CN104887580B - It is a kind of to wash shield composition with scalp anti-aging function - Google Patents
It is a kind of to wash shield composition with scalp anti-aging function Download PDFInfo
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- CN104887580B CN104887580B CN201510312915.0A CN201510312915A CN104887580B CN 104887580 B CN104887580 B CN 104887580B CN 201510312915 A CN201510312915 A CN 201510312915A CN 104887580 B CN104887580 B CN 104887580B
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Abstract
The invention belongs to the technical field of daily-use chemical industry, discloses a kind of washing with scalp anti-aging function and protects combination and preparation method thereof.It is described wash shield combination be made up of shampoo and hair conditioner；The shampoo; by Cocoamidopropyl betaine, cocoyl glutamic acid TEA salt, glycerine, butanediol, polyquaternium 10, hydrolysis jojoba ester, the myristyl glycol of ceteareth 60, glycol distearate, hydrolytic collagen, Salix alba Extract, essence and water composition；The hair conditioner, it is made up of dimethyl silicone polymer, docosyl alcohol, hydroxyethyl cellulose, behenyl base trimethyl ammonium chloride, butanediol, glycerine, hydrolysis jojoba ester, hydrolytic collagen, oligopeptides 1, Salix alba Extract, essence and water.The present invention has good hair cleaning performance, and can repair impaired hair so that hair is smooth, clearly, be easy to comb；Scalp can be nursed simultaneously, there is the good anti-ageing effect of scalp, and is formulated gentle.
Description
Technical field
The invention belongs to the technical field of daily-use chemical industry, is related to one kind and washes shield combination, more particularly to a kind of to resist with scalp
The function that declines washes shield combination and preparation method thereof.
Background technology
Enter us at the beginning of shampoo lives in the later stage seventies, and now the brand of shampoo is less, and function is single, consumer
It is more to focus on cleaning functions, the scope of the effect and function of shampoo not departing from shampoo paste and perfumed soap.Hair conditioner goes out
Life into people now more late than shampoo, compared with traditional hair oil with pomade, hair conditioner does not have greasy feeling, will not
Hair is seemed unnatural or dirty, and effectively and can be uniformly adhered on hair, hair care effect is good, is readily cleaned.
To the later stage eighties, Procter ＆ Gamble, which enters China and invested at home, to found the factory, and releases anti-dandruff Head＆Shoulders, novel bag
Dress and the advertising campaign of domestic unprecedented formula of covering the sky and the earth, have caught rapidly the psychology of consumer, have and then released one after another
Rejoice, the famous brand of Pantene two, and the appearance of " it is two-in-one that Rejoice washes shield " rapidly becomes the primary article of hair-washing hair-care, instead of
The status of traditional shampoo and hair conditioner.For overall bustling about, having no time to attend to the people of hair nursing, two-in-one shampoo without
Different is best selection.Certainly, wash to protect anion remover and cation opsonizing agent in two-in-one product and can produce and suppress to make
With, and influence hair care effect.
Into the nineties, with being in fashion for the serious of environmental pollution and hair-waving, hair dyeing etc., the impaired probability of hair improves
, based on natural plant composition to wash hair products well received.The frequency of hair washing brings up to 2-3 by 1-2 times weekly
More than secondary.
In recent years, the product efficacy for washing hair care market is segmented increasingly, for repairing damaged hair, moistening Anti-hair loss, moist
It is anti-dandruff to wait product to come out one after another；Meanwhile black hair dark hair, anticreep anti-avulsion, the product of promotion natural on-off cycles of hair growth are increasingly becoming and mainly sold
Point.
Since last year, hair care concept rise is washed without silicone oil headed by ring sub- " taste source ", causes and wash new the one of hair care market
Take turns storm.
But so far, most of hair products of washing are cleaned using Sulfateses such as AES, K12 to be main on the market
Agent, such remover excitant is big, and degreasing power is too strong, and correct leatherware has certain infringement；And most products are mainly pin
Nursing to hair, the nursing to scalp (soil of natural on-off cycles of hair growth) are seldom paid close attention to.
The content of the invention
The shortcomings that in order to overcome prior art and deficiency, primary and foremost purpose of the invention are to provide one kind without sulfate without anti-
The shield of washing with scalp anti-aging function of rotten agent combines.Shield combination of washing prepared by the present invention cooperates, mutually synergy,
It is gentle non-stimulated, can hair conditioning and can nursing scalp.
