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CN108432808A - A kind of soya seeds coating agent and preparation method thereof - Google Patents

A kind of soya seeds coating agent and preparation method thereof Download PDF

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Publication number
CN108432808A
CN108432808A CN201810381984.0A CN201810381984A CN108432808A CN 108432808 A CN108432808 A CN 108432808A CN 201810381984 A CN201810381984 A CN 201810381984A CN 108432808 A CN108432808 A CN 108432808A
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Prior art keywords
parts
water
powder
soya seeds
coating agent
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CN201810381984.0A
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Chinese (zh)
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刘利
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Hefei Huigu Agricultural Technology Co Ltd
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Hefei Huigu Agricultural Technology Co Ltd
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Priority to CN201810381984.0A priority Critical patent/CN108432808A/en
Publication of CN108432808A publication Critical patent/CN108432808A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01CPLANTING; SOWING; FERTILISING
    • A01C1/00Apparatus, or methods of use thereof, for testing or treating seed, roots, or the like, prior to sowing or planting
    • A01C1/06Coating or dressing seed
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/36Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/06Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
    • A01N43/12Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings condensed with a carbocyclic ring
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/36Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
    • A01N43/38Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings condensed with carbocyclic rings
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N45/00Biocides, pest repellants or attractants, or plant growth regulators, containing compounds having three or more carbocyclic rings condensed among themselves, at least one ring not being a six-membered ring
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/14Boron; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/03Algae
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    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K17/00Soil-conditioning materials or soil-stabilising materials
    • C09K17/02Soil-conditioning materials or soil-stabilising materials containing inorganic compounds only
    • C09K17/08Aluminium compounds, e.g. aluminium hydroxide
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K17/00Soil-conditioning materials or soil-stabilising materials
    • C09K17/40Soil-conditioning materials or soil-stabilising materials containing mixtures of inorganic and organic compounds
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K2101/00Agricultural use
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Environmental Sciences (AREA)
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  • Zoology (AREA)
  • Agronomy & Crop Science (AREA)
  • Plant Pathology (AREA)
  • Wood Science & Technology (AREA)
  • Chemical & Material Sciences (AREA)
  • Pest Control & Pesticides (AREA)
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  • Biotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Mycology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Microbiology (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
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  • Toxicology (AREA)
  • Pretreatment Of Seeds And Plants (AREA)

Abstract

The invention discloses a kind of soya seeds coating agents, include the raw material of following parts by weight:10~20 parts of kelp, 8~13 parts of montmorillonite, 15~25 parts of attapulgite, 5~15 parts of lactic acid, 7~14 parts of chitosan, 5~9 parts of modified Nano bamboo charcoal powder, 6~10 parts of lychee exocarp, 0.01~0.03 part of poly-aspartate, 0.02~0.04 part of heteroauxin, 0.01~0.02 part of gibberellin, 3~6 parts of borax, 2~3 parts of water-retaining agent, 1~4 part of thickener, 1~2 part of insecticide, 1~3 part of fungicide, 20~30 parts of water.The soya seeds coating agent can improve the germination rate of soya seeds, strengthening root, while improve yield, controlling crop diseases and insect pests, and not to people and animals and environmental danger and pollution.

Description

A kind of soya seeds coating agent and preparation method thereof
Technical field
The invention belongs to coating agent technical fields, and in particular to a kind of soya seeds coating agent and preparation method thereof.
Background technology
Soya bean is called black soyabean with green kernel, soybean, mud beans, SEMEN GLYCINE, fodder food beans, and kind has winter beans, Qiu Dou, kidney bean, China Main product is in the Northeast.It was called in ancient China that bean, is a kind of crop whose seed contained abundant protein.Pulse family plants soybean in ellipse Shape, spherical shape, color have yellow, light green, black etc..Soybean be most commonly used for various bean product, squeeze soya-bean oil, make soy sauce and Extract protein.Bean dregs or the soybean for wearing into coarse powder are also commonly used for poultry and livestock feed.
When present soybean planting, carried out in such a way that full soybean particle is directly planted, seed viability is low, causes It needs secondary benefit to plant when soybean planting, not only substantially increases the amount of labour, can also cause the soybean underproduction.
Invention content
The present invention provides a kind of soya seeds coating agents and preparation method thereof, solve asking in above-mentioned background technology Topic, the soya seeds coating agent can improve the germination rate of soya seeds, and strengthening root improves yield, controlling crop diseases and insect pests Meanwhile and not to people and animals and environmental danger and pollution.
