CN108314908A - Luminous pigment and preparation method thereof - Google Patents
Luminous pigment and preparation method thereof Download PDFInfo
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- CN108314908A CN108314908A CN201810054936.0A CN201810054936A CN108314908A CN 108314908 A CN108314908 A CN 108314908A CN 201810054936 A CN201810054936 A CN 201810054936A CN 108314908 A CN108314908 A CN 108314908A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
- C09K11/77—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
- C09K11/7706—Aluminates
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/40—Compounds of aluminium
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/006—Combinations of treatments provided for in groups C09C3/04 - C09C3/12
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/08—Treatment with low-molecular-weight non-polymer organic compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/10—Treatment with macromolecular organic compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/02—Use of particular materials as binders, particle coatings or suspension media therefor
- C09K11/025—Use of particular materials as binders, particle coatings or suspension media therefor non-luminescent particle coatings or suspension media
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
- C09K11/64—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing aluminium
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
- C09K11/77—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
- C09K11/7756—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals containing neodynium
- C09K11/7758—Aluminates; Silicates
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Luminescent Compositions (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
A kind of luminous pigment of the present invention, includes the raw material of following parts by weight：0.01 part~1 part of 75 parts~85 parts of pure water, 5 parts~15 parts of sugar, 1 part~10 parts of rare earth aluminate, 1 part~5 parts of cellulose, 0.01 part~0.5 part of sodium benzoate and pigment.The luminous pigment of the present invention, production is easy, and energy conservation and environmental protection is safe to use；It is tasteless nontoxic, no chemical substance volatile matter；More preferably, for material without Problem of Shading, film layer brightness is fine for illumination effect.
Description
Technical field
The invention belongs to technical field of biological materials, and in particular to a kind of luminous pigment and preparation method thereof.
Background technology
Luminous pigment is powdered photic light-accumulating luminous material, usually by the sulfide of zinc, calcium, barium or strontium, a small amount of help
Flux (such as sodium chloride) and micro activator are transferred to RED sector by blue, are transferred to by green using copper as activator
RED sector.Existing market luminous pigment effect is undesirable：First, safety is bad, the overwhelming majority is resin emulsion type product；
Second is that easily caking and generation precipitates；Third, material shading and so that product light emission luminance is affected.
Invention content
An object of the present invention is to provide a kind of luminous pigments.
A kind of luminous pigment of the present invention, includes the raw material of following parts by weight：75 parts~85 parts of pure water, 5 parts of sugar~
15 parts, 1 part~10 parts of rare earth aluminate, 1 part~5 parts of cellulose, 0.01 part~0.5 part of sodium benzoate and pigment 0.01 part~1
Part.
The luminous pigment of the embodiment of the present invention, production is easy, and energy conservation and environmental protection is safe to use；It is tasteless nontoxic, no chemistry
Substance volatile matter；More preferably, for material without Problem of Shading, film layer brightness is fine for illumination effect.
In addition, according to the above-mentioned luminous pigment of the present invention, there can also be following additional technical characteristic：
As the preferred embodiment of the present invention, the luminous pigment includes the raw material of following parts by weight：Pure water
85 parts, 5 parts of sugar, 10 parts of rare earth aluminate, 1 part of cellulose, 0.01 part of 0.5 part of sodium benzoate and pigment.
As the preferred embodiment of the present invention, the luminous pigment includes the raw material of following parts by weight：Pure water
75 parts, 15 parts of sugar, 1 part of rare earth aluminate, 5 parts of cellulose, 1 part of 0.01 part of sodium benzoate and pigment.
As the preferred embodiment of the present invention, the luminous pigment includes the raw material of following parts by weight：Pure water
82 parts, 8 parts of sugar, 8 parts of rare earth aluminate, 2 parts of cellulose, 0.2 part of 0.2 part of sodium benzoate and pigment.
As the preferred embodiment of the present invention, the luminous pigment includes the raw material of following parts by weight：Pure water
81.5 parts, 10 parts of sugar, 5 parts of rare earth aluminate, 3 parts of cellulose, 0.1 part of 0.3 part of sodium benzoate and pigment.
