CN109971571A - Beautiful essential oil grinding soap of a kind of promise and preparation method thereof - Google Patents
Beautiful essential oil grinding soap of a kind of promise and preparation method thereof Download PDFInfo
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- CN109971571A CN109971571A CN201910374036.9A CN201910374036A CN109971571A CN 109971571 A CN109971571 A CN 109971571A CN 201910374036 A CN201910374036 A CN 201910374036A CN 109971571 A CN109971571 A CN 109971571A
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- Prior art keywords
- beautiful
- promise
- soap
- essential oil
- soap base
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- Dermatology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses beautiful essential oil grinding soap of a kind of promise and preparation method thereof, the components including following parts by weight: 90~95 parts of the beautiful soap base of promise, 1~5 part of the beautiful essential oil of promise.The beautiful soap base of promise, which refers to, is dissolved in the sodium hydroxide of metering in the beautiful hydrosol of promise, then carries out the soap base that saponification obtains with natural oil.Sodium hydroxide is dissolved in the beautiful hydrosol of promise by grinding soap of the invention when preparing soap base, then carries out saponification with natural oil, so that including Noni fruit water soluble ingredient in part in soap base.In addition, after the pH value of soap base is adjusted to 8.0 or so, the beautiful essential oil of promise is added in when grinding, is added under the conditions of low temperature, weak base and is kept essential oil antibacterial, oxidation resistant activity.
Description
Technical field
The present invention relates to a kind of essential oil soaps, and in particular to beautiful essential oil grinding soap of a kind of promise and preparation method thereof.
Background technique
Handmade soap refer to natural oil (including vegetable fat and animal fat) and sodium hydroxide (or potassium hydroxide) into
Row saponification, soap generated, and any preservative, synthetic food color, essence, surfactant are not added, it protects
The glycerol for staying reaction to generate.Handmade soap contains about 5~8% glycerol, is the optimal moisturizer of skin, can shape on the skin
At one layer of natural protective film.
The preparation method of handmade soap generally uses cold preparation method at present.Cold preparation method is that grease and alkali is allowed to carry out instead at about 40 DEG C
Answer, when saponification to very likely when, soap lye is molded into mould, keeps the temperature two days or so, demoulding obtains molding handmade soap.Cold process soap
Saponification is slow, could use after also needing for 6~8 weeks it was made further to be saponified maturation after demoulding.
Grinding soap is made of ground reprocessing, to be divided into cold system grinding soap on the basis of the handmade soap of maturation and heat is ground
Grind soap.The secondary operation of grinding soap makes its pH value control more preferably, tends to be neutral, and it is more mild comfortable to wash sense.
Noni fruit (Noni) is the fruit of beach wood Morinda offcinalis How.There is Noni fruit nutritive value abundant and plurality kinds of health care to make
With referred to as " magical fruit ".Modern research shows that Noni fruit contains free radical resisting substance such as phenolic substances very rich, has
Machine acid and alkaloid.Noni fruit is anti-oxidant, antibacterial, the significant effect of moisturizing.In addition to developing the beautiful related nutritional health food of promise, promise
Beautiful fruit also starts to be applied to skin care item, such as lotion, facial mask etc..
Chinese patent literature CN 107496255A (application number 201710891251.7) discloses a kind of Noni fruit facial mask,
The Noni fruit facial mask contains each component of following weight percent: Noni fruit 1%~10%, moisturizer 5%~15%, thickening
Agent 0.5%~2%, solubilizer 0.05%~0.2%, nutritional additive 0.015%~0.2%, neutralizer 0.05%~
0.1%, preservative 0.05%~0.2%, deionized water surplus.The Noni fruit is Noni extract, Noni fruit ferment, promise
Any one or more of beautiful fruit juice.But these Noni fruit use forms are not suitable in handmade soap.
Summary of the invention
Technical problem to be solved by the invention is to provide beautiful essential oil grinding soaps of a kind of promise and preparation method thereof.
The technical solution for realizing the object of the invention is a kind of beautiful essential oil grinding soap of promise, the component including following parts by weight: promise
90~95 parts of beautiful soap base, 1~5 part of the beautiful essential oil of promise.
The beautiful soap base of promise, which refers to, is dissolved in the sodium hydroxide of metering in the beautiful hydrosol of promise, then carries out soap with natural oil
Change the soap base that reaction obtains.
