CN104177888B - A kind of preparation technology of cable anticorrosive paint - Google Patents
A kind of preparation technology of cable anticorrosive paint Download PDFInfo
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- CN104177888B CN104177888B CN201410454747.4A CN201410454747A CN104177888B CN 104177888 B CN104177888 B CN 104177888B CN 201410454747 A CN201410454747 A CN 201410454747A CN 104177888 B CN104177888 B CN 104177888B
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- 239000003973 paint Substances 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 239000000463 material Substances 0.000 claims abstract description 33
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 13
- 238000003756 stirring Methods 0.000 claims abstract description 13
- 238000000034 method Methods 0.000 claims abstract description 10
- 238000001816 cooling Methods 0.000 claims abstract description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 24
- 239000000843 powder Substances 0.000 claims description 12
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 8
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 8
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims description 8
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims description 8
- 239000006004 Quartz sand Substances 0.000 claims description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 8
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 8
- 239000000440 bentonite Substances 0.000 claims description 8
- 229910000278 bentonite Inorganic materials 0.000 claims description 8
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 8
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical class CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims description 8
- NKSJNEHGWDZZQF-UHFFFAOYSA-N ethenyl(trimethoxy)silane Chemical compound CO[Si](OC)(OC)C=C NKSJNEHGWDZZQF-UHFFFAOYSA-N 0.000 claims description 8
- 239000010439 graphite Substances 0.000 claims description 8
- 229910002804 graphite Inorganic materials 0.000 claims description 8
- 229910052744 lithium Inorganic materials 0.000 claims description 8
- 239000005543 nano-size silicon particle Substances 0.000 claims description 8
- XNGIFLGASWRNHJ-UHFFFAOYSA-N o-dicarboxybenzene Natural products OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 claims description 8
- 239000002245 particle Substances 0.000 claims description 8
- -1 phthalic acid ester Chemical class 0.000 claims description 8
- 229920002379 silicone rubber Polymers 0.000 claims description 8
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 8
- 239000012467 final product Substances 0.000 claims description 4
- 238000009776 industrial production Methods 0.000 abstract description 2
- 239000011248 coating agent Substances 0.000 description 11
- 238000000576 coating method Methods 0.000 description 11
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
- 239000010410 layer Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 2
- 230000001070 adhesive effect Effects 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 230000007257 malfunction Effects 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 238000012946 outsourcing Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000011241 protective layer Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 238000010850 salt effect Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
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- Paints Or Removers (AREA)
- Organic Insulating Materials (AREA)
- Insulated Conductors (AREA)
Abstract
The invention belongs to paint field, disclose a kind of preparation technology of cable anticorrosive paint, this technique comprises the steps: that step 1) prepares base-material, step 2) prepare auxiliary agent, step 3) prepares nanometer auxiliary material and step 4) stirs cooling. Preparation technology of the present invention is easy, and using method is simple, and material combination is reasonable, and anticorrosion ability is good, is applicable to large-scale industrial production.
Description
Technical field
The invention belongs to paint field, be specifically related to a kind of preparation technology of cable anticorrosive paint.
Background technology
In electric power system, power cable is important transmission line of electricity, and its conductor by one or more mutually insulated and outsourcing insulating protective layer are made, by electric power or information from a wire that is transferred to another place. Power cable is under outdoor environment, especially under damp and hot weather conditions or the more serious region of acid-alkali salt effect, aging, burn into disrepair phenomenon very easily occurs, easily cause transmission line malfunction, bring greater impact to the normal production of people and life, also cause larger loss to power department. In order to overcome above-mentioned defect, there is cable anticorrosive paint in prior art, general hot spray painted zinc or the method such as zinc-plated of adopting brushed, and part adopts anticorrosive paint brushing, and the problem of its existence is: anticorrosion matrix processing requirements is high, film is blocked up easy to crack, when film curing, be subject to temperature, humidity effect larger, hardening time is long, and mostly exists weatherability poor, the shortcoming that cohesive force is not strong, therefore antiseptic property is generally undesirable.
Nanometer technology (nanotechnology) is to manufacture the science and technology of material, character and the application of research structure size material in 1 to 100 nanometer range with single atom, molecule. Nanometer is the least unit of length metering, the length of 1 nanometer be 1 millimeter 1,000,000/, directly assemble with the atom, atomic group, molecule, the micel that form various elements and material the high-quality precision and sophisticated technology that there is the material of specific function or there is special performance product. Successfully nanometer technology can be applicable to the every field such as electronics, chemical industry, military affairs, and countries in the world are all in research and development. Application of micron, in coating, is mainly to utilize the two vegetables mechanism of lotus leaf, improves resistance to water and the anti-fungi performance of coating. As coating, it is to be become to be grouped into by number of chemical, and through science preparation, unique physical and chemical reaction forms, if formula and technique are unreasonable, even if add some nanoscale raw materials, does not also have too large raising in quality, can cause on the contrary the raising of industrial cost.
Summary of the invention
In order to overcome cable material anticorrosive coating complicated process of preparation in prior art, the defect such as anticorrosion effect is poor, the invention provides a kind of preparation technology of cable anticorrosive paint.
