CA2676412C - Degommage enzymatique utilisant un melange de phospholipases pla et plc - Google Patents
Degommage enzymatique utilisant un melange de phospholipases pla et plc Download PDFInfo
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- CA2676412C CA2676412C CA2676412A CA2676412A CA2676412C CA 2676412 C CA2676412 C CA 2676412C CA 2676412 A CA2676412 A CA 2676412A CA 2676412 A CA2676412 A CA 2676412A CA 2676412 C CA2676412 C CA 2676412C
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- oil
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- 239000000203 mixture Substances 0.000 title claims abstract description 219
- 102000015439 Phospholipases Human genes 0.000 title claims abstract description 48
- 108010064785 Phospholipases Proteins 0.000 title claims abstract description 48
- 230000002255 enzymatic effect Effects 0.000 title description 33
- 208000034530 PLAA-associated neurodevelopmental disease Diseases 0.000 title description 5
- 102000004190 Enzymes Human genes 0.000 claims abstract description 194
- 108090000790 Enzymes Proteins 0.000 claims abstract description 194
- 102000014384 Type C Phospholipases Human genes 0.000 claims abstract description 145
- 108010079194 Type C Phospholipases Proteins 0.000 claims abstract description 145
- 238000000034 method Methods 0.000 claims abstract description 115
- 150000003904 phospholipids Chemical class 0.000 claims abstract description 100
- 238000006243 chemical reaction Methods 0.000 claims abstract description 59
- ZIIUUSVHCHPIQD-UHFFFAOYSA-N 2,4,6-trimethyl-N-[3-(trifluoromethyl)phenyl]benzenesulfonamide Chemical compound CC1=CC(C)=CC(C)=C1S(=O)(=O)NC1=CC=CC(C(F)(F)F)=C1 ZIIUUSVHCHPIQD-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000007795 chemical reaction product Substances 0.000 claims abstract description 7
- 238000000926 separation method Methods 0.000 claims abstract description 5
- 239000003921 oil Substances 0.000 claims description 407
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 claims description 134
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 44
- 108010058864 Phospholipases A2 Proteins 0.000 claims description 13
- 239000010779 crude oil Substances 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 9
- 102000006486 Phosphoinositide Phospholipase C Human genes 0.000 claims description 4
- 108010044302 Phosphoinositide phospholipase C Proteins 0.000 claims description 4
- 235000019198 oils Nutrition 0.000 description 391
- 229940088598 enzyme Drugs 0.000 description 169
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 165
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 99
- 206010001497 Agitation Diseases 0.000 description 98
- 238000013019 agitation Methods 0.000 description 97
- 239000000243 solution Substances 0.000 description 60
- 102000004882 Lipase Human genes 0.000 description 56
- 108090001060 Lipase Proteins 0.000 description 56
- 239000004367 Lipase Substances 0.000 description 56
- 235000019421 lipase Nutrition 0.000 description 56
- 235000012424 soybean oil Nutrition 0.000 description 41
- 239000003549 soybean oil Substances 0.000 description 41
- 239000008367 deionised water Substances 0.000 description 39
- 239000003518 caustics Substances 0.000 description 35
- 230000035484 reaction time Effects 0.000 description 34
- 239000000872 buffer Substances 0.000 description 27
- 239000002253 acid Substances 0.000 description 19
- 230000000694 effects Effects 0.000 description 16
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- 230000007935 neutral effect Effects 0.000 description 15
- 238000007670 refining Methods 0.000 description 15
- 239000000047 product Substances 0.000 description 13
- 235000015112 vegetable and seed oil Nutrition 0.000 description 12
- 239000008158 vegetable oil Substances 0.000 description 12
- 102100037611 Lysophospholipase Human genes 0.000 description 11
- 239000000787 lecithin Substances 0.000 description 9
- 235000010445 lecithin Nutrition 0.000 description 9
- 238000009875 water degumming Methods 0.000 description 9
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 8
- 125000000524 functional group Chemical group 0.000 description 8
- 239000011574 phosphorus Substances 0.000 description 8
- 229910052698 phosphorus Inorganic materials 0.000 description 8
- 238000012545 processing Methods 0.000 description 8