A kind of preparation method of the beautiful essential oil grinding soap of promise, comprising the following steps:
1. preparing the beautiful essential oil of promise and the beautiful hydrosol of promise being stand-by.
2. the preparation of soap base；Natural oil is added into reactor and heats；According to the saponification value meter of used grease
Sodium hydroxide concentration is calculated, the fully saponified required sodium hydroxide of corresponding grease is weighed, is dissolved in the 1. beautiful hydrosol of promise that step lifts
In；Cool down to sodium hydroxide solution, sodium hydroxide hydrosol solution is poured slowly into grease and is uniformly mixed, at 60 DEG C~80 DEG C
At a temperature of persistently stir 2~4h, saponification process terminates；Above-mentioned manufactured soap base is put into container, and being put into temperature is 25
DEG C~40 DEG C of incubator in, wait soap lye to solidify completely, it is stand-by to obtain the beautiful soap base of promise.
It carries out first time grinding 3. the 2. beautiful soap base of promise that step obtains is sent into three-roll mill and is sliced, detect soap base
Weak acid is added into sheet soap base after metering if pH is greater than 9 in pH value；The sheet soap base for having added weak acid is mixed in blender
After be re-fed into three-roll mill and ground and be sliced for the second time.
4. the beautiful essential oil of promise of step 1. is added into the alkalescent soap base of step 3., after being mixed in blender, it is sent into fragrant
Extrusion molding in soap billet cutter obtains hand lapping soap after cold printer for perfumed soap prints, is packaged to be finished product after extrusion molding.
The pH value of soap base is 8 ± 0.2 3. above-mentioned steps are ground for the second time after.
Above-mentioned steps 4. in, the mass ratio of alkalescent soap base and the beautiful essential oil of promise is 90~95:1~5.
The present invention has the effect of positive:
(1) sodium hydroxide is dissolved in the beautiful hydrosol of promise by grinding soap of the invention when preparing soap base, then with natural oil
Rouge carries out saponification, so that including Noni fruit water soluble ingredient in part in soap base.In addition, the pH value in soap base is adjusted to 8.0
Behind left and right, promise beautiful essential oil is added when grinding, is added under the conditions of low temperature, weak base and keeps essential oil antibacterial, oxidation resistant activity.
(2) bacteriostatic test is shown, the beautiful essential oil soap good antimicrobial effect of promise of the invention；Due to maintaining the work of the beautiful essential oil of promise
Property, the beautiful essential oil soap of promise also has the effect of anti-oxidant, whitening, moisturizing.
Specific embodiment
(embodiment 1, the beautiful essential oil of promise grind soap)
The beautiful essential oil grinding soap of the promise of the present embodiment includes the component of following parts by weight: 90~95 parts of the beautiful soap base of promise, the beautiful essence of promise
1~5 part of oil.
The beautiful soap base of promise, which refers to, is dissolved in the sodium hydroxide of metering in the beautiful hydrosol of promise, then carries out soap with natural oil
Change the soap base that reaction obtains.
In order to improve the smell of the beautiful essential oil grinding soap of promise, the gas such as Rosa Damascana, chamomile essential oil, lavender can also be added
The essential oil of taste fragrance both plays the role of adjusting smell, while the effect of joined these essential oils.
Such as formula 1: a kind of beautiful essential oil grinding soap of promise, the component including following parts by weight: 90 parts of the beautiful soap base of promise, the beautiful essence of promise
1 part, 1 part of Rosa Damascana of oil.
Formula 2: a kind of beautiful essential oil grinding soap of promise, the component including following parts by weight: 95 parts of the beautiful soap base of promise, the beautiful essential oil 2 of promise
Part, 1 part of chamomile essential oil, 2 parts of Lavender.
(embodiment 2)
The preparation method of the promise of the present embodiment beautiful essential oil grinding soap the following steps are included:
1. the preparation of the beautiful essential oil of promise and the beautiful hydrosol of promise.
500g Noni fruit is washed and chopped, is put into vacuum distillation tank, then 300mL distilled water is added into tank.Steam adds
Thermal distillation enters oil water separator after the steam cooling after distillation.Water-oil separating after cooling, upper oil phase are the beautiful essential oil of promise, under
Layer water phase is the beautiful hydrosol of promise, is collected respectively stand-by.