Further, the cellulose includes carboxyethyl cellulose, hydroxymethyl cellulose and xanthans, and the carboxyethyl
The weight ratio of cellulose, hydroxymethyl cellulose and xanthans is 2:1:1.
Further, the sugar is white granulated sugar.
It is another object of the present invention to the preparation methods for proposing the luminous pigment.
The preparation method of the luminous pigment, includes the following steps：S101：The white sand is added in the pure water
Then the sugared and described sodium benzoate is added the cellulose and stirs 0.3h~0.8h, then stands, after cellulose swelling
Disperseed with dispersion machine；S102：The rare earth aluminate and the pigment are mixed and stirred for；S103：By the step
The product that the step S102 is obtained is added in the product that S101 is obtained under the conditions of dispersion machine high-speed stirred, then stir 1.8h~
Then 2.2h reduces rotating speed and is defoamed, obtains luminous pigment.
Further, in the step S103, rotating speed when high-speed stirred is 1000r/min~3000r/min；It reduces
100r/min~500r/min is down to when rotating speed.
The additional aspect and advantage of the present invention will be set forth in part in the description, and will partly become from the following description
Obviously, or practice through the invention is recognized.
Specific implementation mode
The embodiment of the present invention is described below in detail, the embodiment is exemplary, it is intended to for explaining the present invention, and
It is not considered as limiting the invention.
Embodiment 1
Embodiment 1 proposes a kind of luminous pigment, includes the raw material of following parts by weight：85 parts of pure water, white granulated sugar 5
Part, 10 parts of aluminic acid neodymium calcium, 0.5 part of carboxyethyl cellulose, 0.25 part of hydroxymethyl cellulose, 0.25 part of xanthans, sodium benzoate 0.5
0.01 part of part and pigment.
The preparation method of the luminous pigment of embodiment 1, includes the following steps：
(1) white granulated sugar and the sodium benzoate are added in the pure water, the carboxyethylcellulose is then added
Element, hydroxymethyl cellulose and xanthans simultaneously stir 0.3h~0.8h, then stand, and wait for the carboxyethyl cellulose, hydroxylmethyl cellulose
Disperseed with dispersion machine after element and xanthans swelling.
(2) the aluminic acid neodymium calcium is mixed and stirred for the pigment.
(3) institute is added in the product that the step (1) obtains in dispersion machine under 1000r/min~3000r/min rotating speeds
The product that step (2) obtains is stated, 1.8h~2.2h is then stirred, then reduction rotating speed to 100r/min~500r/min disappears
Bubble, obtains luminous pigment.
Embodiment 2
Embodiment 2 proposes a kind of luminous pigment, includes the raw material of following parts by weight：75 parts of pure water, white granulated sugar 15
Part, 1 part of lanthanum-magnesium aluminate, 2.5 parts of carboxyethyl cellulose, 1.25 parts of hydroxymethyl cellulose, 1.25 parts of xanthans, sodium benzoate 0.01
1 part of part and pigment.
The preparation method of the luminous pigment of embodiment 2, includes the following steps：
(1) white granulated sugar and the sodium benzoate are added in the pure water, the carboxyethylcellulose is then added
Element, hydroxymethyl cellulose and xanthans simultaneously stir 0.3h~0.8h, then stand, and wait for the carboxyethyl cellulose, hydroxylmethyl cellulose
Disperseed with dispersion machine after element and xanthans swelling.
(2) lanthanum-magnesium aluminate and the pigment are mixed and stirred for.
(3) institute is added in the product that the step (1) obtains in dispersion machine under 1000r/min~3000r/min rotating speeds
The product that step (2) obtains is stated, 1.8h~2.2h is then stirred, then reduction rotating speed to 100r/min~500r/min disappears
Bubble, obtains luminous pigment.
Embodiment 3
Embodiment 3 proposes a kind of luminous pigment, includes the raw material of following parts by weight：82 parts of pure water, white granulated sugar 8
Part, 8 parts of strontium aluminate, 1 part of carboxyethyl cellulose, 0.5 part of hydroxymethyl cellulose, 0.5 part of xanthans, 0.2 part of sodium benzoate and color
0.2 part of element.