It is of the existing technology in order to solve the problems, such as, it adopts the following technical scheme that:
A kind of soya seeds coating agent, includes the raw material of following parts by weight:10~20 parts of kelp, 8~13 parts of montmorillonite, concave convex rod 15~25 parts of soil, 5~15 parts of lactic acid, 7~14 parts of chitosan, 5~9 parts of modified Nano bamboo charcoal powder, 6~10 parts of lychee exocarp, poly- day 0.01~0.03 part of winter propylhomoserin, 0.02~0.04 part of heteroauxin, 0.01~0.02 part of gibberellin, 3~6 parts of borax, water-retaining agent 2 ~3 parts, 1~4 part of thickener, 1~2 part of insecticide, 1~3 part of fungicide, 20~30 parts of water.
Preferably, the soya seeds coating agent, includes the raw material of following parts by weight:12~17 parts of kelp, montmorillonite 10 ~12 parts, 18~23 parts of attapulgite, 6~11 parts of lactic acid, 10~13 parts of chitosan, 6~8 parts of modified Nano bamboo charcoal powder, lichee 7~9 parts of shell, 0.015~0.024 part of poly-aspartate, 0.029~0.032 part of heteroauxin, gibberellin 0.013~0.015 Part, 4~5 parts of borax, 2.2~2.8 parts of water-retaining agent, 2~3 parts of thickener, 1.2~1.8 parts of insecticide, fungicide 1.5~2.1 Part, 23~28 parts of water.
Preferably, the soya seeds coating agent, includes the raw material of following parts by weight:It is 15 parts of kelp, 11 parts of montmorillonite, recessed Convex 20 parts of stick soil, 8 parts of lactic acid, 12 parts of chitosan, 7 parts of modified Nano bamboo charcoal powder, 8 parts of lychee exocarp, 0.02 part of poly-aspartate, Yin 0.03 part of indolylbutyric acid, 0.014 part of gibberellin, 4.5 parts of borax, 2.6 parts of water-retaining agent, 2.6 parts of thickener, 1.7 parts of insecticide, sterilization 1.9 parts of agent, 25 parts of water.
Preferably, the preparation method of the modified Nano bamboo charcoal powder is as follows:
Bamboo charcoal is put into after being impregnated 4~5 hours in glacial acetic acid solution, takes out washing, it is small then at 400~450 DEG C of calcinings 4~6 When, then it is ground into nanometer powder to obtain the final product.
Preferably, the water-retaining agent is super absorbent resin.
Preferably, the insecticide be turmeric, cloves, Siberian cocklebur, lime mixed-powder.
A method of the soya seeds coating agent is prepared, is included the following steps:
(1)By above-mentioned formula weigh kelp, montmorillonite, attapulgite, lactic acid, chitosan, modified Nano bamboo charcoal powder, lychee exocarp, Poly-aspartate, heteroauxin, gibberellin, borax, water-retaining agent, thickener, insecticide, fungicide, water, it is spare;
(2)Kelp is air-dried, then shreds, grind into powder, is placed in reaction kettle, water is added, is uniformly mixed, is then added Heat is kept the temperature and quick stirring 2~4 hours to 60~80 DEG C, and re-ultrasonic dispersion 5~10 minutes is to get kelp paste;
(3)Chitosan, lactic acid and thickener are placed in step(2)It in the kelp paste of gained, is subsequently placed in reaction kettle, is passed through nitrogen Gas is warming up to 50 DEG C, quickly stirs 1~2 hour, obtains mixed liquor;
(4)Montmorillonite, attapulgite are placed in 400~500 DEG C of environment and calcined 1~2 hour, is cooled to room temperature, by lychee exocarp It is dry to be less than 5% to water content, then by after calcining montmorillonite, attapulgite, it is dry after lychee exocarp and borax mix it is equal It is even, it is ground into nanometer powder, then be uniformly mixed with modified Nano bamboo charcoal powder, obtains mixed-powder;
(5)Poly-aspartate, heteroauxin, gibberellin are placed in step(3)In the mixed liquor of gained, 45~55 DEG C are heated to, Insulated and stirred 20~30 minutes, then is cooled to room temperature, sequentially adds step(4)Mixed-powder, water-retaining agent, the insecticide of gained And fungicide, high speed dispersion is uniformly to get the soya seeds coating agent.