Not only contain micro essential oil in the beautiful hydrosol of promise, meanwhile, wherein there are also the part aqueous substances in Noni fruit.This
Invention brings the effect of these water-soluble substances in soap into.
2. the preparation of soap base.Natural oil is added into reactor, is warming up to 60~80 DEG C of (the present embodiment after mixing evenly
In be 65 DEG C)；Sodium hydroxide concentration is calculated according to the saponification value of used grease, it is fully saponified required to weigh corresponding grease
Sodium hydroxide is dissolved in the 1. beautiful hydrosol of promise that step lifts, and the quality of the beautiful hydrosol of promise is 1.5 times of sodium hydroxide quality；It will
Sodium hydroxide solution cooling and the grease temperature after heating are almost the same (temperature difference is no more than 2 DEG C), by sodium hydroxide hydrosol
Solution is poured slowly into grease and is uniformly mixed, 60 DEG C~80 DEG C at a temperature of persistently stir 2~4h, saponification process terminates；
Above-mentioned manufactured soap base is put into container, and is put into the incubator that temperature is 25 DEG C~40 DEG C, soap lye is waited to solidify completely,
It is stand-by to obtain the beautiful soap base of promise.
The natural oil is coconut oil, olive oil, palm oil, palm-kernel oil, soybean oil, cottonseed oil, sunflower oil, castor-oil plant
Oil, canola oil, corn oil, white oil, peanut oil, sesame oil, grape seed oil, rice bran oil, apricot kernel oil, shea butter rouge, cocoa butter,
Avocado Oil, camellia seed oil, hazelnut oil, stearic acid, wheat-germ oil, rose hip oil, hemp-seed oil, evening primrose oil, Jojoba Oil,
One of lard, house oil, tallow, suet, ostrich oil, whale oil, beeswax or more than one combination.
Grease used in the present embodiment is olive oil.
It is once ground 3. the 2. beautiful soap base of promise that step obtains is sent into three-roll mill, and is gone out by three-roll grinder
The blade of material mouth is cut into small pieces, obtains the soap base of the sheet of 0.2mm~0.025mm thickness.
Soap base pH value is detected, if pH is added greater than 9, after metering into sheet soap base in weak acid and remaining alkali, so that pH
Value is down to 8 or so.It is re-fed into three-roll mill after the sheet soap base for having added weak acid is mixed in blender and carries out second
Secondary grinding.The pH value of sampling confirmation soap base is reduced to 8 ± 0.2.
Soap base is confirmed in after alkalescent, and three-roll mill discharges to obtain the sheet alkalescent soap of 0.2mm~0.025mm thickness
Base.
4. then according to quality than soap base: the beautiful essential oil of promise of step 1. is added into alkalescent soap base for essential oil=90:1,
After mixing in blender, it is sent into extrusion molding in perfumed soap billet cutter, after extrusion molding through cold printer for perfumed soap after -20 DEG C of printings
Hand lapping soap is obtained, finished product is packaged to be.
Since by grinding twice, after the grinding soap of the present embodiment is cut, section is flat and smooth, no particle pore-free.
Other essential oil components are such as added, He Nuoli essential oil adds simultaneously, and shaping is squeezed out after then mixing and is printed.
(anti-microbial property of test example, the beautiful essential oil grinding soap of promise)
Test specimen: the beautiful essential oil of the promise of 2 step of embodiment 4. grinds soap.
Control sample: according to, 1. to method 3., olive oil and sodium hydrate aqueous solution being carried out soap the step of embodiment 2
Change reaction, then grinds, is adjusted to alkalescent.
Test method: the left hand of subject is cleaned with test specimen, and the right hand is cleaned with control sample, with through excessively high after cleaning
The autoclaved non-woven fabrics wiping of temperature, right-hand man do not contact article, and exposure is in air；In 1h, 2h, 3h, 4h time point nothing
Non-woven fabrics is put into containing Yu Heng in the conical flask containing MH broth bouillon the back of the hand swabing sampling of right-hand man by woven fabric later
Number of bacteria is recorded with than turbid instrument after culture 18h in warm incubator, as follows:
Right-hand man's bacterial concentration (× 108CFUmL-1) variation
Comparison is as it can be seen that the grinding soap anti-microbial property for being added to the beautiful essential oil of promise is more preferable.Derive the antibacterial it is found that Ruo Nuoli essential oil
Activity retains, and illustrates that other activity of essential oil also retain, therefore essential oil soap also has anti-oxidant, moisturizing, Bearberry Extract.