Another object of the present invention is to provide the above-mentioned preparation method for washing shield combination with scalp anti-aging function.
The purpose of the present invention is achieved through the following technical solutions：
It is a kind of to wash shield combination with scalp anti-aging function, it is made up of shampoo and hair conditioner.
The shampoo, it is prepared by following raw material by mass percentage：8.5%~12.5% coconut oleoyl amine third
Base glycine betaine, 9%~12% cocoyl glutamic acid TEA salt, 5%~10% glycerine, 3%~6% butanediol, 0.5%~
0.8% Polyquaternium-10,3%~5% hydrolysis jojoba ester, the myristyl glycol of 3%~5% ceteareth -60,
1%~2% glycol distearate, 0.5%~1.0% hydrolytic collagen, 0.4%~0.6% Salix alba Extract, 0.3%~
0.4% essence and excess water.
The preparation method of the shampoo, comprises the following steps：
(1) hydrolytic collagen is mixed with part water, stirring and dissolving, obtains prefabricated solution A；
(2) remaining water is added in reactor, opens stirring, added Polyquaternium-10, be warming up to 70 DEG C~80 DEG C,
Cocoamidopropyl betaine is added, stirs 3~5min, adds cocoyl glutamic acid TEA salt, continues to stir and is warming up to 80
~85 DEG C, add butanediol, glycerine, hydrolysis jojoba ester, the myristyl of ceteareth -60 glycol, ethylene glycol two
Stearate, after being incubated 25~35min, with micro- sem observation, next step is carried out when without visible crystals；
(3) rotating speed is adjusted, 35~40 DEG C is cooled to, adds prefabricated A, Salix alba Extract, essence, stir, washed
Shampoo.
Described shampoo outward appearance is light yellow fine and smooth pearly-lustre emulsion；PH be 5.0~6.0, viscosity be 6000mpa.s~
8000mpa.s, 45 DEG C heat-resisting 24 hours, is resisted cold 24 hours without significant change, -18 DEG C after recovering room temperature, without bright after recovery room temperature
Aobvious change.
Speed of agitator described in step (1) is 150rpm~200rpm；The mass ratio of the hydrolytic collagen and pure water is 1:
9。
Speed of agitator described in step (2) is 200rpm~300rpm.
The rotating speed adjusted described in step (3) is 100rpm~200rpm；The time to stir be 10min~
15min。
The hair conditioner, it is prepared by following raw material by mass percentage：8%~10% polydimethylsiloxanes
Alkane, 3%~5% docosyl alcohol, 0.3%~0.5% hydroxyethyl cellulose, 2%~3% behenyl base trimethyl ammonium chloride, 5%~
10% butanediol, 10%~15% glycerine, 4%~6% hydrolysis jojoba ester, 1%~1.5% hydrolytic collagen, 0.001%~
The Salix alba Extract of 0.0015% oligopeptides -1,0.6%~0.8%, 0.3%~0.4% essence and excess water.
The preparation method of the hair conditioner, comprises the following steps：
(a) hydrolytic collagen is mixed with part water, stirring and dissolving, obtains prefabricated B；
(b) dimethyl silicone polymer, docosyl alcohol are added into oil phase pot, stirs and be warming up to 80~85 DEG C, insulation 5~
10min, obtain oil phase raw material；
(c) remaining water is added into aqua pot, opens stirring, add hydroxyethyl cellulose, be warming up to 70~80 DEG C, added
Behenyl base trimethyl ammonium chloride, 85~90 DEG C are continuously heating to, add glycerine, hydrolyze jojoba ester, butanediol, insulation 15~
25min, obtain Aqueous Phase Raw Material；
(d) Aqueous Phase Raw Material is pumped into emulsification pot, keeps vacuum, high speed homogenization adds oil phase raw material simultaneously, treats that oil phase adds
After the completion of adding, continue homogeneous to emulsified particles average grain diameter and be less than 2 μm, obtain mixture；
(e) stirring is opened, 35 DEG C~40 DEG C is cooled to, prefabricated B, oligopeptides -1, white willow is added into the mixture of step (d)
Extract and essence, it is well mixed, obtains hair conditioner.
Speed of agitator described in step (a) is 150rpm~200rpm；The mass ratio of the hydrolytic collagen and pure water is 1:
9。
Speed of agitator described in step (b) is 600rpm~800rpm.