For achieving the above object, the technical solution adopted in the present invention is as follows:
A preparation technology for cable anticorrosive paint, this technique comprises the steps:
Step 1) is prepared base-material: in reactor, add successively acrylic acid, 1-METHYLPYRROLIDONE, vinyltrimethoxy silane, ethoxylated dodecyl alcohol, acetone and phthalic acid ester, 1000 turn/min stir 3 minutes, obtain base-material; The weight ratio of acrylic acid, 1-METHYLPYRROLIDONE, vinyltrimethoxy silane, ethoxylated dodecyl alcohol, acetone and phthalic acid ester is 5:3:3:2:1:1;
Step 2) prepare auxiliary agent: quartz sand, white graphite and lithium bentonite are delivered to ball mill, and being milled to particle diameter is powder more than 500 orders, is auxiliary agent; The weight ratio of quartz sand, white graphite and lithium bentonite is 1:1:1;
Step 3) is prepared nanometer auxiliary material: nano-silicon rubber powder and nano titanium oxide are mixed according to the weight ratio of 1:1, be nanometer auxiliary material;
Step 4) stirs cooling: base-material, auxiliary agent and nanometer auxiliary material are mixed according to the weight ratio of 15-20:2-3:1-2, then put in high speed dispersor and stir, then the hygrothermal environment that to be placed in temperature and to be 60 DEG C, relative humidity be 80% 12 hours, finally be cooled to room temperature, pack and get final product.
Preferably, the particle diameter of nano-silicon rubber powder or nano titanium oxide is 10-100nm.
Occupation mode: power cable is soaked in to 10-15 minute in coating, takes out and dry.
The present invention obtain beneficial effect mainly comprise following some:
Anticorrosive paint preparation technology of the present invention is easy, and using method is simple, and material combination is reasonable, and industrial cost is low, is applicable to large-scale industrial production; The present invention, by adding a certain amount of nano material, together with its special molecular structure can closely be fitted to each raw material, and has filled up the space between each raw material, makes coating top layer smooth; Coating of the present invention possesses good anti-acid-alkali salt character, in the service life of having improved power cable, has reduced the generation of potential safety hazard.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the present invention is further detailed explanation, but should not regard the restriction to initiative spirit of the present invention as.
Embodiment 1
A preparation technology for cable anticorrosive paint, this technique comprises the steps:
Step 1) is prepared base-material: in reactor, add successively acrylic acid, 1-METHYLPYRROLIDONE, vinyltrimethoxy silane, ethoxylated dodecyl alcohol, acetone and phthalic acid ester, 1000 turn/min stir 3 minutes, obtain base-material; The weight ratio of acrylic acid, 1-METHYLPYRROLIDONE, vinyltrimethoxy silane, ethoxylated dodecyl alcohol, acetone and phthalic acid ester is 5:3:3:2:1:1;
Step 2) prepare auxiliary agent: quartz sand, white graphite and lithium bentonite are delivered to ball mill, and being milled to particle diameter is powder more than 500 orders, is auxiliary agent; The weight ratio of quartz sand, white graphite and lithium bentonite is 1:1:1;
Step 3) is prepared nanometer auxiliary material: nano-silicon rubber powder and nano titanium oxide are mixed according to the weight ratio of 1:1, be nanometer auxiliary material;
Step 4) stirs cooling: base-material, auxiliary agent and nanometer auxiliary material are mixed according to the weight ratio of 15:2:1, then put in high speed dispersor and stir, then the hygrothermal environment that to be placed in temperature and to be 60 DEG C, relative humidity be 80% 12 hours, is finally cooled to room temperature, packs and get final product.
Wherein, the particle diameter of nano-silicon rubber powder or nano titanium oxide is 20nm.
Occupation mode: power cable is soaked in coating to 10 minutes, takes out and dry.
Use the cable top layer performance parameter of anticorrosive paint as follows: thickness is 80um, and be 43min drying time, and Vickers hardness is 20.7, uses respectively 10%H2SO4, 10%NaOH and 10% sodium chloride soak 100 hours, and coating surface is unchanged, 0 grade of adhesive force.
Embodiment 2
A preparation technology for cable anticorrosive paint, this technique comprises the steps:
Step 1) is prepared base-material: in reactor, add successively acrylic acid, 1-METHYLPYRROLIDONE, vinyltrimethoxy silane, ethoxylated dodecyl alcohol, acetone and phthalic acid ester, 1000 turn/min stir 3 minutes, obtain base-material; The weight ratio of acrylic acid, 1-METHYLPYRROLIDONE, vinyltrimethoxy silane, ethoxylated dodecyl alcohol, acetone and phthalic acid ester is 5:3:3:2:1:1;
Step 2) prepare auxiliary agent: quartz sand, white graphite and lithium bentonite are delivered to ball mill, and being milled to particle diameter is powder more than 500 orders, is auxiliary agent; The weight ratio of quartz sand, white graphite and lithium bentonite is 1:1:1;
Step 3) is prepared nanometer auxiliary material: nano-silicon rubber powder and nano titanium oxide are mixed according to the weight ratio of 1:1, be nanometer auxiliary material;
Step 4) stirs cooling: base-material, auxiliary agent and nanometer auxiliary material are mixed according to the weight ratio of 20:3:2, then put in high speed dispersor and stir, then the hygrothermal environment that to be placed in temperature and to be 60 DEG C, relative humidity be 80% 12 hours, is finally cooled to room temperature, packs and get final product.