Preferably, the step(5)The time of high speed dispersion is 17~23 minutes, and rate of dispersion is 1750~2230r/ min。
Compared with prior art, the present invention it has the advantages that:
Soya seeds coating agent of the present invention can improve the germination rate of soya seeds, and strengthening root improves yield, prevention crop disease It is specific as follows while insect pest, and not to people and animals and environmental danger and pollution:
(1)Soya seeds coating agent of the present invention is received using kelp, montmorillonite, attapulgite, lactic acid, chitosan, modification Rice bamboo charcoal powder etc. is used as raw material, mutually acts synergistically between raw material, and the product prepared can activate soybean to uphold the factor, promotes Germination of Soybean Seed improves the germination rate of soya seeds;
(2)Soya seeds coating agent of the present invention is using montmorillonite, attapulgite as raw material, montmorillonite and attapulgite For porous mineral matter, have good permeability and adsorptivity, the soil that obtained product can improve near soybean planting hole penetrating Property, using the growth of soybean, the yield of soybean is improved, and nutriment can be adsorbed, improves the persistence of fertilizer efficiency;
(3)For soya seeds coating agent of the present invention using kelp as raw material, kelp contains various trace elements, Neng Gouman Sufficient soybean grows demand, promotes soybean growth;
(4)The raw material that soya seeds coating agent of the present invention uses can voluntarily degrade in nature, will not to people and animals and Environmental danger and pollution.
Specific implementation mode
Present invention will be further explained below with reference to specific examples.These embodiments are merely to illustrate the present invention and do not have to In limiting the scope of the invention.
Embodiment 1
The present embodiment is related to a kind of soya seeds coating agent, includes the raw material of following parts by weight:It is 10 parts of kelp, 8 parts of montmorillonite, recessed Convex 15 parts of stick soil, 5 parts of lactic acid, 7 parts of chitosan, 5 parts of modified Nano bamboo charcoal powder, 6 parts of lychee exocarp, 0.01 part of poly-aspartate, Yin 0.02 part of indolylbutyric acid, 0.01 part of gibberellin, 3 parts of borax, 2 parts of water-retaining agent, 1 part of thickener, 1 part of insecticide, 1 part of fungicide, water 20 parts.
Wherein, the preparation method of the modified Nano bamboo charcoal powder is as follows:
Bamboo charcoal is put into after being impregnated 4 hours in glacial acetic acid solution, takes out washing, calcined 4 hours then at 400 DEG C, be then ground into Nanometer powder to obtain the final product.
Wherein, the water-retaining agent is super absorbent resin.
Wherein, the insecticide be turmeric, cloves, Siberian cocklebur, lime mixed-powder.
A method of the soya seeds coating agent is prepared, is included the following steps:
(1)By above-mentioned formula weigh kelp, montmorillonite, attapulgite, lactic acid, chitosan, modified Nano bamboo charcoal powder, lychee exocarp, Poly-aspartate, heteroauxin, gibberellin, borax, water-retaining agent, thickener, insecticide, fungicide, water, it is spare;
(2)Kelp is air-dried, then shreds, grind into powder, is placed in reaction kettle, water is added, is uniformly mixed, is then added Heat is kept the temperature and quick stirring 2 hours to 60 DEG C, and re-ultrasonic dispersion 5 minutes is to get kelp paste;
(3)Chitosan, lactic acid and thickener are placed in step(2)It in the kelp paste of gained, is subsequently placed in reaction kettle, is passed through nitrogen Gas is warming up to 50 DEG C, and quickly stirring 1 hour, obtains mixed liquor;
(4)Montmorillonite, attapulgite are placed in 400 DEG C of environment and calcined 1 hour, is cooled to room temperature, lychee exocarp is dried to containing Water is less than 5%, then by after calcining montmorillonite, attapulgite, it is dry after lychee exocarp and borax be uniformly mixed, be ground into Nanometer powder, then be uniformly mixed with modified Nano bamboo charcoal powder, obtain mixed-powder;
(5)Poly-aspartate, heteroauxin, gibberellin are placed in step(3)In the mixed liquor of gained, 45 DEG C are heated to, heat preservation Stirring 20 minutes, then is cooled to room temperature, sequentially adds step(4)Mixed-powder, water-retaining agent, insecticide and the sterilization of gained Agent, high speed dispersion is uniformly to get the soya seeds coating agent.
