CN104887580A - Shampoo-hair conditioner composition with scalp anti-aging function and preparation method thereof - Google Patents
Shampoo-hair conditioner composition with scalp anti-aging function and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to the technical field of daily chemical industry, and discloses a shampoo-hair conditioner composition with a scalp anti-aging function and a preparation method thereof. The shampoo-hair conditioner composition consists of a shampoo and a hair conditioner, wherein the shampoo consists of cocamidopropyl betaine, a cocoyl glutamate TEA salt, glycerol, butanediol, a polyquaternary salt-10, hydrolyzed jojoba ester, ceteareth-60 myristyl glycol, glycol distearate, hydrolyzed collagen, a white willow extract, an essence and water; and the hair conditioner consists of polydimethylsiloxane, docosyl alcohol, hydroxyethyl cellulose, behentrimonium chloride, butanediol, glycerol, hydrolyzed jojoba ester, hydrolyzed collagen, oligopeptide-1, a white willow extract, an essence and water. The shampoo-hair conditioner composition disclosed by the invention has a good hair cleaning effect, can repair damaged hairs, and can ensure that the hairs are smooth, refreshing and convenient to comb; and meanwhile, the shampoo-hair conditioner composition can nurse the scalp, has a good scalp anti-aging effect, and is mild in formula.
Description
Technical field
The invention belongs to the technical field of daily-use chemical industry, relate to one and wash and protect combination, particularly a kind of have washing of scalp anti-aging function and protect combination and preparation method thereof.
Background technology
What enter us at the beginning of shampoo lives in the later stage seventies, and now the brand of shampoo is less, function singleness, and consumer more focuses on cleaning function, and the effect and function of shampoo does not exceed the scope of shampoo paste and fancy soap.The appearance life that enter people more late than shampoo of hair conditioner, compare with pomade with traditional hair oil, hair conditioner does not have greasy feeling, hair can not be made to seem unnatural or dirty, and can effectively and uniformly be attached on hair, hair care effect be good, be easy to cleaning.
To the later stage eighties, Procter & Gamble enters China and investment is founded the factory at home, release anti-dandruff Head&Shoulders, novel packaging and the advertising campaign of domestic unprecedented formula of covering the sky and the earth, catch rapidly the psychology of consumer, and then release one after another Rejoice, Pantene two famous brand, and the appearance of " Rejoice wash protect two-in-one " becomes rapidly the primary article of hair-washing hair-care, instead of the status of traditional shampoo and hair conditioner.Concerning overall bustling about, have no time to attend to hair nursing people, it is best selection that two-in-one shampoo is as good as.Certainly, wash and protect anion detergent and cation opsonizing agent in two-in-one product and can produce inhibitory action, and affect hair care effect.
Enter the nineties, in fashion along with the serious of environmental pollution and hair-waving, hair dyeing etc., the impaired probability of hair improves, based on natural plant composition to wash hair products well received.The frequency of hair washing brings up to more than 2-3 time by 1-2 time weekly.
In recent years, the product efficacy of washing hair care market is segmented increasingly, for reparation damaged hair, moistens Anti-hair loss, moistens the product such as anti-dandruff and come out one after another; Meanwhile, the product of black hair hair color, anticreep anti-avulsion, promotion natural on-off cycles of hair growth also becomes main selling point gradually.
Since last year, headed by ring Asia " taste source " without silicone oil wash hair care concept rise, cause wash hair care market new round storm.
But so far, most on the market to wash hair products be all main detergent with Sulfateses such as AES, K12, and such detergent zest is large, and degreasing power is too strong, and correct leatherware has certain infringement; And most products is mainly for the nursing of hair, the nursing of scalp (soil of natural on-off cycles of hair growth) is seldom paid close attention to.
Summary of the invention
In order to overcome the shortcoming and defect of prior art, primary and foremost purpose of the present invention is to provide a kind of washing of scalp anti-aging function that have without sulfate preservative free to protect combination.Washing prepared by the present invention is protected combination and is cooperatively interacted, mutual synergism, gentle non-stimulated, can nurse scalp again by hair conditioning.
Another object of the present invention is to provide above-mentioned there is scalp anti-aging function wash the preparation method of protecting combination.
Object of the present invention is achieved through the following technical solutions:
There is washing of scalp anti-aging function and protect a combination, be made up of shampoo and hair conditioner.
