CN107287939A - A kind of preparation method for washing quilt cover with long stitches - Google Patents
A kind of preparation method for washing quilt cover with long stitches Download PDFInfo
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- CN107287939A CN107287939A CN201710617538.0A CN201710617538A CN107287939A CN 107287939 A CN107287939 A CN 107287939A CN 201710617538 A CN201710617538 A CN 201710617538A CN 107287939 A CN107287939 A CN 107287939A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L1/00—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods
- D06L1/12—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods using aqueous solvents
- D06L1/16—Multi-step processes
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
- D06L4/10—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
- D06L4/13—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen using inorganic agents
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
- D06M16/003—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic with enzymes or microorganisms
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
- D06P3/66—Natural or regenerated cellulose using reactive dyes
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/10—After-treatment with compounds containing metal
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
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Abstract
The preparation method of present invention washing quilt cover with long stitches, including：By dyeing fabric, fixation, quilt cover with long stitches fabric is obtained；By quilt cover with long stitches fabric quilting, quilt cover with long stitches is obtained；Quilt cover with long stitches is mixed with float stone, STONEWASH, rinses, obtain the quilt cover with long stitches after granite-wash；The temperature of the granite-wash is 60~70 DEG C；The amount of the float stone is 3%~6%；One or more of the purificant in sodium hypochlorite and dense drift ice；Quilt cover with long stitches enzyme after granite-wash is washed, the quilt cover with long stitches after enzyme is washed is obtained；The enzyme that the enzyme is washed is neutral cellulase；The bath raio that the enzyme is washed is 1：(10~20)；The pH value is 6~7；Quilt cover with long stitches enzyme-deactivating, soft finish after enzyme is washed, dry, go out cylinder, whole scald and obtain product.The present invention is by specific granite-wash, and the specific purificant of cooperation causes frictional force stronger, while removing the dyeing on fabric, selects specific neutral cellulase enzyme to wash and finally prepares low washing quilt cover with long stitches cylinder rate, intensity, color fastness height.
Description
Technical field
The present invention relates to home textile technical field, more particularly, to a kind of preparation method for washing quilt cover with long stitches.
Background technology
Quilt cover with long stitches is popular a thin quilt in home textile market, is divided into precoat and filler layer, then according to difference
Flower pattern very close quilting, the finished product of different-style is made, outward appearance is very high-grade and can machine-wash, it is deep to be liked by guest.
Species is single before quilt cover with long stitches, and selectable fabric species is limited, and the quilt cover with long stitches of prior art is mostly by common
Washing, the following problem of generally existing：(1) because finished product needs COLOR FASTNESS PROBLEM, it is by the finished product made dye to have many finished product companies
Then color, Final finishing is washed.So obtained finished product stonewashed effect reaches demand, but cylinder difference is difficult control.(2) finished product is washed
Factory is immature to the poor control aspect technique of large-sized home textile product cylinder to cause that stone mill water washing cylinder is poor, bar difference greatly.
The content of the invention
In view of this, the technical problem to be solved in the present invention is to provide a kind of preparation method for washing quilt cover with long stitches, this hair
The bright washing quilt cover with long stitches cylinder rate prepared is low, intensity, color fastness high.
The invention provides a kind of preparation method for washing quilt cover with long stitches, comprise the following steps：
A) by dyeing fabric, fixation, quilt cover with long stitches fabric is obtained；
B) by quilt cover with long stitches fabric quilting, quilt cover with long stitches is obtained；
C) quilt cover with long stitches is mixed with float stone, STONEWASH, rinses, obtain the quilt cover with long stitches after granite-wash；The temperature of the granite-wash is
60~70 DEG C；The amount of the float stone is 3%~6%；One or more of the purificant in sodium hypochlorite and dense drift ice；
D) quilt cover with long stitches enzyme after granite-wash is washed, the quilt cover with long stitches after enzyme is washed is obtained；The enzyme that the enzyme is washed is neutral cellulase；Institute
It is 1 to state the bath raio that enzyme washes：(10~20)；The pH value is 6~7；
E quilt cover with long stitches enzyme-deactivating, soft finish after) enzyme is washed, dry, go out cylinder, whole scald and obtain product.
It is preferred that, the step A) be specially：Fabric is mixed when temperature is 40~45 DEG C with dyestuff, mixed with accelerant
Close, 50~55 DEG C of dyeing are warming up to 60~80 DEG C of dyeing, then process soda ash fixation, washing, 80~85 DEG C soap, 60~65
DEG C washing.