The rotating speed stirred described in step (c) is 200rpm~300rpm；The vacuum of vacuum is kept described in step (d)
For -0.03Mpa~-0.05Mpa；The rotating speed of the high speed homogenization is 10000rpm~12000rpm.
Speed of agitator described in step (e) is 300rpm~400rpm；The incorporation time is 10~15min.
Hair conditioner made from this method is the white shape lotion of white, PH 4.5-5.0, viscosity be 15000mpa.s~
20000mpa.s, 45 DEG C heat-resisting 24 hours, is resisted cold 24 hours without significant change, -18 DEG C after recovering room temperature, without bright after recovery room temperature
Aobvious change.
Hydrolysis jojoba ester is the aqueous dispersions that mass fraction is 20%, has good hair nursing and scalp care work(
Can, it is purchased from FLORATECH companies of the U.S..
Hydrolytic collagen is purchased from Cargill companies of the U.S., is white powder, and mean molecule quantity is 3000 dalton；To scalp
Act as supplement scalp collagen content, strengthen scalp elasticity of skin, nutrition skin.
The shampoo and hair conditioner of the present invention, which is used in combination, not only can effectively clean reparation hair, can also be on hair
A kind of film uniform, having relative hardness, transparent air-permeable can wash away is formed, this film can not only make hair look clear
It is bright extremely attractive in appearance, it can more play a protective role；Ventilative film can make hair eupnea, reduce the volatilization of moisture in hair,
Prevent dry and cracked, hair is freshened, be smooth, feel is more preferable.And combination is protected in of the invention washing can nurse scalp, strengthen head
Musculus cutaneus skin collagen synthesis, scalp is become flexible, and promote epidermal growth, repairing hair follicle.
Compared with prior art, the present invention has advantages below and beneficial effect：
1st, shield combination of washing of the invention has good hair cleaning performance, and can repair impaired hair so that head
Luminous profit, salubrious, good hand touch simultaneously are easy to comb；The present invention can nurse scalp simultaneously, strengthen scalp skin collagen synthesis,
Scalp is become flexible, and promote epidermal growth, repairing hair follicle, there is the good anti-ageing effect of scalp, be hair
Grow the material guarantee to provide the foundation；
2nd, the present invention carry out formulation composition optimization, no sulfate, without anti-corrosion etc. potentially stimulate anaphylactogen, be formulated non-normal temperature
With.
Embodiment
With reference to embodiment, the present invention is described in further detail, but the implementation of the present invention is not limited to this.
The shampoo of embodiment 1
A kind of shampoo with scalp anti-aging function, is prepared by following raw material by mass percentage：
The preparation method of the shampoo：
(1) by hydrolytic collagen and pure water (i.e. water) using mass ratio as 1:9 mixed at room temperature, are gently mixed that (rotating speed of stirring is
150rpm) dissolving is complete, obtains prefabricated A；
(2) at room temperature, remaining pure water is added into aqua pot, opens stirring (rotating speed of stirring is 200rpm), added poly-
Quaternary ammonium salt -10, when being warming up to 70 DEG C, Cocoamidopropyl betaine is added, after stirring 5min, adds cocoyl glutamic acid
TEA salt, when continuing to stir and being warming up to 80 DEG C, add butanediol, glycerine, hydrolysis jojoba ester, the meat of ceteareth -60
Myristyl glycol, glycol distearate, after 80 DEG C are incubated 25min, take a small amount of lotion to be applied on slide and cover lid glass
Piece, amplify 400 times of observations with 40 times of object lens of microscope, can continue next step after no visible crystals；
(3) rotating speed (rotating speed of stirring is 100rpm) is adjusted, temperature lowering water is opened and is cooled to 35 DEG C, add prefabricated A, white willow carries
Thing, essence are taken, continues to stir 10min, obtains the shampoo with scalp anti-aging function.
The shampoo outward appearance of gained is light yellow fine and smooth iridescent body；PH is 5.6, and viscosity 6200mpa.s, 45 DEG C heat-resisting
24 hours, resisted cold 24 hours without significant change, -18 DEG C after recovering room temperature, without significant change after recovery room temperature.
