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CN107262224A - A kind of zinc oxygen leaching method for preparing raw material and two sections of vertical stirring mill series connection open-circuit grinding systems - Google Patents

A kind of zinc oxygen leaching method for preparing raw material and two sections of vertical stirring mill series connection open-circuit grinding systems Download PDF

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Publication number
CN107262224A
CN107262224A CN201710640414.4A CN201710640414A CN107262224A CN 107262224 A CN107262224 A CN 107262224A CN 201710640414 A CN201710640414 A CN 201710640414A CN 107262224 A CN107262224 A CN 107262224A
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CN
China
Prior art keywords
vertical stirring
sections
agitator
pulp
section
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710640414.4A
Other languages
Chinese (zh)
Inventor
张国旺
陈万群
赵湘
刘军
黄礼龙
张秉青
张武
刘瑜
肖骁
张玉林
王铧泰
孔俊杰
石立
王成
龙渊
贾雄武
杨建国
李文明
桑艳伟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
West Mining Co Ltd Zinc Industry Branch
Changsha Research Institute of Mining and Metallurgy Co Ltd
Original Assignee
West Mining Co Ltd Zinc Industry Branch
Changsha Research Institute of Mining and Metallurgy Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by West Mining Co Ltd Zinc Industry Branch, Changsha Research Institute of Mining and Metallurgy Co Ltd filed Critical West Mining Co Ltd Zinc Industry Branch
Priority to CN201710640414.4A priority Critical patent/CN107262224A/en
Publication of CN107262224A publication Critical patent/CN107262224A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/16Mills in which a fixed container houses stirring means tumbling the charge
    • B02C17/163Stirring means
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/18Details
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/18Details
    • B02C17/183Feeding or discharging devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/18Details
    • B02C17/20Disintegrating members
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C21/00Disintegrating plant with or without drying of the material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C25/00Control arrangements specially adapted for crushing or disintegrating

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  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

The invention discloses a kind of zinc oxygen leaching method for preparing raw material and two sections of vertical stirring mill series connection open-circuit grinding systems, method is first to obtain zinc concentrate material progress pulp to be ground with certain density ore pulp, the ore pulp obtained after pulp is roughly ground into one section of vertical stirring mill, the material that mog is higher, pulp density holding is constant is obtained after corase grind, material after corase grind enters back into two sections of vertical stirring mills and carries out fine grinding, the material that mog is higher, pulp density holding is constant, that is, the zinc oxygen leaching raw material stablized are obtained after fine grinding.System includes slurrying device, one section of vertical stirring mill and two sections of vertical stirring mills, and the delivery outlet of slurrying device is connected with the charging aperture of one section of vertical stirring mill, and the discharging opening of one section of vertical stirring mill is connected with the charging aperture of two sections of vertical stirring mills.The present invention has the advantages that small investment, with low cost, flow are short, operating cost is low, stable and reliable in work and fine grinding effect is good.