Described shampoo; be prepared from by following raw material by mass percentage: 8.5% ~ 12.5% cocamido propyl betaine; 9% ~ 12% cocoyl glutamic acid TEA salt; 5% ~ 10% glycerol; 3% ~ 6% butanediol; 0.5% ~ 0.8% Polyquaternium-10; 3% ~ 5% hydrolysis Jojoba ester; 3% ~ 5% ceteareth-60 myristyl glycol; 1% ~ 2% glycol distearate; 0.5% ~ 1.0% hydrolytic collagen, 0.4% ~ 0.6% Salix alba Extract, 0.3% ~ 0.4% essence and excess water.
The preparation method of described shampoo, comprises the following steps:
(1) hydrolytic collagen is mixed with part water, stirring and dissolving, obtain prefabricated solution A;
(2) remaining water is added in reactor, open and stir, add Polyquaternium-10, be warming up to 70 DEG C ~ 80 DEG C, add cocamido propyl betaine, stir 3 ~ 5min, add cocoyl glutamic acid TEA salt, continue stir and be warming up to 80 ~ 85 DEG C, add butanediol, glycerol, hydrolysis Jojoba ester, ceteareth-60 myristyl glycol, glycol distearate again, after insulation 25 ~ 35min, with microscopic examination, when carrying out next step without during visible crystals;
(3) adjusting rotary speed, is cooled to 35 ~ 40 DEG C, adds prefabricated A, Salix alba Extract, essence, stirs, obtain shampoo.
Described shampoo outward appearance is light yellow fine and smooth pearly-lustre emulsion; PH is 5.0 ~ 6.0, and viscosity is 6000mpa.s ~ 8000mpa.s, and 45 DEG C heat-resisting 24 hours, and without significant change after recovery room temperature ,-18 DEG C are resisted cold 24 hours, without significant change after recovery room temperature.
Described in step (1), speed of agitator is 150rpm ~ 200rpm; The mass ratio of described hydrolytic collagen and pure water is 1:9.
Described in step (2), speed of agitator is 200rpm ~ 300rpm.
The rotating speed regulated described in step (3) is 100rpm ~ 200rpm; The described time stirred is 10min ~ 15min.
Described hair conditioner, be prepared from by following raw material by mass percentage: 8% ~ 10% polydimethylsiloxane, 3% ~ 5% behenyl alcohol, 0.3% ~ 0.5% hydroxyethyl-cellulose, 2% ~ 3% mountain Yu base trimethyl ammonium chloride, 5% ~ 10% butanediol, 10% ~ 15% glycerol, 4% ~ 6% hydrolysis Jojoba ester, 1% ~ 1.5% hydrolytic collagen, 0.001% ~ 0.0015% oligopeptide-1,0.6% ~ 0.8% Salix alba Extract, 0.3% ~ 0.4% essence and excess water.
The preparation method of described hair conditioner, comprises the following steps:
A hydrolytic collagen mixes with part water by (), stirring and dissolving, obtains prefabricated B;
B polydimethylsiloxane, behenyl alcohol are added oil phase pot by (), stir and be warming up to 80 ~ 85 DEG C, and insulation 5 ~ 10min, obtains oil phase raw material;
C remaining water is added water preparation pot by (), open and stir, add hydroxyethyl-cellulose, be warming up to 70 ~ 80 DEG C, add mountain Yu base trimethyl ammonium chloride, continue to be warming up to 85 ~ 90 DEG C, add glycerol, hydrolysis Jojoba ester, butanediol, insulation 15 ~ 25min, obtains Aqueous Phase Raw Material;
D (), by Aqueous Phase Raw Material suction emulsifying pot, keep vacuum, high speed homogenization adds oil phase raw material simultaneously, after oil phase has added, continued homogenizing and be less than 2 μm to emulsified particles mean diameter, obtain mixture;
E () is opened and is stirred, be cooled to 35 DEG C ~ 40 DEG C, add prefabricated B, oligopeptide-1, Salix alba Extract and essence, mix homogeneously, obtain hair conditioner in the mixture of step (d).
Speed of agitator described in step (a) is 150rpm ~ 200rpm; The mass ratio of described hydrolytic collagen and pure water is 1:9.
Speed of agitator described in step (b) is 600rpm ~ 800rpm.
The rotating speed stirred described in step (c) is 200rpm ~ 300rpm; Keep the vacuum of vacuum for-0.03Mpa ~-0.05Mpa described in step (d); The rotating speed of described high speed homogenization is 10000rpm ~ 12000rpm.