The shampoo of embodiment 2
A kind of shampoo with scalp anti-aging function, is prepared by following raw material by mass percentage：
The preparation method of the shampoo：
(1) by hydrolytic collagen and pure water (i.e. water) using mass ratio as 1:9 mixed at room temperature, are gently mixed that (rotating speed of stirring is
180rpm) dissolving is complete, obtains prefabricated A；
(2) at room temperature, remaining pure water is added into aqua pot, opens stirring (rotating speed of stirring is 240rpm), added poly-
Quaternary ammonium salt -10, when being warming up to 75 DEG C, Cocoamidopropyl betaine is added, cocoyl glutamic acid is added after stirring 4min
TEA salt, continue to stir and butanediol can be added when being warming up to 82 DEG C, glycerine, hydrolysis jojoba ester, ceteareth-
60 myristyl glycol, glycol distearate, after 82 DEG C are incubated 30min, take a small amount of lotion to be applied on slide and cover
Cover glass, amplify 400 times of observations with 40 times of object lens of microscope, can continue next step after no visible crystals；
(3) rotating speed (rotating speed of stirring is 150rpm) is adjusted, temperature lowering water is opened and is cooled to 37 DEG C, add prefabricated A, white willow carries
Thing, essence are taken, continues to stir 12min, obtains the shampoo with scalp anti-aging function.
The shampoo outward appearance of gained is light yellow fine and smooth iridescent body；PH is 5.2, and viscosity 6800mpa.s, 45 DEG C heat-resisting
24 hours, resisted cold 24 hours without significant change, -18 DEG C after recovering room temperature, without significant change after recovery room temperature.
The shampoo of embodiment 3
A kind of shampoo with scalp anti-aging function, is prepared by following raw material by mass percentage：
The preparation method of the shampoo：
(1) by hydrolytic collagen and pure water (i.e. water) using mass ratio as 1:9 mixed at room temperature, open stirring (rotating speed 150rpm)
It is to be dissolved complete, obtain prefabricated A；
(2) at room temperature, remaining pure water is added into aqua pot, opens and stir (rotating speed 200rpm), addition polyquaternium-
10, when being warming up to 80 DEG C, Cocoamidopropyl betaine is added, after stirring 5min, adds cocoyl glutamic acid TEA salt,
When continuing to stir and being warming up to 85 DEG C, butanediol, glycerine, hydrolysis jojoba ester, the myristyl of ceteareth -60 are added
Glycol, glycol distearate, after 85 DEG C of insulation 35min, take a small amount of lotion to be applied on slide and cover cover glass, with aobvious
40 times of object lens of micro mirror amplify 400 times of observations, continue next step after no visible crystals；
(3) adjust rotating speed (rotating speed 200rpm), open temperature lowering water be cooled to 40 DEG C, add prefabricated A, Salix alba Extract,
Essence, continue to stir 15min, obtain the shampoo with scalp anti-aging function.
The shampoo outward appearance of gained is light yellow fine and smooth iridescent body；PH is 5.3, and viscosity 6700mpa.s, 45 DEG C heat-resisting
24 hours, resisted cold 24 hours without significant change, -18 DEG C after recovering room temperature, without significant change after recovery room temperature.
The hair conditioner of embodiment 4
A kind of hair conditioner with scalp anti-aging function, is prepared by following raw material by mass percentage：
The preparation method of the hair conditioner：
(1) by hydrolytic collagen and pure water (i.e. water) using mass ratio as 1:9 mixed at room temperature, are gently mixed that (rotating speed of stirring is
It is 150rpm) to be dissolved complete, obtain prefabricated B；
(2) dimethyl silicone polymer, docosyl alcohol are added into oil phase pot, opens stirring (rotating speed of stirring is 600rpm), risen
Temperature is incubated 5min, obtains oil phase raw material to 85 DEG C；
(3) at room temperature, remaining pure water is added into aqua pot, opens stirring (rotating speed of stirring is 200rpm), and add
Hydroxyethyl cellulose, when being warming up to 70 DEG C, behenyl base trimethyl ammonium chloride is added, is continuously heating to 85 DEG C, add glycerine, hydrolysis
Jojoba ester, butanediol, 85 DEG C of insulation 20min, obtain Aqueous Phase Raw Material；
(4) Aqueous Phase Raw Material is pumped into emulsification pot, keeps vacuum -0.03Mpa, oil phase raw material is added in high speed homogenization (
Matter speed is 11000rpm), after the completion for the treatment of oil phase addition, continue homogeneous extremely：Emulsified particles average grain diameter, which is less than 2 μm, (to be used
Microscope amplifies 400 times of observations)；
(5) stirring (rotating speed of stirring is 300rpm) is cooled to 35 DEG C, adds prefabricated B, oligopeptides -1, Salix alba Extract, perfume (or spice)
Essence, 10min is stirred, obtains the hair conditioner with scalp anti-aging function.