Wherein, the particle diameter of nano-silicon rubber powder or nano titanium oxide is 50nm.
Occupation mode: power cable is soaked in coating to 15 minutes, takes out and dry.
Use the cable top layer performance parameter of anticorrosive paint as follows: thickness is 80um, and be 45min drying time, and Vickers hardness is 21.3, uses respectively 10%H2SO4, 10%NaOH and 10% sodium chloride soak 100 hours, and coating surface is unchanged, 0 grade of adhesive force.
What certainly note is, although carried out description above by example of the present invention, the present invention is made by those skilled in the art apparent like this and other improvement and change should think and fall into as in broad range of the present invention in this paper. Therefore, although the present invention with reference to be preferred embodiment described,, its meaning is not that the product of tool novelty is restricted therefrom, on the contrary, it is intended to comprise various improvement and equivalent modifications within the broad range that meets above-mentioned open part, claim.
Claims (1)
1. a preparation technology for cable anticorrosive paint, is characterized in that, described technique comprises the steps:
Step 1) is prepared base-material: in reactor, add successively acrylic acid, 1-METHYLPYRROLIDONE, vinyltrimethoxy silane, ethoxylated dodecyl alcohol, acetone and phthalic acid ester, 1000 turn/min stir 3 minutes, obtain base-material; The weight ratio of acrylic acid, 1-METHYLPYRROLIDONE, vinyltrimethoxy silane, ethoxylated dodecyl alcohol, acetone and phthalic acid ester is 5:3:3:2:1:1;
Step 2) prepare auxiliary agent: quartz sand, white graphite and lithium bentonite are delivered to ball mill, and being milled to particle diameter is powder more than 500 orders, is auxiliary agent; The weight ratio of quartz sand, white graphite and lithium bentonite is 1:1:1;
Step 3) is prepared nanometer auxiliary material: nano-silicon rubber powder and nano titanium oxide are mixed according to the weight ratio of 1:1, be nanometer auxiliary material; Wherein, the particle diameter of nano-silicon rubber powder or nano titanium oxide is 10-100nm;
Step 4) stirs cooling: base-material, auxiliary agent and nanometer auxiliary material are mixed according to the weight ratio of 15-20:2-3:1-2, then put in high speed dispersor and stir, then the hygrothermal environment that to be placed in temperature and to be 60 DEG C, relative humidity be 80% 12 hours, finally be cooled to room temperature, pack and get final product.
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| CN201410454747.4A CN104177888B (en) | 2014-09-09 | 2014-09-09 | A kind of preparation technology of cable anticorrosive paint |
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| CN201410454747.4A CN104177888B (en) | 2014-09-09 | 2014-09-09 | A kind of preparation technology of cable anticorrosive paint |
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| CN104177888B true CN104177888B (en) | 2016-05-04 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104962114A (en) * | 2015-05-11 | 2015-10-07 | 江苏士林电气设备有限公司 | Tubular bus-bar anticorrosion paint preparation method |
| CN105504908A (en) * | 2015-08-24 | 2016-04-20 | 国网山东省电力公司临沂供电公司 | Method for preventing high voltage line rod corrosion |
| CN108610665A (en) * | 2016-12-02 | 2018-10-02 | 张连瑞 | A kind of preparation method of pylon anticorrosive coating |
| CN108610686A (en) * | 2016-12-03 | 2018-10-02 | 刘杰 | A kind of preparation process of electric power material antiseptic agent |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103756458A (en) * | 2014-01-14 | 2014-04-30 | 李保国 | Environmental-friendly anticorrosive paint for power transmission line |
| CN104098973A (en) * | 2014-07-04 | 2014-10-15 | 国家电网公司 | Anticorrosive paint adopting nano-materials and used for power cable |
| CN104151882A (en) * | 2014-07-31 | 2014-11-19 | 国家电网公司 | Anticorrosive paint for power cables |
| CN104151893A (en) * | 2014-08-25 | 2014-11-19 | 国家电网公司 | Paint used for preventing corrosion on electricity material |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| JPH0670192B2 (en) * | 1984-05-14 | 1994-09-07 | 東亞合成化学工業株式会社 | Metal anticorrosion composition |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103756458A (en) * | 2014-01-14 | 2014-04-30 | 李保国 | Environmental-friendly anticorrosive paint for power transmission line |
| CN104098973A (en) * | 2014-07-04 | 2014-10-15 | 国家电网公司 | Anticorrosive paint adopting nano-materials and used for power cable |
| CN104151882A (en) * | 2014-07-31 | 2014-11-19 | 国家电网公司 | Anticorrosive paint for power cables |
| CN104151893A (en) * | 2014-08-25 | 2014-11-19 | 国家电网公司 | Paint used for preventing corrosion on electricity material |
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