Speed of agitator described in step (e) is 300rpm ~ 400rpm; Described incorporation time is 10 ~ 15min.
The hair conditioner that this method obtains is white white shape mastic, and PH is 4.5-5.0, and viscosity is 15000mpa.s ~ 20000mpa.s, and 45 DEG C heat-resisting 24 hours, and without significant change after recovery room temperature ,-18 DEG C are resisted cold 24 hours, without significant change after recovery room temperature.
Hydrolysis Jojoba ester to be mass fraction be 20% aqueous dispersions, there is good hair nursing and scalp care function, be purchased from FLORATECH company of the U.S..
Hydrolytic collagen is purchased from Cargill company of the U.S., is white powder, and mean molecule quantity is 3000 dalton; Supplementary scalp collagen content is act as to scalp, strengthens scalp elasticity of skin, nutrition skin.
Shampoo of the present invention and hair conditioner conbined usage not only can effectively clean reparation hair, can also be formed on hair a kind of uniform, have relative hardness, thin film that transparent air-permeable can wash away, this film hair can not only be made to look clear light is extremely attractive in appearance, more can play a protective role; Ventilative film can make hair eupnea, reduces the volatilization of moisture in hair, prevents dry and cracked, hair is freshened, smooth, and feel is better.And of the present invention washing is protected combination and can be nursed scalp, strengthen scalp skin collagen protein synthesis, what scalp was become is flexible, and promotes epidermal growth, repairing hair follicle.
Compared with prior art, the present invention has the following advantages and beneficial effect:
1, of the present invention washing is protected combination and is had good hair cleaning performance, and can repair impaired hair, such that hair is smooth, salubrious, good hand touch be convenient to combing; The present invention simultaneously can nurse scalp, and strengthen scalp skin collagen protein synthesis, what scalp was become is flexible, and promotes epidermal growth, repairing hair follicle, has the anti-ageing effect of good scalp, the material guarantee that the growth for hair provides the foundation;
2, the present invention carries out formulation composition optimization, and without sulfate, without the potential stimulation anaphylactogen such as anticorrosion, formula as mild as a dove.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, but embodiments of the present invention are not limited thereto.
Embodiment 1 shampoo
There is a shampoo for scalp anti-aging function, be prepared from by following raw material by mass percentage:
The preparation method of described shampoo:
(1) be 1:9 mixed at room temperature by hydrolytic collagen and pure water (i.e. water) with mass ratio, stir (rotating speed of stirring is 150rpm) gently and dissolve completely, obtain prefabricated A;
(2) under room temperature, remaining pure water is added water preparation pot, open and stir (rotating speed of stirring is 200rpm), add Polyquaternium-10, when being warming up to 70 DEG C, add cocamido propyl betaine, after stirring 5min, add cocoyl glutamic acid TEA salt again, when continuing stir and be warming up to 80 DEG C, add butanediol, glycerol, hydrolysis Jojoba ester, ceteareth-60 myristyl glycol, glycol distearate, after 80 DEG C of insulation 25min, the mastic that takes a morsel to be applied on microscope slide and to build coverslip, 400 times of observations are amplified with microscope 40 times of object lens, next step can be continued without after visible crystals,
(3) adjusting rotary speed (rotating speed of stirring is 100rpm), opens temperature lowering water and is cooled to 35 DEG C, add prefabricated A, Salix alba Extract, essence, continues to stir 10min, obtains the shampoo with scalp anti-aging function.
The shampoo outward appearance of gained is light yellow fine and smooth iridescent body; PH is 5.6, and viscosity is 6200mpa.s, and 45 DEG C heat-resisting 24 hours, and without significant change after recovery room temperature ,-18 DEG C are resisted cold 24 hours, without significant change after recovery room temperature.