Hair conditioner made from this method is the white shape lotion of white, PH 4.6, viscosity 15500mpa.s, 45 DEG C heat-resisting 24
Hour, resisted cold 24 hours without significant change, -18 DEG C after recovering room temperature, without significant change after recovery room temperature.
The hair conditioner of embodiment 5
A kind of hair conditioner with scalp anti-aging function, is prepared by following raw material by mass percentage：
The preparation method of the hair conditioner：
(1) by hydrolytic collagen and pure water (i.e. water) using mass ratio as 1:9 mixed at room temperature, are gently mixed that (rotating speed of stirring is
It is 180rpm) to be dissolved complete, obtain prefabricated B；
(2) dimethyl silicone polymer, docosyl alcohol are added into oil phase pot, opens stirring (rotating speed of stirring is 700rpm), risen
Temperature is incubated 7min, obtains oil phase raw material to 82 DEG C；
(3) at room temperature, remaining pure water is added into aqua pot, opens stirring (rotating speed of stirring is 250rpm), and add
Hydroxyethyl cellulose, when being warming up to 75 DEG C, behenyl base trimethyl ammonium chloride is added, is continuously heating to 87 DEG C, add glycerine, hydrolysis
Jojoba ester, butanediol, 87 DEG C of insulation 20min, obtain Aqueous Phase Raw Material；
(4) Aqueous Phase Raw Material is pumped into emulsification pot, keeps vacuum -0.04Mpa, oil phase raw material is added in high speed homogenization (
Matter speed is 11000rpm), after the completion for the treatment of oil phase addition, continue homogeneous extremely：Emulsified particles average grain diameter, which is less than 2 μm, (to be used
Microscope amplifies 400 times of observations)；
(5) stirring (rotating speed of stirring is 350rpm) is cooled to 35 DEG C, adds prefabricated B, oligopeptides -1, Salix alba Extract, perfume (or spice)
Essence, 12min is stirred, obtains the hair conditioner with scalp anti-aging function.
Hair conditioner made from this method is the white shape lotion of white, PH 4.5, viscosity 18500mpa.s, 45 DEG C heat-resisting 24
Hour, resisted cold 24 hours without significant change, -18 DEG C after recovering room temperature, without significant change after recovery room temperature.
The hair conditioner of embodiment 6
A kind of hair conditioner with scalp anti-aging function, is prepared by following raw material by mass percentage：
The preparation method of the hair conditioner：(1) by hydrolytic collagen and pure water (i.e. water) using mass ratio as 1:9 mixed at room temperature,
Be gently mixed (rotating speed of stirring is 200rpm) it is to be dissolved completely, obtain prefabricated B；
(2) dimethyl silicone polymer, docosyl alcohol are added into oil phase pot, opens stirring (rotating speed of stirring is 800rpm), risen
Temperature is incubated 10min, obtains oil phase raw material to 85 DEG C；
(3) at room temperature, remaining pure water is added into aqua pot, opens stirring (rotating speed of stirring is 300rpm), and add
Hydroxyethyl cellulose, when being warming up to 80 DEG C, behenyl base trimethyl ammonium chloride is added, is continuously heating to 90 DEG C, adds glycerine, water
Jojoba ester, butanediol are solved, 90 DEG C of insulation 15min, obtains Aqueous Phase Raw Material；
(4) Aqueous Phase Raw Material is pumped into emulsification pot, keeps vacuum -0.05Mpa, oil phase raw material is added in high speed homogenization (
Matter speed is 12000rpm), after the completion for the treatment of oil phase addition, continue homogeneous extremely：Emulsified particles average grain diameter, which is less than 2 μm, (to be used
Microscope amplifies 400 times of observations)；
(5) stirring (rotating speed of stirring is 400rpm) is cooled to 40 DEG C, adds prefabricated B, oligopeptides -1, Salix alba Extract, perfume (or spice)
Essence, 15min is stirred, obtains the hair conditioner with scalp anti-aging function.
Hair conditioner made from this method is the white shape lotion of white, PH 4.8, viscosity 17000mpa.s, 45 DEG C heat-resisting 24
Hour, resisted cold 24 hours without significant change, -18 DEG C after recovering room temperature, without significant change after recovery room temperature.