Wherein, the step(5)The time of high speed dispersion is 17 minutes, rate of dispersion 1750r/min.
Embodiment 2
The present embodiment is related to a kind of soya seeds coating agent, includes the raw material of following parts by weight:20 parts of kelp, 13 parts of montmorillonite, 25 parts of attapulgite, 15 parts of lactic acid, 14 parts of chitosan, 9 parts of modified Nano bamboo charcoal powder, 10 parts of lychee exocarp, poly-aspartate 0.03 Part, 0.04 part of heteroauxin, 0.02 part of gibberellin, 6 parts of borax, 3 parts of water-retaining agent, 4 parts of thickener, 2 parts of insecticide, fungicide 3 Part, 30 parts of water.
Wherein, the preparation method of the modified Nano bamboo charcoal powder is as follows:
Bamboo charcoal is put into after being impregnated 5 hours in glacial acetic acid solution, takes out washing, calcined 6 hours then at 450 DEG C, then grind At nanometer powder to obtain the final product.
Wherein, the water-retaining agent is super absorbent resin.
Wherein, the insecticide be turmeric, cloves, Siberian cocklebur, lime mixed-powder.
A method of the soya seeds coating agent is prepared, is included the following steps:
(1)By above-mentioned formula weigh kelp, montmorillonite, attapulgite, lactic acid, chitosan, modified Nano bamboo charcoal powder, lychee exocarp, Poly-aspartate, heteroauxin, gibberellin, borax, water-retaining agent, thickener, insecticide, fungicide, water, it is spare;
(2)Kelp is air-dried, then shreds, grind into powder, is placed in reaction kettle, water is added, is uniformly mixed, is then added Heat is kept the temperature and quick stirring 4 hours to 80 DEG C, and re-ultrasonic dispersion 10 minutes is to get kelp paste;
(3)Chitosan, lactic acid and thickener are placed in step(2)It in the kelp paste of gained, is subsequently placed in reaction kettle, is passed through nitrogen Gas is warming up to 50 DEG C, and quickly stirring 2 hours, obtain mixed liquor;
(4)Montmorillonite, attapulgite are placed in 500 DEG C of environment and calcined 2 hours, is cooled to room temperature, lychee exocarp is dried to containing Water is less than 5%, then by after calcining montmorillonite, attapulgite, it is dry after lychee exocarp and borax be uniformly mixed, be ground into Nanometer powder, then be uniformly mixed with modified Nano bamboo charcoal powder, obtain mixed-powder;
(5)Poly-aspartate, heteroauxin, gibberellin are placed in step(3)In the mixed liquor of gained, 55 DEG C are heated to, heat preservation Stirring 30 minutes, then is cooled to room temperature, sequentially adds step(4)Mixed-powder, water-retaining agent, insecticide and the sterilization of gained Agent, high speed dispersion is uniformly to get the soya seeds coating agent.
Wherein, the step(5)The time of high speed dispersion is 23 minutes, rate of dispersion 2230r/min.
Embodiment 3
The present embodiment is related to a kind of soya seeds coating agent, includes the raw material of following parts by weight:12 parts of kelp, 10 parts of montmorillonite, 18 parts of attapulgite, 6 parts of lactic acid, 10 parts of chitosan, 6 parts of modified Nano bamboo charcoal powder, 7 parts of lychee exocarp, poly-aspartate 0.015 Part, 1.2 parts of insecticide, is killed at 0.029 part of heteroauxin, 0.013 part of gibberellin, 4 parts of borax, 2.2 parts of water-retaining agent, 2 parts of thickener 1.5 parts of microbial inoculum, 23 parts of water.
Wherein, the preparation method of the modified Nano bamboo charcoal powder is as follows:
Bamboo charcoal is put into after being impregnated 4.5 hours in glacial acetic acid solution, takes out washing, calcined 4.5 hours then at 410 DEG C, then grind Wear into nanometer powder to obtain the final product.
Wherein, the water-retaining agent is super absorbent resin.
Wherein, the insecticide be turmeric, cloves, Siberian cocklebur, lime mixed-powder.