The preparation method of the luminous pigment of embodiment 3, includes the following steps：
(1) white granulated sugar and the sodium benzoate are added in the pure water, the carboxyethylcellulose is then added
Element, hydroxymethyl cellulose and xanthans simultaneously stir 0.3h~0.8h, then stand, and wait for the carboxyethyl cellulose, hydroxylmethyl cellulose
Disperseed with dispersion machine after element and xanthans swelling.
(2) strontium aluminate and the pigment are mixed and stirred for.
(3) institute is added in the product that the step (1) obtains in dispersion machine under 1000r/min~3000r/min rotating speeds
The product that step (2) obtains is stated, 1.8h~2.2h is then stirred, then reduction rotating speed to 100r/min~500r/min disappears
Bubble, obtains luminous pigment.
Embodiment 4
Embodiment 4 proposes a kind of luminous pigment, includes the raw material of following parts by weight：81.5 parts of pure water, white granulated sugar
10 parts, 5 parts of aluminic acid radium, 1.5 parts of carboxyethyl cellulose, 0.75 part of hydroxymethyl cellulose, 0.75 part of xanthans, sodium benzoate 0.3
0.1 part of part and pigment.
The preparation method of the luminous pigment of embodiment 4, includes the following steps：
(1) white granulated sugar and the sodium benzoate are added in the pure water, the carboxyethylcellulose is then added
Element, hydroxymethyl cellulose and xanthans simultaneously stir 0.3h~0.8h, then stand, and wait for the carboxyethyl cellulose, hydroxylmethyl cellulose
Disperseed with dispersion machine after element and xanthans swelling.
(2) the aluminic acid radium is mixed and stirred for the pigment.
(3) institute is added in the product that the step (1) obtains in dispersion machine under 1000r/min~3000r/min rotating speeds
The product that step (2) obtains is stated, 1.8h~2.2h is then stirred, then reduction rotating speed to 100r/min~500r/min disappears
Bubble, obtains luminous pigment.
The luminous pigment of the embodiment of the present invention, production is easy, and energy conservation and environmental protection is safe to use；It is tasteless nontoxic, no chemistry
Substance volatile matter；More preferably, for material without Problem of Shading, film layer brightness is fine for illumination effect.
In the description of this specification, reference term " one embodiment ", " some embodiments ", " example ", " specifically show
The description of example " or " some examples " etc. means specific features, structure, material or spy described in conjunction with this embodiment or example
Point is included at least one embodiment or example of the invention.In the present specification, schematic expression of the above terms are not
It must be directed to identical embodiment or example.Moreover, particular features, structures, materials, or characteristics described can be in office
It can be combined in any suitable manner in one or more embodiments or example.In addition, without conflicting with each other, the skill of this field
Art personnel can tie the feature of different embodiments or examples described in this specification and different embodiments or examples
It closes and combines.
Although the embodiments of the present invention has been shown and described above, it is to be understood that above-described embodiment is example
Property, it is not considered as limiting the invention, those skilled in the art within the scope of the invention can be to above-mentioned
Embodiment is changed, changes, replacing and modification.
Claims (9)
1. a kind of luminous pigment, which is characterized in that include the raw material of following parts by weight：75 parts~85 parts of pure water, 5 parts of sugar~
15 parts, 1 part~10 parts of rare earth aluminate, 1 part~5 parts of cellulose, 0.01 part~0.5 part of sodium benzoate and pigment 0.01 part~1
Part.
2. luminous pigment according to claim 1, which is characterized in that include the raw material of following parts by weight：Pure water 85
0.01 part of part, 5 parts of sugar, 10 parts of rare earth aluminate, 1 part of cellulose, 0.5 part of sodium benzoate and pigment.
3. luminous pigment according to claim 1, which is characterized in that include the raw material of following parts by weight：Pure water 75
1 part of part, 15 parts of sugar, 1 part of rare earth aluminate, 5 parts of cellulose, 0.01 part of sodium benzoate and pigment.