Performance test：
1st, the product of embodiment 1~6 is subjected to Microbial Challenge test, as a result sees attached list 1~6：
Subordinate list 1：The shampoo of embodiment 1
Subordinate list 2：The shampoo of embodiment 2
Subordinate list 3：The shampoo of embodiment 3
Subordinate list 4：The hair conditioner of embodiment 4
Subordinate list 5：The hair conditioner of embodiment 5
Subordinate list 6：The hair conditioner of embodiment 6
Detection method：American Pharmacopeia USP32 (51) antimicrobial preservation efficacy test
Bacterium：Pseudomonas aeruginosa (Pseudomonas aeruginosa) ATCC 9027
ETEC (Escherichia coli) ATCC 8739
Staphylococcus aureus (Staphylococcus aureus) ATCC 6538
Mould and saccharomycete：Candida albicans (Candida albicans) ATCC 10231
Aspergillus niger (Aspergillus niger) ATCC 16404
As a result show, the control ability of the microorganism of product is good.
2nd, the test of clearly sense, reflecting feel, cardability and anti-aging performance is carried out to the product of embodiment 1~6：At random
Embodiment 1~6 is combined：
Shampoo embodiment 1 is combined into hair conditioner embodiment 5：Wash shield combination 1；
Shampoo embodiment 2 is combined into hair conditioner embodiment 4：Wash shield combination 2；
Shampoo embodiment 3 is combined into hair conditioner embodiment 6：Wash shield combination 3；
In addition at random from three kinds of shampoos of purchase and three kinds of hair conditioner and six kinds of embodiment random combines on the market：
Commercial shampoos 1 are combined into hair conditioner embodiment 4：Wash shield combination 4；
Commercial shampoos 2 are combined into hair conditioner embodiment 6：Wash shield combination 5；
Commercial shampoos 3 are combined into hair conditioner embodiment 5：Wash shield combination 6；
Commercially available hair conditioner 1 is combined into shampoo embodiment 2：Wash shield combination 7；
Commercially available hair conditioner 2 is combined into shampoo embodiment 3：Wash shield combination 8；
Commercially available hair conditioner 3 is combined into shampoo embodiment 1：Wash shield combination 9；
2-1,9 groups of wet hair carding properties for washing shield combination and hair drying comb rationality can test to more than, and during dry hair
Salubrious sense and reflecting feel evaluated, test result is as shown in subordinate list 7：
Subordinate list 7
Explanation：
1st, hair, wet hair carding force are done using the test of the universal material testers of U.S. Instron 5565, it is wet in 25 DEG C of constant temperature
Under conditions of degree 60%, material of measuring and monitoring the growth of standing timber is true man's topknot, and comb material is nylon plastic(s), tooth pitch 1mm, surface roughness 3.2, topknot
Relative displacement with comb is 600mm/min, and it is to be naturally drooped, without pre-tension along scale, topknot to comb direction；Comb
Power numerical value is smaller to represent that carding property is better, and hair is more smooth.
2nd, do the salubrious sense of hair and reflecting feel (reflecting feel score value is higher, represents that the degree that hair is repaired is better) score value is said
It is bright：Ten point system evaluation criterion, 1 point worst, and 10 points best, and score value is higher to represent that effect is better.
Subject 36, at -55 years old 25 years old age, dryness, oiliness, normal hair contain, random packet.
Application method：First hair is soaked with clear water；Appropriate shampoo is taken on both hands, rub be placed on after foam it is light on head
Light rubbing, you can produce foam, be not required to too firmly rub hair with the hands, stop 1min or so；During flushing, also gently smoothed out with the fingers using finger straight
Hair rinses；After shampoo foam to be washed is rinsed well, appropriate hair conditioner is taken uniformly to be applied on hair and scalp, gently
Forlement 3~5min of scalp, then rinsed well with clear water.
As a result show, the shield combination other products more on the market washed in the present invention have more preferable carding property, more preferable
Salubrious property and Geng Gao repairing performance.
2-2, anti-aging (scalp elasticity, hair follicle health degree) effect to scalp are evaluated, evaluation result such as subordinate list 8,9
It is shown：
Subordinate list 8
Subordinate list 9：
Score value explanation：Ten point system evaluation criterion, 1 point worst, and 10 points best, and score value is higher to represent that effect is more obvious.It is tested
Person 45, -55 years old 25 years old age, random packet.Service life is 2 months.
