6g water-soluble cell plant pigment to be placed in 120mL glacial acetic acid solution, stirring is mixed is incorporated in water-bath at 120 DEG C
Heating 15min, is warming up to 145 DEG C by 1 DEG C/min subsequently, after Heat preservation 5h, stands and is cooled to room temperature, collects acidifying plant color
Cellulose solution；Subsequently at 5 DEG C, 1:1 by volume, by mixed with deionized water stirring for the acidifying plant pigment solution of above-mentioned preparation
Conjunction, ultrasonic disperse 15min under 300W, the 2h of insulation standing subsequently, then vacuum lyophilization also collect charge-modified pigment granule,
Charge-modified pigment granule is placed in mortar, grinds and collect and to obtain charge-modified pigment powder, standby；Again by green tea powder
Broken and cross 70 mesh sieves, collect tea-leaf power be placed at 105 DEG C be dried 8h, the most in mass ratio 1:5, by dry tea-leaf power with
Deionized water stirring mixing, regulates pH to 6.0 with glacial acetic acid, then under 300W sonic oscillation, 60 DEG C of condition of water bath heating, reaction
50min, stops heating centrifugation 15min, the collection supernatant under 2000r/min subsequently, obtains tea polyphenol extract liquid；?
After count by weight, weigh respectively charge-modified pigment powder prepared by 15 parts of above-mentioned steps, 50 parts of deionized waters, on 15 parts
State the tea polyphenol extract liquid of preparation, 6 parts of sodium carboxymethyl cellulose, 2 parts of sodium lauryl sulphates and 5 parts of polyvinyl alcohol and be placed in beaker
In, stirring mixing still aging 8h, a kind of high colouring property natural botanical hair dye can be prepared into.
This example operation is easy, during use, takes the natural botanical hair dye that the 150mL present invention prepares, and uniform application is at head
On Faing, stand 20min afterwash subsequently.After testing, the natural botanical hair dye colorability that the present invention prepares is strong, hair
Colouring is fast, and dyeing time more originally shortened 30%, and hair dye performance is gentle, and after skin sensitivity person uses, allergy rate is only 2%,
And chromatic effect is lasting on this hair dye, after 100 times are had one's hair wash, there is not significant change in hair color development and glossiness.
Claims (1)
1. the preparation method of one kind high colouring natural botanical hair dye, it is characterised in that concrete preparation process is:
(1) choosing 5～6g water-soluble cell plant pigment to be placed in 100～120mL glacial acetic acid solutions, stirring is mixed is incorporated in 110
～heating in water bath 10～15min at 120 DEG C, it is warming up to 140～145 DEG C by 1 DEG C/min subsequently, after Heat preservation 3～5h, stands
It is cooled to room temperature, collects acidifying plant pigment solution；
(2) at 0～5 DEG C, 1:1 by volume, the acidifying plant pigment solution of above-mentioned preparation is mixed with deionized water stirring,
Ultrasonic disperse 10～15min under 200～300W, insulation standing subsequently 1～2h, then vacuum lyophilization are also collected charge-modified
Pigment granule, is placed in charge-modified pigment granule in mortar, grinds and collect and to obtain charge-modified pigment powder, standby；
(3) green tea is pulverized and is crossed 65～70 mesh sieves, collect tea-leaf power and be placed at 100～105 DEG C being dried 6～8h,
1:5 the most in mass ratio, mixes dry tea-leaf power with deionized water stirring, regulates pH to 5.5～6.0 with glacial acetic acid, then
Under 200～300W sonic oscillations, 55～60 DEG C of condition of water bath heating, react 45～50min, stop heating subsequently and 1800
～centrifugation 10～15min under 2000r/min, collect the supernatant, obtain tea polyphenol extract liquid；
(4) count by weight, weigh respectively charge-modified pigment powder prepared by 10～15 parts of steps (2), 45～50 parts go
Ionized water, the tea polyphenol extract liquid of 10～15 parts of above-mentioned preparations, 5～6 parts of sodium carboxymethyl cellulose, 1～2 part of lauryl sulphate acid
Sodium and 3～5 parts of polyvinyl alcohol are placed in beaker, stirring mixing still aging 6～8h, can be prepared into a kind of high colouring property sky
So botanical hair dye.
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| CN201610776541.2A CN106236663A (en) | 2016-08-31 | 2016-08-31 | A kind of preparation method of high colouring natural botanical hair dye |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107446377A (en) * | 2017-08-09 | 2017-12-08 | 安徽省新旭堂茶业有限公司 | The preparation method of green natural tea dye liquor |
| CN112754967A (en) * | 2021-02-04 | 2021-05-07 | 杭州奇燕日用品有限公司 | Black hair dyeing and shaping spray and preparation method thereof |
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2016
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107446377A (en) * | 2017-08-09 | 2017-12-08 | 安徽省新旭堂茶业有限公司 | The preparation method of green natural tea dye liquor |
| CN112754967A (en) * | 2021-02-04 | 2021-05-07 | 杭州奇燕日用品有限公司 | Black hair dyeing and shaping spray and preparation method thereof |
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Application publication date: 20161221 |