Description

A kind of zinc oxygen leaching method for preparing raw material and two sections of vertical stirring mill series connection open circuits Grinding system
Technical field
The present invention relates to nonferrous metallurgy and grinding attachment field, and in particular to a kind of zinc oxygen leaching raw material preparation side Method and two sections of vertical stirring mill series connection open-circuit grinding systems.
Background technology
Traditional zinc oxygen leaching method for preparing raw material is to use ball milling grinding process, as shown in figure 3, ball milling grinding process The grinding system of middle use is made up of traditional ball mill, grader and concentrator, is closed circuit grinding system, is passed through ball mill Zinc concentrate granularity is reached D95=45 μm with grader ore grinding, it is necessary to concentrator by the pulp solids content of cyclone overflow by 30%~40% is concentrated into 65%~70%, and the shortcoming of the closed circuit grinding system is:Product granularity is unstable;Grinding efficiency is low, energy consumption Greatly, long flow path;Floor space is big;Cost of investment is high;Difficult management;Thickener underflow is unstable and system operation cost is high.
Also have at present and the preparation of zinc oxygen leaching raw material is carried out using sand mill, but sand mill is expensive;Its rapid wear Part(Such as abrasive disk and cylinder)Service life it is short;Abrasive media consumption is big, price;The installed power of motor is big;Fortune Row cost is high;Cylinder volume is smaller and grinding efficiency is poor, and product granularity only reaches D85=45 μm, and the follow-up leaching operation of influence refers to Mark.
The content of the invention
The technical problem to be solved in the present invention be overcome the shortcomings of prior art exist there is provided a kind of small investment, cost are low Honest and clean, flow is short, operating cost is low, stable and reliable in work and fine grinding effect is good zinc oxygen leaching method for preparing raw material and two sections it is vertical Formula agitator mill series connection open-circuit grinding system.
In order to solve the above technical problems, the present invention uses following technical scheme:
A kind of zinc oxygen leaching method for preparing raw material, comprises the following steps:
1), will treat that grind materials carry out pulp and obtain granularity in ore pulp, ore pulp to account for 40% ~ 80% for -74 μm of solid particle, ore pulp is dense Spend for 65% ~ 75%;
2), ore pulp fed to one section of vertical stirring mill carry out primary grinding, the mog of primary grinding is D60~D90=45 µm;
3), the ore discharge of primary grinding fed to two sections of vertical stirring mills carry out secondary grinding, the mog of secondary grinding is D96 ~ D98=45 μm, the ore discharge of secondary grinding is zinc oxygen leaching raw material.
Above-mentioned zinc oxygen leaching method for preparing raw material, it is preferred that one section of vertical stirring mill is using a diameter of 15mm ~ 30mm medium, the frequency of one section of vertical stirring mill is 30HZ ~ 50HZ;Two sections of vertical stirring mills are using straight Footpath is 5mm ~ 15mm medium, and the frequency of two sections of vertical stirring mills is 40HZ ~ 50HZ.
Above-mentioned zinc oxygen leaching method for preparing raw material, it is preferred that one section of vertical stirring mill and two sections vertical are stirred The medium for mixing grinding machine use is any one in chromium steel ball, zirconium ball, Ceramic Balls, glass marble and natural sand.
Above-mentioned zinc oxygen leaching method for preparing raw material, it is preferred that one section of vertical stirring mill and two sections vertical are stirred It is any one in spiral, bar type, disc type and combined type to mix the agitator type of grinding machine.
Above-mentioned zinc oxygen leaching method for preparing raw material, it is preferred that one section of vertical stirring mill and two sections vertical are stirred The agitator speed for mixing grinding machine is unequal.
A kind of two sections of vertical stirring mills series connection open-circuit grinding system for above-mentioned zinc oxygen leaching method for preparing raw material, Including slurrying device, one section of vertical stirring mill and two sections of vertical stirring mills, the delivery outlet of the slurrying device passes through first Pipeline is connected with the charging aperture of one section of vertical stirring mill, the discharging opening of one section of vertical stirring mill by the second pipeline with The charging aperture of two sections of vertical stirring mills is connected, and first pipeline is provided with the first pulp conveying pump, second pipeline Provided with the second pulp conveying pump.
Above-mentioned two sections of vertical stirring mills series connection open-circuit grinding system, it is preferred that the slurrying device includes connecting successively The first agitator and the second agitator connect, the outlet of second agitator passes through first pipeline and one section of vertical mixing The charging aperture of grinding machine is connected.