Application method：First hair is soaked with clear water；Appropriate shampoo is taken on both hands, rub be placed on after foam it is light on head
Light rubbing, you can produce foam, be not required to too firmly rub hair with the hands, stop 1min or so；During flushing, also gently smoothed out with the fingers using finger straight
Hair rinses；After shampoo foam to be washed is rinsed well, appropriate hair conditioner is taken uniformly to be applied on hair and scalp, gently
3~5min of massaging scalp, then rinsed well with clear water.
As a result show, washing the correct leatherware of shield combination for of the invention three groups has preferable nursing function.
Shampoo in the present invention, using coconut oil source and origin of amino acid gentle surfactant to clean into
Point, using quaternary ammonium salt conditioner, the esters in jojoba oil source, the hydrolytic collagen in marine fishes source carry out nourishing scalp, head
Skin anti-aging function, and using antibacterial, the of the invention shampoo of the plant antipathogenic composition Salix alba Extract with hair conditioning function
It is gentle non-stimulated for without sulfate, preservative free system, and there is scalp anti-aging function, it is formulated simple, easy to operate, effect and shows
Write.
Hair conditioner in the present invention, using dimethyl silicone polymer and behenyl base trimethyl ammonium chloride as main hair nursing into
Point, using two Lauryl Alcohols as stable system composition, with the hydrolytic collagen in the esters in jojoba oil source and marine fishes source with
And oligopeptides -1 carries out nourishing scalp, scalp anti-aging function, and carried using the plant antipathogenic composition white willow with hair conditioning function
Take thing antibacterial, formula is simple, easy to operate, effect is notable.
Above-described embodiment is the preferable embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, other any Spirit Essences without departing from the present invention with made under principle change, modification, replacement, combine, simplification,
Equivalent substitute mode is should be, is included within protection scope of the present invention.
Claims (9)
1. a kind of wash shield composition with scalp anti-aging function, it is characterised in that：It is made up of shampoo and hair conditioner；
The shampoo, it is prepared by following raw material by mass percentage：8.5%~12.5% cocamidopropyl propyl amide sweet tea
Dish alkali, 9%~12% cocoyl glutamic acid TEA salt, 5%~10% glycerine, 3%~6% butanediol, 0.5%~0.8% is poly-
The hydrolysis jojoba ester of quaternary ammonium salt -10,3%~5%, the myristyl glycol of 3%~5% ceteareth -60,1%~2%
Glycol distearate, 0.5%~1.0% hydrolytic collagen, 0.4%~0.6% Salix alba Extract, 0.3%~0.4% essence
And excess water；
The hair conditioner, it is prepared by following raw material by mass percentage：8%~10% dimethyl silicone polymer, 3%
~5% docosyl alcohol, 0.3%~0.5% hydroxyethyl cellulose, 2%~3% behenyl base trimethyl ammonium chloride, 5%~10% fourth two
Alcohol, 10%~15% glycerine, 4%~6% hydrolysis jojoba ester, 1%~1.5% hydrolytic collagen, 0.001%~0.0015% is few
The Salix alba Extract of peptide -1,0.6%~0.8%, 0.3%~0.4% essence and excess water；
Described shampoo outward appearance is light yellow fine and smooth pearly-lustre emulsion；PH be 5.0~6.0, viscosity be 6000mpa.s~
8000mpa.s, the hair conditioner are the white shape lotion of white, and PH 4.5-5.0, viscosity is 15000mpa.s~20000mpa.s.