It is preferred that, mixed in the dyeing with dyestuff and be specially：First with accounting for total dyestuff quality percent to 40%~80%
Dyestuff together mix；Mixed again with accounting for the road of dyestuff three of total dyestuff quality percent to 20%~60%.
It is preferred that, the float stone is Turkey's float stone；A diameter of 1~4cm of the float stone.
It is preferred that, the bath raio of the STONEWASH is 1：(20~30).
It is preferred that, the step C) rinsing be specially：Add sodium hypochlorite, dense drift ice, 60~70 DEG C of soap flakes processing 20~
40min；Washing, addition dodium thiosulfate mixing, dechlorination handle 5~10min.
It is preferred that, the consumption of the sodium hypochlorite is 1%~5%owf；The consumption of the dense drift ice is 0.5%~1.5%
owf；The consumption of the soap flakes is 2%~4%owf；The consumption of the dodium thiosulfate is 2%~5%owf.
It is preferred that, the neutral cellulase is neutral cellulase Denimax Ultra BT.
It is preferred that, the addition of the enzyme is 1.5%~3.5%；The ferment treatment temperature is 50~60 DEG C；At the enzyme
The reason time is 60~90min.
It is preferred that, the enzyme-deactivating is specially：Enzyme is heated to 80~100 DEG C or adjusts pH value to be more than 8.5, wash 20~
30min。
Compared with prior art, the invention provides a kind of preparation method for washing quilt cover with long stitches, comprise the following steps：A) will
Dyeing fabric, fixation, obtain quilt cover with long stitches fabric；B) by quilt cover with long stitches fabric quilting, quilt cover with long stitches is obtained；C) quilt cover with long stitches is mixed with float stone
Close, STONEWASH, rinse, obtain the quilt cover with long stitches after granite-wash；The temperature of the granite-wash is 60~70 DEG C；The amount of the float stone is 3%
~6%；One or more of the purificant in sodium hypochlorite, dense drift ice and dodium thiosulfate；D) by quilt cover with long stitches enzyme after granite-wash
Wash, obtain the quilt cover with long stitches after enzyme is washed；The enzyme that the enzyme is washed is neutral cellulase；The bath raio that the enzyme is washed is 1：(10~20)；
The pH value is 6~7；E quilt cover with long stitches enzyme-deactivating, soft finish after) enzyme is washed, dry, go out cylinder, whole scald and obtain product.This hair
It is bright to pass through specific granite-wash so that friction is abundant, while coordinating the purificant of specific strong oxidizing property to cause frictional force stronger, together
When can then select specific neutral cellulase enzyme to wash with the dyeing on oxidation removal fabric, coordinate specific bath raio and pH
Value causes product is washed more soft deep, and color is naturally uniform, greatly reduces cylinder rate.The present invention passes through above-mentioned technique
Control with parameter make it that the low washing quilt cover with long stitches cylinder rate finally prepared, intensity, color fastness are high.Test result indicates that,
The washing quilt cover with long stitches cylinder rate that the present invention is prepared is 4~5 grades, strength >=450N, and color fastness is 4 grades.
Embodiment
The invention provides a kind of preparation method for washing quilt cover with long stitches, comprise the following steps：
A) by dyeing fabric, fixation, quilt cover with long stitches fabric is obtained；
B) by quilt cover with long stitches fabric quilting, quilt cover with long stitches is obtained；
C) quilt cover with long stitches is mixed with float stone, STONEWASH, rinses, obtain the quilt cover with long stitches after granite-wash；The temperature of the granite-wash is
60~70 DEG C；The amount of the float stone is 3%~6%；The purificant is selected from the one or more of sodium hypochlorite and dense drift ice；
D) quilt cover with long stitches enzyme after granite-wash is washed, the quilt cover with long stitches after enzyme is washed is obtained；The enzyme that the enzyme is washed is neutral cellulase；Institute
It is 1 to state the bath raio that enzyme washes：(10~20)；The pH value is 6~7；
E quilt cover with long stitches enzyme-deactivating, soft finish after) enzyme is washed, dry, go out cylinder, whole scald and obtain product.
The preparation method for the washing quilt cover with long stitches that the present invention is provided obtains quilt cover with long stitches fabric first by dyeing fabric, fixation.