Above-mentioned two sections of vertical stirring mills series connection open-circuit grinding system, it is preferred that first agitator is cylindricality Vertical mixing bucket, second agitator is the Horizontal stirring bucket of cylindricality, and the transverse width of second agitator is more than first The transverse width of agitator;The longitudinal direction height of second agitator is less than the longitudinal direction height of the first agitator.
Above-mentioned two sections of vertical stirring mills series connection open-circuit grinding system, it is preferred that installing is used in first agitator Spiral agitator;Disc mixer is equiped with second agitator.
Above-mentioned two sections of vertical stirring mills series connection open-circuit grinding system, it is preferred that second agitator is stood with one section The medial launder for being used for storing and adjust mineral pulp level is provided between formula agitator mill;The first pulp conveying pump and the second ore pulp Delivery pump is any one in peristaltic pump, centrifugal pump, ceramic pump and Pulp pump.
Compared with prior art, the advantage of the invention is that:The zinc oxygen leaching method for preparing raw material and its two of the present invention Section vertical stirring mill series connection open-circuit grinding system, first will zinc concentrate material be ground when carrying out the preparation of zinc oxygen leaching raw material Obtain, with certain density ore pulp, ore pulp then being passed through into first by the first pulp conveying pump after slurrying device progress pulp Pipeline from slurrying device be delivered to one section of vertical stirring mill in roughly ground, obtain that mog is higher, ore pulp is dense after corase grind Degree keeps constant material, then by the second pulp conveying pump by the ore pulp after corase grind by the second pipeline from one section of vertical mixing mill Machine, which is delivered in two sections of vertical stirring mills, obtained after fine grinding, fine grinding that mog is higher, pulp density keeps constant Material, that is, the zinc oxygen leaching raw material stablized.Two sections of the zinc oxygen leaching method for preparing raw material and its use vertical to stir Mill coupled in series open-circuit grinding system is mixed compared with existing closed circuit grinding system, it is not necessary to classification and concentrator, with investment Less, with low cost, flow is short, operating cost is low, the stable and reliable in work and good advantage of fine grinding effect.
Brief description of the drawings
Fig. 1 is the flow chart of zinc oxygen leaching method for preparing raw material of the present invention.
Fig. 2 is the structural representation of two sections of vertical stirring mills series connection open-circuit grinding systems of the present invention.
Fig. 3 is the structural representation of traditional ball milling grinding system.
Marginal data:
1st, slurrying device;11st, the first agitator;12nd, the second agitator;2nd, one section of vertical stirring mill;3rd, two sections of vertical mixings Grinding machine;4th, medial launder;5th, the first pulp conveying pump;6th, the second pulp conveying pump.
Embodiment
The present invention is described in further detail below in conjunction with the drawings and specific embodiments.
As shown in figure 1, the zinc oxygen leaching method for preparing raw material of the present embodiment, comprises the following steps:
1), will treat that grind materials carry out pulp and obtain granularity in ore pulp, ore pulp to account for 40% ~ 80% for -74 μm of solid particle, ore pulp is dense Spend for 65% ~ 75%;
2), ore pulp fed to one section of vertical stirring mill 2 carry out primary grinding, the mog of primary grinding for D60~D90= 45µm;
3), the ore discharge of primary grinding fed into two sections of vertical stirring mills 3 carry out secondary grinding, the mog of secondary grinding is D96 ~ D98=45 μm, the ore discharge of secondary grinding is zinc oxygen leaching raw material.
Granularity accounts for 40% ~ 80%, ore deposit for -74 μm of solid particle in the ore pulp obtained after mill zinc concentrate material carries out pulp It is 65% ~ 75% to starch concentration, and granularity accounts for 60%~90% for -45 μm of material after primary grinding, pulp density it is stable 65%~ 75%, then finally give after secondary grinding the material that granularity is -45 μm and account for 96%~98%, pulp density it is stable 65%~ 75%, that is, the zinc oxygen leaching raw material stablized.Obtained zinc oxygen leaching raw material can carry out one section of follow-up oxygen as needed Pressure is leached and flash distillation regulation.The zinc oxygen leaching method for preparing raw material has that short flow, small investment, operating cost is low, ore grinding is thin The high advantage of degree.
In the present embodiment, one section of vertical stirring mill 2 is using a diameter of 15mm ~ 30mm medium, one section of vertical mixing mill The frequency of machine 2 is 30HZ ~ 50HZ;Two sections of vertical stirring mills 3 are using a diameter of 5mm ~ 15mm medium, two sections of vertical mixing mills The frequency of machine 3 is 40HZ ~ 50HZ.One section of vertical stirring mill 2 and two sections of vertical stirring mills 3 use above-mentioned medium and frequency energy Optimal grinding efficiency is enough reached, cost is reduced.The medium that one section of vertical stirring mill 2 and two sections of vertical stirring mills 3 are used It is any one in chromium steel ball, zirconium ball, Ceramic Balls, glass marble and natural sand.One section of vertical stirring mill 2 and two sections it is vertical The agitator type of agitator mill 3 is any one in spiral, bar type, disc type and combined type.In the present embodiment, one section is stood The agitator speed of formula agitator mill 2 and two sections of vertical stirring mills 3 is unequal, realizes varigrained high efficiency ore grinding.