Claims (5)
1. a kind of beautiful essential oil of promise grinds soap, it is characterised in that the component including following parts by weight: 90~95 parts of the beautiful soap base of promise, Nuo Li
1~5 part of essential oil.
2. the beautiful essential oil of promise according to claim 1 grinds soap, it is characterised in that: the beautiful soap base of promise refers to the hydrogen of metering
Sodium oxide molybdena is dissolved in the beautiful hydrosol of promise, then carries out the soap base that saponification obtains with natural oil.
3. a kind of preparation method of the beautiful essential oil grinding soap of promise, it is characterised in that the following steps are included:
1. preparing the beautiful essential oil of promise and the beautiful hydrosol of promise being stand-by；
2. the preparation of soap base；Natural oil is added into reactor and heats；Hydrogen is calculated according to the saponification value of used grease
Sodium oxide molybdena dosage weighs the fully saponified required sodium hydroxide of corresponding grease, is dissolved in the 1. beautiful hydrosol of promise that step lifts；To
Sodium hydroxide solution cooling, sodium hydroxide hydrosol solution is poured slowly into grease and is uniformly mixed, in 60 DEG C~80 DEG C of temperature
2~4h is persistently stirred under degree, saponification process terminates；Above-mentioned manufactured soap base is put into container, and be put into temperature be 25 DEG C~
In 40 DEG C of incubator, waits soap lye to solidify completely, it is stand-by to obtain the beautiful soap base of promise；
It carries out first time grinding 3. the 2. beautiful soap base of promise that step obtains is sent into three-roll mill and is sliced, detect soap base pH
Weak acid is added into sheet soap base after metering if pH is greater than 9 in value；After the sheet soap base for having added weak acid is mixed in blender
It is re-fed into three-roll mill and is ground and be sliced for the second time；
4. the beautiful essential oil of promise of step 1. is added into the alkalescent soap base of step 3., after being mixed in blender, it is sent into perfumed soap and goes out
Extrusion molding in machine obtains hand lapping soap after cold printer for perfumed soap prints, is packaged to be finished product after extrusion molding.
4. the preparation method of the beautiful essential oil grinding soap of promise according to claim 3, it is characterised in that: 3. step is ground for second
The pH value of soap base is 8 ± 0.2 afterwards.
5. the preparation method of the beautiful essential oil grinding soap of promise according to claim 3, it is characterised in that: step 4. in, alkalescent
The mass ratio of soap base and the beautiful essential oil of promise is 90~95:1~5.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910374036.9A CN109971571A (en) | 2019-05-07 | 2019-05-07 | Beautiful essential oil grinding soap of a kind of promise and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910374036.9A CN109971571A (en) | 2019-05-07 | 2019-05-07 | Beautiful essential oil grinding soap of a kind of promise and preparation method thereof |
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| Publication Number | Publication Date |
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| CN109971571A true CN109971571A (en) | 2019-07-05 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910374036.9A Pending CN109971571A (en) | 2019-05-07 | 2019-05-07 | Beautiful essential oil grinding soap of a kind of promise and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115746957A (en) * | 2022-11-21 | 2023-03-07 | 中国热带农业科学院热带作物品种资源研究所 | Application of noni essential oil in inhibiting proteus mirabilis |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103756817A (en) * | 2014-01-26 | 2014-04-30 | 夏程 | Preparation method for manually ground soap |
| CN106833978A (en) * | 2017-01-17 | 2017-06-13 | 孟蕲翾 | It is a kind of with antibacterial, acne-removal function beautiful handmade soap of promise and preparation method thereof |
-
2019
- 2019-05-07 CN CN201910374036.9A patent/CN109971571A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103756817A (en) * | 2014-01-26 | 2014-04-30 | 夏程 | Preparation method for manually ground soap |
| CN106833978A (en) * | 2017-01-17 | 2017-06-13 | 孟蕲翾 | It is a kind of with antibacterial, acne-removal function beautiful handmade soap of promise and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115746957A (en) * | 2022-11-21 | 2023-03-07 | 中国热带农业科学院热带作物品种资源研究所 | Application of noni essential oil in inhibiting proteus mirabilis |
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Application publication date: 20190705 |