Step A of the present invention) be specially：Fabric is mixed when temperature is 40~45 DEG C with dyestuff, mixed with accelerant
Close, 50~55 DEG C of dyeing are warming up to 60~80 DEG C of dyeing, then process soda ash fixation, washing, 80~85 DEG C soap, 60~65
DEG C washing.
The fabric of the present invention is preferably pure-cotton woven fabric 30s*30s, density 68/68, door width 2.8m.The instrument of the present invention is excellent
Choosing is preferably selected using the VCS0 type dye jiggers of Mei Saila companies of Italy, 50~120m/min of speed, the dyestuff used in the present invention
One or more from reactive brilliant B-RV, red B-3BF and golden yellow B-4RFN.
In the present invention, fabric is mixed when temperature is 40~45 DEG C with dyestuff first.Now, preferably also include and chela
Close dispersant and levelling agent mixing.Specific species of the invention for the chelated dispersants and levelling agent is without limiting, originally
Chelated dispersants and levelling agent known to art personnel.The chelated dispersants preferably can be ethylenediamine tetraacetic methene
Sodium phosphate (EDTMPS)；Concentration of the chelated dispersants in total dyestuff working solution is preferably 1~3g/L；The levelling agent preferably may be used
Think AEO；Concentration of the levelling agent in total dyestuff working solution is preferably 1~3g/L.
Wherein, mixed in the dyeing with dyestuff and be specially：First with accounting for total dyestuff quality percent to 40%~80%
Dyestuff is mixed together；The incorporation time is preferably 5~10min；Again with accounting for total dyestuff quality percent to 20%~60%
The road of dyestuff three is mixed；The incorporation time is preferably 3~5min.Dyestuff of the present invention accounts for 1~5%owf of fabric weight.
Contaminated less in this early stage of the present invention, many modes are contaminated on the later stage be conducive to dyeing and fixation.
After mixing, mixed with accelerant, 50~55 DEG C of dyeing.The accelerant is preferably glauber salt；The glauber salt exists
Concentration in total dyestuff working solution is preferably 20~30g/L；More preferably 22~28g/L.
The addition manner of glauber salt of the present invention is preferably specially first to add to account for total glauber salt mass percent 40%~60%
Glauber salt together, promote dye 3~5min；The road of glauber salt two for accounting for total glauber salt mass percent 40%~60% is added, is promoted
Contaminate 3~5min.
After addition is finished, shutdown is warming up to 50~55 DEG C of one of dyeing.The time of the dyeing is preferably 40~60min.
60~80 DEG C of one of dyeing are then warming up to, the time of the dyeing is preferably 40~60min.
Specific staining method of the invention not only make it that dyeing is more uniform, and specific addition sequence and addition
So that the dyestuff and accelerant that add will not be precipitated, specking is not resulted in.
After dyeing is finished, soda ash fixation is used.Concentration of the soda ash in total dyestuff working solution is preferably 5~15g/L；
More preferably 7~13g/L；Most preferably 8~12g/L.
Soda ash fixation mode of the present invention is preferably specially：First add the soda ash one of quality percent to 20%~80%
Road is mixed；The incorporation time is preferably 3~5min；Add the road of soda ash three mixing of quality percent to 20%~80%；
The incorporation time is preferably 3~5min.
The present invention is washing after soda ash fixation.It is preferred that being specially the washing of 2 roads.The present invention for water-washing method herein and
Concrete operations are well known to those skilled in the art without limiting.
It is preferably to soap after washing.Soaping agent of the present invention is coconut oil (acid) diglycollic amide, SAS
SAS.The addition of the soaping agent is preferably 2~4g/L.
It is washing after soaping；Preferably twice are washed；The temperature of the washing is preferably 50~60 DEG C.The time of washing is excellent
Elect 10~20min as.
Then washed again for twice；The temperature of the washing is preferably 50~60 DEG C.The time of washing is preferably 5~
10min。
Go out cloth after washing, obtain quilt cover with long stitches fabric.
The present invention causes loose colour effect by the way of fixation of slightly soaping, i.e., impermeable dye, is easy to follow-up washing to take off.
The present invention make it that cylinder rate is low using above-mentioned specific dyeing and color fixing process, and color fastness is high.
In the present invention, by quilt cover with long stitches fabric quilting, quilt cover with long stitches is obtained.The quilting is preferably specially：By quilting quilt cover
Material carries out quilting with glue-free cotton.
The present invention is for specific quiltmg piocess without restriction, quiltmg piocess well known to those skilled in the art.