- PORPENFLTBBHSG-MGBGTMOVSA-N 1,2-dihexadecanoyl-sn-glycerol-3-phosphate Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP(O)(O)=O)OC(=O)CCCCCCCCCCCCCCC PORPENFLTBBHSG-MGBGTMOVSA-N 0.000 description 7
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 7
- 238000004061 bleaching Methods 0.000 description 7
- 239000000839 emulsion Substances 0.000 description 7
- 235000013305 food Nutrition 0.000 description 7
- 229940067606 lecithin Drugs 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
- 238000011282 treatment Methods 0.000 description 7
- 150000004665 fatty acids Chemical class 0.000 description 6
- 230000001965 increasing effect Effects 0.000 description 6
- 125000002467 phosphate group Chemical group [H]OP(=O)(O[H])O[*] 0.000 description 6
- 150000003839 salts Chemical class 0.000 description 6
- 230000002378 acidificating effect Effects 0.000 description 5
- 239000003925 fat Substances 0.000 description 5
- 235000019197 fats Nutrition 0.000 description 5
- 235000021588 free fatty acids Nutrition 0.000 description 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
- 238000005119 centrifugation Methods 0.000 description 4
- 235000014113 dietary fatty acids Nutrition 0.000 description 4
- 238000004945 emulsification Methods 0.000 description 4
- 239000003995 emulsifying agent Substances 0.000 description 4
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- 230000036571 hydration Effects 0.000 description 4
- 238000006703 hydration reaction Methods 0.000 description 4
- 239000000344 soap Substances 0.000 description 4
- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 4
- 239000011575 calcium Substances 0.000 description 3
- 235000013339 cereals Nutrition 0.000 description 3
- 230000003247 decreasing effect Effects 0.000 description 3
- 238000004332 deodorization Methods 0.000 description 3
- 239000008157 edible vegetable oil Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 229960000367 inositol Drugs 0.000 description 3
- 230000014759 maintenance of location Effects 0.000 description 3
- 102000004169 proteins and genes Human genes 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 240000008415 Lactuca sativa Species 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 229960001231 choline Drugs 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000013400 design of experiment Methods 0.000 description 2
- 150000001982 diacylglycerols Chemical class 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N glycerol group Chemical group OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 235000012045 salad Nutrition 0.000 description 2
- CDAISMWEOUEBRE-UHFFFAOYSA-N scyllo-inosotol Natural products OC1C(O)C(O)C(O)C(O)C1O CDAISMWEOUEBRE-UHFFFAOYSA-N 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 150000003626 triacylglycerols Chemical class 0.000 description 2
- 239000002351 wastewater Substances 0.000 description 2
- 241000228212 Aspergillus Species 0.000 description 1
- 235000004936 Bromus mango Nutrition 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 235000019487 Hazelnut oil Nutrition 0.000 description 1
- SQUHHTBVTRBESD-UHFFFAOYSA-N Hexa-Ac-myo-Inositol Natural products CC(=O)OC1C(OC(C)=O)C(OC(C)=O)C(OC(C)=O)C(OC(C)=O)C1OC(C)=O SQUHHTBVTRBESD-UHFFFAOYSA-N 0.000 description 1
- 108020002496 Lysophospholipase Proteins 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 240000007228 Mangifera indica Species 0.000 description 1
- 235000014826 Mangifera indica Nutrition 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 235000019482 Palm oil Nutrition 0.000 description 1
- 108010019160 Pancreatin Proteins 0.000 description 1
- 101710091688 Patatin Proteins 0.000 description 1
- 235000019483 Peanut oil Nutrition 0.000 description 1
- 235000019484 Rapeseed oil Nutrition 0.000 description 1
- 235000019774 Rice Bran oil Nutrition 0.000 description 1
- 235000019485 Safflower oil Nutrition 0.000 description 1
- 235000009184 Spondias indica Nutrition 0.000 description 1
- 229930182558 Sterol Natural products 0.000 description 1
- 235000019486 Sunflower oil Nutrition 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 125000003158 alcohol group Chemical group 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000006172 buffering agent Substances 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000000828 canola oil Substances 0.000 description 1
- 235000019519 canola oil Nutrition 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 239000002299 complementary DNA Substances 0.000 description 1