A method of the soya seeds coating agent is prepared, is included the following steps:
(1)By above-mentioned formula weigh kelp, montmorillonite, attapulgite, lactic acid, chitosan, modified Nano bamboo charcoal powder, lychee exocarp, Poly-aspartate, heteroauxin, gibberellin, borax, water-retaining agent, thickener, insecticide, fungicide, water, it is spare;
(2)Kelp is air-dried, then shreds, grind into powder, is placed in reaction kettle, water is added, is uniformly mixed, is then added Heat is kept the temperature and quick stirring 2.5 hours to 65 DEG C, and re-ultrasonic dispersion 6 minutes is to get kelp paste;
(3)Chitosan, lactic acid and thickener are placed in step(2)It in the kelp paste of gained, is subsequently placed in reaction kettle, is passed through nitrogen Gas is warming up to 50 DEG C, and quickly stirring 1.2 hours, obtain mixed liquor;
(4)Montmorillonite, attapulgite are placed in 420 DEG C of environment and calcined 1.3 hours, is cooled to room temperature, by lychee exocarp dry to Water content is less than 5%, then by after calcining montmorillonite, attapulgite, it is dry after lychee exocarp and borax be uniformly mixed, grind It is uniformly mixed at nanometer powder, then with modified Nano bamboo charcoal powder, obtains mixed-powder;
(5)Poly-aspartate, heteroauxin, gibberellin are placed in step(3)In the mixed liquor of gained, 48 DEG C are heated to, heat preservation Stirring 23 minutes, then is cooled to room temperature, sequentially adds step(4)Mixed-powder, water-retaining agent, insecticide and the sterilization of gained Agent, high speed dispersion is uniformly to get the soya seeds coating agent.
Wherein, the step(5)The time of high speed dispersion is 18 minutes, rate of dispersion 1900r/min.
Embodiment 4
The present embodiment is related to a kind of soya seeds coating agent, includes the raw material of following parts by weight:17 parts of kelp, 12 parts of montmorillonite, 23 parts of attapulgite, 11 parts of lactic acid, 13 parts of chitosan, 8 parts of modified Nano bamboo charcoal powder, 9 parts of lychee exocarp, poly-aspartate 0.024 Part, 1.8 parts of insecticide, is killed at 0.032 part of heteroauxin, 0.015 part of gibberellin, 5 parts of borax, 2.8 parts of water-retaining agent, 3 parts of thickener 2.1 parts of microbial inoculum, 28 parts of water.
Wherein, the preparation method of the modified Nano bamboo charcoal powder is as follows:
Bamboo charcoal is put into after being impregnated 4.5 hours in glacial acetic acid solution, takes out washing, calcined 5 hours then at 420 DEG C, then grind At nanometer powder to obtain the final product.
Wherein, the water-retaining agent is super absorbent resin.
Wherein, the insecticide be turmeric, cloves, Siberian cocklebur, lime mixed-powder.
A method of the soya seeds coating agent is prepared, is included the following steps:
(1)By above-mentioned formula weigh kelp, montmorillonite, attapulgite, lactic acid, chitosan, modified Nano bamboo charcoal powder, lychee exocarp, Poly-aspartate, heteroauxin, gibberellin, borax, water-retaining agent, thickener, insecticide, fungicide, water, it is spare;
(2)Kelp is air-dried, then shreds, grind into powder, is placed in reaction kettle, water is added, is uniformly mixed, is then added Heat is kept the temperature and quick stirring 3 hours to 70 DEG C, and re-ultrasonic dispersion 7 minutes is to get kelp paste;
(3)Chitosan, lactic acid and thickener are placed in step(2)It in the kelp paste of gained, is subsequently placed in reaction kettle, is passed through nitrogen Gas is warming up to 50 DEG C, and quickly stirring 1.5 hours, obtain mixed liquor;
(4)Montmorillonite, attapulgite are placed in 450 DEG C of environment and calcined 1.5 hours, is cooled to room temperature, by lychee exocarp dry to Water content is less than 5%, then by after calcining montmorillonite, attapulgite, it is dry after lychee exocarp and borax be uniformly mixed, grind It is uniformly mixed at nanometer powder, then with modified Nano bamboo charcoal powder, obtains mixed-powder;
(5)Poly-aspartate, heteroauxin, gibberellin are placed in step(3)In the mixed liquor of gained, 50 DEG C are heated to, heat preservation Stirring 25 minutes, then is cooled to room temperature, sequentially adds step(4)Mixed-powder, water-retaining agent, insecticide and the sterilization of gained Agent, high speed dispersion is uniformly to get the soya seeds coating agent.