Embodiment 2 shampoo
There is a shampoo for scalp anti-aging function, be prepared from by following raw material by mass percentage:
The preparation method of described shampoo:
(1) be 1:9 mixed at room temperature by hydrolytic collagen and pure water (i.e. water) with mass ratio, stir (rotating speed of stirring is 180rpm) gently and dissolve completely, obtain prefabricated A;
(2) under room temperature, remaining pure water is added water preparation pot, open and stir (rotating speed of stirring is 240rpm), add Polyquaternium-10, when being warming up to 75 DEG C, add cocamido propyl betaine, cocoyl glutamic acid TEA salt is added again after stirring 4min, continue can add butanediol when stirring and be warming up to 82 DEG C, glycerol, hydrolysis Jojoba ester, ceteareth-60 myristyl glycol, glycol distearate, after 82 DEG C of insulation 30min, the mastic that takes a morsel to be applied on microscope slide and to build coverslip, 400 times of observations are amplified with microscope 40 times of object lens, next step can be continued without after visible crystals,
(3) adjusting rotary speed (rotating speed of stirring is 150rpm), opens temperature lowering water and is cooled to 37 DEG C, add prefabricated A, Salix alba Extract, essence, continues to stir 12min, obtains the shampoo with scalp anti-aging function.
The shampoo outward appearance of gained is light yellow fine and smooth iridescent body; PH is 5.2, and viscosity is 6800mpa.s, and 45 DEG C heat-resisting 24 hours, and without significant change after recovery room temperature ,-18 DEG C are resisted cold 24 hours, without significant change after recovery room temperature.
Embodiment 3 shampoo
There is a shampoo for scalp anti-aging function, be prepared from by following raw material by mass percentage:
The preparation method of described shampoo:
(1) be 1:9 mixed at room temperature by hydrolytic collagen and pure water (i.e. water) with mass ratio, open stir (rotating speed is 150rpm) completely to be dissolved, obtain prefabricated A;
(2) under room temperature, remaining pure water is added water preparation pot, open and stir (rotating speed is 200rpm), add Polyquaternium-10, when being warming up to 80 DEG C, add cocamido propyl betaine, after stirring 5min, add cocoyl glutamic acid TEA salt again, when continuing stir and be warming up to 85 DEG C, add butanediol, glycerol, hydrolysis Jojoba ester, ceteareth-60 myristyl glycol, glycol distearate, after 85 DEG C of insulation 35min, the mastic that takes a morsel to be applied on microscope slide and to build coverslip, 400 times of observations are amplified with microscope 40 times of object lens, next step is continued without after visible crystals,
(3) adjusting rotary speed (rotating speed is 200rpm), opens temperature lowering water and is cooled to 40 DEG C, add prefabricated A, Salix alba Extract, essence, continues to stir 15min, obtains the shampoo with scalp anti-aging function.
The shampoo outward appearance of gained is light yellow fine and smooth iridescent body; PH is 5.3, and viscosity is 6700mpa.s, and 45 DEG C heat-resisting 24 hours, and without significant change after recovery room temperature ,-18 DEG C are resisted cold 24 hours, without significant change after recovery room temperature.
Embodiment 4 hair conditioner
There is a hair conditioner for scalp anti-aging function, be prepared from by following raw material by mass percentage:
The preparation method of described hair conditioner:
(1) be 1:9 mixed at room temperature by hydrolytic collagen and pure water (i.e. water) with mass ratio, stir gently (rotating speed of stirring is 150rpm) completely to be dissolved, obtain prefabricated B;
(2) polydimethylsiloxane, behenyl alcohol are added oil phase pot, open and stir (rotating speed of stirring is 600rpm), be warming up to 85 DEG C, insulation 5min, obtains oil phase raw material;
(3) under room temperature, remaining pure water is added water preparation pot, open and stir (rotating speed of stirring is 200rpm), and add hydroxyethyl-cellulose, when being warming up to 70 DEG C, add mountain Yu base trimethyl ammonium chloride, continue to be warming up to 85 DEG C, add glycerol, hydrolysis Jojoba ester, butanediol, 85 DEG C of insulation 20min, obtain Aqueous Phase Raw Material;
(4) by Aqueous Phase Raw Material suction emulsifying pot, keep vacuum-0.03Mpa, high speed homogenization limit, limit adds oil phase raw material (homogenizing speed is 11000rpm), after oil phase has added, continue homogenizing extremely: emulsified particles mean diameter is less than 2 μm and gets final product (amplifying 400 times of observations with microscope);
(5) stir (rotating speed of stirring is 300rpm) and be cooled to 35 DEG C, add prefabricated B, oligopeptide-1, Salix alba Extract, essence, stir 10min, obtain the hair conditioner with scalp anti-aging function.
The hair conditioner that this method obtains is white white shape mastic, and PH is 4.6, and viscosity is 15500mpa.s, and 45 DEG C heat-resisting 24 hours, and without significant change after recovery room temperature ,-18 DEG C are resisted cold 24 hours, without significant change after recovery room temperature.