- 239000010636 coriander oil Substances 0.000 description 1
- 235000005687 corn oil Nutrition 0.000 description 1
- 239000002285 corn oil Substances 0.000 description 1
- 235000012343 cottonseed oil Nutrition 0.000 description 1
- 239000002385 cottonseed oil Substances 0.000 description 1
- 230000001877 deodorizing effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 125000001924 fatty-acyl group Chemical group 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- -1 glycerolphosphate ester Chemical class 0.000 description 1
- 239000010468 hazelnut oil Substances 0.000 description 1
- 239000010460 hemp oil Substances 0.000 description 1
- 230000000887 hydrating effect Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 238000002354 inductively-coupled plasma atomic emission spectroscopy Methods 0.000 description 1
- CDAISMWEOUEBRE-GPIVLXJGSA-N inositol Chemical compound O[C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@H](O)[C@@H]1O CDAISMWEOUEBRE-GPIVLXJGSA-N 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000000944 linseed oil Substances 0.000 description 1
- 235000021388 linseed oil Nutrition 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 159000000003 magnesium salts Chemical class 0.000 description 1
- 230000035772 mutation Effects 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- 239000004006 olive oil Substances 0.000 description 1
- 235000008390 olive oil Nutrition 0.000 description 1
- 239000003346 palm kernel oil Substances 0.000 description 1
- 235000019865 palm kernel oil Nutrition 0.000 description 1
- 239000002540 palm oil Substances 0.000 description 1
- 210000000496 pancreas Anatomy 0.000 description 1
- 229940055695 pancreatin Drugs 0.000 description 1
- 239000000312 peanut oil Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 239000008165 rice bran oil Substances 0.000 description 1
- 235000005713 safflower oil Nutrition 0.000 description 1
- 239000003813 safflower oil Substances 0.000 description 1
- 238000007127 saponification reaction Methods 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- IGHGOYDCVRUTSU-UHFFFAOYSA-M sodium;2-hydroxypropane-1,2,3-tricarboxylic acid;hydroxide Chemical compound [OH-].[Na+].OC(=O)CC(O)(C(O)=O)CC(O)=O IGHGOYDCVRUTSU-UHFFFAOYSA-M 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 150000003432 sterols Chemical class 0.000 description 1
- 235000003702 sterols Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000002600 sunflower oil Substances 0.000 description 1
- 235000020238 sunflower seed Nutrition 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 239000003784 tall oil Substances 0.000 description 1
- 229930003799 tocopherol Natural products 0.000 description 1
- 239000011732 tocopherol Substances 0.000 description 1
- 235000019149 tocopherols Nutrition 0.000 description 1
- PHYFQTYBJUILEZ-IUPFWZBJSA-N triolein Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCC\C=C/CCCCCCCC PHYFQTYBJUILEZ-IUPFWZBJSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- QUEDXNHFTDJVIY-UHFFFAOYSA-N γ-tocopherol Chemical class OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/003—Refining fats or fatty oils by enzymes or microorganisms, living or dead
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Biochemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Fats And Perfumes (AREA)
Abstract
L'invention concerne un procédé de dégommage d'une composition huileuse qui comprend les étapes consistant à (a) obtenir une composition huileuse contenant une quantité de phospholipides, (b) mettre en contact ladite composition huileuse simultanément avec une ou plusieurs enzymes de phospholipase A et une ou plusieurs enzymes de phospholipase C, dans des conditions suffisantes pour que les enzymes réagissent avec les phospholipides pour créer des produits de réaction de phospholipide, et (c) séparer les produits de réaction de phospholipides de la composition huileuse, la composition huileuse restante après la séparation étant une composition huileuse dégommée de sorte que, pendant l'étape (b), la réaction de ladite ou desdites enzymes de phospholipase A a lieu à une vitesse plus rapide qu'en l'absence de ladite ou desdites enzymes de phospholipase C. Dans un mode de réalisation préféré, la réaction de l'étape (b) se poursuit pendant une durée inférieure à environ une heure.