As shown in Fig. 2 in the present embodiment, a kind of two sections of vertical stirring mills for zinc oxygen leaching method for preparing raw material Series connection open-circuit grinding system, including slurrying device 1, one section of vertical stirring mill 2 and two sections of vertical stirring mills 3, slurrying device 1 Delivery outlet be connected by the first pipeline with the charging aperture of one section of vertical stirring mill 2, the discharging opening of one section of vertical stirring mill 2 It is connected by the second pipeline with the charging aperture of two sections of vertical stirring mills 3, the first pipeline is provided with the first pulp conveying pump 5, the Two pipelines are provided with the second pulp conveying pump 6.It is preferred that, on-off control valve door is equipped with the first pipeline and the second pipeline.
In the ore pulp obtained after mill zinc concentrate material carries out pulp in slurrying device 1, granularity contains for -74 μm of mineral Amount accounts for 40% ~ 80%, and pulp density is 65% ~ 75%.By the first pulp conveying pump 5 by ore pulp by the first pipeline from slurrying device 1 It is delivered in one section of vertical stirring mill 2 and is roughly ground, granularity accounts for 60%~90%, pulp density for -45 μm of material after corase grind It is stable 65%~75%, then by the second pulp conveying pump 6 by the ore pulp after corase grind by the second pipeline from one section of vertical mixing mill Machine 2, which is delivered to, to carry out obtaining the material that granularity is -45 μm after fine grinding, fine grinding and accounts for 96%~98%, ore deposit in two sections of vertical stirring mills 3 Starch concentration stable in 65%~75%, that is, the zinc oxygen leaching raw material stablized.Two sections of vertical stirring mill series connection open circuit mills Ore deposit system is compared with existing grinding system, it is not necessary to classification and concentrator, and with small investment, with low cost, flow is short, transport The advantage that row cost is low, stable and reliable in work and fine grinding effect is good.
In the present embodiment, slurrying device 1 includes the first agitator 11 and the second agitator 12 being sequentially connected, the second stirring The outlet of bucket 12 is connected by the first pipeline with the charging aperture of one section of vertical stirring mill 2.Zinc concentrate material to be ground is stirred by first Mix and the further pulp of the second agitator 12 is sent into after the pulp of bucket 11, to obtain the ore pulp that concentration is stable, then by the first pulp conveying Ore pulp is delivered in one section of vertical stirring mill 2 and roughly ground by pump 5 by the first pipeline from slurrying device 1.
It is preferred that, the first agitator 11 is the vertical mixing bucket of cylindricality, and the second agitator 12 is the Horizontal stirring bucket of cylindricality, The transverse width of second agitator 12 is more than the transverse width of the first agitator 11;The longitudinal direction height of second agitator 12 is less than the The longitudinal direction height of one agitator 11, the first agitator 11 and the second agitator 12 that ore pulp passes sequentially through this kind of form can be lifted Mixing effect.Still more preferably, it is equiped with spiral agitator in the first agitator 11;It is equiped with second agitator 12 Disc mixer, is so more beneficial for stirring the refinement of the well mixed and particle of slurries, mitigates the ore grinding burden of follow-up equipment And pressure.
In the present embodiment, medial launder 4,4 storages of medial launder are provided between the second agitator 12 and one section of vertical stirring mill 2 The effect of mineral pulp level is deposited and adjusted, the stabilization of two sections of vertical stirring mills series connection open-circuit grinding system mineral pulp levels is can guarantee that, And then stable be fed to one section of vertical stirring mill 2.
In the present embodiment, the first pulp conveying pump 5 and the second pulp conveying pump 6 be peristaltic pump, centrifugal pump, ceramic pump and Any one in Pulp pump.The first pulp conveying pump 5 of the present embodiment and the second pulp conveying pump 6 carry out ore deposit using peristaltic pump Slurry conveying, peristaltic pump uniformly and stably can enter one section of vertical stirring mill 2 and two sections of vertical stirring mills 3 by transfer ore pulp, It is further ensured that the stability of feed.
Described above is only the preferred embodiment of the present invention, and protection scope of the present invention is not limited merely to above-mentioned implementation Example.To those of ordinary skill in the art, the improvement and change resulting in the case where not departing from the technology of the present invention concept thereof Change and also should be regarded as protection scope of the present invention.