It is preferred that being specially：(180 DEG C of ╳ 3min) the good above-mentioned fabric that will shape is cut, and as shell fabric up and down, intermediate layer filler is
160g/m2Wash glue-free cotton entirely.
Quilt cover with long stitches is mixed with float stone, STONEWASH, rinses, obtain the quilt cover with long stitches after granite-wash.
The present invention first mixes quilt cover with long stitches with float stone, STONEWASH.
The float stone that the present invention is selected is Turkey's float stone；The float stone forming process be absmal deposit-lifting-meteorite impact-
Plasma infiltration etc., experience superhigh temperature contains more than 30 kinds of chromium, nickel, copper etc. trace element and rare earth element beneficial to human body.This
The diameter for inventing the float stone is preferably 1~4cm；More preferably 2~4cm.
The present invention preferably washs the stone mill washing machine of Machinery Manufacturing Co., Ltd., XGP-300w types from Shanghai power washing
Number, maximum fabric capacity is 300kg.
The temperature of the granite-wash is 60~70 DEG C；Preferably 62~68 DEG C；The amount of the float stone is 3%~6%o.w.f；
Preferably 4%~5%o.w.f.The bath raio of the STONEWASH is preferably 1：(20~30)；More preferably 1：(22~28).
The above-mentioned bath raio of present invention selection enables the float stone in diameter range of the present invention to be fully contacted without heap with product
Product does not flow in a corner, and granite-wash effect is good.
In the present invention, rinsed after STONEWASH, obtain the quilt cover with long stitches after granite-wash.The purificant is selected from sodium hypochlorite and dense
One or more in drift ice.
In the present invention, the rinsing is preferred is specially：Add sodium hypochlorite, dense drift ice, 60~70 DEG C of processing 20 of soap flakes
~40min；Washing, addition dodium thiosulfate mixing, dechlorination handle 5~10min；More preferably it is specially：Add sodium hypochlorite, dense drift
Water, 62~68 DEG C of 25~35min of processing of soap flakes；Washing, addition dodium thiosulfate mixing, dechlorination handle 6~8min.
Wherein, the consumption of the sodium hypochlorite is preferably 1%~5%owf；The consumption of the dense drift ice is preferably 0.5%
~1.5%owf；The consumption of the soap flakes is preferably 2%~4%owf；The consumption of the dodium thiosulfate is preferably 2%~5%owf.
The present invention uses specific rinse method, and wash effect is good.Wherein, first with sodium hypochlorite, the oxygen of dense drift ice
Change is acted on, and removes the dyestuff on fabric.This process is adding soap flakes, it is therefore an objective to so that the dyestuff washed off will not stain fabric again
Effect.Then wash, mixed with dodium thiosulfate, sodium hypochlorite and dense drift ice are cleaned for thorough.
The excellent float stone of present invention selection so that bulky quilt cover with long stitches can fully contact float stone, friction is abundant, matches somebody with somebody simultaneously
Closing the chemical assistant of other strong oxidizing properties makes product initially big by friction dynamics, and effect is good.
After dechlorination processing, rinse, go out cylinder.The present invention is rinsed for described, goes out the design parameter of cylinder without limiting, ability
Rinsed known to field technique personnel, go out cylinder operation.
In the present invention, quilt cover with long stitches enzyme after granite-wash is washed, obtains the quilt cover with long stitches after enzyme is washed.It is preferred that being specially by above-mentioned granite-wash
Good quilt cover with long stitches carries out enzyme from neutral cellulase in rotary drum stone mill rinsing maching, preferably and washed.
The neutral cellulase is preferably neutral cellulase Denimax Ultra BT；More preferably Novozymes Company
Neutral cellulase Denimax Ultra BT.The consumption of the enzyme is preferably 1.5~3.5%o.w.f；More preferably 1.7
~3.2%o.w.f.The bath raio that the enzyme is washed is 1：(10~20)；Preferably 1：(12~18)；The pH value is 6~7.It is described
Ferment treatment temperature is preferably 50~60 DEG C；More preferably 52~58 DEG C；The enzyme processing time is preferably 60~90min；It is more excellent
Elect 65~85min as.
The specific neutral cellulase of present invention selection, and coordinate specific technological parameter so that final products enzyme washes matter
Easy to control, favorable reproducibility is measured, cylinder rate is low.The specific neutral enzymatic of present invention selection is washed again, and make that product washed is softer
And deeply, the color come out is also more natural and uniform.