Embodiment 5 hair conditioner
There is a hair conditioner for scalp anti-aging function, be prepared from by following raw material by mass percentage:
The preparation method of described hair conditioner:
(1) be 1:9 mixed at room temperature by hydrolytic collagen and pure water (i.e. water) with mass ratio, stir gently (rotating speed of stirring is 180rpm) completely to be dissolved, obtain prefabricated B;
(2) polydimethylsiloxane, behenyl alcohol are added oil phase pot, open and stir (rotating speed of stirring is 700rpm), be warming up to 82 DEG C, insulation 7min, obtains oil phase raw material;
(3) under room temperature, remaining pure water is added water preparation pot, open and stir (rotating speed of stirring is 250rpm), and add hydroxyethyl-cellulose, when being warming up to 75 DEG C, add mountain Yu base trimethyl ammonium chloride, continue to be warming up to 87 DEG C, add glycerol, hydrolysis Jojoba ester, butanediol, 87 DEG C of insulation 20min, obtain Aqueous Phase Raw Material;
(4) by Aqueous Phase Raw Material suction emulsifying pot, keep vacuum-0.04Mpa, high speed homogenization limit, limit adds oil phase raw material (homogenizing speed is 11000rpm), after oil phase has added, continue homogenizing extremely: emulsified particles mean diameter is less than 2 μm and gets final product (amplifying 400 times of observations with microscope);
(5) stir (rotating speed of stirring is 350rpm) and be cooled to 35 DEG C, add prefabricated B, oligopeptide-1, Salix alba Extract, essence, stir 12min, obtain the hair conditioner with scalp anti-aging function.
The hair conditioner that this method obtains is white white shape mastic, and PH is 4.5, and viscosity is 18500mpa.s, and 45 DEG C heat-resisting 24 hours, and without significant change after recovery room temperature ,-18 DEG C are resisted cold 24 hours, without significant change after recovery room temperature.
Embodiment 6 hair conditioner
There is a hair conditioner for scalp anti-aging function, be prepared from by following raw material by mass percentage:
The preparation method of described hair conditioner: hydrolytic collagen and pure water (i.e. water) are 1:9 mixed at room temperature with mass ratio by (1), stir gently (rotating speed of stirring is 200rpm) completely to be dissolved, obtain prefabricated B;
(2) polydimethylsiloxane, behenyl alcohol are added oil phase pot, open and stir (rotating speed of stirring is 800rpm), be warming up to 85 DEG C, insulation 10min, obtains oil phase raw material;
(3) under room temperature, remaining pure water is added water preparation pot, open and stir (rotating speed of stirring is 300rpm), and add hydroxyethyl-cellulose, when being warming up to 80 DEG C, add mountain Yu base trimethyl ammonium chloride, continue to be warming up to 90 DEG C, add glycerol, hydrolysis Jojoba ester, butanediol, 90 DEG C of insulation 15min, obtain Aqueous Phase Raw Material;
(4) by Aqueous Phase Raw Material suction emulsifying pot, keep vacuum-0.05Mpa, high speed homogenization limit, limit adds oil phase raw material (homogenizing speed is 12000rpm), after oil phase has added, continue homogenizing extremely: emulsified particles mean diameter is less than 2 μm and gets final product (amplifying 400 times of observations with microscope);
(5) stir (rotating speed of stirring is 400rpm) and be cooled to 40 DEG C, add prefabricated B, oligopeptide-1, Salix alba Extract, essence, stir 15min, obtain the hair conditioner with scalp anti-aging function.
The hair conditioner that this method obtains is white white shape mastic, and PH is 4.8, and viscosity is 17000mpa.s, and 45 DEG C heat-resisting 24 hours, and without significant change after recovery room temperature ,-18 DEG C are resisted cold 24 hours, without significant change after recovery room temperature.