2. wash shield composition with scalp anti-aging function according to claim 1, it is characterised in that：The system of the shampoo
Preparation Method, concretely comprise the following steps：
(1) hydrolytic collagen is mixed with part water, stirring and dissolving, obtains prefabricated solution A；
(2) remaining water is added in reactor, opens stirring, add Polyquaternium-10, be warming up to 70 DEG C~80 DEG C, added
Cocoamidopropyl betaine, 3~5min is stirred, add cocoyl glutamic acid TEA salt, continued to stir and be warming up to 80~85
DEG C, add butanediol, glycerine, hydrolysis jojoba ester, the myristyl of ceteareth -60 glycol, ethylene glycol distearyl
Acid esters, after being incubated 25~35min, with micro- sem observation, next step is carried out when without visible crystals；
(3) rotating speed is adjusted, 35~40 DEG C is cooled to, adds prefabricated solution A, Salix alba Extract, essence, stir, washed
Shampoo；
The preparation method of the hair conditioner, is concretely comprised the following steps：
(a) hydrolytic collagen is mixed with part water, stirring and dissolving, obtains prefabricated B；
(b) dimethyl silicone polymer, docosyl alcohol are added into oil phase pot, stirs and be warming up to 80~85 DEG C, be incubated 5~10min, obtain
To oil phase raw material；
(c) remaining water is added into aqua pot, opens stirring, add hydroxyethyl cellulose, be warming up to 70~80 DEG C, add behenyl
Base trimethyl ammonium chloride, 85~90 DEG C are continuously heating to, add glycerine, hydrolysis jojoba ester, butanediol, be incubated 15~25min,
Obtain Aqueous Phase Raw Material；
(d) Aqueous Phase Raw Material is pumped into emulsification pot, keeps vacuum, high speed homogenization adds oil phase raw material simultaneously, treats that oil phase has added
Cheng Hou, continue homogeneous to emulsified particles average grain diameter and be less than 2 μm, obtain mixture；
(e) stirring is opened, is cooled to 35 DEG C~40 DEG C, prefabricated B, oligopeptides -1, white willow extraction are added into the mixture of step (d)
Thing and essence, it is well mixed, obtains hair conditioner.
3. wash shield composition with scalp anti-aging function according to claim 2, it is characterised in that：Described in step (1)
Speed of agitator is 150rpm~200rpm；The mass ratio of the hydrolytic collagen and part water is 1:9.
4. wash shield composition with scalp anti-aging function according to claim 2, it is characterised in that：Described in step (2)
Speed of agitator is 200rpm~300rpm.
5. wash shield composition with scalp anti-aging function according to claim 2, it is characterised in that：Described in step (3)
The rotating speed of regulation is 100rpm~200rpm；The time to stir is 10min~15min.
6. wash shield composition with scalp anti-aging function according to claim 2, it is characterised in that：Described in step (a)
Speed of agitator is 150rpm~200rpm；The mass ratio of the hydrolytic collagen and part water is 1:9.
7. wash shield composition with scalp anti-aging function according to claim 2, it is characterised in that：Described in step (b)
Speed of agitator is 600rpm~800rpm；
The rotating speed stirred described in step (c) is 200rpm~300rpm.
8. wash shield composition with scalp anti-aging function according to claim 2, it is characterised in that：Described in step (d)
The vacuum for keeping vacuum is -0.03Mpa~-0.05Mpa；The rotating speed of the high speed homogenization is 10000rpm~12000rpm.
9. wash shield composition with scalp anti-aging function according to claim 2, it is characterised in that：Described in step (e)
Speed of agitator is 300rpm~400rpm；The incorporation time is 10~15min.
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| CN107468570A (en) * | 2017-08-25 | 2017-12-15 | 广西和桂集团有限公司 | Traditional Chinese medicine hair conditioner and preparation method thereof |
| CN109303731A (en) * | 2018-11-26 | 2019-02-05 | 庄雪芸 | A kind of shampoo formula with scalp anti-aging function |
| CN113509406A (en) * | 2021-06-07 | 2021-10-19 | 泉后(广州)生物科技研究院有限公司 | Semi-permeable gel liquid crystal hair mask and preparation method thereof |
| CN114533608B (en) * | 2022-01-17 | 2023-05-16 | 广州环亚化妆品科技股份有限公司 | Scalp anti-sensitivity composition and preparation method and application thereof |
| CN116473884B (en) * | 2022-09-21 | 2024-03-05 | 百肽德医药生物科技(广东)有限公司 | Cell membrane complex hair care factor and hair conditioner thereof |
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| CN101697940A (en) * | 2009-11-10 | 2010-04-28 | 广州市迪彩化妆品有限公司 | Hair care composition and preparation method thereof |
| CN102895151A (en) * | 2012-10-22 | 2013-01-30 | 广州立白企业集团有限公司 | Sulfate-free hair cleanser and preparation method thereof |
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| CN101697940A (en) * | 2009-11-10 | 2010-04-28 | 广州市迪彩化妆品有限公司 | Hair care composition and preparation method thereof |
| CN102895151A (en) * | 2012-10-22 | 2013-01-30 | 广州立白企业集团有限公司 | Sulfate-free hair cleanser and preparation method thereof |
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