After enzyme is washed, quilt cover with long stitches enzyme-deactivating, soft finish after enzyme is washed, dry, go out cylinder, whole scald and obtain product.
In the present invention, the enzyme-deactivating is preferably specially：Enzyme is heated to 80~100 DEG C or adjusts pH value to be more than 8.5, washes
20~30min, you can inactivation.
The present invention for the soft finish, dry, go out cylinder, whole boiling hot specific steps and parameter without restriction, ability
Known to field technique personnel.
The invention provides a kind of preparation method for washing quilt cover with long stitches, comprise the following steps：A) by dyeing fabric, fixation,
Obtain quilt cover with long stitches fabric；B) by quilt cover with long stitches fabric quilting, quilt cover with long stitches is obtained；C) quilt cover with long stitches is mixed with float stone, STONEWASH, drift
Wash, obtain the quilt cover with long stitches after granite-wash；The temperature of the granite-wash is 60~70 DEG C；The amount of the float stone is 3%~6%；The drift
One or more of the lotion in sodium hypochlorite, dense drift ice and dodium thiosulfate；D) quilt cover with long stitches enzyme after granite-wash is washed, obtained after enzyme washes
Quilt cover with long stitches；The enzyme that the enzyme is washed is neutral cellulase；The bath raio that the enzyme is washed is 1：(10~20)；The pH value be 6~
7；E quilt cover with long stitches enzyme-deactivating, soft finish after) enzyme is washed, dry, go out cylinder, whole scald and obtain product.The present invention passes through specific stone
Wash so that friction is abundant, while coordinating the purificant of specific strong oxidizing property to cause frictional force stronger, while can be with oxidation removal
Dyeing on fabric, then selects specific neutral cellulase enzyme to wash, and coordinates specific bath raio and pH value make it that product is washed
It is more soft deep, color is naturally uniform, greatly reduces cylinder rate.The present invention is made by the control of above-mentioned technique and parameter
Obtain the low washing quilt cover with long stitches cylinder rate finally prepared, intensity, color fastness high.
The performance of quilt cover with long stitches is measured present invention preferably employs in the following manner：
Washing shrinkage is washed, according to the standards of AATCC 135, is controlled ± 5%；Color fastness is controlled at 3 grades according to AATCC 61
More than；Colorfastness to rubbing is controlled more than 3.5 grades according to AATCC 8, strongly according to ASTMD 5034, it is desirable to more than 300N；First
Aldehyde is according to the standards of AATCC 112；PH value is according to EN 1413A；Content of beary metal is according to ISO 105E04.
In order to further illustrate the present invention, the preparation method of the washing quilt cover with long stitches provided with reference to embodiments the present invention
It is described in detail.
Embodiment 1
Fabric selects pure-cotton woven fabric 30s*30s, density 68/68, door width 2.8m to use Italian Mei Saila companies
VCS0 type dye jiggers, speed 50m/min, reactive brilliant B-RV, red B-3BF, golden yellow B-4RFN, glauber salt 20g/l, soda ash 5g/
L, levelling agent 50C 1g/l, chelated dispersants 1g/l.Chelated dispersants and levelling agent are firstly added, are warming up in 40 DEG C (1 roads), plus
Enter 2/5 (reactive brilliant B-RV 1.2%o.w.f, red B-3BF 2.3%o.w.f, golden yellow B-4RFN 0.5%o.w.f) dyestuff (1
Road) processing 5min；1/5 dyestuff (3 road) processing 3min is added, 1/2 glauber salt (1 road) processing 3min is added, adds 1/2 glauber salt
(2 road) handles 3min, and shutdown is warming up to 50 DEG C of dyeing (1 road), handles 40min.Shutdown is warming up to 60 DEG C of dyeing 40min (1 road).
1/5 soda ash fixation (1 road) processing 3min is then added, 1/5 soda ash fixation (3 road) is added and handles 3min, then washing (2 road),
Soap in (roads of 80 DEG C ╳ 2), wash (roads of 60 DEG C ╳ 2), washing (2 road), go out cloth.
(180 DEG C of ╳ 3min) the good above-mentioned fabric that will shape is cut, and as shell fabric up and down, intermediate layer filler is
160g/m2Wash glue-free cotton entirely.
