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BR0011403A - Processos para a purificação e para a preparação de ácido acrìlico ou ácido metacrìlico - Google Patents

Processos para a purificação e para a preparação de ácido acrìlico ou ácido metacrìlico

Info

Publication number
BR0011403A
BR0011403A BR0011403-0A BR0011403A BR0011403A BR 0011403 A BR0011403 A BR 0011403A BR 0011403 A BR0011403 A BR 0011403A BR 0011403 A BR0011403 A BR 0011403A
Authority
BR
Brazil
Prior art keywords
acid
purification
processes
preparation
methacrylic acid
Prior art date
Application number
BR0011403-0A
Other languages
English (en)
Inventor
Bernd Eck
J Rg Heilek
Dieter Baumann
Volker Schliephake
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of BR0011403A publication Critical patent/BR0011403A/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/47—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Glass Compositions (AREA)

Abstract

"PROCESSOS PARA A PURIFICAçãO E PARA A PREPARAçãO DE áCIDO ACRìLICO OU áCIDO METACRìLICO". A invenção refere-se a um método de purificação e produção de ácido acrílico ou metacrílico por cristalização. Como um resultado da cristalização, um produto cristalizado e um licor mãe são obtidos e o produto cristalizado é lavado em uma temperatura de 15 a 40<198>C com uma solução de lavagem que contém o ácido. A invenção refere-se ainda a um método de produção de ácido acrílico ou ácido metacrílico, que compreende o método de purificação acima mencionado.
BR0011403-0A 1999-06-08 2000-05-31 Processos para a purificação e para a preparação de ácido acrìlico ou ácido metacrìlico BR0011403A (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19926082A DE19926082A1 (de) 1999-06-08 1999-06-08 Verfahren zur Reinigung und Herstellung von Acrylsäure oder Methacrylsäure
PCT/EP2000/005004 WO2000075097A1 (de) 1999-06-08 2000-05-31 Verfahren zur reiningung und herstellung von acrylsäure oder methacrylsäure

Publications (1)

Publication Number Publication Date
BR0011403A true BR0011403A (pt) 2002-05-14

Family

ID=7910541

Family Applications (1)

Application Number Title Priority Date Filing Date
BR0011403-0A BR0011403A (pt) 1999-06-08 2000-05-31 Processos para a purificação e para a preparação de ácido acrìlico ou ácido metacrìlico

Country Status (8)

Country Link
US (2) US6700016B1 (pt)
EP (1) EP1189861B1 (pt)
JP (1) JP5162069B2 (pt)
CN (1) CN1170807C (pt)
BR (1) BR0011403A (pt)
DE (2) DE19926082A1 (pt)
MY (2) MY122594A (pt)
WO (1) WO2000075097A1 (pt)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19926082A1 (de) * 1999-06-08 2000-12-14 Basf Ag Verfahren zur Reinigung und Herstellung von Acrylsäure oder Methacrylsäure
BR0109929B1 (pt) * 2000-04-11 2012-08-07 processo para a purificaÇço de uma massa fundida de Ácido acrÍlico bruto.
DE10122787A1 (de) * 2001-05-10 2002-06-06 Basf Ag Verfahren zur Herstellung einer gereinigten Schmelze wenigstens eines Monomeren
DE10122788A1 (de) 2001-05-10 2002-06-06 Basf Ag Verfahren der kristallisativen Reinigung einer Roh-Schmelze wenigstens eines Monomeren
JP2005247731A (ja) * 2004-03-03 2005-09-15 Mitsubishi Chemicals Corp （メタ）アクリル酸組成物及びその製造方法
DE102004055765A1 (de) * 2004-11-18 2006-05-24 Basf Ag Verfahren zur Herstellung wasserabsorbierender Polymere
EP1856020B1 (de) * 2005-03-01 2015-07-08 Basf Se Verfahren zur abtrennung von methacrylsäure aus acrylsäure als hauptbestandteil sowie zielprodukt und methacrylsäure als nebenkomponente enthaltender flüssiger phase
US7705181B2 (en) 2005-03-01 2010-04-27 Basf Akiengesellschaft Process for removing methacrylic acid from liquid phase comprising acrylic acid as a main constituent and target product, and methacrylic acid as a secondary component
US7601866B2 (en) 2005-03-01 2009-10-13 Basf Aktiengesellschaft Process for removing methacrolein from liquid phase comprising acrylic acid as a main constituent and target product, and methacrolein as a secondary component
MY140513A (en) * 2005-03-01 2009-12-31 Basf Ag Process for removing methacrolein from liquid phase comprising acrylic acid as a main constituent and target product, and methacrolein as a secondary component
DE102006036177B4 (de) * 2006-07-21 2013-05-08 Evonik Degussa Gmbh Vorrichtung und Verfahren zur Herstellung von Acrylsäure mit verminderter Autoxidationsneigung
JP2010506881A (ja) * 2006-10-19 2010-03-04 ビーエーエスエフ ソシエタス・ヨーロピア アクリル酸のｃ３前駆体化合物の不均一系触媒気相部分酸化の生成物ガス混合物中に含有されるアクリル酸および安息香酸の分離法
JP5274005B2 (ja) * 2007-12-25 2013-08-28 三菱レイヨン株式会社 易重合性化合物の晶析方法、および晶析装置
JP5112898B2 (ja) * 2008-02-07 2013-01-09 三菱レイヨン株式会社 （メタ）アクリル酸の晶析方法およびその晶析システム
JP5507111B2 (ja) * 2008-05-30 2014-05-28 ローム アンド ハース カンパニー 水性（メタ）アクリル酸の製造方法
RU2515279C9 (ru) 2008-07-28 2015-02-20 Басф Се Способ разделения акриловой кислоты, содержащейся в качестве основного компонента, и глиоксаля, содержащегося в качестве побочного продукта в газообразной смеси продуктов частичного гетерогенно катализируемого парофазного окисления соединения-предшественника акриловой кислоты, содержащего 3 атома углерода
DE102008041573A1 (de) 2008-08-26 2010-03-04 Basf Se Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enhaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal
DE102008040799A1 (de) 2008-07-28 2008-12-11 Basf Se Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enthaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal
JP5630078B2 (ja) * 2010-06-10 2014-11-26 三菱レイヨン株式会社 （メタ）アクリル酸の精製方法
DE102011050288A1 (de) * 2011-05-11 2012-11-15 Crenox Gmbh Verfahren und Vorrichtung zur Abtrennung von Kristallen aus einer Lösung
EP3012244A1 (en) 2014-10-24 2016-04-27 Sulzer Chemtech AG Process and apparatus for purification of acrylic acid