Claims (10)

1. a kind of zinc oxygen leaching method for preparing raw material, it is characterised in that:Comprise the following steps:
1), will treat that grind materials carry out pulp and obtain granularity in ore pulp, ore pulp to account for 40% ~ 80% for -74 μm of solid particle, ore pulp is dense Spend for 65% ~ 75%;
2), ore pulp is fed to one section of vertical stirring mill(2)Primary grinding is carried out, the mog of primary grinding is D60~D90 =45µm;
3), the ore discharge of primary grinding is fed to two sections of vertical stirring mills(3)Carry out secondary grinding, the mog of secondary grinding For D96 ~ D98=45 μm, the ore discharge of secondary grinding is zinc oxygen leaching raw material.
2. zinc oxygen leaching method for preparing raw material according to claim 1, it is characterised in that:One section of vertical mixing mill Machine(2)Using a diameter of 15mm ~ 30mm medium, one section of vertical stirring mill(2)Frequency be 30HZ ~ 50HZ;Described two sections Vertical stirring mill(3)Using a diameter of 5mm ~ 15mm medium, two sections of vertical stirring mills(3)Frequency be 40HZ ~ 50HZ.
3. zinc oxygen leaching method for preparing raw material according to claim 1, it is characterised in that:One section of vertical mixing mill Machine(2)With two sections of vertical stirring mills(3)During the medium of use is chromium steel ball, zirconium ball, Ceramic Balls, glass marble and natural sand Any one.
4. zinc oxygen leaching method for preparing raw material according to claim 1, it is characterised in that:One section of vertical mixing mill Machine(2)With two sections of vertical stirring mills(3)Agitator type be any one in spiral, bar type, disc type and combined type.
5. zinc oxygen leaching method for preparing raw material according to claim 1, it is characterised in that:One section of vertical mixing mill Machine(2)With two sections of vertical stirring mills(3)Agitator speed it is unequal.
6. a kind of two sections of vertical stirring mills series connection open circuit mill for zinc oxygen leaching method for preparing raw material described in claim 1 Ore deposit system, it is characterised in that:Including slurrying device(1), one section of vertical stirring mill(2)With two sections of vertical stirring mills(3), institute State slurrying device(1)Delivery outlet pass through the first pipeline and one section of vertical stirring mill(2)Charging aperture be connected, described one section stand Formula agitator mill(2)Discharging opening pass through the second pipeline and two sections of vertical stirring mills(3)Charging aperture be connected, it is described first pipe Road is provided with the first pulp conveying pump(5), second pipeline is provided with the second pulp conveying pump(6).
The open-circuit grinding system 7. two sections of vertical stirring mills according to claim 6 are connected, it is characterised in that:The pulp Device(1)Including the first agitator being sequentially connected(11)With the second agitator(12), second agitator(12)Outlet Pass through first pipeline and one section of vertical stirring mill(2)Charging aperture be connected.
The open-circuit grinding system 8. two sections of vertical stirring mills according to claim 7 are connected, it is characterised in that:Described first Agitator(11)For the vertical mixing bucket of cylindricality, second agitator(12)For the Horizontal stirring bucket of cylindricality, described second stirs Mix bucket(12)Transverse width be more than the first agitator(11)Transverse width;Second agitator(12)Longitudinal direction it is highly small In the first agitator(11)Longitudinal direction height.
The open-circuit grinding system 9. two sections of vertical stirring mills according to claim 8 are connected, it is characterised in that:Described first Agitator(11)Inside it is equiped with spiral agitator;Second agitator(12)Inside it is equiped with disc mixer.
10. two sections of vertical stirring mills series connection open-circuit grinding system according to any one of claim 6 ~ 9, its feature exists In:Second agitator(12)With one section of vertical stirring mill(2)Between be provided be used for store and adjust in mineral pulp level Between groove(4);The first pulp conveying pump(5)With the second pulp conveying pump(6)It is peristaltic pump, centrifugal pump, ceramic pump and slag Any one in stock pump.
CN201710640414.4A 2017-07-31 2017-07-31 A kind of zinc oxygen leaching method for preparing raw material and two sections of vertical stirring mill series connection open-circuit grinding systems Pending CN107262224A (en)

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CN201710640414.4A CN107262224A (en) 2017-07-31 2017-07-31 A kind of zinc oxygen leaching method for preparing raw material and two sections of vertical stirring mill series connection open-circuit grinding systems

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108034816A (en) * 2017-12-20 2018-05-15 宁波市鄞州智伴信息科技有限公司 A kind of rare earths separation method in monazite
CN112295709A (en) * 2020-11-19 2021-02-02 宝钢磁业(江苏)有限公司 Vertical sanding system capable of improving grinding efficiency of manganese-zinc ferrite slurry

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