From a diameter of 1~4cm Turkey float stone, the stone mill for washing Machinery Manufacturing Co., Ltd. from Shanghai power washing is washed
Machine, XGP-300w models, maximum fabric capacity is 300kg, and the above-mentioned quilt cover with long stitches made is carried out into STONEWASH, bath raio 1:20,
60 DEG C are warming up to, 3%o.w.f float stones are added, 1%o.w.f sodium hypochlorite and the dense drift ices of 0.5%o.w.f is added, 2% is added
O.w.f soap flakes, add the processed 20min of quilting, and draining washes secondary, adds 2%o.w.f dodium thiosulfate, and dechlorination handles 5min,
Rinse, go out cylinder.
By the good quilt cover with long stitches of above-mentioned granite-wash in rotary drum stone mill rinsing maching, from the neutral cellulase of Novozymes Company
Denimax Ultra BT carry out enzyme and washed, 1.5%o.w.f, bath raio 1:10, pH=6~7, temperature 50 C handles 60min.Rapidly
Enzyme washing lotion is heated to more than 80 DEG C, or adjusts more than pH=8.5 to wash 20min, you can enzyme is inactivated.Then conventional is soft whole
Manage, dry, go out cylinder, it is whole scald, obtain quilt cover with long stitches.
Performance measurement is carried out to the quilt cover with long stitches prepared using mode of the present invention, as a result shown：Present invention system
Standby obtained washing quilt cover with long stitches cylinder rate is 4~5 grades, and strength >=450N, color fastness is 4 grades, quilt cover with long stitches dry and wet crock fastness 3.5
Level, quilt cover with long stitches pH value 7；Quilt cover with long stitches shrinkage -1%, the equal nothing of quilt cover with long stitches heavy metal, formaldehyde, aromatic amine.
Embodiment 2
Fabric selects pure-cotton woven fabric 30s*30s, density 68/68, door width 2.8m to use Italian Mei Saila companies
VCS0 type dye jiggers, speed 70m/min, reactive brilliant B-RV, red B-3BF, golden yellow B-4RFN, glauber salt 25g/l, soda ash 10g/
L, levelling agent 50C 2g/l, chelated dispersants 2g/l.Chelated dispersants and levelling agent are firstly added, are warming up in 40 DEG C (1 roads), plus
Enter 3/5 (reactive brilliant B-RV 0.8%o.w.f, red B-3BF 1.9%o.w.f, golden yellow B-4RFN 0.6%o.w.f) dyestuff (1
Road) processing 8min；Add 2/5 dyestuff (3 road) processing 4min；Add 1/2 glauber salt (1 road) processing 4min；Add 1/2 glauber salt
(2 road) handles 4min；Shutdown is warming up to 50 DEG C of dyeing (1 road) processing 50min.Shutdown is warming up to 70 DEG C of dyeing 50min (1 road).
Add 3/5 soda ash fixation (1 road) processing 4min；Add 3/5 soda ash fixation (3 road) processing 4min；Wash in (2 road)；Soap (80 DEG C
The roads of ╳ 2)；Wash (60 DEG C, 2 roads)；Wash in (2 road), go out cloth.
(180 DEG C of ╳ 3min) the good above-mentioned fabric that will shape is cut, and as shell fabric up and down, intermediate layer filler is
160g/m2Wash glue-free cotton entirely.
From a diameter of 2~4cm Turkey float stone, the stone mill for washing Machinery Manufacturing Co., Ltd. from Shanghai power washing is washed
Machine, XGP-300w models, maximum fabric capacity is 300kg, and the above-mentioned quilt cover with long stitches made is carried out into STONEWASH, bath raio 1:25,
65 DEG C are warming up to, 5%o.w.f float stones are added, 3%o.w.f sodium hypochlorite and the dense drift ices of 1%o.w.f is added, 3%o.w.f is added
Soap flakes, add the processed 30min of quilting, and draining washes secondary, add 3%o.w.f dodium thiosulfate, and dechlorination processing 8min is rinsed,
Go out cylinder.
By the good quilt cover with long stitches of above-mentioned granite-wash in rotary drum stone mill rinsing maching, from the neutral cellulase of Novozymes Company
Denimax Ultra BT carry out enzyme and washed, 2.5%o.w.f, bath raio 1:15, pH=6~7,55 DEG C of temperature handles 75min.Rapidly
Enzyme washing lotion is heated to more than 80 DEG C, or adjusts more than pH=8.5 to wash 20min, you can enzyme is inactivated.Then conventional is soft whole
Manage, dry, go out cylinder, it is whole scald, obtain quilt cover with long stitches.