Wherein, the step(5)The time of high speed dispersion is 20 minutes, rate of dispersion 2000r/min.
Embodiment 5
The present embodiment is related to a kind of soya seeds coating agent, includes the raw material of following parts by weight:15 parts of kelp, 11 parts of montmorillonite, 20 parts of attapulgite, 8 parts of lactic acid, 12 parts of chitosan, 7 parts of modified Nano bamboo charcoal powder, 8 parts of lychee exocarp, 0.02 part of poly-aspartate, 0.03 part of heteroauxin, 4.5 parts of borax, 2.6 parts of water-retaining agent, 2.6 parts of thickener, 1.7 parts of insecticide, kills at 0.014 part of gibberellin 1.9 parts of microbial inoculum, 25 parts of water.
Wherein, the preparation method of the modified Nano bamboo charcoal powder is as follows:
Bamboo charcoal is put into after being impregnated 4.5 hours in glacial acetic acid solution, take out washing, then at 440 DEG C calcine 5.5 hours, then It is ground into nanometer powder to obtain the final product.
Wherein, the water-retaining agent is super absorbent resin.
Wherein, the insecticide be turmeric, cloves, Siberian cocklebur, lime mixed-powder.
A method of the soya seeds coating agent is prepared, is included the following steps:
(1)By above-mentioned formula weigh kelp, montmorillonite, attapulgite, lactic acid, chitosan, modified Nano bamboo charcoal powder, lychee exocarp, Poly-aspartate, heteroauxin, gibberellin, borax, water-retaining agent, thickener, insecticide, fungicide, water, it is spare;
(2)Kelp is air-dried, then shreds, grind into powder, is placed in reaction kettle, water is added, is uniformly mixed, is then added Heat is kept the temperature and quick stirring 3.5 hours to 75 DEG C, and re-ultrasonic dispersion 9 minutes is to get kelp paste;
(3)Chitosan, lactic acid and thickener are placed in step(2)It in the kelp paste of gained, is subsequently placed in reaction kettle, is passed through nitrogen Gas is warming up to 50 DEG C, and quickly stirring 1.8 hours, obtain mixed liquor;
(4)Montmorillonite, attapulgite are placed in 470 DEG C of environment and calcined 1.8 hours, is cooled to room temperature, by lychee exocarp dry to Water content is less than 5%, then by after calcining montmorillonite, attapulgite, it is dry after lychee exocarp and borax be uniformly mixed, grind It is uniformly mixed at nanometer powder, then with modified Nano bamboo charcoal powder, obtains mixed-powder;
(5)Poly-aspartate, heteroauxin, gibberellin are placed in step(3)In the mixed liquor of gained, 52 DEG C are heated to, heat preservation Stirring 28 minutes, then is cooled to room temperature, sequentially adds step(4)Mixed-powder, water-retaining agent, insecticide and the sterilization of gained Agent, high speed dispersion is uniformly to get the soya seeds coating agent.
Wherein, the step(5)The time of high speed dispersion is 22 minutes, rate of dispersion 2100r/min.
Using the soya seeds coating agent described in embodiment 1, embodiment 2, embodiment 3, embodiment 4, embodiment 5, to same A batch of soya seeds are coated, and as experimental group, then are chosen with a batch of seed, will be real without Cotton seeds The seed of the seed and control group of testing group is sowed respectively on same soil, its germination percentage and per mu yield are observed, and records result Such as following table:
Group Germination percentage Per mu yield
Embodiment 1 98.5% 600 jin
Embodiment 2 98.6% 570 jin
Embodiment 3 99% 580 jin
Embodiment 4 98.7% 610 jin
Embodiment 5 99% 620 jin
Control group 95% 500 jin
As can be seen from the above table, soya seeds coating agent of the present invention can improve the germination percentage of soybean, promote the production of soybean Amount.
Specific embodiments of the present invention are described above.It is to be appreciated that the invention is not limited in above-mentioned Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow Ring the substantive content of the present invention.

Claims (8)

1. a kind of soya seeds coating agent, which is characterized in that include the raw material of following parts by weight:10~20 parts of kelp, montmorillonite 8 ~13 parts, 15~25 parts of attapulgite, 5~15 parts of lactic acid, 7~14 parts of chitosan, 5~9 parts of modified Nano bamboo charcoal powder, lychee exocarp 6~10 parts, 0.01~0.03 part of poly-aspartate, 0.02~0.04 part of heteroauxin, 0.01~0.02 part of gibberellin, borax 3 ~6 parts, 2~3 parts of water-retaining agent, 1~4 part of thickener, 1~2 part of insecticide, 1~3 part of fungicide, 20~30 parts of water.