Performance test:
1, the product of embodiment 1 ~ 6 is carried out Microbial Challenge test, the results are shown in subordinate list 1 ~ 6:
Subordinate list 1: embodiment 1 shampoo
Subordinate list 2: embodiment 2 shampoo
Subordinate list 3: embodiment 3 shampoo
Subordinate list 4: embodiment 4 hair conditioner
Subordinate list 5: embodiment 5 hair conditioner
Subordinate list 6: embodiment 6 hair conditioner
Detection method: American Pharmacopeia USP32 (51) antimicrobial preservation efficacy test
Antibacterial: Pseudomonas aeruginosa (Pseudomonas aeruginosa) ATCC 9027
Colon bacillus (Escherichia coli) ATCC 8739
Staphylococcus aureus (Staphylococcus aureus) ATCC 6538
Mycete and yeast: candida albicans (Candida albicans) ATCC 10231
Aspergillus niger (Aspergillus niger) ATCC 16404
Result all shows, and the control ability of the microorganism of product is good.
2, the product of embodiment 1 ~ 6 is clearly felt, the test of reflecting feel, cardability and defying age performance: at random embodiment 1 ~ 6 is combined:
Shampoo embodiment 1 and hair conditioner embodiment 5 are combined into: wash and protect combination 1;
Shampoo embodiment 2 and hair conditioner embodiment 4 are combined into: wash and protect combination 2;
Shampoo embodiment 3 and hair conditioner embodiment 6 are combined into: wash and protect combination 3;
Random from buying three kinds of shampoos and three kinds of hair conditioner and six kinds of embodiment random combines on the market in addition:
Commercial shampoos 1 and hair conditioner embodiment 4 are combined into: wash and protect combination 4;
Commercial shampoos 2 and hair conditioner embodiment 6 are combined into: wash and protect combination 5;
Commercial shampoos 3 and hair conditioner embodiment 5 are combined into: wash and protect combination 6;
Commercially available hair conditioner 1 is combined into shampoo embodiment 2: wash and protect combination 7;
Commercially available hair conditioner 2 is combined into shampoo embodiment 3: wash and protect combination 8;
Commercially available hair conditioner 3 is combined into shampoo embodiment 1: wash and protect combination 9;
2-1, above 9 groups washed to protect combination wet and send out carding property and hair drying comb rationality can be tested, and dry salubrious sense when sending out and reflecting feel are evaluated, test result is as shown in subordinate list 7:
Subordinate list 7
Illustrate:
1, the test of dry, wet carding force employing American I nstron 5565 universal material tester, constant temperature 25 DEG C, under the condition of humidity 60%, material of measuring and monitoring the growth of standing timber is true man's topknot, and comb material is nylon plastic(s), tooth pitch 1mm, surface roughness 3.2, the relative displacement of topknot and comb is 600mm/min, and combing direction is that topknot naturally droops, without pre-tension along scale; The less expression carding property of carding force numerical value is better, and hair is more smooth.
2, dry salubrious sense and reflecting feel (reflecting feel score value is higher, represents that the degree that hair is repaired is better) score value illustrate: ten point system evaluation criterion, 1 point the poorest, and 10 points best, and the higher expression effect of score value is better.
Experimenter 36, at 25 years old-55 years old age, dryness, oiliness, normal hair all contain, random packet.
Using method: first use clear water moistening hair; Get appropriate shampoo on both hands, be placed on after rubbing foam on head and rub gently, can foam be produced, do not need too firmly to rub hair with the hands, stop about 1min; During flushing, also applying finger is smoothed out with the fingers straight peen gently and is sent out and rinse; After the foam that floods to be washed is rinsed well, get appropriate hair conditioner uniform application on hair and scalp, massaging scalp 3 ~ 5min gently, then rinse well with clear water.
Result shows, and washing in the present invention protects the repairing performance that combination other products more on the market has better carding property, better salubrious property and Geng Gao.
2-2, evaluate defying age (scalp elasticity, the hair follicle health degree) effect of scalp, evaluation result is as shown in subordinate list 8,9:
Subordinate list 8
Subordinate list 9:
Score value illustrates: ten point system evaluation criterion, 1 point the poorest, and 10 points best, and score value higher expression effect is more obvious.Experimenter 45,25 years old-55 years old age, random packet.Life cycle is 2 months.
Using method: first use clear water moistening hair; Get appropriate shampoo on both hands, be placed on after rubbing foam on head and rub gently, can foam be produced, do not need too firmly to rub hair with the hands, stop about 1min; During flushing, also applying finger is smoothed out with the fingers straight peen gently and is sent out and rinse; After the foam that floods to be washed is rinsed well, get appropriate hair conditioner uniform application on hair and scalp, massaging scalp 3 ~ 5min gently, then rinse well with clear water.