Performance measurement is carried out to the quilt cover with long stitches prepared using mode of the present invention, as a result shown：Present invention system
Standby obtained washing quilt cover with long stitches cylinder rate is 4~5 grades, and strength >=450N, color fastness is 4 grades, quilt cover with long stitches dry and wet crock fastness 3.5
Level, quilt cover with long stitches pH value 7；Quilt cover with long stitches shrinkage -1%, the equal nothing of quilt cover with long stitches heavy metal, formaldehyde, aromatic amine.
Embodiment 3
Fabric selects pure-cotton woven fabric 30s*30s, density 68/68, door width 2.8m to use Italian Mei Saila companies
VCS0 type dye jiggers, speed 120m/min, reactive brilliant B-RV, red B-3BF, golden yellow B-4RFN, glauber salt 30g/l, soda ash
15g/l, levelling agent 50C 3g/l, chelated dispersants 3g/l.Chelated dispersants and levelling agent are firstly added, 40 DEG C (1 is warming up to
Road), add 4/5 (reactive brilliant B-RV 2.2%o.w.f, red B-3BF 1.0%o.w.f, golden yellow B-4RFN 1.4%o.w.f)
Dyestuff (1 road) handles 10min；3/5 dyestuff (3 road) processing 5min is added, 1/2 glauber salt (1 road) processing 5min is added, adds 1/
2 glauber salt (2 road) handle 5min, and shutdown is warming up to 50 DEG C of dyeing 60min (1 road), and shutdown is warming up to 80 DEG C of dyeing 60min (1
Road), 4/5 soda ash fixation (1 road) 5min is then added, 4/5 soda ash fixation (3 road) 5min is added, then (2 road) is washed, soap
Wash (80 DEG C, 2 roads), wash (60 DEG C, 2 roads), wash in (2 road), go out cloth.
(180 DEG C of ╳ 3min) the good above-mentioned fabric that will shape is cut, and as shell fabric up and down, intermediate layer filler is
160g/m2Wash glue-free cotton entirely.
From a diameter of 2~4cm Turkey float stone, the stone mill for washing Machinery Manufacturing Co., Ltd. from Shanghai power washing is washed
Machine, XGP-300w models, maximum fabric capacity is 300kg, and the above-mentioned quilt cover with long stitches made is carried out into STONEWASH, bath raio 1:30,
70 DEG C are warming up to, 6%o.w.f float stones are added, 5%o.w.f sodium hypochlorite and the dense drift ices of 1.5%o.w.f is added, 4% is added
O.w.f soap flakes, add the processed 40min of quilting, and draining washes secondary, adds 5%o.w.f dodium thiosulfate, and dechlorination handles 10min,
Rinse, go out cylinder.
By the good quilt cover with long stitches of above-mentioned granite-wash in rotary drum stone mill rinsing maching, from the neutral cellulase of Novozymes Company
Denimax Ultra BT carry out enzyme and washed, 3.5%o.w.f, bath raio 1:20, pH=6~7, temperature 60 C handles 90min.Rapidly
Enzyme washing lotion is heated to more than 80 DEG C, or adjusts more than pH=8.5 to wash 20min, you can enzyme is inactivated.Then conventional is soft whole
Manage, dry, go out cylinder, it is whole scald, obtain quilt cover with long stitches.
Performance measurement is carried out to the quilt cover with long stitches prepared using mode of the present invention, as a result shown：Present invention system
Standby obtained washing quilt cover with long stitches cylinder rate is 4~5 grades, and strength >=450N, color fastness is 4 grades, quilt cover with long stitches dry and wet crock fastness 3.5
Level, quilt cover with long stitches pH value 7；Quilt cover with long stitches shrinkage -1%, the equal nothing of quilt cover with long stitches heavy metal, formaldehyde, aromatic amine.
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (10)
1. a kind of preparation method for washing quilt cover with long stitches, it is characterised in that comprise the following steps：
A) by dyeing fabric, fixation, quilt cover with long stitches fabric is obtained；
B) by quilt cover with long stitches fabric quilting, quilt cover with long stitches is obtained；
C) quilt cover with long stitches is mixed with float stone, STONEWASH, rinses, obtain the quilt cover with long stitches after granite-wash；The temperature of the granite-wash be 60~
70℃；The amount of the float stone is 3%~6%；One or more of the purificant in sodium hypochlorite and dense drift ice；
D) quilt cover with long stitches enzyme after granite-wash is washed, the quilt cover with long stitches after enzyme is washed is obtained；The enzyme that the enzyme is washed is neutral cellulase；The enzyme
The bath raio washed is 1：(10~20)；The pH value is 6~7；
E quilt cover with long stitches enzyme-deactivating, soft finish after) enzyme is washed, dry, go out cylinder, whole scald and obtain product.