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/668,921 | 2007-01-30 | ||
| US11/668,921 US8956853B2 (en) | 2007-01-30 | 2007-01-30 | Enzymatic degumming utilizing a mixture of PLA and PLC phospholipases |
| US11/853,339 US8460905B2 (en) | 2007-09-11 | 2007-09-11 | Enzymatic degumming utilizing a mixture of PLA and PLC phospholipases with reduced reaction time |
| US11/853,339 | 2007-09-11 | ||
| PCT/US2008/052162 WO2008094847A1 (fr) | 2007-01-30 | 2008-01-28 | Dégommage enzymatique utilisant un mélange de phospholipases pla et plc |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2676412A1 CA2676412A1 (fr) | 2008-08-07 |
| CA2676412C true CA2676412C (fr) | 2015-10-06 |
Family
ID=39428274
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2676412A Active CA2676412C (fr) | 2007-01-30 | 2008-01-28 | Degommage enzymatique utilisant un melange de phospholipases pla et plc |
Country Status (10)
| Country | Link |
|---|---|
| EP (1) | EP2118248B1 (fr) |
| CN (1) | CN105038978B (fr) |
| BR (1) | BRPI0808024B1 (fr) |
| CA (1) | CA2676412C (fr) |
| DK (1) | DK2118248T3 (fr) |
| ES (1) | ES2523300T3 (fr) |
| MX (1) | MX2009007919A (fr) |
| PL (1) | PL2118248T3 (fr) |
| RU (1) | RU2477746C2 (fr) |
| WO (1) | WO2008094847A1 (fr) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6936289B2 (en) | 1995-06-07 | 2005-08-30 | Danisco A/S | Method of improving the properties of a flour dough, a flour dough improving composition and improved food products |
| DK1387616T3 (da) | 2001-05-18 | 2007-09-24 | Danisco | Fremgangsmåde til fremstilling af en dej med et enzym |
| MXPA05007654A (es) | 2003-01-17 | 2005-09-30 | Danisco | Metodo. |
| CN102277231A (zh) | 2004-07-16 | 2011-12-14 | 丹尼斯科公司 | 用酶使油脱胶的方法 |
| WO2009081094A2 (fr) | 2007-12-21 | 2009-07-02 | Danisco A/S | Procédé |
| GB0904787D0 (en) | 2009-03-20 | 2009-05-06 | Desmet Ballestra Engineering Sa | Improved enzymatic oil recuperation process |
| DE102009051013A1 (de) | 2009-10-28 | 2011-06-09 | Ab Enzymes Gmbh | Klonierung, Expression und Verwendung saurer Phospholipasen |
| EP2638135B1 (fr) * | 2010-11-12 | 2017-01-11 | Novozymes A/S | Polypeptides ayant une activité phospholipase c et acides nucléiques codant ces derniers |
| EP2592133B1 (fr) * | 2011-11-09 | 2014-06-04 | Alfa Laval Corporate AB | Dégommage enzymatique |
| US9677027B2 (en) * | 2012-02-17 | 2017-06-13 | Clariant Produkte (Deutschland) Gmbh | Composition for enzymatic oil degumming |
| CN104487558B (zh) * | 2012-06-14 | 2018-07-17 | 邦吉全球创新有限责任公司 | 用于生产低饱和油的方法 |
| WO2014067569A1 (fr) * | 2012-10-31 | 2014-05-08 | Alfa Laval Corporate Ab | Démucilagination enzymatique |
| RU2015126866A (ru) | 2012-12-11 | 2017-01-19 | Новозимс А/С | Полипептиды, обладающие активностью фосфолипазы с, и полинуклеотиды, кодирующие их |
| EP2792735A1 (fr) | 2013-04-16 | 2014-10-22 | Clariant Produkte (Deutschland) GmbH | Procédé d'amélioration de la démucilagination enzymatique aqueuse d'huiles végétales |