4. luminous pigment according to claim 1, which is characterized in that include the raw material of following parts by weight：Pure water 82
0.2 part of part, 8 parts of sugar, 8 parts of rare earth aluminate, 2 parts of cellulose, 0.2 part of sodium benzoate and pigment.
5. luminous pigment according to claim 1, which is characterized in that include the raw material of following parts by weight：Pure water
81.5 parts, 10 parts of sugar, 5 parts of rare earth aluminate, 3 parts of cellulose, 0.1 part of 0.3 part of sodium benzoate and pigment.
6. according to claim 1-5 any one of them luminous pigments, which is characterized in that the cellulose includes carboxyethylcellulose
Element, hydroxymethyl cellulose and xanthans, and the weight ratio of the carboxyethyl cellulose, hydroxymethyl cellulose and xanthans is 2:1:
1。
7. according to claim 1-5 any one of them luminous pigments, which is characterized in that the sugar is white granulated sugar.
8. the preparation method of claim 1-7 any one of them luminous pigments, which is characterized in that include the following steps：
S101：The white granulated sugar and the sodium benzoate are added in the pure water, the cellulose is then added and stirs
0.3h~0.8h, then stand, disperseed with dispersion machine after cellulose swelling；
S102：The rare earth aluminate and the pigment are mixed and stirred for；
S103：The product that the step S101 is obtained is added what the step S102 was obtained under the conditions of dispersion machine high-speed stirred
Then product stirs 1.8h~2.2h, then reduce rotating speed and defoamed, obtain luminous pigment.
9. the preparation method of luminous pigment according to claim 8, which is characterized in that in the step S103, high speed
Rotating speed when stirring is 1000r/min~3000r/min；It is down to 100r/min~500r/min when reducing rotating speed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810054936.0A CN108314908A (en) | 2018-01-19 | 2018-01-19 | Luminous pigment and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810054936.0A CN108314908A (en) | 2018-01-19 | 2018-01-19 | Luminous pigment and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108314908A true CN108314908A (en) | 2018-07-24 |
Family
ID=62887109
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810054936.0A Pending CN108314908A (en) | 2018-01-19 | 2018-01-19 | Luminous pigment and preparation method thereof |
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| CN (1) | CN108314908A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109337423A (en) * | 2018-10-30 | 2019-02-15 | 宁波市家羽塑业科技有限公司 | A kind of novel washable finger painting pigment |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101298705A (en) * | 2008-05-26 | 2008-11-05 | 清华大学深圳研究生院 | Method for preparing luminous Lyocell fibre |
| CN101386719A (en) * | 2008-08-28 | 2009-03-18 | 冯守中 | Multifunctional coatings and preparation method thereof |
| CN103265904A (en) * | 2013-05-07 | 2013-08-28 | 浙江大学宁波理工学院 | Luminescence gel and preparation method thereof |
| CN104277645A (en) * | 2013-07-02 | 2015-01-14 | 海安华盛化工有限公司 | Noctilucent paint |
| CN105086590A (en) * | 2014-05-13 | 2015-11-25 | 内蒙古蒙牛乳业（集团）股份有限公司 | Noctilucent printing ink for food packaging and preparation method thereof |
-
2018
- 2018-01-19 CN CN201810054936.0A patent/CN108314908A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101298705A (en) * | 2008-05-26 | 2008-11-05 | 清华大学深圳研究生院 | Method for preparing luminous Lyocell fibre |
| CN101386719A (en) * | 2008-08-28 | 2009-03-18 | 冯守中 | Multifunctional coatings and preparation method thereof |
| CN103265904A (en) * | 2013-05-07 | 2013-08-28 | 浙江大学宁波理工学院 | Luminescence gel and preparation method thereof |
| CN104277645A (en) * | 2013-07-02 | 2015-01-14 | 海安华盛化工有限公司 | Noctilucent paint |
| CN105086590A (en) * | 2014-05-13 | 2015-11-25 | 内蒙古蒙牛乳业（集团）股份有限公司 | Noctilucent printing ink for food packaging and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109337423A (en) * | 2018-10-30 | 2019-02-15 | 宁波市家羽塑业科技有限公司 | A kind of novel washable finger painting pigment |
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