Result show, of the present invention three groups wash protect combination correct leatherware have good nursing function.
Shampoo in the present invention, is clean composition with Oleum Cocois source with the gentle surfactant of origin of amino acid, adopt quaternary ammonium salt conditioner, the esters in Jojoba oil source, the hydrolytic collagen in marine fishes source carry out nourishing scalp, scalp anti-aging function, and adopt the plant antipathogenic composition Salix alba Extract with hair conditioning function antibacterial, shampoo of the present invention is without sulfate, preservative free system, gentle non-stimulated, and there is scalp anti-aging function, formula is simple, easy to operate, effect is remarkable.
Hair conditioner in the present invention, be main hair nursing composition with polydimethylsiloxane and mountain Yu base trimethyl ammonium chloride, with two Lauryl Alcohols for stable system composition, the hydrolytic collagen of originating with the esters in Jojoba oil source and marine fishes and oligopeptide-1 carry out nourishing scalp, scalp anti-aging function, and adopting the plant antipathogenic composition Salix alba Extract with hair conditioning function antibacterial, formula is simple, easy to operate, effect is remarkable.
Above-described embodiment is the present invention's preferably embodiment; but embodiments of the present invention are not restricted to the described embodiments; change, the modification done under other any does not deviate from spirit of the present invention and principle, substitute, combine, simplify; all should be the substitute mode of equivalence, be included within protection scope of the present invention.
Claims (10)
1. there is washing of scalp anti-aging function and protect a combination, it is characterized in that: be made up of shampoo and hair conditioner;
Described shampoo, be prepared from by following raw material by mass percentage: 8.5% ~ 12.5% cocamido propyl betaine, 9% ~ 12% cocoyl glutamic acid TEA salt, 5% ~ 10% glycerol, 3% ~ 6% butanediol, 0.5% ~ 0.8% Polyquaternium-10,3% ~ 5% hydrolysis Jojoba ester, 3% ~ 5% ceteareth-60 myristyl glycol, 1% ~ 2% glycol distearate, 0.5% ~ 1.0% hydrolytic collagen, 0.4% ~ 0.6% Salix alba Extract, 0.3% ~ 0.4% essence and excess water;
Described hair conditioner, be prepared from by following raw material by mass percentage: 8% ~ 10% polydimethylsiloxane, 3% ~ 5% behenyl alcohol, 0.3% ~ 0.5% hydroxyethyl-cellulose, 2% ~ 3% mountain Yu base trimethyl ammonium chloride, 5% ~ 10% butanediol, 10% ~ 15% glycerol, 4% ~ 6% hydrolysis Jojoba ester, 1% ~ 1.5% hydrolytic collagen, 0.001% ~ 0.0015% oligopeptide-1,0.6% ~ 0.8% Salix alba Extract, 0.3% ~ 0.4% essence and excess water.
2. what have scalp anti-aging function according to claim 1 washes the preparation method of protecting combination, it is characterized in that: the preparation method comprising shampoo, and concrete steps are:
(1) hydrolytic collagen is mixed with part water, stirring and dissolving, obtain prefabricated solution A;
(2) remaining water is added in reactor, open and stir, add Polyquaternium-10, be warming up to 70 DEG C ~ 80 DEG C, add cocamido propyl betaine, stir 3 ~ 5min, add cocoyl glutamic acid TEA salt, continue stir and be warming up to 80 ~ 85 DEG C, add butanediol, glycerol, hydrolysis Jojoba ester, ceteareth-60 myristyl glycol, glycol distearate again, after insulation 25 ~ 35min, with microscopic examination, when carrying out next step without during visible crystals;
(3) adjusting rotary speed, is cooled to 35 ~ 40 DEG C, adds prefabricated A, Salix alba Extract, essence, stirs, obtain shampoo.
3. what have scalp anti-aging function according to claim 2 washes the preparation method of protecting combination, it is characterized in that: described in step (1), speed of agitator is 150rpm ~ 200rpm; The mass ratio of described hydrolytic collagen and part water is 1:9.
4. what have scalp anti-aging function according to claim 2 washes the preparation method of protecting combination, it is characterized in that: described in step (2), speed of agitator is 200rpm ~ 300rpm.
5. what have scalp anti-aging function according to claim 2 washes the preparation method of protecting combination, it is characterized in that: the rotating speed regulated described in step (3) is 100rpm ~ 200rpm; The described time stirred is 10min ~ 15min.