2. preparation method according to claim 1, it is characterised in that the step A) be specially：It is in temperature by fabric
Mix, mixed with accelerant with dyestuff at 40~45 DEG C, 50~55 DEG C of dyeing are warming up to 60~80 DEG C of dyeing, then by pure
Alkali fixation, washing, 80~85 DEG C soap, 60~65 DEG C washing.
3. preparation method according to claim 2, it is characterised in that mixed in the dyeing with dyestuff and be specially：First with
The dyestuff for accounting for total dyestuff quality percent to 40%~80% is mixed together；Again with account for total dyestuff quality percent to 20%~
60% road of dyestuff three mixing.
4. preparation method according to claim 3, it is characterised in that the float stone is Turkey's float stone；The float stone
A diameter of 1~4cm.
5. preparation method according to claim 1, it is characterised in that the bath raio of the STONEWASH is 1：(20~30).
6. preparation method according to claim 1, it is characterised in that the step C) rinsing is specially：Add hypochlorous acid
Sodium, dense drift ice, 60~70 DEG C of 20~40min of processing of soap flakes；Washing, addition dodium thiosulfate mixing, dechlorination handle 5~10min.
7. preparation method according to claim 6, it is characterised in that the consumption of the sodium hypochlorite is 1%~5%owf；
The consumption of the dense drift ice is 0.5%~1.5%owf；The consumption of the soap flakes is 2%~4%owf；The use of the dodium thiosulfate
Measure as 2%~5%owf.
8. preparation method according to claim 1, it is characterised in that the neutral cellulase is neutral cellulase
Denimax Ultra BT。
9. preparation method according to claim 1, it is characterised in that the addition of the enzyme is 1.5%~3.5%；Institute
Ferment treatment temperature is stated for 50~60 DEG C；The enzyme processing time is 60~90min.
10. preparation method according to claim 1, it is characterised in that the enzyme-deactivating is specially：Enzyme is heated to 80~
100 DEG C or adjust pH value be more than 8.5, wash 20~30min.
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| CN201710617538.0A CN107287939B (en) | 2017-07-26 | 2017-07-26 | Preparation method of water-washing quilting quilt |
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| CN201710617538.0A CN107287939B (en) | 2017-07-26 | 2017-07-26 | Preparation method of water-washing quilting quilt |
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| CN107287939B CN107287939B (en) | 2020-09-18 |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102587134A (en) * | 2011-01-12 | 2012-07-18 | 香港纺织及成衣研发中心 | Processing method of ready-made garment with washed effect and ready-made garment processed by same |
| CN102704283A (en) * | 2012-03-28 | 2012-10-03 | 太仓棨淂服装有限公司 | Resist-dye method of clothes |
| CN104631126A (en) * | 2013-11-08 | 2015-05-20 | 青岛鑫益发工贸有限公司 | Cellulase mill finishing technology |
| CN105586687A (en) * | 2016-01-21 | 2016-05-18 | 福建七匹狼实业股份有限公司 | Cotton-covered spandex T400 twin-core elastic series shell fabric |
-
2017
- 2017-07-26 CN CN201710617538.0A patent/CN107287939B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102587134A (en) * | 2011-01-12 | 2012-07-18 | 香港纺织及成衣研发中心 | Processing method of ready-made garment with washed effect and ready-made garment processed by same |
| CN102704283A (en) * | 2012-03-28 | 2012-10-03 | 太仓棨淂服装有限公司 | Resist-dye method of clothes |
| CN104631126A (en) * | 2013-11-08 | 2015-05-20 | 青岛鑫益发工贸有限公司 | Cellulase mill finishing technology |
| CN105586687A (en) * | 2016-01-21 | 2016-05-18 | 福建七匹狼实业股份有限公司 | Cotton-covered spandex T400 twin-core elastic series shell fabric |
Non-Patent Citations (1)
| Title |
|---|
| 王悦 等编著: "《服装设计基础》", 31 July 2011, 东华大学出版社 * |
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