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE633450A (pt) 1962-06-11
NL6918448A (pt) 1968-12-16 1970-06-18
DE2251364B2 (de) 1971-10-22 1975-07-03 Asahi Glass Co. Ltd., Tokio Verfahren zur Herstellung von Acrylsäure bzw. Methacrylsäure aus Acrolein bzw. Methacrolein
DE2309657A1 (de) 1973-02-27 1974-09-12 Basf Ag Verfahren zur herstellung von carbonsaeuren oder dicarbonsaeureanhydriden
US4224187A (en) 1978-11-13 1980-09-23 Celanese Corporation Olefin oxidation catalyst and process for its preparation
DE3106557A1 (de) 1981-02-21 1982-09-16 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von (alpha)-alkylacroleinen
DE3213681A1 (de) 1982-04-14 1983-10-27 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von (alpha)-alkylacroleinen
EP0117146B1 (en) 1983-02-22 1986-12-30 The Halcon Sd Group, Inc. Conversion of propane to acrylic acid
CA1299193C (en) 1986-07-17 1992-04-21 Gordon Gene Harkreader Anhydrous diluents for the propylene oxidation reaction to acrolein and acrolein oxidation to acrylic acid
CA1305178C (en) 1986-08-21 1992-07-14 Gordon Gene Harkreader Anhydrous diluent process for the propylene oxidation reaction to acrolein and acrolein oxidation to acrylic acid
AU606160B2 (en) 1987-05-27 1991-01-31 Nippon Shokubai Kagaku Kogyo Co. Ltd. Process for production of acrylic acid
US5510558A (en) 1993-12-29 1996-04-23 Sun Company, Inc. (R&M) Oxidative dehydrogenation of hydrocarbons with active carbon catalyst
CN1035762C (zh) 1994-11-23 1997-09-03 大庆石油学院 丙烷均相氧化脱氢及丙烯氧化制取丙烯酸的方法及其装置
DE19508558A1 (de) 1995-03-10 1996-09-12 Basf Ag Verfahren zur Herstellung von Acrolein, Acrylsäure oder deren Gemisch aus Propan
DE19627847A1 (de) 1996-07-10 1998-01-15 Basf Ag Verfahren zur Herstellung von Acrylsäure
DE19740252A1 (de) * 1997-09-12 1999-03-18 Basf Ag Verfahren zur Herstellung von Acrylsäure und Methacrylsäure
DE19833049A1 (de) * 1998-07-22 2000-01-27 Basf Ag Verfahren zur Herstellung von Acrylsäure
DE19832962A1 (de) 1998-07-22 2000-01-27 Basf Ag Reinigung von Acrylsäure durch Kristallisation mittels Vakuumverdampfung
DE19926082A1 (de) * 1999-06-08 2000-12-14 Basf Ag Verfahren zur Reinigung und Herstellung von Acrylsäure oder Methacrylsäure

Also Published As

Publication number Publication date
EP1189861A1 (de) 2002-03-27
DE50004737D1 (de) 2004-01-22
JP2003501409A (ja) 2003-01-14
JP5162069B2 (ja) 2013-03-13
US20040049077A1 (en) 2004-03-11
MY122594A (en) 2006-04-29
DE19926082A1 (de) 2000-12-14
CN1170807C (zh) 2004-10-13
CN1354738A (zh) 2002-06-19
US6921837B2 (en) 2005-07-26
WO2000075097A1 (de) 2000-12-14
MY150402A (en) 2014-01-15
EP1189861B1 (de) 2003-12-10
US6700016B1 (en) 2004-03-02

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Legal Events

Date Code Title Description
B07A Technical examination (opinion): publication of technical examination (opinion) [chapter 7.1 patent gazette]
B09B Patent application refused [chapter 9.2 patent gazette]

Free format text: INDEFERIDO O PEDIDO COM BASE NOS ARTIGOS 8O, 11 E 13 DA LPI.

B12B Appeal: appeal against refusal