6. what have scalp anti-aging function according to claim 1 washes the preparation method of protecting combination, it is characterized in that: the preparation method comprising hair conditioner, and concrete steps are:
A hydrolytic collagen mixes with part water by (), stirring and dissolving, obtains prefabricated B;
B polydimethylsiloxane, behenyl alcohol are added oil phase pot by (), stir and be warming up to 80 ~ 85 DEG C, and insulation 5 ~ 10min, obtains oil phase raw material;
C remaining water is added water preparation pot by (), open and stir, add hydroxyethyl-cellulose, be warming up to 70 ~ 80 DEG C, add mountain Yu base trimethyl ammonium chloride, continue to be warming up to 85 ~ 90 DEG C, add glycerol, hydrolysis Jojoba ester, butanediol, insulation 15 ~ 25min, obtains Aqueous Phase Raw Material;
D (), by Aqueous Phase Raw Material suction emulsifying pot, keep vacuum, high speed homogenization adds oil phase raw material simultaneously, after oil phase has added, continued homogenizing and be less than 2 μm to emulsified particles mean diameter, obtain mixture;
E () is opened and is stirred, be cooled to 35 DEG C ~ 40 DEG C, add prefabricated B, oligopeptide-1, Salix alba Extract and essence, mix homogeneously, obtain hair conditioner in the mixture of step (d).
7. what have scalp anti-aging function according to claim 6 washes the preparation method of protecting combination, it is characterized in that: speed of agitator described in step (a) is 150rpm ~ 200rpm; The mass ratio of described hydrolytic collagen and part water is 1:9.
8. what have scalp anti-aging function according to claim 6 washes the preparation method of protecting combination, it is characterized in that: speed of agitator described in step (b) is 600rpm ~ 800rpm;
The rotating speed stirred described in step (c) is 200rpm ~ 300rpm.
9. what have scalp anti-aging function according to claim 6 washes the preparation method of protecting combination, it is characterized in that: keep the vacuum of vacuum for-0.03Mpa ~-0.05Mpa described in step (d); The rotating speed of described high speed homogenization is 10000rpm ~ 12000rpm.
10. what have scalp anti-aging function according to claim 6 washes the preparation method of protecting combination, it is characterized in that: speed of agitator described in step (e) is 300rpm ~ 400rpm; Described incorporation time is 10 ~ 15min.
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Cited By (5)
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| CN107468570A (en) * | 2017-08-25 | 2017-12-15 | 广西和桂集团有限公司 | Traditional Chinese medicine hair conditioner and preparation method thereof |
| CN109303731A (en) * | 2018-11-26 | 2019-02-05 | 庄雪芸 | A kind of shampoo formula with scalp anti-aging function |
| CN113509406A (en) * | 2021-06-07 | 2021-10-19 | 泉后(广州)生物科技研究院有限公司 | Semi-permeable gel liquid crystal hair mask and preparation method thereof |
| CN114533608A (en) * | 2022-01-17 | 2022-05-27 | 广州环亚化妆品科技股份有限公司 | Scalp anti-sensitivity composition and preparation method and application thereof |
| CN116473884A (en) * | 2022-09-21 | 2023-07-25 | 百肽德医药生物科技(广东)有限公司 | Cell membrane complex hair care factor and hair conditioner thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107468570A (en) * | 2017-08-25 | 2017-12-15 | 广西和桂集团有限公司 | Traditional Chinese medicine hair conditioner and preparation method thereof |
| CN109303731A (en) * | 2018-11-26 | 2019-02-05 | 庄雪芸 | A kind of shampoo formula with scalp anti-aging function |
| CN113509406A (en) * | 2021-06-07 | 2021-10-19 | 泉后(广州)生物科技研究院有限公司 | Semi-permeable gel liquid crystal hair mask and preparation method thereof |
| CN114533608A (en) * | 2022-01-17 | 2022-05-27 | 广州环亚化妆品科技股份有限公司 | Scalp anti-sensitivity composition and preparation method and application thereof |
| CN116473884A (en) * | 2022-09-21 | 2023-07-25 | 百肽德医药生物科技(广东)有限公司 | Cell membrane complex hair care factor and hair conditioner thereof |
| CN116473884B (en) * | 2022-09-21 | 2024-03-05 | 百肽德医药生物科技(广东)有限公司 | Cell membrane complex hair care factor and hair conditioner thereof |
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