| EP2799531A1 (fr) | 2013-05-03 | 2014-11-05 | Clariant Produkte (Deutschland) GmbH | Utilisation de phosphatases pour la démucilagination enzymatique de triglycérides |
| EP2910129A1 (fr) | 2014-02-21 | 2015-08-26 | Clariant Produkte (Deutschland) GmbH | Composition pour la démucilagination enzymatique d'huiles |
| WO2015140275A1 (fr) * | 2014-03-19 | 2015-09-24 | Novozymes A/S | Polypeptides présentant une activité phospholipase c et polynucléotides codant pour ceux-ci |
| WO2015173426A1 (fr) | 2014-05-15 | 2015-11-19 | Novozymes A/S | Compositions comprenant des polypeptides ayant une activité phospholipase c et leur utilisation |
| AR104205A1 (es) | 2015-04-09 | 2017-07-05 | Dsm Ip Assets Bv | Fosfolipasa c |
| WO2018186734A1 (fr) * | 2017-04-06 | 2018-10-11 | Purac Biochem B.V. | Démucilagination enzymatique d'huile de triglycéride non raffinée |
| CN108085131A (zh) * | 2017-12-25 | 2018-05-29 | 无锡德合食品科技有限公司 | 低温技术集成制备高品质菜籽油的方法 |
| CN115678674A (zh) * | 2022-10-31 | 2023-02-03 | 武汉轻工大学 | 脱胶米糠毛油及利用吸附剂和复合磷脂酶精炼米糠油的脱胶方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06306386A (ja) * | 1993-04-25 | 1994-11-01 | Showa Sangyo Co Ltd | 油脂の精製方法 |
| DE4339556C1 (de) * | 1993-11-19 | 1995-02-02 | Metallgesellschaft Ag | Verfahren zum Entschleimen von Pflanzenöl mittels Enzymen |
| AR017484A1 (es) * | 1998-04-08 | 2001-09-05 | Novozymes As | Un proceso de desgomado enzimatico de aceites comestibles |
| US7226771B2 (en) * | 2002-04-19 | 2007-06-05 | Diversa Corporation | Phospholipases, nucleic acids encoding them and methods for making and using them |
-
2008
- 2008-01-28 PL PL08728362T patent/PL2118248T3/pl unknown
- 2008-01-28 CN CN201510408407.2A patent/CN105038978B/zh active Active
- 2008-01-28 RU RU2009132518/10A patent/RU2477746C2/ru not_active IP Right Cessation
- 2008-01-28 BR BRPI0808024A patent/BRPI0808024B1/pt active IP Right Grant
- 2008-01-28 DK DK08728362.8T patent/DK2118248T3/da active
- 2008-01-28 MX MX2009007919A patent/MX2009007919A/es active IP Right Grant
- 2008-01-28 EP EP08728362.8A patent/EP2118248B1/fr active Active
- 2008-01-28 CA CA2676412A patent/CA2676412C/fr active Active
- 2008-01-28 WO PCT/US2008/052162 patent/WO2008094847A1/fr active Application Filing
- 2008-01-28 ES ES08728362.8T patent/ES2523300T3/es active Active
Also Published As
| Publication number | Publication date |
|---|---|
| RU2477746C2 (ru) | 2013-03-20 |
| PL2118248T3 (pl) | 2015-03-31 |
| MX2009007919A (es) | 2009-08-27 |
| WO2008094847A1 (fr) | 2008-08-07 |
| CA2676412A1 (fr) | 2008-08-07 |
| ES2523300T3 (es) | 2014-11-24 |
| CN105038978A (zh) | 2015-11-11 |
| CN105038978B (zh) | 2017-09-29 |
| EP2118248A1 (fr) | 2009-11-18 |
| RU2009132518A (ru) | 2011-03-10 |
| BRPI0808024B1 (pt) | 2017-05-16 |
| DK2118248T3 (da) | 2014-11-03 |
| EP2118248B1 (fr) | 2014-08-27 |
| BRPI0808024A2 (pt) | 2014-06-17 |
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