2. soya seeds coating agent according to claim 1, which is characterized in that include the raw material of following parts by weight:Kelp 12~17 parts, 10~12 parts of montmorillonite, 18~23 parts of attapulgite, 6~11 parts of lactic acid, 10~13 parts of chitosan, modified Nano It is 6~8 parts of bamboo charcoal powder, 7~9 parts of lychee exocarp, 0.015~0.024 part of poly-aspartate, 0.029~0.032 part of heteroauxin, red 0.013~0.015 part of mycin, 4~5 parts of borax, 2.2~2.8 parts of water-retaining agent, 2~3 parts of thickener, 1.2~1.8 parts of insecticide, 1.5~2.1 parts of fungicide, 23~28 parts of water.
3. soya seeds coating agent according to claim 1, which is characterized in that include the raw material of following parts by weight:Kelp 15 parts, 11 parts of montmorillonite, 20 parts of attapulgite, 8 parts of lactic acid, 12 parts of chitosan, 7 parts of modified Nano bamboo charcoal powder, 8 parts of lychee exocarp, 0.02 part of poly-aspartate, 0.03 part of heteroauxin, 0.014 part of gibberellin, 4.5 parts of borax, 2.6 parts of water-retaining agent, thickener 2.6 Part, 1.7 parts of insecticide, 1.9 parts of fungicide, 25 parts of water.
4. soya seeds coating agent according to claim 1, which is characterized in that the preparation side of the modified Nano bamboo charcoal powder Method is as follows:
Bamboo charcoal is put into after being impregnated 4~5 hours in glacial acetic acid solution, takes out washing, it is small then at 400~450 DEG C of calcinings 4~6 When, then it is ground into nanometer powder to obtain the final product.
5. soya seeds coating agent according to claim 1, which is characterized in that the water-retaining agent is super absorbent resin.
6. soya seeds coating agent according to claim 1, which is characterized in that the insecticide is turmeric, cloves, grey The mixed-powder of ear, lime.
7. a kind of method preparing any one of claim 1~6 soya seeds coating agent, which is characterized in that including following Step:
(1)By above-mentioned formula weigh kelp, montmorillonite, attapulgite, lactic acid, chitosan, modified Nano bamboo charcoal powder, lychee exocarp, Poly-aspartate, heteroauxin, gibberellin, borax, water-retaining agent, thickener, insecticide, fungicide, water, it is spare;
(2)Kelp is air-dried, then shreds, grind into powder, is placed in reaction kettle, water is added, is uniformly mixed, is then added Heat is kept the temperature and quick stirring 2~4 hours to 60~80 DEG C, and re-ultrasonic dispersion 5~10 minutes is to get kelp paste;
(3)Chitosan, lactic acid and thickener are placed in step(2)It in the kelp paste of gained, is subsequently placed in reaction kettle, is passed through nitrogen Gas is warming up to 50 DEG C, quickly stirs 1~2 hour, obtains mixed liquor;
(4)Montmorillonite, attapulgite are placed in 400~500 DEG C of environment and calcined 1~2 hour, is cooled to room temperature, by lychee exocarp It is dry to be less than 5% to water content, then by after calcining montmorillonite, attapulgite, it is dry after lychee exocarp and borax mix it is equal It is even, it is ground into nanometer powder, then be uniformly mixed with modified Nano bamboo charcoal powder, obtains mixed-powder;
(5)Poly-aspartate, heteroauxin, gibberellin are placed in step(3)In the mixed liquor of gained, 45~55 DEG C are heated to, Insulated and stirred 20~30 minutes, then is cooled to room temperature, sequentially adds step(4)Mixed-powder, water-retaining agent, the insecticide of gained And fungicide, high speed dispersion is uniformly to get the soya seeds coating agent.
8. preparation method according to claim 7, which is characterized in that the step(5)The time of high speed dispersion is 17 ~23 minutes, rate of dispersion was 1750~2230r/min.
CN201810381984.0A 2018-04-26 2018-04-26 A kind of soya seeds coating agent and preparation method thereof Withdrawn CN108432808A (en)

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